#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:36:18 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181260 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/38/2233861.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2233861_Fobs loop_ _publ_author_name 'Selvakumaran, N.' 'Karvembu, R.' 'Ng, Seik Weng' 'Tiekink, Edward R. T.' _publ_section_title ; Dibenzylazanium chloride ; _journal_coeditor_code HG5170 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o577 _journal_volume 68 _journal_year 2012 _space_group_IT_number 62 _symmetry_space_group_name_Hall '-P 2ac 2n' _symmetry_space_group_name_H-M 'P n m a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 10.1524 _cell_length_b 23.8858 _cell_length_c 5.0922 _exptl_crystal_F_000 496.00 _reflns_d_resolution_high 0.7683 _cod_data_source_file hg5170Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Pnma' _shelx_refln_list_code 4 _shelx_f_calc_maximum 125.93 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z' 'x+1/2, -y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z' '-x-1/2, y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 4854.73 5053.51 84.72 o 6 0 0 1332.59 1737.12 61.25 o 10 0 0 0.25 24.04 12.81 o 12 0 0 70.16 72.20 19.65 o 2 1 0 257.32 197.98 11.67 o 4 1 0 9207.31 9587.70 114.58 o 6 1 0 77.28 108.02 11.34 o 10 1 0 305.24 273.74 22.06 o 12 1 0 62.25 64.51 14.31 o 2 2 0 1068.47 1173.67 22.76 o 4 2 0 0.26 3.22 5.47 o 6 2 0 772.69 846.54 30.55 o 10 2 0 156.18 152.66 16.79 o 12 2 0 412.42 394.88 33.40 o 2 3 0 645.49 600.65 13.78 o 4 3 0 4050.59 4252.40 75.22 o 6 3 0 688.16 739.86 39.92 o 10 3 0 69.81 61.79 12.38 o 12 3 0 682.21 686.73 51.67 o 2 4 0 4531.98 4742.86 38.25 o 4 4 0 119.79 115.72 8.86 o 6 4 0 1569.49 1686.49 57.84 o 10 4 0 0.39 1.72 7.70 o 12 4 0 172.44 182.99 41.70 o 2 5 0 6668.39 6692.57 68.96 o 4 5 0 1688.30 1581.31 31.32 o 6 5 0 137.40 133.51 16.40 o 10 5 0 1.61 1.28 7.12 o 12 5 0 564.74 541.13 33.56 o 0 6 0 15858.85 15159.30 71.25 o 2 6 0 87.30 95.86 5.88 o 4 6 0 1047.65 1095.06 26.02 o 6 6 0 130.80 92.71 13.94 o 10 6 0 20.86 14.77 8.18 o 12 6 0 22.91 36.32 11.64 o 2 7 0 675.60 640.94 15.28 o 4 7 0 2584.47 2616.96 40.40 o 6 7 0 63.06 46.45 10.14 o 10 7 0 460.40 473.94 27.95 o 12 7 0 237.75 279.19 24.94 o 0 8 0 1535.00 1440.65 25.85 o 2 8 0 559.71 496.59 14.08 o 4 8 0 81.21 65.66 6.78 o 6 8 0 409.26 378.29 27.11 o 10 8 0 253.99 274.77 21.80 o 12 