#------------------------------------------------------------------------------ #$Date: 2012-09-11 12:26:43 +0300 (Tue, 11 Sep 2012) $ #$Revision: 66590 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/38/2233846.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2233846_Fobs loop_ _publ_author_name 'Akhtar, Tasleem' 'Siddiqui, Waseeq Ahmad' 'Ashraf, Adnan' 'Tahir, M. Nawaz' _publ_section_title ; 2,2'-(4-Methyl-4H-1,2,4-triazole-3,5-diyl)dibenzenesulfonamide ; _journal_coeditor_code HB6629 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o754 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 102.243 _cell_angle_gamma 90.000 _cell_length_a 13.4190 _cell_length_b 6.9043 _cell_length_c 19.0498 _exptl_crystal_F_000 816.00 _reflns_d_resolution_high 0.7599 _[local]_cod_data_source_file hb6629Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' T4UOS_0m in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 195.41 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 21697.95 21511.06 302.74 o 4 0 0 1581.98 1578.15 52.17 o 6 0 0 403.27 480.21 34.06 o 8 0 0 649.10 640.79 53.21 o 10 0 0 885.15 849.57 63.85 o 12 0 0 135.94 44.19 29.13 o 14 0 0 11.01 -18.48 18.48 o 16 0 0 139.46 120.20 28.33 o 1 1 0 9707.23 9522.40 91.89 o 2 1 0 6018.20 5604.01 57.13 o 3 1 0 35.21 37.43 4.14 o 4 1 0 891.03 873.50 20.40 o 5 1 0 897.25 906.94 35.79 o 6 1 0 89.05 81.79 10.98 o 7 1 0 3701.47 3603.85 65.13 o 8 1 0 163.79 162.70 15.45 o 9 1 0 524.27 451.21 25.09 o 10 1 0 385.71 402.03 25.23 o 11 1 0 171.93 195.46 22.19 o 12 1 0 285.07 287.28 27.36 o 13 1 0 54.97 52.34 17.18 o 14 1 0 45.50 6.57 13.00 o 15 1 0 0.85 13.32 12.97 o 16 1 0 121.36 134.02 22.07 o 17 1 0 5.54 10.60 16.82 o 0 2 0 1357.26 1224.79 49.10 o 1 2 0 4929.06 4750.61 57.63 o 2 2 0 912.06 963.95 13.76 o 3 2 0 1327.82 1056.73 16.18 o 4 2 0 403.38 415.97 13.09 o 5 2 0 940.32 662.01 18.25 o 6 2 0 213.08 273.19 14.28 o 7 2 0 642.91 545.69 24.06 o 8 2 0 0.07 -1.56 7.22 o 9 2 0 325.02 344.10 26.94 o 10 2 0 329.47 328.32 22.91 o 11 2 0 1230.77 1314.28 50.25 o 12 2 0 62.17 36.18 15.51 o 13 2 0 1.55 -2.84 12.23 o 14 2 0 6.20 13.29 12.66 o 15 2 0 6.46 24.97 15.05 o 16 2 0 1.23 13.52 16.04 o 1 3 0 303.87 350.04 12.15 o 2 3 0 34.67 39.50 4.90 o 3 3 0 852.94 1005.02 15.19 o 4 3 0 794.88 933.14 18.75 o 5 3 0 306.77 323.61 13.04 o 6 3 0 0.08 1.40 