#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:36:18 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181260 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/38/2233857.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2233857_Fobs loop_ _publ_author_name 'El-Azab, Adel S.' 'Abdel-Aziz, Alaa A.-M.' 'Ng, Seik Weng' 'Tiekink, Edward R. T.' _publ_section_title ; 2-Methyl-3-(2-methylphenyl)-7-nitroquinazolin-4(3H)-one ; _journal_coeditor_code HB6642 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o863 _journal_volume 68 _journal_year 2012 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 119.072 _cell_angle_gamma 90.000 _cell_length_a 14.4614 _cell_length_b 16.5383 _cell_length_c 12.9968 _exptl_crystal_F_000 1232.00 _reflns_d_resolution_high 0.7924 _cod_data_source_file hb6642Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 246.40 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 8 0 0 93.30 111.76 10.08 o 10 0 0 2816.25 2706.38 37.36 o 12 0 0 383.36 378.30 20.97 o 14 0 0 376.66 386.65 17.75 o 1 1 0 6006.35 5188.99 19.66 o 3 1 0 16837.40 14693.97 48.30 o 5 1 0 17905.72 17299.14 52.33 o 7 1 0 214.29 225.99 19.05 o 9 1 0 7163.85 7128.42 58.78 o 11 1 0 1453.00 1472.41 28.79 o 13 1 0 151.32 162.26 9.17 o 15 1 0 97.73 112.12 5.61 o 2 2 0 106.23 106.98 4.18 o 4 2 0 12257.26 11263.56 74.80 o 6 2 0 1174.14 1143.13 15.14 o 8 2 0 384.29 455.99 19.42 o 10 2 0 3719.82 3733.75 29.24 o 12 2 0 1561.84 1512.83 22.82 o 14 2 0 209.00 234.76 9.69 o 3 3 0 16464.77 14882.03 44.33 o 5 3 0 16092.03 16016.57 89.59 o 7 3 0 20451.09 20521.03 71.83 o 9 3 0 513.95 495.86 22.00 o 11 3 0 2477.34 2588.28 30.42 o 13 3 0 128.77 133.28 7.84 o 15 3 0 25.16 8.15 1.84 o 0 4 0 1683.66 1842.29 19.85 o 2 4 0 6360.63 5652.73 76.48 o 4 4 0 1279.42 1239.21 15.20 o 6 4 0 46.25 63.68 4.10 o 8 4 0 76.38 99.87 9.66 o 10 4 0 138.56 140.01 6.26 o 12 4 0 207.10 233.62 11.06 o 14 4 0 0.66 6.41 1.61 o 1 5 0 15794.90 14310.05 64.30 o 3 5 0 864.50 943.36 13.31 o 5 5 0 1149.11 1330.99 49.90 o 7 5 0 1319.34 1267.98 19.52 o 9 5 0 347.13 412.57 14.11 o 11 5 0 253.55 235.19 9.24 o 13 5 0 1798.95 1701.28 35.47 o 15 5 0 370.65 362.64 12.37 o 0 6 0 920.51 1127.77 19.88 o 2 6 0 1060.98 1097.40 14.72 o 4 6 0 1152.32 1067.74 16.32 o 6 6 0 0.72 7.46 