8 0 278.88 237.25 30.82 o 2 9 0 1095.62 1095.65 21.76 o 4 9 0 261.17 274.30 13.18 o 6 9 0 732.11 721.74 61.08 o 8 9 0 5.06 9.07 13.77 o 10 9 0 1583.03 1496.35 48.38 o 12 9 0 27.10 29.25 11.22 o 0 10 0 6818.76 6933.01 63.75 o 2 10 0 1.67 7.39 2.80 o 4 10 0 124.28 135.17 8.35 o 6 10 0 942.48 893.23 31.91 o 8 10 0 866.71 841.63 34.91 o 10 10 0 137.21 127.72 16.26 o 12 10 0 26.48 12.71 14.59 o 2 11 0 1655.80 1697.72 29.53 o 4 11 0 2958.50 2883.30 42.93 o 6 11 0 510.20 521.40 16.16 o 8 11 0 33.12 41.82 8.89 o 10 11 0 106.39 99.58 13.67 o 12 11 0 400.42 408.64 47.70 o 0 12 0 81.11 60.34 5.76 o 2 12 0 985.10 941.38 34.02 o 4 12 0 84.70 78.32 7.62 o 6 12 0 2293.34 2151.80 31.62 o 8 12 0 206.30 202.04 17.97 o 10 12 0 205.68 208.53 18.62 o 12 12 0 54.27 28.96 16.74 o 2 13 0 404.48 387.35 16.27 o 4 13 0 1296.90 1355.33 30.57 o 6 13 0 20.64 11.97 3.48 o 8 13 0 80.40 80.36 14.76 o 10 13 0 43.31 59.92 19.83 o 12 13 0 633.35 642.29 60.23 o 0 14 0 0.27 14.62 3.96 o 2 14 0 997.13 1032.14 27.03 o 4 14 0 29.71 34.42 4.94 o 6 14 0 134.79 121.66 9.65 o 8 14 0 695.66 672.56 25.55 o 10 14 0 148.17 155.39 28.58 o 2 15 0 741.71 755.20 23.83 o 4 15 0 0.40 5.05 3.38 o 6 15 0 1990.40 1959.83 37.20 o 8 15 0 434.44 403.24 52.29 o 10 15 0 368.41 378.65 43.43 o 0 16 0 7321.01 7850.96 166.65 o 2 16 0 1.99 3.58 4.45 o 4 16 0 1106.86 1105.94 25.56 o 6 16 0 141.51 126.02 10.36 o 8 16 0 626.65 581.68 48.11 o 10 16 0 144.63 135.07 28.78 o 2 17 0 5.16 0.25 4.32 o 4 17 0 3088.61 3110.56 56.37 o 6 17 0 158.93 128.41 10.29 o 8 17 0 164.67 167.99 28.44 o 10 17 0 0.13 -11.31 14.96 o 0 18 0 2833.18 3135.79 44.95 o 2 18 0 0.89 -1.82 3.81 o 4 18 0 35.59 46.72 9.89 o 6 18 0 255.33 232.72 13.72 o 8 18 0 338.42 363.17 39.46 o 10 18 0 4.43 -18.54 18.54 o 2 19 0 77.02 70.19 9.23 o 4 19 0 1866.37 1892.47 46.03 o 6 19 0 2.23 -1.21 8.59 o 8 19 0 64.26 93.20 22.94 o 10 19 0 45.64 51.27 20.43 o 0 20 0 561.33 599.30 37.31 o 2 20 0 8.55 10.50 5.98 o 4 20 0 194.79 225.77 16.98 o 6 20 0 255.26 245.65 19.06 o 8 20 0 787.12 928.30 63.36 o 10 20 0 10.68 38.54 20.09 o 2 21 0 106.40 104.42 10.89 o 4 21 0 498.78 500.49 25.06 o 6 21 0 34.70 23.36 7.44 o 8 21 0 22.94 49.19 19.96 o 0 22 0 1575.48 1837.94 68.84 o 2 22 0 19.78 29.85 5.89 o 4 22 0 261.86 274.04 19.29 o 6 22 0 3.40 2.80 12.81 o 8 22 0 169.65 156.79 29.33 o 2 23 0 37.68 39.18 6.45 o 4 23 0 935.16 986.74 40.11 o 6 23 0 2.39 -15.09 15.09 o 8 23 0 128.36 142.74 