#------------------------------------------------------------------------------ #$Date: 2012-09-11 12:26:43 +0300 (Tue, 11 Sep 2012) $ #$Revision: 66590 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/38/2233844.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2233844_Fobs loop_ _publ_author_name 'Almutairi, Maha S.' 'Al-Shehri, Mona M.' 'El-Emam, Ali A.' 'Ng, Seik Weng' 'Tiekink, Edward R. T.' _publ_section_title ; 3-(Adamantan-1-yl)-4-(prop-2-en-1-yl)-1H-1,2,4-triazole-5(4H)-thione ; _journal_coeditor_code HB6626 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o656 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 115.938 _cell_angle_gamma 90.000 _cell_length_a 13.5833 _cell_length_b 8.6483 _cell_length_c 13.6973 _exptl_crystal_F_000 592.00 _reflns_d_resolution_high 0.7671 _[local]_cod_data_source_file hb6626Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P21/n 34.5(4)% twin' _shelx_refln_list_code 4 _shelx_f_calc_maximum 160.74 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1190.89 1195.64 24.89 o 4 0 0 17910.82 18962.55 138.20 o 6 0 0 260.37 197.22 24.41 o 8 0 0 0.98 289.43 282.39 o 10 0 0 585.80 576.11 29.68 o 12 0 0 1.75 24.11 6.95 o 14 0 0 102.17 80.78 23.54 o 1 1 0 1303.55 1329.74 18.29 o 2 1 0 16772.03 15387.57 91.62 o 3 1 0 260.12 267.07 13.63 o 4 1 0 1237.54 1183.00 31.04 o 5 1 0 820.66 517.62 101.96 o 6 1 0 5073.97 5166.15 36.17 o 7 1 0 0.52 1.99 1.43 o 8 1 0 0.12 1.66 0.84 o 9 1 0 125.46 141.77 11.50 o 10 1 0 55.32 94.74 7.44 o 11 1 0 133.85 140.68 8.41 o 12 1 0 163.96 111.27 9.94 o 13 1 0 23.07 28.69 7.14 o 14 1 0 4.35 1.24 2.14 o 15 1 0 9.04 0.17 3.83 o 0 2 0 3088.14 3528.45 48.91 o 1 2 0 2713.62 2838.99 24.30 o 2 2 0 2230.83 2458.56 32.67 o 3 2 0 3544.41 3609.56 120.50 o 4 2 0 2844.84 2813.58 86.89 o 5 2 0 64.25 43.68 10.20 o 6 2 0 3.58 2.88 1.88 o 7 2 0 171.31 205.07 14.54 o 8 2 0 676.08 734.77 29.24 o 9 2 0 107.67 114.85 12.40 o 10 2 0 387.03 436.02 30.26 o 11 2 0 14.55 10.73 5.13 o 12 2 0 10.13 6.19 3.07 o 13 2 0 21.50 16.37 6.20 o 14 2 0 128.94 136.58 19.39 o 15 2 0 0.84 5.14 1.65 o 1 3 0 553.19 665.01 15.09 o 2 3 0 291.69 280.16 9.31 o 3 3 0 179.65 153.12 24.26 o 4 3 0 275.59 250.43 8.00 o 5 3 0 502.13 460.41 18.85 o 6 3 0 938.32 798.84 32.26 o 7 3 0 62.54 76.50 9.07 o 8 3 0 941.54 960.31 