#------------------------------------------------------------------------------ #$Date: 2012-09-11 12:26:43 +0300 (Tue, 11 Sep 2012) $ #$Revision: 66590 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/38/2233851.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2233851_Fobs loop_ _publ_author_name 'El-Azab, Adel S.' 'Abdel-Aziz, Alaa A.-M.' 'Ng, Seik Weng' 'Tiekink, Edward R. T.' _publ_section_title ; 2-Methyl-3-(2-methylphenyl)-4-oxo-3,4-dihydroquinazolin-8-yl 4-bromobenzene-1-sulfonate ; _journal_coeditor_code HB6634 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o759 _journal_page_last o760 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 102.804 _cell_angle_gamma 90.000 _cell_length_a 11.0587 _cell_length_b 14.4794 _cell_length_c 13.1357 _exptl_crystal_F_000 984.00 _reflns_d_resolution_high 0.7928 _[local]_cod_data_source_file hb6634Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 214.54 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 164.47 174.06 4.21 o 2 0 0 4002.24 3896.31 57.73 o 3 0 0 28904.98 26126.46 120.24 o 4 0 0 1147.85 1465.16 33.55 o 5 0 0 2132.82 2522.60 50.02 o 6 0 0 2279.15 2209.13 52.74 o 7 0 0 2917.36 2969.51 67.68 o 8 0 0 441.73 432.86 28.18 o 9 0 0 10314.37 11136.71 119.58 o 10 0 0 390.06 425.15 40.33 o 11 0 0 85.69 95.76 20.41 o 12 0 0 767.73 636.30 44.01 o 13 0 0 65.62 38.56 8.54 o 1 1 0 5289.75 4433.79 24.94 o 2 1 0 2823.91 2607.78 81.35 o 3 1 0 46028.90 41258.52 155.68 o 4 1 0 8176.11 8174.36 39.98 o 5 1 0 1575.07 1358.68 28.10 o 6 1 0 4004.02 3930.10 58.97 o 7 1 0 1217.74 1349.22 32.30 o 8 1 0 445.44 416.72 19.62 o 9 1 0 49.04 66.84 9.08 o 10 1 0 562.56 466.96 29.82 o 11 1 0 320.67 278.85 23.04 o 12 1 0 1329.45 1204.48 42.14 o 13 1 0 205.81 193.59 20.58 o 0 2 0 2679.39 2513.91 21.45 o 1 2 0 13591.13 12541.99 80.03 o 2 2 0 1431.33 1322.94 13.45 o 3 2 0 840.97 916.09 11.44 o 4 2 0 2358.19 2372.42 21.45 o 5 2 0 682.85 788.11 13.96 o 6 2 0 56.75 48.47 8.36 o 7 2 0 1241.64 1201.48 48.74 o 8 2 0 4009.05 4378.02 156.45 o 9 2 0 2075.98 2006.58 90.54 o 10 2 0 325.93 299.64 23.69 o 11 2 0 97.33 118.66 14.93 o 12 2 0 23.97 11.84 8.61 o 13 2 0 176.21 159.28 19.72 o 1 3 0 3986.71 3695.83 38.14 o 2 3 0 4337.45 4065.25 33.75 o 3 3 0 1905.36 1807.52 27.03 o 4 3 0 6692.49 6565.22 43.53 