3.89 o 8 6 0 9.89 6.51 3.41 o 10 6 0 417.69 339.68 11.89 o 12 6 0 101.18 59.89 5.69 o 14 6 0 2.22 3.88 1.29 o 1 7 0 5586.01 5576.03 48.82 o 3 7 0 2329.97 2395.17 24.83 o 5 7 0 14.89 18.63 2.72 o 7 7 0 423.98 348.34 17.64 o 9 7 0 41.69 49.41 3.53 o 11 7 0 1.07 7.36 2.15 o 13 7 0 88.93 79.49 8.73 o 2 8 0 423.52 437.97 11.01 o 4 8 0 61.61 42.25 3.90 o 6 8 0 2596.86 2551.94 42.30 o 8 8 0 385.76 492.55 13.02 o 10 8 0 233.82 214.40 11.60 o 12 8 0 8.18 8.13 4.39 o 14 8 0 20.17 27.47 3.85 o 1 9 0 203.72 332.03 11.70 o 3 9 0 365.82 418.47 12.07 o 5 9 0 1885.09 2019.71 28.18 o 7 9 0 358.79 325.78 10.35 o 9 9 0 253.09 234.92 11.30 o 11 9 0 28.08 36.25 7.36 o 13 9 0 135.18 141.71 10.21 o 0 10 0 634.53 618.83 21.52 o 2 10 0 305.11 290.00 10.44 o 4 10 0 1628.77 1728.09 26.76 o 6 10 0 2235.77 2165.06 31.01 o 8 10 0 143.87 163.69 7.66 o 10 10 0 642.38 591.67 17.31 o 12 10 0 188.14 173.97 12.38 o 14 10 0 76.42 77.56 4.85 o 1 11 0 903.51 754.94 26.24 o 3 11 0 3623.59 3600.14 39.53 o 5 11 0 88.03 103.96 5.77 o 7 11 0 2311.58 2318.20 44.88 o 9 11 0 143.72 166.56 9.63 o 11 11 0 326.37 277.82 10.29 o 0 12 0 175.34 140.38 11.83 o 2 12 0 95.52 116.84 7.77 o 4 12 0 133.60 132.73 6.74 o 6 12 0 1.15 1.36 1.80 o 8 12 0 281.21 263.29 9.50 o 10 12 0 225.80 217.47 9.77 o 12 12 0 42.90 33.70 12.78 o 1 13 0 80.52 109.41 6.35 o 3 13 0 1010.21 1001.66 18.75 o 5 13 0 412.94 421.01 14.33 o 7 13 0 667.74 670.44 14.67 o 9 13 0 59.31 62.50 4.25 o 11 13 0 239.68 240.54 7.93 o 0 14 0 1.84 4.54 2.70 o 2 14 0 78.93 67.80 7.40 o 4 14 0 791.30 759.33 28.77 o 6 14 0 195.72 215.09 13.86 o 8 14 0 18.64 24.97 3.00 o 10 14 0 9.45 13.29 2.30 o 1 15 0 17.96 11.99 3.11 o 3 15 0 562.25 597.39 17.49 o 5 15 0 79.92 75.67 9.39 o 7 15 0 110.86 131.60 10.84 o 9 15 0 31.32 33.36 5.16 o 0 16 0 42.66 20.39 5.22 o 2 16 0 333.47 268.46 11.78 o 4 16 0 307.16 295.50 11.45 o 6 16 0 64.96 73.16 7.50 o 8 16 0 268.11 292.20 15.53 o 1 17 0 892.40 771.86 19.37 o 3 17 0 143.85 141.85 7.99 o 5 17 0 0.16 1.52 2.97 o 7 17 0 3.70 2.33 1.76 o 9 17 0 1.86 0.08 1.32 o 0 18 0 6.28 3.87 2.92 o 2 18 0 18.67 17.35 2.45 o 4 18 0 104.03 128.09 9.50 o 6 18 0 163.49 181.81 7.10 o 8 18 0 517.42 576.93 12.80 o 1 19 0 1.35 2.03 1.52 o 3 19 0 306.26 299.67 8.26 o 5 19 0 16.57 12.03 1.97 o 0 20 0 187.54 190.30 