#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:36:18 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181260 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/38/2233839.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2233839_Fobs loop_ _publ_author_name 'Fun, Hoong-Kun' 'Quah, Ching Kheng' 'Attia, Mohamed I.' 'El-Behairy, Mohammed F.' 'Al-Deeb, Omar A.' _publ_section_title ; (E)-1-(1,3-Benzodioxol-5-yl)-4,4-dimethylpent-1-en-3-one ; _journal_coeditor_code HB6621 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o634 _journal_volume 68 _journal_year 2012 _space_group_IT_number 11 _symmetry_space_group_name_Hall '-P 2yb' _symmetry_space_group_name_H-M 'P 1 21/m 1' _cell_angle_alpha 90.000 _cell_angle_beta 96.676 _cell_angle_gamma 90.000 _cell_length_a 6.5305 _cell_length_b 6.6798 _cell_length_c 13.7264 _exptl_crystal_F_000 248.00 _reflns_d_resolution_high 0.6570 _cod_data_source_file hb6621Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' mav_0m in P2(1)/m (100K)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 126.38 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' '-x, -y, -z' 'x, -y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 4870.97 4120.46 74.60 o 2 0 0 49.59 54.34 1.20 o 3 0 0 35.80 31.92 0.50 o 4 0 0 386.88 366.97 4.75 o 5 0 0 742.29 682.27 7.03 o 6 0 0 1075.00 1021.21 10.42 o 7 0 0 102.41 100.36 2.78 o 8 0 0 2.07 1.46 0.45 o 9 0 0 0.00 -0.02 0.33 o 1 1 0 298.82 269.08 2.54 o 2 1 0 0.02 0.17 0.05 o 3 1 0 256.72 270.92 2.29 o 4 1 0 256.87 261.13 1.89 o 5 1 0 47.34 44.30 0.51 o 6 1 0 220.99 224.72 2.36 o 7 1 0 0.00 0.24 0.12 o 8 1 0 0.03 0.34 0.23 o 9 1 0 27.97 27.11 1.05 o 0 2 0 15970.64 14224.91 249.63 o 1 2 0 6219.99 5979.14 86.48 o 2 2 0 107.44 103.99 1.00 o 3 2 0 92.75 94.04 0.92 o 4 2 0 30.41 26.27 0.41 o 5 2 0 1104.91 1075.64 9.36 o 6 2 0 713.98 692.24 7.33 o 7 2 0 80.14 79.06 1.17 o 8 2 0 4.34 4.74 0.49 o 9 2 0 13.63 14.44 0.78 o 1 3 0 5.01 6.02 0.13 o 2 3 0 61.72 65.94 0.65 o 3 3 0 423.39 415.78 3.19 o 4 3 0 36.99 38.28 0.52 o 5 3 0 61.87 60.42 0.87 o 6 3 0 61.51 61.81 1.06 o 7 3 0 17.77 18.72 0.85 o 8 3 0 7.63 7.46 0.44 o 9 3 0 26.66 29.19 1.33 o 0 4 0 5119.74 5205.49 46.55 o 1 4 0 1202.86 