#------------------------------------------------------------------------------ #$Date: 2012-09-11 12:26:43 +0300 (Tue, 11 Sep 2012) $ #$Revision: 66590 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/38/2233850.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2233850_Fobs loop_ _publ_author_name 'Wardell, James L.' 'Tiekink, Edward R. T.' _publ_section_title ; 6-Methoxy-2-phenyl-4,4a,6,7,8,8a-hexahydro-2H-pyrano[3,2-d][1,3]dioxine-7,8-diyl bis(4-methylbenzene-1-sulfonate) ; _journal_coeditor_code HB6633 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o758 _journal_volume 68 _journal_year 2012 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 5.7031 _cell_length_b 17.0201 _cell_length_c 28.0840 _exptl_crystal_F_000 1240.00 _reflns_d_resolution_high 0.7696 _[local]_cod_data_source_file hb6633Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 0301' _shelx_refln_list_code 4 _shelx_f_calc_maximum 239.94 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 13312.21 13220.27 198.96 o 4 0 0 438.30 418.79 65.97 o 6 0 0 838.15 890.08 229.39 o 1 1 0 5300.01 4827.01 61.85 o 2 1 0 5148.63 5152.60 68.00 o 3 1 0 15.99 37.90 11.09 o 4 1 0 33.21 63.94 40.14 o 5 1 0 741.94 656.37 96.57 o 6 1 0 226.55 101.61 52.28 o 7 1 0 406.06 318.28 117.13 o 1 2 0 57572.48 53740.35 938.68 o 2 2 0 8.08 23.47 17.87 o 3 2 0 143.08 129.17 25.91 o 4 2 0 874.26 1073.22 141.78 o 5 2 0 3830.11 3557.18 171.69 o 6 2 0 141.33 241.14 137.13 o 7 2 0 221.99 251.15 79.23 o 1 3 0 21843.70 20834.46 200.23 o 2 3 0 274.26 279.01 24.20 o 3 3 0 511.65 494.12 54.53 o 4 3 0 6.92 89.63 34.66 o 5 3 0 188.41 203.15 47.22 o 6 3 0 3.41 24.22 49.21 o 7 3 0 1.62 56.93 82.00 o 0 4 0 1484.77 1385.22 70.55 o 1 4 0 8236.35 7408.21 80.81 o 2 4 0 334.53 313.59 22.50 o 3 4 0 5522.03 5642.11 225.05 o 4 4 0 2231.07 2459.17 362.39 o 5 4 0 458.13 561.87 98.12 o 6 4 0 596.40 560.54 130.95 o 7 4 0 0.08 36.20 50.50 o 1 5 0 3065.89 3062.12 38.68 o 2 5 0 785.08 901.60 57.43 o 3 5 0 242.27 249.87 28.15 o 4 5 0 174.27 139.17 38.78 o 5 5 0 4.11 78.94 36.32 o 6 5 0 392.23 328.90 82.52 o 7 5 0 676.29 389.36 91.60 o 0 6 0 1546.87 1370.53 74.92 o 1 6 0 23.47 49.23 13.56 o 2 6 0 2798.52 2681.97 60.82 o 3 6 0 1795.50 1825.98 99.47 o 4 6 0 305.60 474.29 67.92 o 5 6 0 359.63 375.98 53.13 