44.25 o 9 3 0 453.39 467.27 25.51 o 10 3 0 239.80 351.66 28.93 o 11 3 0 94.09 94.79 16.17 o 12 3 0 118.67 157.63 20.57 o 13 3 0 17.84 7.70 5.88 o 14 3 0 100.81 115.37 19.33 o 15 3 0 178.76 205.31 41.57 o 0 4 0 1061.85 1084.33 24.74 o 1 4 0 682.99 741.07 16.05 o 2 4 0 1368.45 1445.05 28.02 o 3 4 0 17.04 15.58 2.78 o 4 4 0 946.62 956.16 20.30 o 5 4 0 313.71 305.58 14.86 o 6 4 0 411.14 358.04 25.69 o 7 4 0 219.89 212.25 15.11 o 8 4 0 3.48 144.01 19.14 o 9 4 0 56.45 63.85 9.49 o 10 4 0 0.12 3.03 4.24 o 11 4 0 93.64 107.57 17.31 o 12 4 0 30.44 29.23 8.96 o 13 4 0 255.48 207.98 26.14 o 14 4 0 10.57 2.28 9.93 o 1 5 0 847.01 794.35 21.77 o 2 5 0 822.71 821.82 21.22 o 3 5 0 247.52 275.37 12.37 o 4 5 0 427.21 415.33 18.56 o 5 5 0 498.33 472.04 20.66 o 6 5 0 31.37 5.37 9.10 o 7 5 0 16.10 181.38 20.69 o 8 5 0 95.03 113.46 11.60 o 9 5 0 11.37 8.98 3.46 o 10 5 0 0.04 -4.67 4.67 o 11 5 0 84.29 67.69 14.06 o 12 5 0 45.57 29.22 9.25 o 13 5 0 20.27 28.23 9.62 o 14 5 0 1.65 2.81 9.13 o 0 6 0 21.26 33.22 5.01 o 1 6 0 2227.82 2201.50 36.29 o 2 6 0 227.82 204.96 11.47 o 3 6 0 905.65 859.99 30.68 o 4 6 0 45.75 55.10 7.59 o 5 6 0 207.15 193.88 15.61 o 6 6 0 138.25 123.87 10.03 o 7 6 0 20.73 70.92 69.07 o 8 6 0 15.02 136.52 48.85 o 9 6 0 83.65 165.42 23.53 o 10 6 0 1.22 0.12 1.78 o 11 6 0 3.58 1.65 4.27 o 12 6 0 1.90 15.26 8.68 o 13 6 0 6.60 5.39 4.48 o 1 7 0 581.84 529.96 18.95 o 2 7 0 182.33 206.00 12.44 o 3 7 0 154.39 167.45 12.57 o 4 7 0 130.32 132.44 12.88 o 5 7 0 1559.45 1553.59 59.93 o 6 7 0 341.19 306.85 25.25 o 7 7 0 64.81 66.78 13.86 o 8 7 0 5.25 11.19 6.94 o 9 7 0 73.71 82.77 19.89 o 10 7 0 0.00 2.64 0.50 o 11 7 0 87.20 78.16 16.89 o 12 7 0 50.73 61.69 15.81 o 0 8 0 9.20 2.32 4.34 o 1 8 0 676.24 791.33 32.10 o 2 8 0 167.26 194.27 17.46 o 3 8 0 65.18 68.13 10.20 o 4 8 0 46.05 55.17 8.92 o 5 8 0 279.82 260.61 19.05 o 6 8 0 78.05 69.73 9.67 o 7 8 0 34.81 188.96 28.66 o 8 8 0 18.09 27.86 9.67 o 9 8 0 1.65 0.03 2.04 o 10 8 0 1.60 -0.72 17.60 o 11 8 0 62.64 68.83 24.63 o 1 9 0 69.79 95.01 11.17 o 2 9 0 35.93 33.20 7.40 o 3 9 0 294.64 343.20 24.62 o 4 9 0 56.16 66.18 10.52 o 5 9 0 392.90 403.48 25.62 o 6 9 0 8.20 1.75 2.31 o 7 9 0 6.98 34.69 11.94 o 8 9 0 6.50 2.53 4.88 o 9 9 0 210.41 225.12 30.31 o 0 10 0 136.03 139.07 21.02 o 1 10 0 128.93 145.26 14.90 o 