4.45 o 7 3 0 160.75 157.96 10.47 o 8 3 0 694.14 668.04 27.10 o 9 3 0 88.67 101.94 15.20 o 10 3 0 1218.84 1288.52 38.39 o 11 3 0 0.32 6.79 11.64 o 12 3 0 268.68 293.91 25.33 o 13 3 0 156.28 155.74 21.05 o 14 3 0 163.28 118.78 41.18 o 15 3 0 9.43 -1.36 15.86 o 16 3 0 160.77 189.76 30.76 o 0 4 0 5739.21 5642.00 149.93 o 1 4 0 938.25 931.56 21.38 o 2 4 0 3194.70 3380.13 50.12 o 3 4 0 23.87 32.59 7.65 o 4 4 0 608.15 678.47 25.21 o 5 4 0 68.32 68.21 7.60 o 6 4 0 233.59 223.89 16.92 o 7 4 0 238.75 271.15 17.48 o 8 4 0 115.14 118.48 17.34 o 9 4 0 410.86 430.21 26.79 o 10 4 0 72.47 70.66 16.23 o 11 4 0 170.18 179.95 35.03 o 12 4 0 140.75 138.81 33.04 o 13 4 0 2.44 -0.85 16.56 o 14 4 0 5.04 -2.52 19.19 o 15 4 0 42.49 31.79 24.88 o 1 5 0 46.55 38.85 7.35 o 2 5 0 47.00 52.63 10.37 o 3 5 0 371.63 402.77 17.87 o 4 5 0 97.17 108.79 18.33 o 5 5 0 1246.84 1153.34 47.81 o 6 5 0 184.23 203.53 19.95 o 7 5 0 208.32 277.31 23.78 o 8 5 0 39.20 35.92 14.77 o 9 5 0 345.24 421.09 44.65 o 10 5 0 7.48 -0.65 20.66 o 11 5 0 17.12 34.31 20.61 o 12 5 0 41.43 45.19 22.80 o 13 5 0 28.03 28.33 24.14 o 14 5 0 64.87 94.96 30.44 o 0 6 0 816.51 753.81 41.21 o 1 6 0 103.73 125.86 14.29 o 2 6 0 644.96 632.92 29.79 o 3 6 0 1753.55 1691.29 44.12 o 4 6 0 211.87 242.29 28.98 o 5 6 0 519.77 561.04 36.53 o 6 6 0 116.97 149.49 28.30 o 7 6 0 338.17 374.78 29.00 o 8 6 0 11.03 -20.45 20.45 o 9 6 0 267.65 267.72 34.02 o 10 6 0 72.33 101.90 25.40 o 11 6 0 13.31 18.07 23.48 o 12 6 0 32.52 65.29 27.59 o 1 7 0 86.74 97.43 19.42 o 2 7 0 224.69 245.49 32.82 o 3 7 0 112.48 139.00 28.10 o 4 7 0 551.49 468.98 45.30 o 5 7 0 105.57 147.54 23.65 o 6 7 0 71.50 43.64 23.31 o 7 7 0 25.35 19.79 22.42 o 8 7 0 11.43 12.41 35.10 o 9 7 0 46.01 47.73 32.69 o 10 7 0 168.65 171.63 50.22 o 0 8 0 62.25 120.98 52.65 o 1 8 0 8.35 27.07 40.33 o 2 8 0 171.05 176.06 33.13 o 3 8 0 12.81 3.02 18.94 o 4 8 0 0.64 2.80 27.20 o 5 8 0 7.42 45.93 42.19 o 6 8 0 6.16 -37.71 37.71 o 7 8 0 46.37 165.42 66.84 o 8 8 0 1.94 38.83 54.14 o -17 0 1 82.17 95.92 39.33 o -15 0 1 137.36 173.98 68.71 o -13 0 1 353.01 318.55 41.74 o -11 0 1 1716.10 1620.80 74.27 o -9 0 1 1419.80 1472.88 64.16 o -7 0 1 887.11 1044.79 46.85 o -5 0 1 2021.94 2405.41 70.50 o -3 0 1 346.44 381.40 16.37 o 1 0 1 872.24 831.24 15.20 o 3 0 1 3725.52 3183.97 55.50 o 5 0 1 20.07 0.68 9.23 o 7 0 1 632.94 528.65 