o 6 6 0 298.13 215.60 58.12 o 7 6 0 7.41 55.27 43.23 o 1 7 0 255.10 259.85 16.01 o 2 7 0 5080.18 5364.43 160.53 o 3 7 0 321.87 341.96 52.77 o 4 7 0 2515.89 2497.64 94.56 o 5 7 0 1051.13 942.59 106.96 o 6 7 0 133.99 155.15 50.61 o 7 7 0 1.93 44.51 43.33 o 0 8 0 39395.78 38993.15 611.47 o 1 8 0 2412.70 2420.33 80.54 o 2 8 0 129.18 225.31 29.00 o 3 8 0 514.16 552.30 58.57 o 4 8 0 203.85 179.49 33.09 o 5 8 0 188.10 163.61 59.97 o 6 8 0 25.88 69.80 48.27 o 1 9 0 244.11 289.06 33.28 o 2 9 0 367.34 428.46 46.12 o 3 9 0 3161.32 3290.13 174.07 o 4 9 0 57.86 55.54 17.52 o 5 9 0 45.41 40.81 39.69 o 6 9 0 150.03 116.70 45.41 o 0 10 0 2.72 61.16 54.94 o 1 10 0 443.37 519.31 51.83 o 2 10 0 606.76 741.35 86.61 o 3 10 0 164.64 153.04 28.10 o 4 10 0 566.33 646.53 76.40 o 5 10 0 8.27 65.61 38.06 o 6 10 0 296.25 165.67 125.66 o 1 11 0 1547.97 1587.84 93.51 o 2 11 0 834.68 886.42 108.24 o 3 11 0 1405.40 1615.70 103.13 o 4 11 0 193.75 261.47 45.40 o 5 11 0 294.17 331.97 69.25 o 6 11 0 96.11 104.84 65.51 o 0 12 0 563.00 524.18 75.77 o 1 12 0 269.08 315.87 38.78 o 2 12 0 136.80 92.53 24.46 o 3 12 0 1776.77 1793.44 120.09 o 4 12 0 70.65 98.23 32.06 o 5 12 0 1676.66 1544.16 143.67 o 6 12 0 25.00 147.07 57.01 o 1 13 0 983.61 1012.13 84.66 o 2 13 0 892.50 905.52 99.04 o 3 13 0 0.03 41.00 16.46 o 4 13 0 936.50 890.95 77.30 o 5 13 0 291.61 356.34 98.81 o 0 14 0 4802.97 4535.71 191.62 o 1 14 0 114.49 117.98 38.94 o 2 14 0 2.44 36.49 20.60 o 3 14 0 58.02 100.42 30.23 o 4 14 0 17.99 111.98 41.23 o 5 14 0 77.28 81.38 93.27 o 1 15 0 1415.32 1343.24 89.35 o 2 15 0 261.98 206.24 40.72 o 3 15 0 66.09 45.81 21.53 o 4 15 0 668.41 639.84 113.33 o 5 15 0 0.08 20.02 53.21 o 0 16 0 167.56 237.38 60.63 o 1 16 0 624.88 558.07 64.01 o 2 16 0 108.25 128.58 45.37 o 3 16 0 9.67 62.89 38.27 o 4 16 0 203.92 186.10 72.97 o 5 16 0 195.90 163.56 54.86 o 1 17 0 72.35 116.26 22.08 o 2 17 0 103.04 110.95 33.65 o 3 17 0 126.21 118.15 58.66 o 4 17 0 18.84 54.04 37.39 o 0 18 0 3486.32 2587.08 346.45 o 1 18 0 599.81 591.63 52.56 o 2 18 0 162.15 134.85 44.88 o 3 18 0 43.49 156.24 46.47 o 4 18 0 147.90 176.08 61.58 o 1 19 0 28.08 26.50 19.94 o 2 19 0 15.41 47.97 52.06 o 3 19 0 0.44 98.93 39.76 o 0 20 0 1000.81 824.49 125.97 o 1 20 0 640.03 582.44 109.07 o 2 20 0 51.29 76.54 81.34 o 3 