2 10 0 143.96 112.35 14.89 o 3 10 0 660.96 638.92 35.67 o 4 10 0 177.81 162.90 25.16 o 5 10 0 113.12 134.46 22.85 o 6 10 0 37.12 34.19 11.48 o 7 10 0 189.83 206.46 29.05 o 1 11 0 276.00 288.00 25.42 o 2 11 0 69.95 52.53 10.35 o 3 11 0 33.97 33.32 11.82 o -15 0 1 167.69 171.26 36.76 o -13 0 1 3.93 11.04 7.26 o -11 0 1 325.74 401.08 18.81 o -9 0 1 319.94 341.35 25.22 o -7 0 1 6302.56 8015.80 108.30 o -3 0 1 25836.44 16314.11 73.02 o 1 0 1 1390.48 904.95 27.48 o 3 0 1 7017.59 6327.82 102.78 o 5 0 1 750.84 836.83 49.84 o 7 0 1 1121.44 1283.27 41.28 o 9 0 1 701.22 697.41 33.01 o 11 0 1 353.83 437.65 28.15 o 13 0 1 21.80 23.00 11.87 o 15 0 1 27.89 49.89 20.43 o -16 1 1 0.56 -2.01 5.61 o -15 1 1 3.51 2.64 2.59 o -14 1 1 82.96 77.06 11.72 o -13 1 1 242.55 274.13 24.53 o -12 1 1 141.85 136.25 16.61 o -11 1 1 88.45 83.16 6.34 o -10 1 1 0.16 2.59 1.60 o -9 1 1 255.46 283.30 10.23 o -8 1 1 98.67 208.31 46.98 o -7 1 1 1171.29 1143.15 27.82 o -6 1 1 237.46 200.53 16.94 o -5 1 1 768.87 694.37 65.53 o -4 1 1 1351.20 1256.99 17.72 o -3 1 1 6744.58 6366.40 72.89 o -2 1 1 938.01 923.13 14.88 o -1 1 1 15532.88 15590.11 334.53 o 0 1 1 821.05 917.55 21.00 o 1 1 1 1371.85 1154.85 133.49 o 2 1 1 190.36 173.27 7.22 o 3 1 1 607.05 597.05 71.25 o 4 1 1 277.67 278.88 14.02 o 5 1 1 2278.39 1918.97 73.09 o 6 1 1 570.95 1186.68 42.04 o 7 1 1 967.12 1090.48 46.02 o 8 1 1 19.12 15.96 3.16 o 9 1 1 175.90 197.17 13.10 o 10 1 1 9.11 14.89 2.79 o 11 1 1 7.79 7.05 2.48 o 12 1 1 158.16 141.95 15.37 o 13 1 1 169.55 175.37 17.58 o 14 1 1 16.98 8.89 4.59 o 15 1 1 3.98 3.87 9.24 o -16 2 1 16.70 11.76 4.41 o -15 2 1 3.03 -1.10 2.93 o -14 2 1 2.58 3.06 2.82 o -13 2 1 3.76 11.17 6.26 o -12 2 1 48.34 110.38 31.25 o -11 2 1 384.86 399.19 29.94 o -10 2 1 3.09 0.86 1.25 o -9 2 1 697.59 957.05 48.62 o -8 2 1 536.44 539.73 26.79 o -7 2 1 501.04 489.46 48.18 o -6 2 1 1111.35 1318.65 41.83 o -5 2 1 3718.97 3535.93 89.90 o -4 2 1 1639.84 1730.11 27.56 o -3 2 1 5296.87 5824.64 70.57 o -2 2 1 70.84 82.49 7.70 o -1 2 1 1122.87 1251.51 17.25 o 0 2 1 2390.30 2604.96 27.85 o 1 2 1 781.47 805.79 12.03 o 2 2 1 2850.90 2584.54 55.92 o 3 2 1 888.84 883.12 25.14 o 4 2 1 169.10 154.98 8.50 o 5 2 1 95.24 104.47 5.33 o 6 2 1 649.03 689.97 31.12 o 7 2 1 2.17 1.88 1.37 o 8 2 1 34.53 57.69 29.03 o 9 2 1 22.87 