27.89 o 0 24 0 1013.61 1236.36 59.59 o 2 24 0 23.62 26.25 6.05 o 4 24 0 241.54 255.91 19.07 o 6 24 0 9.10 -2.44 12.91 o 8 24 0 258.46 278.27 37.90 o 2 25 0 149.00 161.59 12.27 o 4 25 0 8.13 40.10 13.68 o 6 25 0 595.03 638.35 50.73 o 0 26 0 2.50 2.52 7.26 o 2 26 0 256.01 284.82 21.95 o 4 26 0 6.28 14.70 10.75 o 6 26 0 214.30 163.59 26.59 o 2 27 0 133.89 141.70 18.24 o 4 27 0 242.25 313.30 24.47 o 6 27 0 13.14 22.87 12.00 o 0 28 0 44.98 64.35 14.90 o 2 28 0 82.26 76.35 18.06 o 4 28 0 42.20 51.81 18.12 o 2 29 0 155.44 210.33 30.77 o 4 29 0 285.03 352.42 42.30 o 2 30 0 21.47 67.93 19.34 o 1 0 1 7.45 7.96 2.57 o 2 0 1 387.86 408.28 18.52 o 3 0 1 49.79 61.93 6.84 o 4 0 1 724.92 707.26 23.14 o 5 0 1 135.81 160.48 18.63 o 6 0 1 1376.99 1517.88 61.54 o 7 0 1 116.15 103.50 17.19 o 8 0 1 322.31 333.33 30.31 o 9 0 1 10.74 -1.74 10.12 o 10 0 1 564.61 560.88 44.74 o 11 0 1 15.80 -1.99 10.16 o 12 0 1 185.35 155.31 27.40 o 13 0 1 98.32 91.02 16.69 o 0 1 1 380.43 324.60 9.85 o 1 1 1 5023.38 4881.83 24.15 o 2 1 1 4585.65 4756.35 33.90 o 3 1 1 171.12 191.69 7.00 o 4 1 1 4.95 8.32 2.82 o 5 1 1 461.23 503.92 15.80 o 6 1 1 2214.03 2393.40 54.55 o 7 1 1 74.92 90.21 15.79 o 8 1 1 215.43 188.09 17.16 o 9 1 1 0.84 -3.32 7.37 o 10 1 1 12.73 27.53 10.35 o 11 1 1 45.51 29.62 9.68 o 12 1 1 6.55 21.51 10.31 o 13 1 1 8.48 34.91 8.50 o 1 2 1 1623.40 1586.70 12.94 o 2 2 1 8260.17 8499.35 45.61 o 3 2 1 1155.64 1210.39 16.90 o 4 2 1 217.01 189.12 10.15 o 5 2 1 13.87 13.70 5.08 o 6 2 1 420.70 464.14 19.97 o 7 2 1 15.11 6.77 5.09 o 8 2 1 38.00 29.00 8.40 o 9 2 1 1.05 -3.90 7.09 o 10 2 1 541.91 549.29 30.68 o 11 2 1 14.43 13.43 7.18 o 12 2 1 131.87 104.14 16.41 o 13 2 1 17.27 28.51 7.90 o 0 3 1 7.87 12.56 2.02 o 1 3 1 4626.69 4748.75 50.78 o 2 3 1 5596.04 5742.51 37.66 o 3 3 1 357.70 362.25 9.31 o 4 3 1 169.95 185.97 8.73 o 5 3 1 204.90 237.14 10.82 o 6 3 1 2442.72 2487.07 37.62 o 7 3 1 0.06 -3.62 4.60 o 8 3 1 5.45 5.13 4.44 o 9 3 1 4.34 3.17 10.16 o 10 3 1 115.61 140.30 17.06 o 11 3 1 0.77 4.59 7.59 o 12 3 1 58.31 39.94 11.66 o 13 3 1 39.61 36.95 8.52 o 1 4 1 84.05 89.89 5.37 o 2 4 1 12972.02 13343.25 57.26 o 3 4 1 473.39 508.35 10.12 o 4 4 1 1.70 6.88 2.03 o 5 4 1 133.84 146.34 7.37 o 6 4 1 82.91 80.01 8.13 o 7 4 1 15.66 8.09 5.56 o 8 4 1 138.38 155.70 12.34 o 9 4 1 26.25 17.11 7.90 o 10 4 1 1336.57 1358.83 47.61 o 11 4 1 120.83 117.05 16.06 o 12 4 1 50.46 66.25 13.31 o 0 5 1 11997.32 