20 0 88.51 117.78 42.84 o 1 21 0 0.02 52.67 22.65 o 2 21 0 30.79 37.76 24.71 o 0 22 0 1127.23 739.55 162.41 o 1 0 1 3314.56 3175.75 56.28 o 2 0 1 0.14 36.99 15.55 o 3 0 1 3965.16 4023.23 114.41 o 4 0 1 52.07 68.81 23.67 o 5 0 1 70.79 38.95 11.54 o 6 0 1 1438.44 1373.66 209.08 o 7 0 1 30.06 132.41 82.33 o -7 1 1 41.38 54.10 115.01 o -6 1 1 166.14 114.97 179.14 o -5 1 1 1476.19 1568.62 70.64 o -4 1 1 1878.79 1914.42 106.81 o -3 1 1 862.35 865.28 61.43 o -2 1 1 1932.23 1897.73 32.38 o -1 1 1 2618.76 2566.18 38.35 o 1 1 1 2586.69 2395.74 45.90 o 2 1 1 1995.60 1978.32 35.99 o 3 1 1 844.25 836.11 60.26 o 4 1 1 1900.81 1822.40 138.51 o 5 1 1 1463.74 1648.54 229.98 o 6 1 1 153.40 136.67 110.26 o 7 1 1 43.21 210.30 95.66 o -7 2 1 53.24 182.56 98.48 o -6 2 1 13.60 111.70 48.30 o -5 2 1 2029.51 2053.15 121.71 o -4 2 1 1720.19 1842.45 145.09 o -3 2 1 2553.37 2568.26 80.78 o -2 2 1 1925.45 1922.28 58.45 o -1 2 1 11274.85 10735.13 162.07 o 0 2 1 264.15 298.44 16.95 o 1 2 1 11226.66 10680.66 125.00 o 2 2 1 1892.02 1958.85 41.12 o 3 2 1 2582.12 2651.98 145.90 o 4 2 1 1696.76 1649.72 123.10 o 5 2 1 2057.55 1966.83 115.48 o 6 2 1 11.90 66.91 68.55 o 7 2 1 52.41 127.95 60.41 o -7 3 1 169.72 294.82 99.15 o -6 3 1 647.37 882.16 230.48 o -5 3 1 883.15 765.07 99.75 o -4 3 1 1873.20 1971.05 164.10 o -3 3 1 664.81 675.89 76.01 o -2 3 1 895.46 956.25 54.08 o -1 3 1 2225.77 2120.48 30.65 o 0 3 1 103.08 126.99 9.32 o 1 3 1 2183.59 2089.44 25.14 o 2 3 1 889.00 942.37 54.45 o 3 3 1 625.99 626.12 52.98 o 4 3 1 1856.23 1821.78 142.89 o 5 3 1 853.26 863.04 125.71 o 6 3 1 665.77 939.70 271.35 o 7 3 1 164.86 175.77 73.72 o -7 4 1 32.53 96.07 47.65 o -6 4 1 187.59 147.13 57.97 o -5 4 1 411.48 469.88 84.75 o -4 4 1 2491.13 2489.18 142.87 o -3 4 1 63.23 92.17 31.94 o -2 4 1 2486.97 2271.07 44.76 o -1 4 1 1791.00 1832.26 33.76 o 0 4 1 37.96 119.33 19.26 o 1 4 1 1804.89 1816.20 28.04 o 2 4 1 2466.43 2257.94 38.19 o 3 4 1 55.53 68.96 21.75 o 4 4 1 2510.99 2654.91 236.95 o 5 4 1 400.37 399.13 90.91 o 6 4 1 190.88 158.45 63.95 o 7 4 1 31.04 16.59 40.08 o -7 5 1 729.90 558.56 126.05 o -6 5 1 174.87 314.85 105.96 o -5 5 1 2322.06 2446.22 202.24 o -4 5 1 211.78 260.10 68.29 o -3 5 1 200.60 207.23 24.18 o -2 5 1 2288.59 2376.84 113.79 o -1 5 1 11711.07 11048.44 89.82 o 