11.48 5.16 o 10 2 1 0.04 1.38 2.53 o 11 2 1 69.09 76.60 13.67 o 12 2 1 89.74 106.45 16.54 o 13 2 1 1.11 0.52 4.22 o 14 2 1 10.27 14.99 5.42 o 15 2 1 179.94 173.87 26.73 o -15 3 1 155.38 164.94 23.15 o -14 3 1 1.58 1.89 12.52 o -13 3 1 1.43 -0.15 8.70 o -12 3 1 71.81 75.96 14.80 o -11 3 1 22.72 44.60 10.64 o -10 3 1 282.67 459.98 56.92 o -9 3 1 0.12 -1.03 3.53 o -8 3 1 426.71 457.74 23.06 o -7 3 1 2476.53 2315.35 118.31 o -6 3 1 2327.01 2198.38 74.94 o -5 3 1 83.63 91.71 7.82 o -4 3 1 2396.96 2362.21 45.52 o -3 3 1 946.78 970.74 20.12 o -2 3 1 310.33 351.55 9.31 o -1 3 1 2135.81 2213.04 23.88 o 0 3 1 910.04 917.03 16.92 o 1 3 1 984.70 1023.24 16.79 o 2 3 1 133.35 146.00 7.01 o 3 3 1 322.70 236.59 12.07 o 4 3 1 223.72 168.61 16.87 o 5 3 1 1177.41 704.41 198.49 o 6 3 1 12.03 112.22 12.15 o 7 3 1 0.47 -0.36 2.58 o 8 3 1 132.97 140.93 13.74 o 9 3 1 102.15 77.29 10.65 o 10 3 1 99.01 91.25 16.71 o 11 3 1 171.71 168.40 21.39 o 12 3 1 32.38 36.10 10.07 o 13 3 1 239.52 251.61 35.06 o 14 3 1 179.18 179.68 24.21 o -15 4 1 0.10 15.81 8.35 o -14 4 1 44.51 41.13 11.93 o -13 4 1 119.08 124.69 19.77 o -12 4 1 136.81 147.54 20.52 o -11 4 1 8.24 35.71 16.93 o -10 4 1 10.98 29.73 10.03 o -9 4 1 13.49 28.44 9.80 o -8 4 1 475.02 487.03 28.31 o -7 4 1 119.54 99.06 10.04 o -6 4 1 780.31 792.41 30.82 o -5 4 1 570.99 648.36 24.40 o -4 4 1 102.43 102.36 7.36 o -3 4 1 190.01 189.08 12.52 o -2 4 1 3216.72 3284.20 49.61 o -1 4 1 2130.36 2307.97 24.69 o 0 4 1 488.32 602.95 12.40 o 1 4 1 766.46 812.17 14.68 o 2 4 1 98.19 70.45 4.63 o 3 4 1 281.60 323.48 10.01 o 4 4 1 395.75 157.47 75.61 o 5 4 1 968.95 871.50 17.04 o 6 4 1 12.71 35.18 11.61 o 7 4 1 3.32 10.26 4.77 o 8 4 1 170.82 179.52 19.07 o 9 4 1 10.59 13.31 4.16 o 10 4 1 195.13 214.88 24.90 o 11 4 1 410.03 414.21 34.95 o 12 4 1 164.18 160.89 26.47 o 13 4 1 56.18 62.26 14.12 o 14 4 1 0.05 2.68 3.28 o -14 5 1 46.14 51.32 13.68 o -13 5 1 43.84 54.87 15.50 o -12 5 1 0.15 2.67 2.83 o -11 5 1 26.72 22.93 7.81 o -10 5 1 8.97 17.43 7.72 o -9 5 1 171.71 532.47 96.53 o -8 5 1 114.82 265.11 25.40 o -7 5 1 23.38 10.27 2.03 o -6 5 1 159.69 143.42 6.66 o -5 5 1 37.95 32.27 8.30 o -4 5 1 617.39 470.56 87.22 o -3 5 1 425.93 475.35 16.50 o -2 5 1 1166.73 1203.96 18.97 o -1 5 1 9.22 10.62 1.65 o 0 5 1 478.89 535.17 14.34 o 1 5 1 