9.21 o 2 20 0 147.72 165.03 12.95 o 4 20 0 71.39 89.14 5.54 o -15 1 1 153.93 173.30 7.62 o -13 1 1 22.27 20.69 3.70 o -11 1 1 4178.33 3987.20 28.56 o -9 1 1 291.77 297.66 14.61 o -7 1 1 1188.56 1233.41 27.60 o -5 1 1 5715.31 5520.99 48.20 o -3 1 1 9585.10 8450.60 20.47 o -1 1 1 7042.83 6252.43 19.96 o 3 1 1 15.41 23.98 1.84 o 5 1 1 5087.98 4845.11 39.81 o 7 1 1 67.97 56.90 4.25 o 9 1 1 5004.04 5010.12 35.57 o 11 1 1 854.84 868.89 31.32 o 13 1 1 229.19 233.10 10.50 o 15 1 1 566.87 624.44 15.32 o -16 2 1 68.66 101.67 6.30 o -14 2 1 9.33 12.39 2.78 o -12 2 1 360.12 388.74 10.23 o -10 2 1 489.56 518.22 13.10 o -8 2 1 5442.23 5594.62 64.76 o -6 2 1 445.84 480.68 26.93 o -4 2 1 3065.92 3178.54 18.09 o -2 2 1 203.49 158.19 3.35 o 0 2 1 712.67 637.17 14.87 o 2 2 1 3836.91 3531.04 19.86 o 4 2 1 1372.09 1362.79 20.93 o 6 2 1 3288.87 3722.28 36.07 o 8 2 1 337.43 252.96 15.19 o 10 2 1 8302.91 8295.34 42.19 o 12 2 1 897.98 948.65 17.73 o 14 2 1 8.34 3.45 1.74 o -15 3 1 221.24 274.45 8.94 o -13 3 1 1570.73 1567.40 22.63 o -11 3 1 3040.12 2944.62 22.66 o -9 3 1 2966.75 2894.65 51.14 o -7 3 1 113.21 187.82 11.29 o -5 3 1 7486.71 6882.73 32.48 o -1 3 1 5301.66 4861.27 24.76 o 1 3 1 198.86 270.96 3.23 o 3 3 1 2555.17 2201.90 18.82 o 5 3 1 653.02 693.75 12.67 o 7 3 1 384.71 338.71 9.95 o 9 3 1 20.63 22.84 2.98 o 11 3 1 1107.43 1024.82 23.37 o 13 3 1 2.47 3.32 1.70 o 15 3 1 51.39 53.11 4.48 o -16 4 1 314.96 261.72 9.26 o -14 4 1 232.71 284.19 10.14 o -12 4 1 624.06 560.07 14.04 o -10 4 1 864.87 884.64 19.33 o -8 4 1 1324.41 1341.64 32.93 o -6 4 1 11097.42 11720.51 48.89 o -4 4 1 228.44 231.75 6.17 o -2 4 1 27.05 2.69 0.45 o 0 4 1 172.51 161.77 7.33 o 2 4 1 6.97 7.87 4.30 o 4 4 1 4095.00 4202.01 30.04 o 6 4 1 441.02 470.64 11.76 o 8 4 1 421.66 407.50 19.65 o 10 4 1 0.15 -1.83 1.83 o 12 4 1 333.57 365.26 13.39 o 14 4 1 31.68 29.99 2.81 o -15 5 1 812.00 800.35 19.48 o -13 5 1 75.96 67.41 4.76 o -11 5 1 64.17 69.53 5.06 o -9 5 1 10.08 30.26 5.78 o -7 5 1 621.78 602.31 21.14 o -5 5 1 493.82 600.58 11.48 o -3 5 1 4809.80 4526.63 27.68 o -1 5 1 2350.22 2262.04 26.50 o 1 5 1 11.22 12.52 1.62 o 3 5 1 4345.06 4308.04 88.95 o 5 5 1 1444.47 1595.65 21.23 o 7 5 1 41.35 66.02 4.93 o 9 5 1 7.92 9.71 1.89 o 11 5 1 1483.62 1398.51 28.16 o 13 5 1 141.72 178.90 