70.76 o 9 0 1 5185.22 5532.02 153.52 o 11 0 1 1643.01 1452.44 71.36 o 13 0 1 127.91 86.86 22.28 o 15 0 1 25.88 15.17 18.01 o 17 0 1 77.33 78.44 57.50 o -17 1 1 3.85 33.99 17.52 o -16 1 1 24.15 62.49 19.83 o -15 1 1 87.13 100.10 21.05 o -14 1 1 89.11 53.39 29.54 o -13 1 1 131.33 111.05 20.66 o -12 1 1 93.14 89.15 17.85 o -11 1 1 196.32 207.39 23.31 o -10 1 1 190.68 220.17 32.14 o -9 1 1 161.68 157.99 21.36 o -8 1 1 523.25 563.90 26.51 o -7 1 1 63.65 72.79 10.63 o -6 1 1 475.27 486.75 21.31 o -5 1 1 87.91 72.68 9.01 o -4 1 1 4402.07 4263.11 49.03 o -3 1 1 1276.63 1227.28 21.09 o -2 1 1 11699.13 10848.10 106.34 o -1 1 1 452.77 395.04 10.07 o 0 1 1 4018.34 3884.06 42.47 o 1 1 1 1114.22 1059.81 14.34 o 2 1 1 29315.39 27795.71 239.05 o 3 1 1 9169.83 8589.33 82.60 o 4 1 1 11179.36 12082.20 137.59 o 5 1 1 229.55 201.05 21.45 o 6 1 1 760.63 855.51 36.14 o 7 1 1 443.12 567.55 24.70 o 8 1 1 371.22 354.58 35.98 o 9 1 1 103.88 126.76 14.96 o 10 1 1 794.91 798.22 34.38 o 11 1 1 10.59 18.96 12.93 o 12 1 1 371.51 373.07 30.44 o 13 1 1 49.73 45.11 12.97 o 14 1 1 1.49 13.36 12.22 o 15 1 1 1.25 -4.25 13.84 o 16 1 1 12.14 17.11 15.91 o -16 2 1 73.76 52.28 19.32 o -15 2 1 13.89 36.53 14.92 o -14 2 1 50.76 29.46 15.03 o -13 2 1 6.25 -8.61 16.71 o -12 2 1 225.32 221.79 24.82 o -11 2 1 127.92 156.36 20.43 o -10 2 1 776.80 795.84 43.81 o -9 2 1 283.85 270.99 22.08 o -8 2 1 1172.06 1242.08 42.55 o -7 2 1 0.22 -3.30 6.42 o -6 2 1 506.64 431.79 18.13 o -5 2 1 133.16 135.78 10.10 o -4 2 1 155.01 80.91 5.56 o -3 2 1 2650.11 2732.60 32.44 o -2 2 1 2088.22 2430.83 27.84 o -1 2 1 3255.27 3378.27 41.58 o 0 2 1 7857.93 8010.14 109.21 o 1 2 1 2877.54 2681.90 33.71 o 2 2 1 1016.69 1024.16 16.62 o 3 2 1 315.23 284.90 9.48 o 4 2 1 703.97 715.20 15.33 o 5 2 1 262.44 279.25 13.01 o 6 2 1 1294.44 1540.40 34.23 o 7 2 1 127.95 140.95 13.15 o 8 2 1 1516.09 1563.61 38.73 o 9 2 1 77.31 121.43 17.05 o 10 2 1 2648.65 2704.69 55.71 o 11 2 1 34.04 36.31 16.27 o 12 2 1 607.91 669.73 32.58 o 13 2 1 78.88 77.96 16.79 o 14 2 1 243.65 218.97 24.57 o 15 2 1 68.93 92.47 20.49 o 16 2 1 45.12 51.13 17.85 o -16 3 1 1.35 -17.49 32.50 o -15 3 1 0.37 -7.46 16.80 o -14 3 1 2.83 -12.12 14.80 o -13 3 1 260.38 218.72 27.92 o -12 3 1 20.38 31.41 14.51 o -11 3 1 8.42 1.79 11.03 o -10 3 1 1462.55 1549.06 42.71 o -9 3 1 367.28 332.69 31.93 o -8 3 