12371.38 70.64 o 1 5 1 223.52 184.86 6.72 o 2 5 1 653.56 727.78 14.69 o 3 5 1 0.84 1.19 1.31 o 4 5 1 92.30 98.69 5.39 o 5 5 1 180.86 201.03 8.40 o 6 5 1 266.64 223.77 18.43 o 7 5 1 27.75 20.21 5.24 o 8 5 1 1700.81 1708.16 49.27 o 9 5 1 25.30 21.45 8.09 o 10 5 1 38.33 60.61 14.68 o 11 5 1 87.16 78.55 13.98 o 12 5 1 55.93 71.23 14.22 o 1 6 1 87.97 95.21 5.07 o 2 6 1 51.37 47.46 3.29 o 3 6 1 96.60 97.52 4.32 o 4 6 1 3757.63 3950.15 31.97 o 5 6 1 38.55 37.18 3.97 o 6 6 1 57.48 52.35 5.57 o 7 6 1 34.99 38.30 6.81 o 8 6 1 21.78 29.09 8.13 o 9 6 1 181.42 174.99 16.84 o 10 6 1 647.54 618.06 32.25 o 11 6 1 83.61 74.85 14.23 o 12 6 1 124.25 162.85 19.06 o 0 7 1 1321.31 1276.33 25.06 o 1 7 1 450.41 406.74 10.72 o 2 7 1 1796.83 1751.81 19.13 o 3 7 1 0.02 2.20 1.28 o 4 7 1 54.98 45.53 4.19 o 5 7 1 376.60 425.11 11.74 o 6 7 1 1197.36 1180.12 30.22 o 7 7 1 18.02 16.49 4.72 o 8 7 1 165.18 175.36 13.39 o 9 7 1 56.19 63.85 10.86 o 10 7 1 133.32 113.60 14.99 o 11 7 1 7.47 7.31 18.04 o 12 7 1 51.85 52.73 12.47 o 1 8 1 2904.51 3065.74 30.98 o 2 8 1 20.04 17.63 2.66 o 3 8 1 2656.95 2849.43 30.81 o 4 8 1 2658.40 2679.26 47.23 o 5 8 1 9.49 9.72 2.33 o 6 8 1 431.51 424.70 12.88 o 7 8 1 17.89 10.28 6.28 o 8 8 1 1154.63 1128.27 32.44 o 9 8 1 5.00 9.08 5.79 o 10 8 1 0.35 13.03 13.90 o 11 8 1 6.30 0.47 6.87 o 12 8 1 72.82 65.67 10.36 o 0 9 1 1320.45 1202.70 29.92 o 1 9 1 1123.79 1181.15 16.21 o 2 9 1 2908.74 3043.59 25.23 o 3 9 1 628.79 688.60 14.22 o 4 9 1 1286.71 1311.73 32.89 o 5 9 1 40.66 32.18 3.33 o 6 9 1 532.54 509.21 13.89 o 7 9 1 252.90 250.96 14.37 o 8 9 1 34.19 39.27 10.43 o 9 9 1 5.98 11.38 9.45 o 10 9 1 420.69 373.04 24.92 o 11 9 1 4.93 -1.17 6.29 o 12 9 1 237.20 244.46 18.24 o 1 10 1 108.31 112.03 4.98 o 2 10 1 935.98 841.34 13.31 o 3 10 1 47.71 45.88 4.03 o 4 10 1 89.52 58.75 6.01 o 5 10 1 16.55 8.86 2.66 o 6 10 1 997.68 1011.10 19.14 o 7 10 1 136.94 124.19 8.97 o 8 10 1 533.40 526.56 23.36 o 9 10 1 4.20 7.16 8.14 o 10 10 1 192.56 203.28 18.56 o 11 10 1 0.58 12.41 8.58 o 12 10 1 44.91 48.30 19.44 o 0 11 1 3736.37 3685.84 47.64 o 1 11 1 812.23 923.54 12.82 o 2 11 1 22.85 17.34 1.90 o 3 11 1 144.99 165.12 10.12 o 4 11 1 76.58 61.05 9.70 o 5 11 1 0.64 -0.11 2.00 o 6 11 1 7.03 11.59 3.19 o 7 11 1 0.35 5.31 5.00 o 8 11 1 1485.85 1468.97 51.77 o 9 11 1 46.84 37.86 15.87 o 10 11 1 30.28 36.00 9.45 o 11 11 1 207.97 188.36 32.57 o 12 11 1 409.91 497.62 45.15 o 1 12 1 0.01 