6.77 o -14 6 1 727.11 699.30 22.88 o -12 6 1 936.83 778.17 15.93 o -10 6 1 440.94 409.11 15.84 o -8 6 1 2352.22 2401.86 46.75 o -6 6 1 4954.90 5358.08 39.98 o -4 6 1 2080.97 1984.80 21.26 o -2 6 1 80.03 76.23 5.66 o 0 6 1 605.66 606.67 17.98 o 2 6 1 1201.91 1223.38 16.06 o 4 6 1 2578.62 2344.54 38.64 o 6 6 1 3278.88 3288.10 33.51 o 8 6 1 25.72 30.72 4.13 o 10 6 1 106.55 60.36 8.41 o 12 6 1 804.67 742.26 18.42 o 14 6 1 0.95 6.70 1.29 o -15 7 1 11.37 1.58 1.67 o -13 7 1 102.39 135.03 11.79 o -11 7 1 1604.81 1320.07 29.79 o -9 7 1 253.96 291.87 14.46 o -7 7 1 383.68 349.27 17.41 o -5 7 1 1.90 18.59 2.65 o -3 7 1 6756.89 6935.86 59.92 o -1 7 1 10562.21 10360.59 68.64 o 1 7 1 3465.59 3487.59 27.95 o 3 7 1 339.10 330.63 9.58 o 5 7 1 2909.36 2670.07 78.77 o 7 7 1 6.42 2.85 1.70 o 9 7 1 344.50 342.04 10.64 o 11 7 1 206.63 227.87 10.84 o 13 7 1 29.36 37.40 2.94 o -14 8 1 99.87 118.43 8.94 o -12 8 1 129.43 116.86 11.91 o -10 8 1 471.36 470.04 24.24 o -8 8 1 168.54 158.51 8.92 o -6 8 1 25.60 45.05 4.68 o -4 8 1 431.50 512.63 12.62 o -2 8 1 7190.40 7258.54 63.26 o 0 8 1 22542.72 22962.71 112.54 o 2 8 1 697.97 579.32 12.89 o 4 8 1 1031.67 978.94 21.09 o 6 8 1 420.24 416.44 13.04 o 8 8 1 225.89 146.81 6.11 o 10 8 1 718.18 662.05 14.62 o 12 8 1 3.09 1.34 3.00 o 14 8 1 657.51 587.71 13.02 o -13 9 1 426.95 392.06 18.15 o -11 9 1 106.55 118.85 12.38 o -9 9 1 156.16 123.85 11.94 o -7 9 1 237.55 193.24 14.00 o -5 9 1 0.08 23.55 3.61 o -3 9 1 58.96 58.38 4.56 o -1 9 1 154.32 170.61 10.66 o 1 9 1 298.87 367.48 10.69 o 3 9 1 351.41 363.75 11.47 o 5 9 1 51.24 66.97 5.35 o 7 9 1 956.36 988.72 15.51 o 9 9 1 3077.20 2784.35 32.80 o 11 9 1 67.31 83.97 9.85 o 13 9 1 5.97 4.20 1.84 o -14 10 1 0.00 0.28 1.03 o -12 10 1 23.90 45.94 7.18 o -10 10 1 1388.54 1235.82 25.19 o -8 10 1 5606.54 5560.34 95.35 o -6 10 1 524.70 463.60 14.18 o -4 10 1 70.48 41.60 4.29 o -2 10 1 47.30 68.00 5.23 o 0 10 1 7.48 8.48 3.73 o 2 10 1 1015.64 1141.54 20.65 o 4 10 1 4673.51 4642.50 44.18 o 6 10 1 1130.02 1149.64 14.60 o 8 10 1 812.27 869.81 17.17 o 10 10 1 1224.98 1225.76 25.81 o 12 10 1 710.61 675.65 58.73 o -13 11 1 124.51 113.96 8.37 o -11 11 1 88.85 71.14 7.73 o -9 11 1 266.56 280.87 12.73 o -7 11 1 5710.41 5562.74 36.97 o -5 11 1 806.79 856.27 19.88 o -3 11 1 112.85 