1 121.74 116.82 10.70 o -7 3 1 549.98 607.74 19.40 o -6 3 1 667.30 693.20 18.20 o -5 3 1 826.65 891.02 18.58 o -4 3 1 194.98 188.00 9.52 o -3 3 1 95.59 81.81 6.66 o -2 3 1 3624.54 3542.73 46.71 o -1 3 1 25.53 61.42 6.96 o 0 3 1 2594.91 2604.54 40.26 o 1 3 1 1933.16 2506.93 39.99 o 2 3 1 101.15 96.67 8.10 o 3 3 1 2614.50 2603.10 35.37 o 4 3 1 1.56 3.50 4.76 o 5 3 1 264.33 314.00 15.43 o 6 3 1 32.01 38.36 7.76 o 7 3 1 598.27 615.08 22.62 o 8 3 1 610.89 578.50 23.57 o 9 3 1 109.86 105.72 12.35 o 10 3 1 38.11 39.82 11.24 o 11 3 1 34.36 24.08 13.09 o 12 3 1 19.20 10.25 12.18 o 13 3 1 80.70 77.43 17.61 o 14 3 1 3.04 2.47 16.95 o 15 3 1 46.40 48.36 20.87 o 16 3 1 18.15 27.64 20.79 o -15 4 1 182.14 247.14 39.61 o -14 4 1 58.48 102.84 33.68 o -13 4 1 225.90 240.05 30.01 o -12 4 1 19.46 18.06 17.89 o -11 4 1 604.25 615.93 39.04 o -10 4 1 1.47 -6.00 11.59 o -9 4 1 6.59 -2.36 12.22 o -8 4 1 550.00 522.17 26.69 o -7 4 1 377.63 400.17 17.94 o -6 4 1 179.61 173.11 16.86 o -5 4 1 208.09 196.46 10.44 o -4 4 1 503.19 489.39 18.89 o -3 4 1 881.90 921.20 19.13 o -2 4 1 591.43 566.77 15.98 o -1 4 1 44.64 52.51 4.60 o 0 4 1 53.86 65.39 7.26 o 1 4 1 150.89 172.90 10.97 o 2 4 1 40.06 36.00 7.11 o 3 4 1 0.44 6.94 5.09 o 4 4 1 91.95 84.21 8.59 o 5 4 1 1308.92 1317.69 29.59 o 6 4 1 108.98 104.91 11.53 o 7 4 1 1800.29 1727.96 38.48 o 8 4 1 37.15 11.07 11.80 o 9 4 1 228.33 257.40 26.36 o 10 4 1 203.16 219.03 38.81 o 11 4 1 120.61 123.68 21.12 o 12 4 1 134.82 155.18 24.85 o 13 4 1 22.42 49.56 18.91 o 14 4 1 26.00 52.80 20.82 o 15 4 1 21.94 47.92 21.75 o -14 5 1 61.19 9.32 25.11 o -13 5 1 0.00 -2.04 21.96 o -12 5 1 7.78 -1.02 23.30 o -11 5 1 0.47 5.07 16.84 o -10 5 1 0.31 -7.26 16.78 o -9 5 1 246.21 242.73 25.36 o -8 5 1 192.73 205.96 23.06 o -7 5 1 113.28 130.83 20.76 o -6 5 1 154.59 190.32 19.11 o -5 5 1 835.72 895.27 42.21 o -4 5 1 1303.28 1308.01 37.77 o -3 5 1 139.79 137.45 11.06 o -2 5 1 842.83 764.00 21.10 o -1 5 1 175.40 160.52 9.48 o 0 5 1 403.64 423.54 18.05 o 1 5 1 56.98 59.90 8.80 o 2 5 1 20.41 17.05 7.66 o 3 5 1 291.33 267.42 14.43 o 4 5 1 360.22 374.36 27.21 o 5 5 1 1203.11 1136.65 49.05 o 6 5 1 39.93 40.43 12.72 o 7 5 1 431.47 432.60 28.78 o 8 5 1 51.71 71.33 16.93 o 9 5 1 71.63 44.40 18.87 o 10 5 1 19.15 7.06 17.12 o 11 5 1 26.57 19.76 19.82 o 12 5 1 27.64 21.76 22.20 o 13 5 1 106.67 81.90 