1357.14 9.86 o 2 4 0 8.95 7.56 0.16 o 3 4 0 3.66 4.20 0.18 o 4 4 0 54.07 57.23 0.91 o 5 4 0 568.97 565.77 7.77 o 6 4 0 506.53 498.32 4.69 o 7 4 0 65.16 64.30 1.35 o 8 4 0 0.18 0.12 0.32 o 9 4 0 1.91 2.75 0.39 o 1 5 0 28.00 24.64 0.34 o 2 5 0 21.22 16.95 0.37 o 3 5 0 3.53 2.28 0.17 o 4 5 0 50.97 55.48 0.97 o 5 5 0 13.62 14.60 0.44 o 6 5 0 113.55 110.73 1.64 o 7 5 0 4.36 4.08 0.35 o 8 5 0 0.86 1.12 0.31 o 0 6 0 1943.22 1997.12 26.54 o 1 6 0 316.38 346.08 3.32 o 2 6 0 0.02 0.03 0.10 o 3 6 0 0.39 0.68 0.17 o 4 6 0 61.79 60.02 1.39 o 5 6 0 235.64 236.72 2.86 o 6 6 0 326.02 330.42 3.90 o 7 6 0 27.96 27.09 0.76 o 1 7 0 0.31 0.13 0.19 o 2 7 0 10.75 11.40 0.74 o 3 7 0 13.94 14.53 0.62 o 4 7 0 7.86 8.00 0.91 o 5 7 0 14.67 14.72 1.10 o 6 7 0 15.24 14.67 0.60 o 7 7 0 1.55 1.54 0.31 o 0 8 0 440.55 442.20 8.57 o 1 8 0 268.11 271.68 3.26 o 2 8 0 0.37 2.65 0.56 o 3 8 0 5.45 5.53 0.48 o 4 8 0 3.39 1.99 0.58 o 6 8 0 104.34 112.59 3.64 o 1 9 0 0.17 0.62 0.32 o 2 9 0 4.03 4.17 0.44 o 3 9 0 3.54 2.69 0.63 o 4 9 0 0.53 0.37 0.47 o 0 10 0 275.30 279.16 5.89 o 1 10 0 55.20 56.86 2.46 o -9 0 1 19.38 19.52 1.25 o -8 0 1 55.99 56.27 2.06 o -7 0 1 0.04 0.10 0.22 o -6 0 1 117.49 112.93 1.63 o -5 0 1 420.31 399.84 3.67 o -4 0 1 82.88 83.62 0.93 o -3 0 1 154.05 158.05 1.51 o -2 0 1 582.23 611.11 10.48 o -1 0 1 464.95 480.27 6.49 o 1 0 1 1084.86 1068.94 18.54 o 2 0 1 504.58 480.48 8.34 o 3 0 1 362.59 380.00 4.81 o 4 0 1 96.44 113.97 1.72 o 5 0 1 152.43 138.19 2.11 o 6 0 1 7.46 7.26 0.71 o 7 0 1 0.16 0.13 0.24 o 8 0 1 0.08 -0.02 0.25 o 9 0 1 4.70 5.38 0.80 o -9 1 1 8.63 8.01 0.66 o -8 1 1 72.72 72.52 1.70 o -7 1 1 11.70 12.74 0.41 o -6 1 1 4.48 4.49 0.23 o -5 1 1 28.24 26.62 0.36 o -4 1 1 30.91 25.23 0.32 o -3 1 1 340.64 401.14 2.98 o -2 1 1 702.18 756.88 6.28 o -1 1 1 1054.77 1032.21 8.73 o 0 1 1 31.54 38.89 0.63 o 1 1 1 827.64 850.62 9.01 o 2 1 1 2.49 3.05 0.35 o 3 1 1 1.91 2.92 0.16 o 4 1 1 1.06 1.55 0.10 o 5 1 1 0.38 0.26 0.17 o 6 1 1 73.76 76.78 1.23 o 7 1 1 8.82 9.86 0.55 o 8 1 1 8.39 8.40 0.78 o 9 1 1 16.86 18.59 0.86 o -9 2 1 2.54 3.53 0.47 o -8 2 1 3.64 4.05 0.54 o -7 2 1 30.06 28.53 0.61 o -6 2 1 44.44 40.18 0.73 o -5 2 1 283.36 277.99 2.70 o -4 2 1 316.50 317.70 2.85 o -3 