0 5 1 17410.56 16193.19 120.65 o 1 5 1 11690.64 11101.48 86.48 o 2 5 1 2286.06 2346.35 55.31 o 3 5 1 213.04 257.60 29.67 o 4 5 1 214.11 360.02 69.11 o 5 5 1 2317.15 2451.61 183.22 o 6 5 1 175.40 230.18 81.71 o 7 5 1 739.58 636.48 132.65 o -7 6 1 201.85 250.50 46.68 o -6 6 1 11.77 73.35 80.44 o -5 6 1 1156.08 994.88 83.09 o -4 6 1 362.63 306.30 57.16 o -3 6 1 720.07 693.32 66.09 o -2 6 1 2295.58 2258.93 59.11 o -1 6 1 1666.98 1710.16 36.83 o 0 6 1 5997.17 5424.89 46.63 o 1 6 1 1679.31 1674.73 48.05 o 2 6 1 2356.65 2271.62 37.64 o 3 6 1 724.62 831.37 78.49 o 4 6 1 376.84 336.51 61.17 o 5 6 1 1146.60 1055.09 109.71 o 6 6 1 11.03 60.34 69.81 o 7 6 1 201.35 109.36 72.99 o -7 7 1 567.01 508.63 128.99 o -6 7 1 1305.75 1153.11 125.64 o -5 7 1 646.39 588.30 74.21 o -4 7 1 36.30 46.71 32.13 o -3 7 1 301.54 348.22 42.04 o -2 7 1 4383.87 4383.60 136.62 o -1 7 1 1655.40 1684.13 46.01 o 0 7 1 5184.91 5021.09 50.16 o 1 7 1 1661.25 1614.33 27.42 o 2 7 1 4323.34 4267.69 123.83 o 3 7 1 304.09 368.11 42.90 o 4 7 1 31.93 72.67 31.95 o 5 7 1 632.17 701.77 85.88 o 6 7 1 1315.96 1261.18 154.28 o 7 7 1 557.86 504.75 171.61 o -6 8 1 9.14 57.31 56.49 o -5 8 1 146.69 185.84 58.46 o -4 8 1 590.41 568.56 64.05 o -3 8 1 775.99 714.79 75.69 o -2 8 1 804.90 737.39 72.87 o -1 8 1 3999.14 4036.50 65.94 o 0 8 1 24.32 61.21 9.81 o 1 8 1 4056.46 4127.93 54.24 o 2 8 1 823.85 802.68 55.96 o 3 8 1 793.19 713.16 77.45 o 4 8 1 591.58 503.46 85.02 o 5 8 1 144.31 175.64 39.97 o 6 8 1 10.64 77.13 35.55 o -6 9 1 108.91 143.22 126.46 o -5 9 1 175.50 84.89 101.65 o -4 9 1 18.51 40.05 28.77 o -3 9 1 136.48 122.62 31.80 o -2 9 1 58.31 85.81 39.08 o -1 9 1 2367.93 2555.30 75.48 o 0 9 1 2210.05 2283.71 72.94 o 1 9 1 2319.39 2391.68 74.82 o 2 9 1 59.51 92.23 16.52 o 3 9 1 134.12 196.10 31.50 o 4 9 1 22.02 82.54 21.46 o 5 9 1 178.11 223.95 55.17 o 6 9 1 109.85 325.37 100.25 o -6 10 1 25.67 48.66 31.52 o -5 10 1 207.44 144.25 58.42 o -4 10 1 448.66 446.87 64.01 o -3 10 1 1501.91 1565.28 87.94 o -2 10 1 1435.88 1603.33 131.49 o -1 10 1 1499.88 1542.78 81.87 o 0 10 1 305.47 367.80 46.95 o 1 10 1 1462.10 1510.59 89.20 o 2 10 1 1448.23 1355.46 78.62 o 3 10 1 1491.48 1475.36 103.48 o 4 10 1 461.14 429.61 69.77 o 5 10 1 206.68 156.05 45.78 o 6 10 1 26.14 121.91 59.25 o -6 11 1 116.51 