30.16 o 14 5 1 41.85 68.67 30.44 o -13 6 1 3.12 -20.78 25.77 o -12 6 1 88.54 135.76 30.34 o -11 6 1 154.31 204.12 70.82 o -10 6 1 37.66 -0.29 18.96 o -9 6 1 172.15 230.83 31.23 o -8 6 1 180.68 194.86 29.37 o -7 6 1 390.51 361.19 28.79 o -6 6 1 322.96 357.58 27.17 o -5 6 1 40.05 46.57 16.87 o -4 6 1 232.83 256.55 25.49 o -3 6 1 54.53 84.51 13.33 o -2 6 1 25.27 9.51 9.19 o -1 6 1 206.50 223.69 17.17 o 0 6 1 329.03 320.80 20.93 o 1 6 1 11.03 -4.23 8.77 o 2 6 1 738.64 767.33 31.11 o 3 6 1 329.36 391.10 29.43 o 4 6 1 157.80 189.38 22.53 o 5 6 1 246.76 292.05 22.07 o 6 6 1 29.44 41.99 13.43 o 7 6 1 254.56 290.83 31.08 o 8 6 1 38.68 61.74 20.05 o 9 6 1 39.16 36.08 20.94 o 10 6 1 232.49 283.84 38.03 o 11 6 1 12.38 22.45 22.98 o 12 6 1 150.69 99.73 32.38 o -11 7 1 0.09 9.42 31.92 o -10 7 1 26.59 68.47 34.27 o -9 7 1 20.83 13.23 27.98 o -8 7 1 9.02 4.97 30.62 o -7 7 1 42.55 49.74 23.30 o -6 7 1 36.90 57.20 18.64 o -5 7 1 30.56 10.65 17.85 o -4 7 1 197.49 176.12 30.47 o -3 7 1 49.09 39.17 20.08 o -2 7 1 31.87 8.55 16.19 o -1 7 1 21.10 31.52 14.78 o 0 7 1 30.48 17.48 13.41 o 1 7 1 409.07 407.49 40.38 o 2 7 1 0.63 3.15 15.34 o 3 7 1 491.30 536.48 54.95 o 4 7 1 0.23 19.28 17.35 o 5 7 1 459.12 429.96 35.68 o 6 7 1 102.41 98.37 31.63 o 7 7 1 156.74 82.88 28.52 o 8 7 1 3.28 47.54 30.12 o 9 7 1 53.98 18.63 29.77 o 10 7 1 1.21 -3.54 29.30 o -8 8 1 120.57 117.25 59.74 o -7 8 1 13.69 -40.33 40.33 o -6 8 1 393.51 495.88 89.62 o -5 8 1 39.91 44.81 45.93 o -4 8 1 12.47 19.78 22.44 o -3 8 1 53.08 75.91 27.93 o -2 8 1 8.41 28.52 27.05 o -1 8 1 14.84 12.36 25.47 o 0 8 1 3.57 29.50 24.29 o 1 8 1 1.29 24.83 26.63 o 2 8 1 1.04 -4.89 19.94 o 3 8 1 8.03 39.22 22.05 o 4 8 1 71.85 76.55 51.16 o 5 8 1 42.49 30.25 44.06 o 6 8 1 65.69 119.49 55.26 o 7 8 1 117.37 129.95 60.49 o -16 0 2 6.65 0.88 21.66 o -14 0 2 302.45 225.51 37.76 o -12 0 2 159.25 153.58 29.66 o -10 0 2 469.80 365.63 67.96 o -8 0 2 703.22 756.50 49.09 o -6 0 2 476.17 349.70 28.89 o -4 0 2 2640.65 2261.44 111.05 o -2 0 2 6207.64 5998.40 177.26 o 0 0 2 5905.24 5719.61 70.72 o 2 0 2 38185.37 36572.92 419.92 o 4 0 2 85.06 100.90 12.32 o 6 0 2 6189.32 5524.69 139.81 o 8 0 2 532.00 404.22 50.78 o 10 0 2 309.91 338.74 35.66 o 12 0 2 762.13 754.47 59.72 o 14 0 2 0.07 5.28 22.28 o 16 0 2 42.06 36.03 24.03 o -17 1 2 41.04 34.89 17.93 o -16 1 2 0.00 10.32 14.91 