1.88 1.54 o 2 12 1 453.42 407.19 14.03 o 3 12 1 11.82 8.44 2.39 o 4 12 1 1113.53 1083.12 27.37 o 5 12 1 458.60 433.32 12.73 o 6 12 1 20.28 17.41 4.97 o 7 12 1 399.59 381.77 17.11 o 8 12 1 1.98 4.51 3.54 o 9 12 1 52.71 43.11 10.83 o 10 12 1 414.14 397.86 25.19 o 11 12 1 175.11 142.77 28.06 o 12 12 1 219.89 279.78 28.69 o 0 13 1 1306.94 1282.26 80.91 o 1 13 1 300.40 311.21 8.79 o 2 13 1 379.45 365.15 9.90 o 3 13 1 28.59 17.82 2.47 o 4 13 1 32.49 31.42 5.47 o 5 13 1 3.04 4.24 2.26 o 6 13 1 523.41 504.66 18.95 o 7 13 1 0.94 -0.01 2.82 o 8 13 1 213.15 202.15 19.89 o 9 13 1 0.32 -0.25 9.94 o 10 13 1 48.38 43.04 17.44 o 11 13 1 1.87 0.30 13.65 o 1 14 1 139.37 143.98 6.28 o 2 14 1 1302.05 1272.20 33.04 o 3 14 1 16.43 14.00 2.32 o 4 14 1 513.91 483.89 22.93 o 5 14 1 233.00 190.25 11.05 o 6 14 1 94.36 67.39 13.51 o 7 14 1 95.83 82.05 8.03 o 8 14 1 85.85 67.58 15.34 o 9 14 1 15.44 -2.75 7.05 o 10 14 1 276.34 328.30 40.72 o 11 14 1 6.00 0.03 12.76 o 0 15 1 492.19 520.33 33.23 o 1 15 1 70.80 74.07 5.79 o 2 15 1 374.07 364.43 10.37 o 3 15 1 17.85 13.66 2.10 o 4 15 1 9.10 4.70 3.28 o 5 15 1 289.73 272.36 17.76 o 6 15 1 1028.67 840.95 42.92 o 7 15 1 223.26 219.67 20.55 o 8 15 1 13.84 10.51 8.03 o 9 15 1 2.42 5.32 7.05 o 10 15 1 10.13 32.57 16.47 o 11 15 1 40.81 40.17 13.35 o 1 16 1 22.43 20.00 3.41 o 2 16 1 94.77 76.10 5.52 o 3 16 1 6.08 2.73 2.61 o 4 16 1 808.83 630.61 75.75 o 5 16 1 15.53 22.55 8.95 o 6 16 1 158.67 126.89 11.02 o 7 16 1 17.96 7.33 7.83 o 8 16 1 67.09 79.59 23.85 o 9 16 1 59.51 91.34 43.64 o 10 16 1 381.88 419.36 45.23 o 11 16 1 0.78 10.24 10.55 o 0 17 1 70.57 45.76 12.28 o 1 17 1 172.97 185.45 10.81 o 2 17 1 414.77 416.53 13.56 o 3 17 1 10.47 4.22 2.58 o 4 17 1 24.53 11.09 6.00 o 5 17 1 169.30 110.11 25.61 o 6 17 1 677.79 661.53 64.69 o 7 17 1 7.68 14.21 7.33 o 8 17 1 164.36 167.90 19.01 o 9 17 1 48.75 44.87 10.91 o 10 17 1 6.39 21.58 10.99 o 1 18 1 81.19 69.64 8.21 o 2 18 1 699.85 718.68 18.86 o 3 18 1 169.54 159.92 9.65 o 4 18 1 156.95 140.65 20.11 o 5 18 1 212.89 188.86 17.35 o 6 18 1 68.00 64.46 11.62 o 7 18 1 125.88 121.90 16.06 o 8 18 1 8.97 23.17 11.93 o 9 18 1 11.20 23.64 11.84 o 10 18 1 327.06 362.91 30.71 o 0 19 1 13.23 16.79 5.45 o 1 19 1 3.01 4.36 2.79 o 2 19 1 738.45 814.06 20.25 o 3 19 1 255.79 275.82 17.45 o 4 19 1 36.57 25.98 5.46 o 5 19 1 100.87 98.26 13.14 o 6 19 1 450.58 453.70 38.68 o 7 19 1 6.65 12.18 7.64 o 8 19 1 91.91 85.16 