2 1 29.10 31.65 0.41 o -2 2 1 5.78 5.86 0.15 o -1 2 1 310.05 323.27 2.75 o 0 2 1 1714.66 1759.52 32.74 o 1 2 1 36.36 27.27 0.40 o 2 2 1 58.89 71.92 0.93 o 3 2 1 36.55 38.07 0.47 o 4 2 1 19.16 23.63 0.38 o 5 2 1 30.84 24.50 0.48 o 6 2 1 85.99 86.50 1.37 o 7 2 1 15.53 13.22 0.50 o 8 2 1 0.43 0.90 0.28 o 9 2 1 12.68 12.19 0.98 o -9 3 1 0.63 0.49 0.29 o -8 3 1 62.30 63.75 1.50 o -7 3 1 29.37 30.45 0.59 o -6 3 1 17.45 16.00 0.42 o -5 3 1 123.80 125.60 1.42 o -4 3 1 2.16 2.63 0.15 o -3 3 1 239.47 261.08 2.37 o -2 3 1 38.98 35.92 0.56 o -1 3 1 0.51 0.35 0.05 o 0 3 1 112.99 100.99 0.94 o 1 3 1 485.62 562.69 4.14 o 2 3 1 1.09 0.93 0.07 o 3 3 1 86.27 94.09 0.93 o 4 3 1 91.65 92.73 0.98 o 5 3 1 7.00 6.69 0.26 o 6 3 1 52.60 56.54 0.95 o 7 3 1 0.34 0.55 0.18 o 8 3 1 1.18 1.03 0.27 o 9 3 1 2.08 2.39 0.41 o -9 4 1 4.96 5.43 0.68 o -8 4 1 10.14 9.39 0.74 o -7 4 1 5.15 3.97 0.29 o -6 4 1 53.06 51.81 0.95 o -5 4 1 202.35 203.98 2.11 o -4 4 1 124.86 125.71 1.24 o -3 4 1 5.48 4.09 0.16 o -2 4 1 5.53 5.59 0.14 o -1 4 1 80.12 84.47 0.78 o 0 4 1 339.43 366.96 2.43 o 1 4 1 65.81 75.79 0.65 o 2 4 1 0.01 0.17 0.08 o 3 4 1 21.08 23.59 0.45 o 4 4 1 5.60 5.75 0.22 o 5 4 1 61.79 61.52 0.88 o 6 4 1 31.11 30.94 0.62 o 7 4 1 2.34 2.39 0.34 o 8 4 1 0.67 0.75 0.22 o -8 5 1 30.51 32.24 0.90 o -7 5 1 1.80 2.31 0.27 o -6 5 1 8.35 9.20 0.45 o -5 5 1 0.79 1.38 0.18 o -4 5 1 22.40 21.67 1.19 o -3 5 1 59.94 59.31 0.88 o -2 5 1 128.40 126.94 1.29 o -1 5 1 164.15 163.76 1.40 o 0 5 1 25.75 27.26 0.32 o 1 5 1 44.31 58.32 1.17 o 2 5 1 1.30 0.25 0.07 o 3 5 1 2.88 1.78 0.24 o 4 5 1 0.04 0.01 0.08 o 5 5 1 7.86 8.68 0.30 o 6 5 1 40.40 41.50 0.75 o 7 5 1 19.75 18.00 0.82 o 8 5 1 7.71 6.60 0.62 o -8 6 1 13.96 15.07 1.35 o -7 6 1 0.31 0.43 0.20 o -6 6 1 34.78 35.29 0.83 o -5 6 1 162.96 167.72 2.91 o -4 6 1 39.38 39.13 1.08 o -3 6 1 13.97 13.23 0.45 o -2 6 1 18.13 18.18 0.49 o -1 6 1 33.98 36.73 0.55 o 0 6 1 76.16 82.05 0.84 o 1 6 1 87.79 91.56 1.87 o 2 6 1 6.35 4.66 0.32 o 3 6 1 20.20 21.56 0.72 o 4 6 1 0.43 0.05 0.18 o 5 6 1 54.23 53.72 1.07 o 6 6 1 8.43 7.31 0.42 o 7 6 1 2.26 2.32 0.92 o -7 7 1 3.02 2.79 0.56 o -6 7 1 0.97 1.34 0.26 o -5 7 1 19.72 20.49 0.86 o -4 7 1 0.02 -0.18 0.18 o -3 7 1 35.17 37.21 