o 5 3 0 2099.83 2138.25 148.92 o 6 3 0 6.58 25.18 6.56 o 7 3 0 291.52 310.87 24.81 o 8 3 0 23.86 32.64 6.86 o 9 3 0 170.87 194.70 28.40 o 10 3 0 191.24 174.44 29.64 o 11 3 0 1126.04 937.12 65.08 o 12 3 0 11.44 11.61 10.76 o 13 3 0 675.52 596.28 38.15 o 0 4 0 3778.97 3689.73 43.42 o 1 4 0 7875.38 7237.23 50.96 o 2 4 0 139.58 134.35 7.60 o 3 4 0 45.80 64.38 8.00 o 4 4 0 123.37 82.20 5.04 o 5 4 0 2320.40 2392.76 35.12 o 6 4 0 53.96 68.11 10.24 o 7 4 0 4.74 28.14 7.61 o 8 4 0 209.33 235.63 18.17 o 9 4 0 302.81 266.03 34.22 o 10 4 0 1636.91 1410.30 81.30 o 11 4 0 4.13 7.63 10.20 o 12 4 0 34.16 38.12 5.90 o 13 4 0 19.28 11.63 7.31 o 1 5 0 18.79 18.67 1.71 o 2 5 0 8.91 19.58 3.78 o 3 5 0 620.76 681.91 16.92 o 4 5 0 11.11 25.20 2.84 o 5 5 0 240.22 259.96 15.77 o 6 5 0 6.13 17.53 4.28 o 7 5 0 945.93 1028.92 31.85 o 8 5 0 457.94 500.64 20.68 o 9 5 0 120.57 99.80 22.66 o 10 5 0 46.17 54.05 18.24 o 11 5 0 55.80 45.63 17.48 o 12 5 0 134.81 134.37 21.91 o 13 5 0 1.42 13.38 6.56 o 0 6 0 6482.33 6655.51 54.05 o 1 6 0 5597.61 5111.53 30.47 o 2 6 0 1628.58 1453.21 28.47 o 3 6 0 3155.33 3454.24 38.82 o 4 6 0 1575.20 1560.06 29.94 o 5 6 0 1665.37 1827.79 36.29 o 6 6 0 123.08 144.41 11.48 o 7 6 0 741.87 865.18 31.32 o 8 6 0 817.04 847.16 57.20 o 9 6 0 76.47 88.43 20.13 o 10 6 0 4.92 9.55 11.89 o 11 6 0 10.58 13.70 5.16 o 12 6 0 34.19 40.38 6.25 o 1 7 0 1003.04 1021.11 24.40 o 2 7 0 4504.20 4632.96 165.87 o 3 7 0 5680.52 6035.23 78.48 o 4 7 0 8839.90 8719.87 149.28 o 5 7 0 5008.94 5234.90 82.83 o 6 7 0 6.95 5.57 2.94 o 7 7 0 2954.05 3008.20 48.24 o 8 7 0 942.67 936.17 60.33 o 9 7 0 2.09 7.86 9.05 o 10 7 0 6.68 18.35 11.11 o 11 7 0 423.16 433.40 47.22 o 12 7 0 63.68 58.50 6.37 o 0 8 0 5923.47 5703.43 88.65 o 1 8 0 5175.14 4785.52 125.53 o 2 8 0 1582.17 1577.25 52.75 o 3 8 0 2798.17 2841.99 75.45 o 4 8 0 3292.02 3122.05 85.39 o 5 8 0 2861.21 2933.01 85.76 o 6 8 0 197.25 208.72 16.73 o 7 8 0 1546.63 1434.71 52.40 o 8 8 0 4253.80 4183.22 125.93 o 9 8 0 569.87 580.79 48.20 o 10 8 0 215.99 216.26 28.14 o 11 8 0 248.90 247.14 38.54 o 12 8 0 73.87 81.30 7.37 o 1 9 0 164.85 178.21 16.68 o 2 9 0 1932.01 1982.45 64.46 o 3 9 0 1611.71 1494.44 57.99 o 4 9 0 6446.05 6227.74 122.15 o 5 9 0 3491.09 3163.44 64.75 o 6 9 0 2117.84 1938.82 126.88 o 7 9 0 22.70 33.26 