14.54 o 9 19 1 72.74 64.24 11.35 o 10 19 1 13.59 7.92 12.33 o 1 20 1 7.46 6.93 2.45 o 2 20 1 3284.70 3570.13 51.96 o 3 20 1 14.57 15.60 3.89 o 4 20 1 448.38 429.76 25.23 o 5 20 1 31.81 25.49 8.87 o 6 20 1 400.04 395.96 31.11 o 7 20 1 61.40 57.84 11.56 o 8 20 1 1.87 14.20 7.19 o 9 20 1 67.67 80.88 15.53 o 0 21 1 2.41 0.04 3.57 o 1 21 1 1.13 1.36 3.42 o 2 21 1 548.32 602.79 18.46 o 3 21 1 83.80 87.83 7.42 o 4 21 1 9.55 13.77 3.91 o 5 21 1 2.33 -7.68 7.68 o 6 21 1 539.49 532.77 30.56 o 7 21 1 19.94 14.01 12.82 o 8 21 1 38.51 34.41 10.77 o 9 21 1 22.50 25.89 10.48 o 1 22 1 0.94 0.89 4.15 o 2 22 1 92.00 101.54 8.17 o 3 22 1 1.64 1.71 3.68 o 4 22 1 416.49 459.22 29.96 o 5 22 1 42.75 27.85 15.79 o 6 22 1 24.72 15.51 10.74 o 7 22 1 44.15 40.78 9.06 o 8 22 1 4.35 0.60 8.82 o 9 22 1 26.38 29.94 10.98 o 0 23 1 103.30 108.10 12.50 o 1 23 1 13.92 16.63 3.65 o 2 23 1 114.42 110.17 8.51 o 3 23 1 41.38 54.04 7.43 o 4 23 1 47.19 55.00 8.14 o 5 23 1 154.08 131.66 13.04 o 6 23 1 478.93 445.88 28.87 o 7 23 1 2.12 10.60 9.99 o 8 23 1 65.37 71.69 15.14 o 1 24 1 41.04 50.89 5.57 o 2 24 1 0.20 -0.59 2.96 o 3 24 1 28.44 32.57 6.26 o 4 24 1 686.76 736.41 25.21 o 5 24 1 12.60 11.66 8.06 o 6 24 1 2.44 -1.76 5.48 o 7 24 1 55.44 71.48 14.44 o 8 24 1 16.60 20.35 11.32 o 0 25 1 688.54 772.86 38.27 o 1 25 1 3.32 -0.73 3.57 o 2 25 1 17.51 27.08 6.48 o 3 25 1 10.55 8.42 4.82 o 4 25 1 34.34 46.83 8.00 o 5 25 1 46.58 57.01 8.44 o 6 25 1 84.59 112.07 16.73 o 7 25 1 80.38 97.02 22.60 o 1 26 1 20.58 32.71 7.44 o 2 26 1 407.06 417.72 22.95 o 3 26 1 0.37 2.92 5.17 o 4 26 1 10.49 24.38 6.28 o 5 26 1 38.81 30.48 8.71 o 6 26 1 65.75 76.32 14.14 o 0 27 1 167.63 143.08 24.87 o 1 27 1 11.58 0.71 8.17 o 2 27 1 105.81 126.88 13.55 o 3 27 1 12.35 3.72 20.39 o 4 27 1 48.12 59.09 9.62 o 5 27 1 6.94 4.31 10.56 o 6 27 1 31.92 33.05 10.95 o 1 28 1 0.64 -4.72 6.98 o 2 28 1 27.94 35.25 9.34 o 3 28 1 9.79 8.77 6.27 o 4 28 1 157.95 225.81 35.68 o 5 28 1 140.77 159.62 31.26 o 0 29 1 164.55 205.52 30.32 o 1 29 1 65.73 68.38 13.30 o 2 29 1 28.75 19.00 9.00 o 3 29 1 33.34 54.08 12.55 o 4 29 1 7.60 7.40 10.72 o 1 30 1 9.77 16.08 11.78 o 2 30 1 20.03 12.36 12.76 o 0 0 2 9158.01 9683.68 102.26 o 1 0 2 40.23 44.00 4.04 o 2 0 2 24.14 36.49 4.63 o 3 0 2 60.44 55.55 5.59 o 4 0 2 43.42 57.64 17.18 o 5 0 2 341.08 376.53 20.99 o 6 0 2 0.82 -0.49 4.86 o 7 0 2 187.43 191.15 17.44 o 8 0 2 1931.17 1980.43 74.63 o 9 0 2 30.86 