124.52 6.16 o -1 11 1 517.07 432.88 25.77 o 1 11 1 240.55 246.34 15.13 o 3 11 1 1181.12 1142.91 22.52 o 5 11 1 2617.97 2603.52 24.54 o 7 11 1 3270.61 3255.95 33.87 o 9 11 1 512.99 475.76 15.74 o 11 11 1 475.46 488.55 12.44 o -12 12 1 15.97 14.33 3.57 o -10 12 1 441.57 444.61 15.62 o -8 12 1 7.64 9.57 2.58 o -6 12 1 92.91 90.32 5.72 o -4 12 1 1437.25 1336.56 17.87 o -2 12 1 255.64 284.00 11.76 o 0 12 1 22.09 24.31 3.90 o 2 12 1 2114.80 2103.81 31.93 o 4 12 1 594.32 594.70 13.98 o 6 12 1 1642.34 1620.89 25.45 o 8 12 1 97.92 118.18 6.43 o 10 12 1 76.13 84.49 5.90 o 12 12 1 1445.62 1599.29 25.47 o -11 13 1 0.40 1.60 1.59 o -9 13 1 0.87 4.52 2.37 o -7 13 1 1106.77 1107.94 18.88 o -5 13 1 3767.24 3600.57 38.69 o -3 13 1 605.87 640.08 12.53 o -1 13 1 502.29 500.55 13.02 o 1 13 1 172.36 152.43 7.46 o 3 13 1 1194.98 1196.09 25.42 o 5 13 1 61.95 91.98 10.51 o 7 13 1 10.68 12.59 3.72 o 9 13 1 134.39 165.98 8.42 o 11 13 1 13.43 18.38 2.64 o -10 14 1 1.21 3.54 2.45 o -8 14 1 865.22 889.49 15.70 o -6 14 1 756.54 787.93 19.71 o -4 14 1 403.64 390.80 13.60 o -2 14 1 163.92 180.40 7.03 o 0 14 1 246.08 287.15 10.34 o 2 14 1 0.16 0.84 2.47 o 4 14 1 1462.05 1488.80 40.60 o 6 14 1 409.44 446.37 15.41 o 8 14 1 644.25 629.43 12.69 o 10 14 1 139.51 138.75 5.73 o -11 15 1 1.98 2.85 1.29 o -9 15 1 139.58 146.63 6.51 o -7 15 1 818.17 844.05 18.82 o -5 15 1 53.75 40.72 5.13 o -3 15 1 2305.95 2031.32 37.73 o -1 15 1 61.21 47.22 5.35 o 1 15 1 357.95 348.80 13.76 o 3 15 1 27.97 38.77 6.93 o 5 15 1 155.02 158.61 9.35 o 7 15 1 123.87 135.02 7.75 o 9 15 1 7.39 10.47 3.04 o -10 16 1 79.82 96.20 6.08 o -8 16 1 426.10 478.18 12.41 o -6 16 1 0.00 0.21 2.82 o -4 16 1 10.34 11.63 2.95 o -2 16 1 45.87 39.00 4.85 o 0 16 1 294.15 196.19 10.29 o 2 16 1 546.13 489.96 15.88 o 4 16 1 855.86 876.77 16.28 o 6 16 1 126.75 131.86 7.71 o 8 16 1 45.95 44.18 5.45 o -9 17 1 8.84 20.09 3.18 o -7 17 1 2.81 1.87 2.91 o -5 17 1 113.26 113.74 9.96 o -3 17 1 203.07 213.51 9.73 o -1 17 1 260.23 265.54 11.43 o 1 17 1 391.15 351.25 10.21 o 3 17 1 757.33 768.73 14.72 o 5 17 1 357.46 417.14 12.87 o 7 17 1 10.81 13.84 3.43 o -8 18 1 32.34 55.80 4.68 o -6 18 1 108.59 130.88 6.32 o -4 18 1 137.53 145.29 10.85 o -2 18 1 0.02 -1.80 2.05 o 0 18 1 438.57 445.33 13.63 o 2 18 1 0.01 2.66 1.47 