1.03 o -2 7 1 4.40 4.74 0.40 o -1 7 1 11.57 10.89 0.47 o 0 7 1 2.61 2.68 0.17 o 1 7 1 46.84 45.16 0.98 o 2 7 1 3.36 4.24 0.42 o 3 7 1 3.52 3.41 0.59 o 4 7 1 24.97 23.42 1.34 o 5 7 1 0.00 0.04 0.34 o 6 7 1 36.04 35.59 1.00 o 7 7 1 2.59 2.39 0.65 o -6 8 1 10.72 11.25 1.22 o -5 8 1 62.87 63.11 2.49 o -4 8 1 74.80 77.52 2.69 o -3 8 1 6.82 6.96 1.22 o -2 8 1 0.17 0.42 0.20 o -1 8 1 19.56 18.60 0.69 o 0 8 1 91.34 91.25 1.53 o 1 8 1 2.25 2.58 0.24 o 2 8 1 15.90 17.00 0.99 o 3 8 1 0.02 0.13 0.36 o 4 8 1 0.72 0.76 0.42 o 5 8 1 6.61 4.59 0.82 o 6 8 1 33.13 32.33 1.83 o -4 9 1 0.26 0.89 0.49 o -3 9 1 16.86 16.89 1.27 o -2 9 1 0.46 0.44 0.25 o -1 9 1 5.52 6.56 0.38 o 0 9 1 0.30 0.49 0.23 o 1 9 1 22.34 19.00 0.54 o 2 9 1 0.87 0.57 0.23 o 3 9 1 0.27 0.74 0.43 o 4 9 1 14.46 15.64 1.24 o -1 10 1 7.11 7.98 0.72 o 0 10 1 17.63 16.90 1.13 o 1 10 1 29.31 29.44 0.85 o -9 0 2 0.09 -0.29 0.29 o -8 0 2 0.19 0.18 0.33 o -7 0 2 0.67 0.32 0.27 o -6 0 2 261.15 250.06 2.56 o -5 0 2 118.40 103.51 1.17 o -4 0 2 145.09 165.00 1.69 o -3 0 2 11.29 11.39 0.22 o -2 0 2 1404.24 1471.40 13.43 o -1 0 2 154.13 161.43 2.23 o 0 0 2 208.82 199.63 1.89 o 1 0 2 1707.04 1618.70 28.08 o 2 0 2 4.15 4.75 0.30 o 3 0 2 80.69 75.57 1.18 o 4 0 2 72.75 77.88 1.29 o 5 0 2 211.83 199.21 2.86 o 6 0 2 70.58 70.09 2.06 o 7 0 2 75.55 75.62 2.33 o 8 0 2 2.41 1.88 0.51 o 9 0 2 0.91 1.83 0.55 o -9 1 2 7.61 8.15 0.68 o -8 1 2 109.76 117.59 2.31 o -7 1 2 0.02 0.63 0.16 o -6 1 2 219.49 205.34 1.93 o -5 1 2 39.34 41.62 0.58 o -4 1 2 0.01 0.27 0.12 o -3 1 2 79.84 88.83 0.67 o -2 1 2 365.13 412.34 3.14 o -1 1 2 509.66 532.17 4.03 o 0 1 2 2942.90 2972.43 23.04 o 1 1 2 1.23 1.00 0.15 o 2 1 2 14.58 15.16 0.31 o 3 1 2 72.28 83.60 1.09 o 4 1 2 1.00 1.60 0.11 o 5 1 2 24.64 24.05 0.56 o 6 1 2 19.43 19.18 0.54 o 7 1 2 3.51 5.18 0.46 o 8 1 2 18.31 19.77 0.90 o 9 1 2 5.17 3.85 0.51 o -9 2 2 0.82 0.39 0.30 o -8 2 2 4.32 4.11 0.33 o -7 2 2 26.26 25.62 0.59 o -6 2 2 41.70 36.22 0.58 o -5 2 2 298.83 285.33 2.49 o -4 2 2 79.37 83.32 0.84 o -3 2 2 45.76 41.41 0.41 o -2 2 2 11.87 12.48 0.19 o -1 2 2 388.52 375.04 3.18 o 0 2 2 2.83 5.11 0.13 o 1 2 2 638.51 653.15 8.20 o 2 2 2 410.38 443.18 3.57 o 3 2 2 412.34 417.38 3.44 o 4 2 2 2.59 