159.50 52.49 o -5 11 1 82.42 160.35 51.37 o -4 11 1 341.16 375.45 68.21 o -3 11 1 374.50 450.47 60.67 o -2 11 1 185.68 202.48 37.17 o -1 11 1 381.90 389.33 41.37 o 0 11 1 1920.66 1948.80 83.44 o 1 11 1 371.26 380.32 42.79 o 2 11 1 185.07 137.94 37.89 o 3 11 1 374.97 373.85 57.78 o 4 11 1 346.30 361.13 57.51 o 5 11 1 76.92 86.32 29.32 o 6 11 1 113.45 138.62 45.44 o -6 12 1 88.01 85.46 36.73 o -5 12 1 13.72 82.46 31.62 o -4 12 1 116.35 86.40 25.31 o -3 12 1 542.31 530.75 75.96 o -2 12 1 798.84 736.37 98.39 o -1 12 1 1861.19 1990.19 115.02 o 0 12 1 464.92 397.09 44.16 o 1 12 1 1867.83 1770.58 114.16 o 2 12 1 784.30 814.62 91.90 o 3 12 1 542.02 576.54 74.91 o 4 12 1 119.72 130.12 23.07 o 5 12 1 13.90 15.99 39.57 o 6 12 1 87.50 110.66 42.70 o -5 13 1 405.69 328.29 83.28 o -4 13 1 58.50 100.54 50.37 o -3 13 1 145.01 171.33 41.74 o -2 13 1 170.18 250.42 47.78 o -1 13 1 440.37 460.41 52.43 o 0 13 1 1937.57 1894.95 74.75 o 1 13 1 438.41 481.38 50.15 o 2 13 1 174.63 151.59 26.99 o 3 13 1 144.17 160.46 33.22 o 4 13 1 55.81 70.13 45.44 o 5 13 1 408.16 515.77 110.36 o -5 14 1 14.20 135.52 57.39 o -4 14 1 460.37 515.46 75.06 o -3 14 1 241.68 344.78 60.21 o -2 14 1 1130.24 1030.41 132.85 o -1 14 1 233.08 247.58 40.80 o 0 14 1 541.24 563.15 63.43 o 1 14 1 228.02 237.74 37.40 o 2 14 1 1122.50 952.17 110.47 o 3 14 1 244.86 225.86 48.65 o 4 14 1 457.67 454.79 88.71 o 5 14 1 14.26 69.57 49.50 o -5 15 1 357.85 418.14 85.41 o -4 15 1 214.01 180.59 51.61 o -3 15 1 35.82 45.50 39.67 o -2 15 1 85.17 126.79 54.62 o -1 15 1 486.52 538.83 63.19 o 0 15 1 20.81 74.51 21.46 o 1 15 1 474.31 496.97 57.49 o 2 15 1 88.70 138.12 32.94 o 3 15 1 39.32 99.03 33.53 o 4 15 1 219.32 250.29 68.25 o 5 15 1 361.96 340.28 83.87 o -5 16 1 115.45 90.02 47.31 o -4 16 1 256.34 363.80 65.80 o -3 16 1 408.01 462.94 89.11 o -2 16 1 216.44 205.72 51.36 o -1 16 1 175.01 196.39 34.38 o 0 16 1 15.09 63.30 26.38 o 1 16 1 181.50 220.90 36.38 o 2 16 1 229.50 324.63 48.86 o 3 16 1 400.56 302.53 56.44 o 4 16 1 259.16 401.18 107.57 o 5 16 1 118.71 30.84 40.73 o -4 17 1 36.15 137.36 49.70 o -3 17 1 163.92 237.95 49.07 o -2 17 1 24.68 51.70 43.52 o -1 17 1 256.45 335.72 45.92 o 0 17 1 345.90 328.75 42.56 o 1 17 1 250.89 238.55 40.56 o 2 17 1 24.42 53.41 35.66 o 3 17 1 172.91 183.03 52.06 