45.03 14.22 o 10 0 2 6.95 9.26 11.67 o 11 0 2 36.07 22.71 11.59 o 12 0 2 311.28 312.75 39.04 o 1 1 2 797.33 832.49 11.37 o 2 1 2 589.22 563.44 10.57 o 3 1 2 4.74 4.03 1.82 o 4 1 2 1327.14 1422.96 26.69 o 5 1 2 845.73 862.41 22.27 o 6 1 2 82.81 75.02 7.60 o 7 1 2 152.43 149.52 12.74 o 8 1 2 48.20 74.54 12.06 o 9 1 2 130.25 161.01 16.79 o 10 1 2 304.81 309.68 23.97 o 11 1 2 4.02 1.70 7.01 o 12 1 2 160.05 195.78 22.14 o 0 2 2 1967.32 1973.93 24.45 o 1 2 2 1061.34 1167.59 14.09 o 2 2 2 1058.01 1034.89 15.31 o 3 2 2 337.82 400.36 9.46 o 4 2 2 409.75 444.89 15.11 o 5 2 2 46.31 51.05 6.03 o 6 2 2 377.33 376.07 19.00 o 7 2 2 336.15 346.59 18.35 o 8 2 2 294.99 333.16 19.21 o 9 2 2 480.75 492.40 28.24 o 10 2 2 138.98 131.82 16.39 o 11 2 2 1.25 -3.71 6.88 o 12 2 2 179.24 181.39 21.02 o 1 3 2 187.86 206.32 5.97 o 2 3 2 487.20 465.71 10.36 o 3 3 2 558.17 648.12 12.55 o 4 3 2 1414.65 1412.71 26.60 o 5 3 2 9.46 5.63 3.73 o 6 3 2 384.36 374.09 18.11 o 7 3 2 536.06 548.07 22.83 o 8 3 2 702.36 730.61 27.80 o 9 3 2 3.11 7.81 7.32 o 10 3 2 64.23 57.17 11.81 o 11 3 2 11.02 5.97 7.19 o 12 3 2 35.07 35.50 10.78 o 0 4 2 606.23 583.08 14.87 o 1 4 2 5.18 4.58 1.32 o 2 4 2 1500.29 1616.71 20.52 o 3 4 2 794.71 862.96 13.43 o 4 4 2 190.59 244.54 11.34 o 5 4 2 45.79 48.83 8.86 o 6 4 2 823.37 800.42 26.05 o 7 4 2 26.41 21.05 6.65 o 8 4 2 88.78 86.14 8.89 o 9 4 2 0.02 -0.33 6.84 o 10 4 2 108.99 88.50 14.11 o 11 4 2 163.51 159.82 18.93 o 12 4 2 31.38 16.24 9.98 o 1 5 2 19.02 16.14 1.97 o 2 5 2 11.60 10.26 1.97 o 3 5 2 521.74 552.32 11.15 o 4 5 2 2627.91 2703.99 28.38 o 5 5 2 339.20 357.02 20.22 o 6 5 2 157.96 180.67 13.01 o 7 5 2 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5.06 o 2 6 4 73.55 78.89 7.76 o 3 6 4 263.86 289.66 14.09 o 4 6 4 102.41 117.55 9.44 o 5 6 4 97.57 83.13 8.05 o 6 6 4 457.58 472.24 18.75 o 7 6 4 0.75 20.07 8.34 o 8 6 4 180.30 204.94 28.17 o 9 6 4 15.21 23.00 9.37 o 10 6 4 0.10 35.65 17.31 o 1 7 4 106.69 101.64 8.48 o 2 7 4 1213.65 1278.80 28.99 o 3 7 4 2.53 -1.99 4.88 o 4 7 4 22.26 13.61 3.82 o 5 7 4 2.86 1.39 3.52 o 6 7 4 141.47 134.61 11.08 o 7 7 4 261.43 313.57 33.15 o 8 7 4 37.98 45.80 11.44 o 9 7 4 16.17 18.34 13.03 o 10 7 4 460.46 472.42 36.19 o 0 8 4 96.57 87.94 10.79 o 1 8 4 898.25 908.99 20.65 o 2 8 4 358.71 358.80 15.60 o 3 8 4 266.98 257.40 12.90 o 4 8 4 24.83 13.06 4.18 o 5 8 4 65.14 45.95 8.60 o 6 8 4 287.38 327.16 26.46 o 7 8 4 32.24 30.12 