10.81 o 8 9 0 89.56 105.45 14.43 o 9 9 0 27.03 28.44 7.32 o 10 9 0 5.23 7.86 4.06 o 11 9 0 298.97 274.46 41.47 o 0 10 0 2562.25 2217.08 63.19 o 1 10 0 5429.82 5249.01 101.28 o 2 10 0 2594.25 2593.23 76.43 o 3 10 0 626.74 604.01 38.79 o 4 10 0 59.34 66.84 11.05 o 5 10 0 51.98 49.96 7.14 o 6 10 0 4659.17 4303.75 146.04 o 7 10 0 814.48 775.78 33.74 o 8 10 0 460.98 447.46 55.67 o 9 10 0 1184.54 1286.21 52.13 o 10 10 0 88.17 90.26 12.37 o 11 10 0 439.61 434.29 19.76 o 1 11 0 25.21 48.74 10.54 o 2 11 0 620.85 635.73 37.59 o 3 11 0 10539.97 10407.35 297.12 o 4 11 0 544.04 557.73 19.43 o 5 11 0 1894.61 1812.21 51.97 o 6 11 0 2916.12 2820.42 64.28 o 7 11 0 2.80 6.33 4.33 o 8 11 0 14.81 9.83 4.24 o 9 11 0 347.82 324.28 30.04 o 10 11 0 269.13 295.03 19.22 o 0 12 0 5835.12 5902.88 124.66 o 1 12 0 2.55 29.10 13.19 o 2 12 0 247.18 230.97 26.72 o 3 12 0 4119.71 4247.75 127.74 o 4 12 0 25.27 30.89 7.10 o 5 12 0 70.32 75.92 8.84 o 6 12 0 1585.03 1545.87 95.91 o 7 12 0 492.66 480.95 25.09 o 8 12 0 13.92 9.32 3.97 o 9 12 0 886.34 946.18 36.54 o 10 12 0 420.38 363.32 17.14 o 1 13 0 35.76 48.36 13.18 o 2 13 0 521.78 517.64 40.65 o 3 13 0 209.78 200.29 18.17 o 4 13 0 62.80 73.20 14.31 o 5 13 0 273.50 305.75 16.24 o 6 13 0 452.92 450.22 23.41 o 7 13 0 377.15 351.98 19.36 o 8 13 0 7.51 5.97 3.17 o 9 13 0 1.76 7.89 3.54 o 0 14 0 6023.75 6136.63 128.91 o 1 14 0 1274.49 1231.95 60.08 o 2 14 0 37.54 85.47 17.87 o 3 14 0 287.74 335.72 22.37 o 4 14 0 312.34 332.55 21.46 o 5 14 0 399.43 404.77 22.18 o 6 14 0 210.28 198.06 13.96 o 7 14 0 88.89 87.89 8.43 o 8 14 0 406.02 367.64 19.09 o 1 15 0 80.80 84.18 11.10 o 2 15 0 18.75 18.04 6.59 o 3 15 0 1656.57 1785.42 46.86 o 4 15 0 11.75 8.72 7.67 o 5 15 0 7.13 12.70 7.44 o 6 15 0 594.23 582.71 32.94 o 7 15 0 1.87 3.24 3.39 o 0 16 0 577.29 592.57 24.02 o 1 16 0 1261.82 1359.93 37.31 o 2 16 0 25.65 25.58 5.45 o 3 16 0 141.31 151.30 11.87 o 4 16 0 0.88 5.12 2.58 o 5 16 0 120.48 118.04 14.03 o 6 16 0 58.01 58.28 8.37 o 1 17 0 8.34 9.29 3.32 o 2 17 0 1442.33 1496.55 29.39 o 3 17 0 725.14 692.48 16.20 o 4 17 0 724.70 664.48 19.85 o 0 18 0 209.18 209.34 13.36 o 1 18 0 1779.43 1606.66 86.34 o 2 18 0 519.72 438.23 18.49 o -13 1 1 102.46 82.21 9.16 o -12 1 1 40.09 41.47 9.08 o -11 1 1 1457.95 1315.85 50.04 o -10 1 1 435.14 393.07 