654.80 733.14 15.47 o 2 5 1 1.86 0.78 0.85 o 3 5 1 179.93 160.08 9.06 o 4 5 1 123.65 105.53 7.94 o 5 5 1 488.03 523.33 33.43 o 6 5 1 524.70 470.77 34.23 o 7 5 1 165.40 142.48 11.93 o 8 5 1 4.68 7.77 2.58 o 9 5 1 340.74 339.94 31.07 o 10 5 1 572.18 551.10 40.98 o 11 5 1 0.74 -1.93 3.81 o 12 5 1 3.62 -4.23 4.23 o 13 5 1 87.85 72.83 16.36 o -13 6 1 33.82 38.81 11.99 o -12 6 1 82.09 84.98 17.07 o -11 6 1 1.76 -1.74 5.58 o -10 6 1 5.65 -2.54 7.47 o -9 6 1 117.07 139.23 20.21 o -8 6 1 140.07 122.78 6.98 o -7 6 1 190.94 157.43 10.92 o -6 6 1 162.64 153.52 11.47 o -5 6 1 502.96 591.86 24.57 o -4 6 1 215.80 229.69 15.66 o -3 6 1 710.32 703.51 23.80 o -2 6 1 38.26 38.22 4.82 o -1 6 1 6.53 6.62 1.48 o 0 6 1 1269.36 1455.83 50.82 o 1 6 1 769.91 760.62 20.00 o 2 6 1 1129.98 1124.25 31.58 o 3 6 1 454.71 559.60 24.63 o 4 6 1 147.78 145.17 11.07 o 5 6 1 6.10 4.60 1.89 o 6 6 1 12.08 44.21 12.49 o 7 6 1 79.32 102.86 16.45 o 8 6 1 980.33 1219.14 78.59 o 9 6 1 30.33 30.59 10.23 o 10 6 1 1.53 1.39 5.99 o 11 6 1 71.07 59.90 14.50 o 12 6 1 87.28 90.33 18.17 o -12 7 1 21.74 32.58 12.50 o -11 7 1 11.18 15.87 8.04 o -10 7 1 98.01 94.77 20.98 o -9 7 1 43.14 57.26 14.00 o -8 7 1 4.06 11.43 6.71 o -7 7 1 163.17 125.73 9.51 o -6 7 1 301.58 286.03 21.70 o -5 7 1 511.04 500.84 24.66 o -4 7 1 178.77 216.14 16.79 o -3 7 1 743.44 768.03 31.79 o -2 7 1 1135.35 1273.86 30.21 o -1 7 1 393.74 430.95 16.52 o 0 7 1 335.83 386.57 21.64 o 1 7 1 0.74 -1.73 1.73 o 2 7 1 142.50 135.94 13.26 o 3 7 1 29.98 32.19 7.76 o 4 7 1 194.01 205.40 18.96 o 5 7 1 267.57 279.28 26.08 o 6 7 1 467.40 421.36 30.70 o 7 7 1 12.92 66.50 14.25 o 8 7 1 164.35 165.20 23.27 o 9 7 1 23.83 20.45 10.60 o 10 7 1 105.25 118.37 20.57 o 11 7 1 36.97 35.31 11.55 o -11 8 1 5.98 1.80 5.56 o -10 8 1 32.07 57.23 15.19 o -9 8 1 0.87 0.06 4.40 o -8 8 1 404.65 415.15 37.41 o -7 8 1 58.39 52.13 13.71 o -6 8 1 142.41 138.38 13.43 o -5 8 1 76.17 67.22 9.80 o -4 8 1 186.72 201.20 17.39 o -3 8 1 68.73 61.23 14.33 o -2 8 1 553.86 618.67 22.22 o -1 8 1 61.28 66.99 6.54 o 0 8 1 1185.27 1108.03 35.87 o 1 8 1 23.33 18.60 4.78 o 2 8 1 357.28 426.90 25.98 o 3 8 1 382.21 445.32 26.12 o 4 8 1 128.45 136.69 13.90 o 5 8 1 4.04 5.78 2.71 o 6 8 1 2.08 158.14 22.83 o 7 8 1 31.09 23.04 15.13 o 8 8 1 1.62 -1.21 3.76 o 9 8 1 1.01 -0.62 5.00 o 