o 4 18 1 0.43 0.43 1.79 o 6 18 1 47.34 40.74 3.24 o -7 19 1 27.60 20.53 2.66 o -5 19 1 140.02 166.79 6.34 o -3 19 1 50.01 36.51 2.63 o -1 19 1 91.96 108.11 6.76 o 1 19 1 140.45 164.08 7.28 o 3 19 1 28.06 46.53 2.76 o 5 19 1 511.97 622.33 16.36 o -4 20 1 1128.94 1271.05 21.34 o -2 20 1 382.20 403.98 60.50 o 0 20 1 105.10 115.41 5.75 o 2 20 1 184.42 223.83 9.75 o -16 0 2 195.06 180.56 9.23 o -14 0 2 9.21 8.11 2.60 o -12 0 2 168.11 169.35 13.84 o -10 0 2 335.28 332.03 17.33 o -8 0 2 160.53 158.64 10.38 o -6 0 2 12482.44 12517.60 73.44 o -4 0 2 17674.50 16029.93 42.88 o 0 0 2 5578.70 5183.19 28.86 o 2 0 2 3671.27 3311.02 29.44 o 4 0 2 792.07 1003.45 19.55 o 6 0 2 124.17 173.89 9.70 o 8 0 2 41.21 41.90 6.86 o 10 0 2 661.55 709.79 28.37 o 12 0 2 90.06 93.86 10.02 o 14 0 2 139.85 144.26 8.78 o -15 1 2 57.46 55.33 4.70 o -13 1 2 1316.96 1344.88 28.15 o -11 1 2 281.55 290.87 8.62 o -9 1 2 2841.62 2798.69 33.31 o -7 1 2 8117.91 8363.96 67.12 o -5 1 2 13277.19 12551.29 35.20 o -1 1 2 7570.38 6454.75 28.78 o 1 1 2 14400.39 12897.38 37.83 o 3 1 2 339.33 310.86 7.22 o 5 1 2 1231.76 1221.28 23.02 o 7 1 2 432.36 465.04 32.20 o 9 1 2 365.37 354.77 9.61 o 11 1 2 1633.65 1682.21 30.51 o 13 1 2 31.74 29.39 3.82 o -16 2 2 5.89 6.02 1.48 o -14 2 2 36.17 41.91 4.36 o -12 2 2 552.10 525.27 17.03 o -10 2 2 3146.76 3198.59 61.13 o -8 2 2 254.78 318.45 14.83 o -6 2 2 37.02 23.51 1.55 o -4 2 2 513.45 506.70 5.17 o -2 2 2 3672.59 3222.05 15.44 o 0 2 2 4289.04 3806.27 27.08 o 2 2 2 6519.08 6257.21 30.31 o 4 2 2 189.70 219.08 18.31 o 6 2 2 0.10 2.59 1.58 o 8 2 2 547.86 571.54 23.76 o 10 2 2 2496.35 2438.82 35.63 o 12 2 2 232.27 236.59 16.33 o 14 2 2 0.72 5.26 1.62 o -15 3 2 597.63 574.79 10.78 o -13 3 2 2191.18 2214.84 23.59 o -11 3 2 2279.19 2313.26 23.98 o -9 3 2 1013.50 1072.26 30.10 o -7 3 2 1763.14 2028.68 34.70 o -5 3 2 804.51 840.62 8.42 o -3 3 2 5763.55 5470.53 23.03 o -1 3 2 17.46 15.56 1.14 o 1 3 2 11905.64 11235.75 36.74 o 3 3 2 25.68 18.48 4.10 o 5 3 2 157.10 197.14 7.47 o 7 3 2 9.96 16.09 13.29 o 9 3 2 234.10 238.62 9.20 o 11 3 2 277.92 299.06 10.33 o 13 3 2 416.45 414.94 12.29 o -16 4 2 1122.78 1080.94 21.89 o -14 4 2 368.44 403.08 10.55 o -12 4 2 3754.31 3787.04 35.00 o -10 4 2 174.02 158.28 12.76 o -8 4 2 962.89 911.21 26.56 o -6 4 