27.88 o -9 1 1 422.22 460.92 16.87 o -8 1 1 925.86 1009.90 29.27 o -7 1 1 167.85 164.29 14.76 o -6 1 1 644.76 636.09 48.66 o -5 1 1 117.88 133.18 6.14 o -4 1 1 336.99 361.57 25.45 o -3 1 1 7879.51 7576.81 40.34 o -1 1 1 274.59 320.49 6.55 o 0 1 1 33.70 70.48 2.53 o 1 1 1 1023.16 1001.19 16.24 o 2 1 1 2491.95 2294.15 157.72 o 3 1 1 1620.44 1516.30 91.19 o 4 1 1 2081.36 1937.49 28.79 o 5 1 1 2852.65 3177.73 71.91 o 6 1 1 278.33 338.35 15.50 o 7 1 1 72.60 92.60 14.58 o 8 1 1 428.58 562.22 25.48 o 9 1 1 386.85 386.18 25.86 o 10 1 1 642.80 573.95 32.56 o 11 1 1 128.44 125.25 15.40 o 12 1 1 2.38 4.29 4.32 o 13 1 1 320.62 245.69 20.90 o -13 2 1 12.05 30.85 10.26 o -12 2 1 526.94 430.34 24.98 o -11 2 1 351.85 339.53 25.26 o -10 2 1 0.33 27.66 19.39 o -9 2 1 1071.35 1091.63 25.82 o -8 2 1 269.73 286.88 15.64 o -7 2 1 540.00 523.47 32.02 o -6 2 1 700.20 625.24 19.24 o -5 2 1 7829.59 7752.43 92.73 o -4 2 1 1509.11 1386.21 20.25 o -3 2 1 1642.66 2019.95 29.92 o -2 2 1 918.33 840.77 18.08 o -1 2 1 6739.84 6061.34 29.52 o 0 2 1 5642.01 5102.19 28.50 o 1 2 1 13839.00 12881.10 94.94 o 2 2 1 636.12 651.67 28.48 o 3 2 1 2766.93 2550.95 26.56 o 4 2 1 3006.06 3054.39 57.33 o 5 2 1 3939.63 4372.41 122.00 o 6 2 1 918.62 820.49 24.28 o 7 2 1 434.17 434.94 27.91 o 8 2 1 1039.28 1250.64 37.28 o 9 2 1 52.96 69.48 11.18 o 10 2 1 1368.62 1317.08 48.58 o 11 2 1 6.35 9.37 5.26 o 12 2 1 1039.70 825.85 52.93 o 13 2 1 292.25 243.82 22.05 o -13 3 1 13.75 10.25 7.21 o -12 3 1 8.00 5.77 8.26 o -11 3 1 839.07 700.78 57.07 o -10 3 1 576.31 586.17 52.27 o -9 3 1 2017.62 1879.79 87.74 o -8 3 1 1939.67 2040.47 66.38 o -7 3 1 1810.33 1989.34 37.72 o -6 3 1 86.57 74.83 14.90 o -5 3 1 1683.43 1716.66 22.09 o -4 3 1 2997.37 3013.29 75.53 o -3 3 1 9078.70 8411.18 44.80 o -2 3 1 1406.29 1186.51 12.69 o -1 3 1 8341.77 7860.90 45.75 o 0 3 1 12349.02 11144.91 50.18 o 1 3 1 22366.27 19871.91 122.58 o 2 3 1 27827.44 25161.56 433.17 o 3 3 1 4763.51 4049.73 46.84 o 4 3 1 5090.27 5117.70 69.67 o 5 3 1 17.76 34.68 6.84 o 6 3 1 2097.90 2509.51 61.09 o 7 3 1 4694.13 5328.06 73.09 o 8 3 1 58.54 88.26 20.57 o 9 3 1 4300.21 4511.92 137.26 o 10 3 1 496.67 515.42 48.26 o 11 3 1 733.38 713.43 55.95 o 12 3 1 170.44 160.25 25.09 o 13 3 1 18.64 10.39 5.76 o -13 4 1 1198.13 1091.72 52.55 o -12 4 1 232.52 205.95 17.98 o -11 4 1 639.00 562.95 51.53 o -10 4 1 522.67 463.61 47.13 o -9 4 1 12.19 18.36 11.25 o -8 4 1 44.22 53.65 8.33 o -7 4 1 4.38 14.03 5.37 o -6 4 1 10420.33 11227.31 215.53 o -5 4 1 7313.49 7380.57 114.90 o -4 4 1 548.04 356.00 10.73 o -3 4 1 4619.71 4611.42 47.63 o -2 4 1 30205.44 27912.62 269.48 o -1 4 1 13258.62 12452.94 85.53 o 0 4 1 9.05 15.62 7.28 o 1 4 1 808.80 776.67 12.99 o 2 4 1 319.60 299.66 16.41 o 3 4 1 7985.32 7747.59 57.47 o 4 4 1 10293.55 10515.50 76.43 o 5 4 1 3795.46 3785.49 51.65 o 6 4 1 4141.86 4263.37 99.86 o 7 4 1 6165.40 7142.30 85.78 o 8 4 1 591.27 623.30 27.28 o 9 4 1 0.22 18.68 11.09 o 10 4 1 443.08 394.31 43.40 o 11 4 1 663.89 632.69 54.76 o 12 4 1 402.45 342.27 35.31 o 13 4 1 124.17 102.19 14.35 o -13 5 1 38.37 40.08 11.12 o -12 5 1 264.06 265.47 22.75 o -11 5 1 210.28 196.73 30.77 o -10 5 1 2047.49 1766.33 91.43 o -9 5 1 2269.26 2079.39 95.48 o -8 5 1 1950.87 1989.37 42.51 o -7 5 1 3734.45 3946.13 81.32 o -6 5 1 268.37 259.11 19.26 o -5 5 1 6783.34 6926.61 90.78 o -4 5 1 472.33 478.54 15.08 o -3 5 1 901.13 785.96 20.19 o -2 5 1 10279.76 9947.56 47.94 o -1 5 1 16960.71 15913.98 79.73 o 0 5 1 5054.64 4645.85 35.74 o 1 5 1 8030.56 7376.55 100.32 o 2 5 1 5725.79 5058.51 41.54 o 3 5 1 98.60 107.69 5.34 o 4 5 1 5007.46 5226.57 56.14 o 5 5 1 1253.93 1440.49 54.00 o 6 5 1 2119.81 2350.43 56.97 o 7 5 1 288.57 323.99 18.84 o 8 5 1 4214.16 4713.50 85.43 o 9 5 1 1736.46 1591.88 83.87 o 10 5 1 2712.36 2370.19 104.15 o 11 5 1 877.14 899.08 72.94 o 12 5 1 5.97 8.68 9.49 o -12 6 1 321.42 351.84 29.44 o -11 6 1 519.89 445.32 44.04 o -10 6 1 1490.19 1264.59 76.70 o -9 6 1 141.66 144.24 25.99 o -8 6 1 181.69 181.20 12.42 o -7 6 1 2059.74 2235.35 46.02 o -6 6 1 1373.18 1400.39 33.75 o -5 6 1 1707.24 1669.62 34.33 o -4 6 1 10300.45 10118.33 65.23 o -3 6 1 1074.50 1027.89 18.21 o -2 6 1 2414.18 2286.14 41.08 o -1 6 1 282.12 255.04 7.39 o 0 6 1 160.40 179.11 7.35 o 1 6 1 2087.86 2175.15 34.31 o 2 6 1 4472.28 4282.04 179.31 o 3 6 1 1646.37 1602.15 27.95 o 4 6 1 3478.04 3236.40 100.45 o 5 6 1 8998.39 9190.47 84.94 o 6 6 1 540.65 541.22 22.82 o 7 6 1 3858.80 4063.97 53.76 o 8 6 1 30.89 47.68 14.89 o 9 6 1 703.08 707.74 55.75 o 10 6 1 66.18 68.78 10.34 o 11 6 1 843.99 856.84 43.23 o 12 6 1 25.92 33.70 