10 8 1 12.37 36.44 10.57 o -9 9 1 2.64 5.86 4.04 o -8 9 1 68.57 108.79 20.77 o -7 9 1 42.64 38.14 11.73 o -6 9 1 95.41 92.00 17.79 o -5 9 1 12.45 22.63 5.89 o -4 9 1 319.87 320.56 23.55 o -3 9 1 62.04 61.93 10.12 o -2 9 1 182.87 205.95 19.06 o -1 9 1 0.36 0.87 1.75 o 0 9 1 122.01 121.57 12.57 o 1 9 1 73.85 72.74 9.69 o 2 9 1 112.33 128.04 14.87 o 3 9 1 1.59 4.27 2.86 o 4 9 1 80.87 89.88 12.31 o 5 9 1 4.01 -3.51 5.15 o 6 9 1 25.41 26.90 9.69 o 7 9 1 89.04 98.29 19.26 o 8 9 1 2.26 -5.07 5.07 o 9 9 1 76.87 103.60 20.38 o -7 10 1 90.95 95.38 19.43 o -6 10 1 10.56 12.88 8.68 o -5 10 1 57.12 67.97 16.11 o -4 10 1 160.78 202.04 19.88 o -3 10 1 427.25 417.70 28.94 o -2 10 1 121.26 123.52 15.62 o -1 10 1 0.54 -3.70 3.70 o 0 10 1 188.11 156.65 15.42 o 1 10 1 182.23 166.93 18.26 o 2 10 1 263.33 265.75 22.99 o 3 10 1 10.92 11.49 5.31 o 4 10 1 77.76 73.01 20.53 o 5 10 1 10.94 13.50 7.01 o 6 10 1 156.39 219.93 29.96 o -3 11 1 9.28 11.99 6.48 o -2 11 1 41.61 45.16 10.07 o -1 11 1 14.27 5.15 6.36 o 0 11 1 293.25 304.80 22.88 o 1 11 1 0.58 12.78 5.92 o 2 11 1 49.09 37.78 8.63 o -16 0 2 226.77 247.68 45.34 o -14 0 2 104.05 80.76 23.13 o -12 0 2 30.18 26.15 5.37 o -10 0 2 93.98 119.84 16.11 o -8 0 2 431.95 442.61 18.92 o -6 0 2 138.22 117.29 7.17 o -4 0 2 1242.83 1201.22 42.42 o -2 0 2 75.65 88.46 7.71 o 0 0 2 676.75 463.67 319.55 o 2 0 2 1761.87 1266.07 46.15 o 4 0 2 3746.47 3811.10 70.36 o 6 0 2 309.14 436.57 26.59 o 8 0 2 243.87 246.43 19.56 o 10 0 2 335.35 324.94 24.47 o 12 0 2 24.36 15.15 5.48 o 14 0 2 190.01 198.05 38.91 o -16 1 2 40.71 39.65 12.44 o -15 1 2 135.95 140.56 23.27 o -14 1 2 299.90 302.30 23.65 o -13 1 2 32.69 44.72 10.04 o -12 1 2 277.30 230.21 10.71 o -11 1 2 98.50 82.44 6.31 o -10 1 2 109.26 105.25 6.84 o -9 1 2 47.13 46.96 4.39 o -8 1 2 406.90 402.47 13.04 o -7 1 2 958.92 824.36 55.45 o -6 1 2 651.14 623.53 16.56 o -5 1 2 101.82 94.29 4.22 o -4 1 2 4268.45 3960.35 29.49 o -3 1 2 310.48 331.44 8.82 o -2 1 2 4769.73 5155.96 66.29 o -1 1 2 682.68 771.01 10.88 o 0 1 2 12592.14 12837.24 46.19 o 1 1 2 102.56 41.97 14.40 o 2 1 2 695.25 625.59 36.66 o 3 1 2 1303.57 1219.25 33.36 o 4 1 2 1034.15 563.73 58.15 o 5 1 2 13.06 18.98 4.04 o 6 1 2 732.54 794.50 30.19 o 7 1 2 16.98 11.12 3.65 o 8 1 2 538.47 566.35 23.18 o 9 1 2 161.68 171.18 13.20 o 10 