2.40 0.26 o 5 2 2 153.75 148.71 1.93 o 6 2 2 14.24 13.90 0.48 o 7 2 2 8.93 9.70 0.53 o 8 2 2 6.02 6.82 0.60 o 9 2 2 0.32 0.13 0.23 o -9 3 2 26.95 28.05 2.70 o -8 3 2 30.82 32.39 0.74 o -7 3 2 4.82 7.48 0.41 o -6 3 2 111.67 107.97 1.46 o -5 3 2 110.11 112.26 1.29 o -4 3 2 83.53 84.44 0.90 o -3 3 2 163.86 173.36 1.50 o -2 3 2 172.33 182.93 2.56 o -1 3 2 518.51 559.88 3.92 o 0 3 2 368.39 413.60 3.07 o 1 3 2 239.80 251.66 1.96 o 2 3 2 79.14 82.53 1.06 o 3 3 2 53.64 56.94 0.70 o 4 3 2 16.47 18.48 0.34 o 5 3 2 85.17 83.99 1.08 o 6 3 2 1.46 1.05 0.20 o 7 3 2 6.57 8.75 0.50 o 8 3 2 24.63 23.93 0.75 o 9 3 2 0.10 0.11 0.23 o -9 4 2 0.10 0.01 0.24 o -8 4 2 2.57 2.17 0.26 o -7 4 2 3.89 3.64 0.29 o -6 4 2 56.77 54.54 0.85 o -5 4 2 107.47 105.08 1.24 o -4 4 2 74.78 74.39 1.37 o -3 4 2 0.47 0.33 0.07 o -2 4 2 53.26 51.21 0.52 o -1 4 2 6.57 5.27 0.14 o 0 4 2 11.57 7.42 0.15 o 1 4 2 304.90 320.72 2.44 o 2 4 2 84.58 98.95 1.00 o 3 4 2 67.60 59.45 0.74 o 4 4 2 5.26 6.82 0.33 o 5 4 2 83.24 86.83 1.12 o 6 4 2 20.84 20.81 0.63 o 7 4 2 21.12 21.90 0.69 o 8 4 2 1.04 0.95 0.25 o -8 5 2 69.63 69.79 1.21 o -7 5 2 0.15 0.31 0.16 o -6 5 2 79.66 79.22 1.32 o -5 5 2 1.21 1.02 0.16 o -4 5 2 2.11 2.07 0.57 o -3 5 2 1.22 2.14 0.22 o -2 5 2 65.04 64.43 0.79 o -1 5 2 33.66 38.92 0.58 o 0 5 2 425.58 434.81 3.18 o 1 5 2 19.53 16.90 0.24 o 2 5 2 5.42 5.41 0.22 o 3 5 2 17.01 14.51 0.43 o 4 5 2 2.19 2.35 0.18 o 5 5 2 0.01 0.09 0.11 o 6 5 2 10.23 12.01 0.80 o 7 5 2 0.53 0.63 0.27 o 8 5 2 6.27 5.70 1.14 o -8 6 2 0.01 0.19 0.22 o -7 6 2 0.67 0.90 0.20 o -6 6 2 44.44 45.01 0.91 o -5 6 2 38.14 39.91 1.85 o -4 6 2 43.30 43.15 1.15 o -3 6 2 11.19 11.30 0.43 o -2 6 2 45.03 43.78 0.83 o -1 6 2 4.37 4.78 0.22 o 0 6 2 9.73 9.65 0.31 o 1 6 2 112.08 114.89 1.36 o 2 6 2 16.05 21.45 0.51 o 3 6 2 1.35 0.84 0.34 o 4 6 2 6.51 7.75 0.39 o 5 6 2 66.14 66.36 1.13 o 6 6 2 13.45 14.66 0.73 o 7 6 2 25.14 26.14 1.03 o -7 7 2 3.82 3.89 0.33 o -6 7 2 30.15 29.70 1.19 o -5 7 2 11.74 10.77 0.65 o -4 7 2 13.92 14.83 1.28 o -3 7 2 12.85 14.66 0.51 o -2 7 2 15.91 16.43 0.51 o -1 7 2 34.40 36.03 0.91 o 0 7 2 39.47 41.19 0.79 o 1 7 2 1.95 2.06 0.22 o 2 7 2 3.01 3.86 0.49 o 3 7 2 8.40 7.66 0.89 o 4 7 2 5.33 6.16 0.81 o 5 7 2 