4.69 o -12 7 1 19.25 21.63 5.13 o -11 7 1 12.73 21.60 5.84 o -10 7 1 616.64 586.44 50.79 o -9 7 1 1241.40 1215.23 72.88 o -8 7 1 453.05 431.18 26.49 o -7 7 1 112.80 103.87 7.83 o -6 7 1 1278.28 1310.46 44.83 o -5 7 1 89.41 78.12 6.46 o -4 7 1 0.99 5.65 2.03 o -3 7 1 595.39 548.39 20.11 o -2 7 1 162.71 226.71 11.16 o -1 7 1 1886.42 1872.88 37.44 o 0 7 1 5856.81 5722.72 57.75 o 1 7 1 3517.24 3673.52 124.47 o 2 7 1 535.22 508.11 19.09 o 3 7 1 5685.89 6099.76 55.96 o 4 7 1 823.89 849.46 23.65 o 5 7 1 338.03 386.80 17.87 o 6 7 1 344.11 370.22 19.06 o 7 7 1 1490.93 1557.68 42.56 o 8 7 1 2867.34 2905.57 106.20 o 9 7 1 441.33 509.13 27.90 o 10 7 1 159.09 166.71 15.05 o 11 7 1 177.32 181.03 13.57 o 12 7 1 157.61 130.86 16.91 o -12 8 1 163.98 143.75 20.84 o -11 8 1 177.96 152.86 12.50 o -10 8 1 17.20 17.52 10.02 o -9 8 1 5.54 7.84 4.92 o -8 8 1 1030.03 959.47 39.41 o -7 8 1 1113.02 1062.10 54.42 o -6 8 1 485.81 601.99 129.27 o -5 8 1 1240.05 1157.74 49.40 o -4 8 1 292.97 347.39 26.66 o -3 8 1 6305.18 6594.08 111.01 o -2 8 1 1218.95 1304.97 80.97 o -1 8 1 1946.37 1940.00 36.02 o 0 8 1 568.82 677.54 21.84 o 1 8 1 110.35 87.62 12.42 o 2 8 1 1319.99 1349.73 52.25 o 3 8 1 318.18 291.67 16.30 o 4 8 1 7554.21 8226.83 283.75 o 5 8 1 54.81 54.21 8.62 o 6 8 1 2035.47 1918.48 50.60 o 7 8 1 185.92 200.14 38.84 o 8 8 1 142.84 149.26 15.57 o 9 8 1 10.43 28.83 10.35 o 10 8 1 18.25 26.10 6.69 o 11 8 1 2.92 6.56 3.75 o -11 9 1 1.34 4.64 3.04 o -10 9 1 16.70 12.26 16.51 o -9 9 1 188.26 199.48 17.67 o -8 9 1 296.98 276.65 29.03 o -7 9 1 3.42 4.51 5.39 o -6 9 1 1078.97 1070.23 56.29 o -5 9 1 1267.47 1129.73 37.79 o -4 9 1 1438.70 1501.46 58.29 o -3 9 1 70.17 110.73 15.47 o -2 9 1 1211.66 1252.02 48.85 o -1 9 1 117.65 176.75 11.78 o 0 9 1 684.32 703.85 23.77 o 1 9 1 399.92 367.57 26.93 o 2 9 1 146.79 132.11 17.06 o 3 9 1 177.26 175.80 21.31 o 4 9 1 1749.45 1742.70 68.37 o 5 9 1 1521.26 1431.68 37.11 o 6 9 1 164.19 155.24 12.23 o 7 9 1 67.60 74.66 10.73 o 8 9 1 13.79 23.22 6.71 o 9 9 1 204.44 216.08 17.19 o 10 9 1 1.81 7.28 4.46 o 11 9 1 3.04 10.52 4.74 o -11 10 1 3.52 0.42 2.55 o -10 10 1 179.21 193.72 17.99 o -9 10 1 0.38 7.53 4.64 o -8 10 1 345.56 355.75 21.93 o -7 10 1 214.64 215.50 26.79 o -6 10 1 1142.84 992.61 38.88 o -5 10 1 2688.76 2565.08 48.35 o -4 