o -15 1 2 261.03 269.92 33.63 o -14 1 2 39.40 48.80 16.75 o -13 1 2 1013.65 827.26 46.51 o -12 1 2 568.72 585.91 46.94 o -11 1 2 774.13 734.13 39.88 o -10 1 2 2017.72 1977.43 112.91 o -9 1 2 2219.56 2330.72 53.04 o -8 1 2 3661.08 3600.56 67.95 o -7 1 2 28.57 26.31 13.12 o -6 1 2 38.13 17.51 7.60 o -5 1 2 3562.93 3910.99 58.88 o -4 1 2 198.18 228.60 9.42 o -3 1 2 4113.63 4119.70 48.90 o -2 1 2 1597.36 1780.14 22.08 o -1 1 2 97.26 97.08 3.92 o 0 1 2 2314.98 2175.77 26.72 o 1 1 2 682.07 728.27 10.54 o 2 1 2 2820.37 2947.56 28.60 o 3 1 2 1860.08 1820.30 22.57 o 4 1 2 11712.25 12543.38 126.31 o 5 1 2 0.10 -4.08 4.98 o 6 1 2 828.39 784.84 24.56 o 7 1 2 309.93 290.59 16.63 o 8 1 2 184.44 116.33 15.06 o 9 1 2 172.86 186.82 14.26 o 10 1 2 402.13 363.68 30.49 o 11 1 2 23.35 22.08 9.78 o 12 1 2 219.32 205.32 19.35 o 13 1 2 220.09 192.96 20.42 o 14 1 2 2.63 -1.05 11.70 o 15 1 2 406.40 440.05 34.31 o 16 1 2 0.23 -4.63 15.79 o -17 2 2 144.53 104.12 22.51 o -16 2 2 18.54 8.03 17.25 o -15 2 2 7.86 3.93 14.06 o -14 2 2 40.82 8.82 14.32 o -13 2 2 13.93 1.78 13.12 o -12 2 2 34.35 32.01 14.11 o -11 2 2 12.13 20.18 12.22 o -10 2 2 9.25 5.59 10.62 o -9 2 2 48.00 51.91 10.93 o -8 2 2 1067.30 1091.82 32.10 o -7 2 2 789.39 934.70 26.02 o -6 2 2 22.08 14.65 6.53 o -5 2 2 1862.00 1839.45 34.01 o -4 2 2 2486.02 2411.73 31.53 o -3 2 2 14661.67 15513.78 152.81 o -2 2 2 1609.52 1622.93 22.67 o -1 2 2 33625.05 32029.39 325.62 o 0 2 2 239.98 256.24 9.75 o 1 2 2 2794.49 2679.77 34.64 o 2 2 2 783.93 831.14 14.69 o 3 2 2 5116.31 5266.15 58.09 o 4 2 2 29.79 40.24 5.85 o 5 2 2 2257.39 2314.53 35.56 o 6 2 2 1629.98 1650.65 32.83 o 7 2 2 133.92 194.34 12.13 o 8 2 2 57.49 60.39 8.83 o 9 2 2 93.90 110.16 11.47 o 10 2 2 16.29 11.95 8.33 o 11 2 2 1096.47 1083.60 42.05 o 12 2 2 6.36 6.09 10.12 o 13 2 2 146.54 111.18 18.69 o 14 2 2 10.26 10.03 13.35 o 15 2 2 61.33 79.79 18.17 o 16 2 2 15.65 17.87 16.34 o -16 3 2 1.39 21.59 19.30 o -15 3 2 77.07 70.29 25.50 o -14 3 2 18.68 2.88 16.41 o -13 3 2 262.01 275.58 34.82 o -12 3 2 0.99 -12.26 12.26 o -11 3 2 9.83 -3.49 12.54 o -10 3 2 284.36 268.01 29.16 o -9 3 2 23.68 32.11 10.06 o -8 3 2 1903.99 1907.83 36.56 o -7 3 2 143.66 157.30 11.27 o -6 3 2 682.67 658.12 18.22 o -5 3 2 1.42 5.84 4.95 o -4 3 2 1116.95 1115.26 20.47 o -3 3 2 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