10.68 11.19 0.51 o 6 7 2 0.03 -0.19 0.38 o -6 8 2 0.31 0.22 0.32 o -5 8 2 42.16 44.50 2.02 o -3 8 2 0.04 0.05 0.18 o -2 8 2 3.37 3.96 0.41 o -1 8 2 10.01 9.80 0.51 o 0 8 2 0.19 -0.06 0.22 o 1 8 2 24.96 26.32 0.61 o 2 8 2 50.90 54.55 1.47 o 3 8 2 20.19 20.80 1.28 o 4 8 2 4.74 4.91 0.79 o 5 8 2 28.50 27.25 1.60 o -4 9 2 5.55 5.74 0.84 o -3 9 2 2.88 2.74 0.39 o -2 9 2 6.70 7.52 0.53 o -1 9 2 12.19 12.72 0.44 o 0 9 2 13.29 14.54 0.51 o 1 9 2 0.31 0.09 0.19 o 2 9 2 2.44 2.96 0.30 o 3 9 2 6.52 8.69 1.04 o 4 9 2 1.17 1.32 0.55 o -1 10 2 2.77 3.30 0.32 o 0 10 2 0.86 1.64 0.25 o 1 10 2 18.91 20.40 1.24 o -9 0 3 282.66 299.76 6.72 o -8 0 3 86.24 96.86 2.87 o -7 0 3 14.40 12.12 0.84 o -6 0 3 4.00 3.84 0.33 o -5 0 3 25.42 22.00 0.44 o -4 0 3 32.77 40.81 0.88 o -3 0 3 2236.01 2379.64 54.49 o -2 0 3 1473.51 1493.52 20.01 o -1 0 3 618.31 603.50 6.75 o 0 0 3 354.60 347.99 3.26 o 1 0 3 252.00 247.94 4.41 o 2 0 3 206.36 261.23 3.35 o 3 0 3 234.19 292.05 3.90 o 4 0 3 544.38 601.99 7.58 o 5 0 3 154.19 156.49 2.35 o 6 0 3 10.88 8.72 0.66 o 7 0 3 96.61 103.20 2.88 o 8 0 3 88.27 85.63 2.70 o 9 0 3 0.00 -0.07 0.30 o -9 1 3 0.95 0.97 0.37 o -8 1 3 37.47 35.52 1.11 o -7 1 3 0.43 0.63 0.13 o -6 1 3 37.01 33.81 0.55 o -5 1 3 44.53 45.17 0.50 o -4 1 3 12.80 13.11 0.22 o -3 1 3 391.66 419.74 2.48 o -2 1 3 27.52 26.80 0.29 o -1 1 3 8.09 5.68 0.18 o 0 1 3 517.62 522.11 4.04 o 1 1 3 469.13 489.24 4.91 o 2 1 3 103.73 132.52 1.52 o 3 1 3 1133.00 1240.36 13.07 o 4 1 3 141.68 166.18 1.68 o 5 1 3 0.24 0.51 0.13 o 6 1 3 6.28 5.43 0.49 o 7 1 3 8.94 10.97 0.59 o 8 1 3 20.27 23.03 0.91 o 9 1 3 8.23 9.41 0.75 o -9 2 3 139.72 146.41 2.83 o -8 2 3 128.76 138.20 1.57 o -7 2 3 8.48 7.05 0.30 o -6 2 3 59.95 59.09 0.79 o -5 2 3 33.90 34.48 0.52 o -4 2 3 273.17 299.42 2.29 o -3 2 3 1008.05 1091.51 6.56 o -2 2 3 533.50 559.56 3.66 o -1 2 3 95.88 101.89 0.94 o 0 2 3 308.78 301.12 2.14 o 1 2 3 25.33 24.82 0.40 o 2 2 3 181.27 216.50 2.36 o 3 2 3 360.95 431.77 4.07 o 4 2 3 148.59 164.03 1.79 o 5 2 3 276.07 285.40 3.30 o 6 2 3 3.54 2.01 0.26 o 7 2 3 113.81 117.52 1.79 o 8 2 3 29.56 31.09 1.39 o 9 2 3 10.11 10.96 0.80 o -9 3 3 0.14 0.07 0.25 o -8 3 3 1.88 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