o 4 17 1 36.74 177.59 64.27 o -4 18 1 28.61 132.80 47.84 o -3 18 1 867.39 858.71 130.13 o -2 18 1 72.67 126.73 50.23 o -1 18 1 252.97 282.86 48.20 o 0 18 1 0.06 110.77 27.98 o 1 18 1 254.24 243.44 41.13 o 2 18 1 70.39 146.30 38.61 o 3 18 1 852.76 726.67 100.40 o 4 18 1 31.92 188.19 61.60 o -3 19 1 41.52 130.84 68.02 o -2 19 1 61.46 88.29 35.39 o -1 19 1 88.68 132.90 30.84 o 0 19 1 102.43 185.94 33.60 o 1 19 1 91.49 116.29 31.32 o 2 19 1 66.07 49.86 23.28 o 3 19 1 45.84 124.61 54.09 o -3 20 1 197.89 216.18 56.99 o -2 20 1 70.55 -8.08 65.49 o -1 20 1 181.55 200.62 44.86 o 0 20 1 33.74 33.28 41.89 o 1 20 1 178.94 206.03 36.21 o 2 20 1 67.27 59.90 29.58 o 3 20 1 196.77 178.26 54.86 o -2 21 1 10.67 46.79 32.63 o -1 21 1 84.52 136.26 47.21 o 0 21 1 57.53 129.77 31.17 o 1 21 1 87.97 68.60 32.94 o 2 21 1 10.43 93.44 36.80 o 0 22 1 0.04 100.35 39.43 o 1 0 2 25553.48 24739.21 234.18 o 2 0 2 1.17 1.34 9.92 o 3 0 2 173.37 214.33 25.54 o 4 0 2 3518.92 3692.41 182.16 o 5 0 2 147.90 99.90 46.21 o 6 0 2 0.98 35.50 114.11 o 7 0 2 454.14 327.57 121.30 o -7 1 2 623.49 302.30 129.04 o -6 1 2 803.01 958.83 145.88 o -5 1 2 1721.76 1742.55 78.82 o -4 1 2 688.99 738.94 76.66 o -3 1 2 978.24 979.24 66.02 o -2 1 2 3883.62 3754.28 50.85 o -1 1 2 539.40 557.06 28.08 o 1 1 2 557.81 581.36 35.02 o 2 1 2 3807.99 3785.30 59.57 o 3 1 2 931.35 994.23 76.91 o 4 1 2 670.90 678.86 79.69 o 5 1 2 1707.45 1442.12 87.76 o 6 1 2 811.70 691.02 116.14 o 7 1 2 625.74 721.17 163.97 o -7 2 2 28.88 115.39 67.44 o -6 2 2 6.91 112.08 60.79 o -5 2 2 1639.67 1714.82 87.55 o -4 2 2 454.02 463.87 48.93 o -3 2 2 482.41 597.13 45.48 o -2 2 2 1169.38 1136.52 65.73 o -1 2 2 15242.21 14520.73 140.70 o 0 2 2 2703.67 2475.47 29.74 o 1 2 2 15212.64 14143.77 138.01 o 2 2 2 1203.93 1224.93 72.38 o 3 2 2 498.27 642.30 52.28 o 4 2 2 461.24 455.43 58.53 o 5 2 2 1639.13 1845.21 184.30 o 6 2 2 6.40 126.21 57.78 o 7 2 2 27.29 104.87 67.34 o -7 3 2 43.60 103.40 181.50 o -6 3 2 161.83 315.22 107.38 o -5 3 2 1394.61 1336.66 102.96 o -4 3 2 1782.38 1672.20 153.46 o -3 3 2 911.62 904.77 76.10 o -2 3 2 699.24 748.18 41.55 o -1 3 2 16016.33 15583.78 174.70 o 0 3 2 7686.17 7247.43 61.55 o 1 3 2 16012.37 15224.73 159.14 o 2 3 2 732.86 826.13 61.39 o 3 3 2 917.58 900.94 78.14 o 4 3 2 1802.08 1685.31 