2 3533.21 3772.20 49.76 o -4 4 2 803.66 857.12 7.49 o -2 4 2 11455.79 10344.47 29.18 o 0 4 2 8645.75 7631.19 39.82 o 2 4 2 427.79 439.84 11.86 o 4 4 2 4184.48 4500.26 33.73 o 6 4 2 647.43 747.94 15.86 o 8 4 2 44.92 39.17 5.67 o 10 4 2 1231.80 1231.99 26.20 o 12 4 2 74.05 75.84 4.93 o 14 4 2 61.81 86.91 4.19 o -15 5 2 0.86 3.77 1.88 o -13 5 2 567.35 511.83 16.50 o -11 5 2 85.18 86.30 6.10 o -9 5 2 1930.79 1968.30 42.52 o -7 5 2 3459.70 3949.15 52.25 o -5 5 2 658.07 765.64 13.85 o -3 5 2 8382.59 7790.26 22.78 o -1 5 2 613.03 572.81 9.29 o 1 5 2 7377.04 6669.96 33.59 o 3 5 2 2837.82 3065.51 26.95 o 5 5 2 3841.99 4334.75 37.20 o 7 5 2 163.24 167.46 8.10 o 9 5 2 41.83 46.35 5.33 o 11 5 2 22.83 42.82 5.07 o 13 5 2 295.16 336.99 8.10 o -16 6 2 932.18 875.78 17.36 o -14 6 2 57.88 70.99 8.10 o -12 6 2 1687.28 1683.97 34.40 o -10 6 2 1017.08 1088.12 18.89 o -8 6 2 1670.03 1558.76 36.89 o -6 6 2 5472.70 6276.32 72.14 o -4 6 2 1862.34 2101.53 21.13 o -2 6 2 8.14 43.44 33.18 o 0 6 2 1409.73 1406.75 10.64 o 2 6 2 65.72 117.22 10.26 o 4 6 2 2412.85 2834.72 29.29 o 6 6 2 638.96 539.85 14.46 o 8 6 2 119.99 153.73 6.20 o 10 6 2 55.36 61.73 6.26 o 12 6 2 278.27 305.37 9.06 o -15 7 2 0.98 4.21 2.36 o -13 7 2 4.37 5.85 3.04 o -11 7 2 974.29 871.92 28.99 o -9 7 2 338.24 348.71 13.11 o -7 7 2 17.96 10.95 3.63 o -5 7 2 4392.42 4182.85 33.77 o -3 7 2 70.97 77.18 6.61 o -1 7 2 82.50 92.16 6.90 o 1 7 2 186.49 176.90 6.60 o 3 7 2 520.06 420.22 13.68 o 5 7 2 61.33 64.90 12.09 o 7 7 2 94.69 93.14 3.80 o 9 7 2 546.12 503.12 13.21 o 11 7 2 445.53 384.83 13.66 o 13 7 2 93.69 80.70 5.39 o -14 8 2 63.73 63.71 7.29 o -12 8 2 10.47 12.38 3.56 o -10 8 2 42.49 38.83 5.44 o -8 8 2 9.64 11.06 3.85 o -6 8 2 4.12 5.93 3.28 o -4 8 2 759.10 657.78 13.95 o -2 8 2 4150.49 4631.81 81.84 o 0 8 2 1080.28 1086.93 29.03 o 2 8 2 2105.30 2103.67 25.13 o 4 8 2 1550.45 1580.44 24.00 o 6 8 2 123.52 127.43 7.59 o 8 8 2 762.82 809.84 16.86 o 10 8 2 116.78 106.17 5.92 o 12 8 2 859.98 878.97 15.71 o -15 9 2 21.06 23.87 3.43 o -13 9 2 453.87 453.84 20.73 o -11 9 2 783.15 737.56 30.14 o -9 9 2 0.42 13.99 7.41 o -7 9 2 2247.07 2307.53 47.39 o -5 9 2 0.55 4.43 1.82 o -3 9 2 2591.09 2727.13 24.47 o -1 9 2 749.99 873.12 24.43 o 1 9 2 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