10 1 2.61 10.60 6.13 o -3 10 1 1371.36 1439.04 57.14 o -2 10 1 36.63 48.48 10.14 o -1 10 1 463.88 424.10 19.41 o 0 10 1 169.27 164.79 17.73 o 1 10 1 134.53 162.99 19.02 o 2 10 1 208.79 217.13 23.22 o 3 10 1 74.26 78.79 14.85 o 4 10 1 208.16 201.37 16.31 o 5 10 1 13.54 19.64 6.14 o 6 10 1 373.04 367.65 32.48 o 7 10 1 736.24 706.60 44.21 o 8 10 1 28.41 18.31 8.24 o 9 10 1 10.42 8.18 6.15 o 10 10 1 116.75 115.38 13.30 o 11 10 1 92.49 79.40 7.73 o -10 11 1 307.28 338.21 20.98 o -9 11 1 242.18 256.38 34.95 o -8 11 1 499.94 487.06 29.82 o -7 11 1 445.23 400.82 61.42 o -6 11 1 130.03 142.46 11.79 o -5 11 1 893.39 883.51 28.58 o -4 11 1 2268.86 2211.60 45.46 o -3 11 1 3393.04 3274.33 65.19 o -2 11 1 929.63 938.41 48.67 o -1 11 1 43.59 42.28 9.84 o 0 11 1 2190.58 2047.01 64.32 o 1 11 1 327.92 328.83 20.18 o 2 11 1 1559.93 1562.34 77.39 o 3 11 1 210.65 188.91 13.00 o 4 11 1 113.08 108.59 12.58 o 5 11 1 634.86 655.60 32.55 o 6 11 1 418.06 441.81 57.10 o 7 11 1 1082.33 1090.55 40.33 o 8 11 1 130.18 123.53 12.90 o 9 11 1 1042.58 1146.28 44.99 o 10 11 1 297.80 261.10 17.12 o -10 12 1 202.58 176.39 12.44 o -9 12 1 19.05 24.89 4.87 o -8 12 1 545.68 499.81 38.50 o -7 12 1 0.71 8.03 6.72 o -6 12 1 690.20 687.11 33.96 o -5 12 1 6136.88 5922.06 127.39 o -4 12 1 596.33 555.51 30.22 o -3 12 1 425.17 406.39 25.60 o -2 12 1 1631.25 1564.15 68.13 o -1 12 1 928.87 920.22 34.98 o 0 12 1 6.38 14.92 3.93 o 1 12 1 1425.33 1407.64 42.77 o 2 12 1 19.98 12.24 7.59 o 3 12 1 1825.62 1777.90 40.43 o 4 12 1 892.35 860.26 35.01 o 5 12 1 973.01 1008.49 58.25 o 6 12 1 3294.99 3231.87 67.76 o 7 12 1 39.94 35.45 7.40 o 8 12 1 82.53 78.07 9.11 o 9 12 1 6.51 12.66 5.33 o 10 12 1 408.91 381.79 16.03 o -9 13 1 581.24 493.60 25.10 o -8 13 1 2041.22 1894.63 97.24 o -7 13 1 51.00 63.06 12.05 o -6 13 1 766.53 724.63 23.90 o -5 13 1 43.76 54.87 9.20 o -4 13 1 85.49 119.54 14.28 o -3 13 1 284.34 266.27 24.56 o -2 13 1 6610.60 6582.05 142.83 o -1 13 1 318.00 314.35 23.70 o 0 13 1 393.52 379.13 23.03 o 1 13 1 5085.22 5008.46 124.54 o 2 13 1 1209.37 1244.01 63.40 o 3 13 1 1403.73 1453.81 49.16 o 4 13 1 6.97 16.66 6.52 o 5 13 1 132.12 126.28 13.27 o 6 13 1 637.76 605.50 27.34 o 7 13 1 1737.23 1723.92 42.12 o 8 13 1 695.73 641.00 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