1 2 12.16 17.23 4.26 o 11 1 2 99.27 102.13 7.43 o 12 1 2 441.63 389.72 26.26 o 13 1 2 34.16 41.69 8.70 o 14 1 2 93.08 112.62 20.64 o -16 2 2 2.86 9.37 7.49 o -15 2 2 9.37 10.53 5.56 o -14 2 2 222.73 210.90 23.44 o -13 2 2 48.81 54.37 11.89 o -12 2 2 202.85 194.89 21.23 o -11 2 2 2.12 0.73 0.63 o -10 2 2 1761.07 2148.48 67.97 o -9 2 2 283.16 541.04 30.86 o -8 2 2 1462.94 1761.61 71.92 o -7 2 2 1000.82 956.66 30.94 o -6 2 2 3185.31 3201.63 44.88 o -5 2 2 77.35 88.75 5.75 o -4 2 2 137.65 128.29 11.61 o -3 2 2 3417.60 3732.41 62.40 o -2 2 2 63.68 82.82 6.02 o -1 2 2 114.80 105.85 4.93 o 0 2 2 3834.10 3651.28 56.29 o 1 2 2 1747.84 1460.43 220.14 o 2 2 2 396.06 355.38 21.77 o 3 2 2 380.52 358.07 12.95 o 4 2 2 187.54 134.76 15.61 o 5 2 2 204.04 221.44 14.66 o 6 2 2 472.87 501.98 23.38 o 7 2 2 4.78 -0.45 4.46 o 8 2 2 4.53 10.32 5.45 o 9 2 2 8.81 3.61 1.73 o 10 2 2 175.97 149.59 13.76 o 11 2 2 24.97 18.37 6.85 o 12 2 2 18.32 18.30 8.37 o 13 2 2 2.04 2.28 5.10 o 14 2 2 67.54 57.44 14.71 o -16 3 2 159.82 134.16 34.19 o -15 3 2 60.95 84.72 16.24 o -14 3 2 130.45 135.64 20.30 o -13 3 2 273.43 279.39 27.86 o -12 3 2 244.04 219.24 23.86 o -11 3 2 560.33 669.77 42.91 o -10 3 2 313.56 327.60 21.44 o -9 3 2 317.20 348.91 34.65 o -8 3 2 1426.81 1439.48 51.82 o -7 3 2 1732.68 1759.01 32.59 o -6 3 2 339.92 358.78 13.88 o -5 3 2 123.52 109.14 6.67 o -4 3 2 3375.19 3404.56 45.52 o -3 3 2 2952.74 3321.54 63.51 o -2 3 2 507.06 657.64 14.47 o -1 3 2 195.71 254.37 7.47 o 0 3 2 176.91 198.52 6.86 o 1 3 2 158.38 163.84 5.26 o 2 3 2 824.75 617.08 33.68 o 3 3 2 50.53 39.32 2.66 o 4 3 2 471.64 69.04 63.07 o 5 3 2 90.75 192.65 55.32 o 6 3 2 5.56 18.94 4.26 o 7 3 2 17.23 11.03 5.51 o 8 3 2 11.95 5.38 2.64 o 9 3 2 0.72 18.96 39.67 o 10 3 2 11.02 10.00 4.66 o 11 3 2 9.19 12.04 5.72 o 12 3 2 251.76 242.27 27.45 o 13 3 2 24.58 21.74 7.80 o 14 3 2 14.40 13.66 6.25 o -15 4 2 6.42 -0.03 0.57 o -14 4 2 423.94 404.60 36.33 o -13 4 2 180.65 174.30 23.17 o -12 4 2 0.55 20.15 9.59 o -11 4 2 2.42 12.56 6.34 o -10 4 2 1892.14 1710.76 68.55 o -9 4 2 1912.06 2141.88 131.30 o -8 4 2 384.42 319.10 29.35 o -7 4 2 168.43 168.59 10.12 o -6 4 2 601.71 608.02 21.07 o -5 4 2 1013.88 1126.78 22.73 o -4 4 2 192.04 284.49 13.09 o -3 4 2 808.28 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