86.06 o 5 3 2 1422.97 1850.00 352.87 o 6 3 2 162.96 371.24 106.63 o 7 3 2 48.72 147.60 122.87 o -7 4 2 13.32 63.57 112.87 o -6 4 2 145.58 190.69 68.53 o -5 4 2 392.81 418.96 85.49 o -4 4 2 299.37 333.60 49.41 o -3 4 2 2823.75 2932.52 185.30 o -2 4 2 934.77 986.06 62.64 o -1 4 2 1797.43 1700.13 45.20 o 0 4 2 7689.52 7225.56 60.05 o 1 4 2 1817.28 1777.85 25.82 o 2 4 2 916.54 919.64 55.47 o 3 4 2 2831.45 2819.21 123.74 o 4 4 2 301.49 270.61 36.16 o 5 4 2 405.66 420.67 132.06 o 6 4 2 140.01 132.12 69.97 o 7 4 2 14.19 175.61 72.90 o -7 5 2 78.73 -7.01 95.18 o -6 5 2 709.44 659.35 108.33 o -5 5 2 348.42 441.48 74.33 o -4 5 2 2740.68 3117.62 199.70 o -3 5 2 1100.43 1069.26 70.13 o -2 5 2 757.59 769.39 51.45 o -1 5 2 6266.65 5936.48 90.85 o 0 5 2 4754.01 4306.76 42.91 o 1 5 2 6204.66 5981.34 73.81 o 2 5 2 766.64 840.96 53.05 o 3 5 2 1078.50 1016.80 68.67 o 4 5 2 2777.77 2566.81 96.36 o 5 5 2 349.24 350.34 124.71 o 6 5 2 731.50 657.64 161.44 o 7 5 2 81.20 158.60 57.33 o -7 6 2 30.42 55.61 39.21 o -6 6 2 27.30 41.99 39.56 o -5 6 2 550.08 510.01 76.50 o -4 6 2 304.03 316.43 62.79 o -3 6 2 820.75 835.08 83.02 o -2 6 2 4190.40 4179.47 69.10 o -1 6 2 158.92 213.95 15.14 o 0 6 2 1011.50 1010.95 45.01 o 1 6 2 149.65 195.85 12.32 o 2 6 2 4193.47 4246.41 58.39 o 3 6 2 812.23 869.55 87.07 o 4 6 2 308.57 359.11 45.75 o 5 6 2 545.14 510.90 70.07 o 6 6 2 26.65 84.60 61.46 o 7 6 2 31.99 227.80 96.23 o -7 7 2 123.71 85.06 43.90 o -6 7 2 196.40 77.31 53.84 o -5 7 2 806.13 697.80 85.67 o -4 7 2 4553.43 4723.40 241.94 o -3 7 2 670.45 689.92 72.85 o -2 7 2 2393.09 2346.12 85.67 o -1 7 2 484.14 554.55 33.93 o 0 7 2 9607.73 9240.93 90.97 o 1 7 2 501.26 504.95 33.64 o 2 7 2 2377.77 2325.80 65.90 o 3 7 2 676.65 704.76 71.54 o 4 7 2 4573.04 4575.86 154.26 o 5 7 2 831.10 840.50 100.71 o 6 7 2 189.85 179.65 59.67 o 7 7 2 123.60 128.28 49.09 o -6 8 2 42.47 119.20 46.59 o -5 8 2 267.90 314.08 72.26 o -4 8 2 1915.68 1638.83 126.82 o -3 8 2 24.46 43.38 35.85 o -2 8 2 1505.55 1534.71 123.05 o -1 8 2 1121.76 1204.01 62.72 o 0 8 2 245.97 273.14 18.35 o 1 8 2 1160.57 1112.69 70.91 o 2 8 2 1531.20 1517.23 72.23 o 3 8 2 25.23 69.50 16.25 o 4 8 2 1879.25 1758.97 137.96 o 5 8 2 264.38 251.27 74.84 o 6 8 2 42.41 113.80 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