10.20 o 8 8 4 74.98 77.36 14.62 o 9 8 4 12.50 13.77 9.34 o 1 9 4 66.42 62.91 6.00 o 2 9 4 1816.65 1851.28 38.33 o 3 9 4 129.03 128.56 9.02 o 4 9 4 93.75 57.35 6.65 o 5 9 4 245.46 222.93 21.98 o 6 9 4 206.76 189.31 21.53 o 7 9 4 85.08 93.26 15.06 o 8 9 4 8.77 11.97 17.78 o 9 9 4 1.25 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215.45 20.42 o 4 0 5 662.02 720.05 36.59 o 5 0 5 230.46 246.43 22.29 o 6 0 5 15.90 29.41 10.63 o 7 0 5 284.96 356.62 28.27 o 8 0 5 10.53 14.31 15.55 o 0 1 5 168.40 156.41 17.59 o 1 1 5 384.02 371.44 18.30 o 2 1 5 45.47 50.86 7.70 o 3 1 5 200.29 258.60 15.73 o 4 1 5 12.60 34.43 7.16 o 5 1 5 1.62 18.40 5.69 o 6 1 5 245.61 265.78 16.51 o 7 1 5 6.29 28.53 8.22 o 8 1 5 45.22 57.84 15.74 o 1 2 5 2.79 9.51 4.68 o 2 2 5 273.64 284.20 16.16 o 3 2 5 463.94 451.19 20.30 o 4 2 5 34.99 47.29 7.10 o 5 2 5 340.29 384.75 19.42 o 6 2 5 31.46 42.16 8.12 o 7 2 5 74.22 83.81 12.38 o 8 2 5 0.01 2.33 6.56 o 0 3 5 137.41 125.50 15.47 o 1 3 5 100.71 84.68 9.50 o 2 3 5 92.54 94.48 10.17 o 3 3 5 15.32 17.46 5.49 o 4 3 5 7.26 11.23 6.73 o 5 3 5 89.46 112.58 11.04 o 6 3 5 88.76 84.44 12.33 o 7 3 5 155.28 180.99 17.80 o 8 3 5 118.22 118.70 14.83 o 1 4 5 270.02 271.41 15.72 o 2 4 5 355.57 356.03 18.10 o 3 4 5 28.51 30.11 6.51 o 4 4 5 4.41 0.78 4.12 o 5 4 5 27.51 28.60 7.02 o 6 4 5 64.57 58.51 11.04 o 7 4 5 35.81 32.78 9.21 o 8 4 5 2.94 4.65 38.43 o 0 5 5 19.64 7.76 6.13 o 1 5 5 62.92 58.55 7.88 o 2 5 5 223.57 230.88 14.66 o 3 5 5 281.21 288.17 20.38 o 4 5 5 18.43 18.94 7.11 o 5 5 5 5.27 2.14 5.37 o 6 5 5 47.89 40.42 9.04 o 7 5 5 9.64 8.21 12.06 o 8 5 5 121.19 114.70 17.49 o 1 6 5 352.57 363.34 18.17 o 2 6 5 15.23 15.87 6.79 o 3 6 5 52.99 56.99 10.19 o 4 6 5 240.43 224.01 18.56 o 5 6 5 21.55 9.50 6.84 o 6 6 5 45.02 48.27 10.72 o 7 6 5 168.28 194.87 22.49 o 8 6 5 58.09 57.73 14.18 o 0 7 5 468.61 448.70 29.79 o 1 7 5 0.78 11.79 5.55 o 2 7 5 10.06 0.46 4.81 o 3 7 5 234.29 276.36 20.39 o 4 7 5 33.46 42.55 9.57 o 5 7 5 92.44 103.07 13.54 o 6 7 5 9.24 3.79 6.84 o 7 7 5 39.63 62.15 14.47 o 8 7 5 112.96 121.51 19.36 o 1 8 5 11.81 10.39 8.29 o 2 8 5 0.20 -8.82 8.82 o 3 8 5 798.18 802.86 34.06 o 4 8 5 425.34 413.83 25.27 o 5 8 5 329.44 326.76 22.91 o 6 8 5 27.88 43.50 14.40 o 7 8 5 123.97 116.68 18.93 o 0 9 5 578.89 552.36 31.22 o 1 9 5 177.81 181.77 16.12 o 2 9 5 0.48 -4.90 4.91 o 3 9 5 0.56 9.67 8.71 o 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