#------------------------------------------------------------------------------ #$Date: 2012-09-11 12:26:43 +0300 (Tue, 11 Sep 2012) $ #$Revision: 66590 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/38/2233864.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2233864_Fobs loop_ _publ_author_name 'Al-Deeb, Omar A.' 'El-Emam, Ali A.' 'Al-Turkistani, Abdulghafoor A.' 'Ng, Seik Weng' 'Tiekink, Edward R. T.' _publ_section_title ; 6-(2-Methylpropyl)-4-oxo-2-sulfanylidene-1,2,3,4-tetrahydropyrimidine-5-carbonitrile ; _journal_coeditor_code HG5174 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o676 _journal_page_last o677 _journal_volume 68 _journal_year 2012 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 98.527 _cell_angle_gamma 90.000 _cell_length_a 25.8985 _cell_length_b 7.0479 _cell_length_c 11.1811 _exptl_crystal_F_000 880.00 _reflns_d_resolution_high 0.7934 _[local]_cod_data_source_file hg5174Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 197.62 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 288.09 275.05 6.31 o 6 0 0 5425.32 4794.91 37.12 o 8 0 0 30751.67 27900.99 102.48 o 10 0 0 8099.05 7707.79 104.35 o 12 0 0 1683.27 1672.57 23.40 o 14 0 0 1099.02 978.41 33.28 o 16 0 0 1921.05 1899.07 64.10 o 18 0 0 13034.01 13273.90 329.53 o 20 0 0 13555.45 14057.20 181.67 o 22 0 0 571.02 552.31 24.62 o 24 0 0 578.42 613.13 26.20 o 26 0 0 1605.65 1630.71 40.75 o 28 0 0 2053.02 2069.68 41.12 o 30 0 0 419.08 437.71 26.48 o 32 0 0 1793.76 1713.90 37.91 o 1 1 0 282.52 323.00 5.11 o 3 1 0 2063.67 1930.62 27.49 o 5 1 0 4062.69 4013.97 26.17 o 7 1 0 114.17 148.12 3.86 o 9 1 0 854.73 874.65 15.73 o 11 1 0 269.53 279.29 6.17 o 13 1 0 2.12 -0.23 1.35 o 15 1 0 1130.80 1127.34 41.80 o 17 1 0 62.33 72.37 11.73 o 19 1 0 175.11 180.68 13.18 o 21 1 0 41.59 38.08 5.43 o 23 1 0 2083.51 2033.27 49.84 o 25 1 0 103.76 96.22 9.24 o 27 1 0 329.25 308.39 15.08 o 29 1 0 22.87 21.82 4.61 o 31 1 0 303.99 312.26 22.09 o 4 2 0 2594.89 2462.69 41.81 o 6 2 0 3538.99 3772.84 120.60 o 8 2 0 2204.15 2136.13 56.35 o 10 2 0 5068.31 5180.66 31.10 o 12 2 0 2166.37 2367.83 37.93 o 14 2 0 305.96 329.60 24.15 o 16 2 0 2580.77 2695.74 73.16 o 18 2 0 5615.05 5492.61 109.95 o 20 2 0 8332.90 8201.71 125.54 o 22 2 0 302.18 286.27 19.72 o 24 2 0 1963.36 2008.89 50.97 o 26 2 0 756.61 774.53 23.77 o 28 2 0 769.90 783.14 18.12 o 30 2 0 1609.33 1459.56 77.41 o 1 3 0 8656.76 9544.08 75.50 o 3 3 0 5348.54 5673.40 245.93 o 5 3 0 931.14 1140.94 26.57 o 7 3 0 406.88 390.73 15.21 o 9 3 0 53.43 55.84 6.20 o 11 3 0 2666.04 2909.10 53.02 o 13 3 0 1716.87 1875.98 63.67 o 15 3 0 186.01 151.65 19.27 o 17 3 0 3.16 6.85 5.28 o 19 3 0 68.71 60.25 13.86 o 21 3 0 1406.55 1483.55 63.89 o 23 3 0 4286.83 4337.94 73.85 o 25 3 0 656.46 647.79 26.75 o 27 3 0 352.36 375.53 11.11 o 29 3 0 1230.07 1174.69 42.31 o 0 4 0 4310.29 4618.12 83.20 o 2 4 0 17466.96 18678.04 153.82 o 4 4 0 1818.67 2060.41 25.78 o 6 4 0 394.99 468.48 15.60 o 8 4 0 90.40 134.90 8.67 o 10 4 0 1384.50 1451.59 27.65 o 12 4 0 146.13 141.19 12.19 o 14 4 0 261.90 247.92 14.68 o 16 4 0 1114.18 1126.41 23.75 o 18 4 0 2091.97 2205.20 43.76 o 20 4 0 579.32 575.77 21.97 o 22 4 0 2732.06 2969.66 63.14 o 24 4 0 436.16 463.39 18.34 o 26 4 0 1070.06 1082.64 20.22 o 28 4 0 60.44 50.04 4.01 o 1 5 0 1166.11 1405.20 27.64 o 3 5 0 1187.99 1289.51 37.28 o 5 5 0 1094.09 1306.78 37.94 o 7 5 0 995.14 1050.21 33.14 o 9 5 0 1252.25 1376.36 22.75 o 11 5 0 1430.53 1500.41 25.62 o 13 5 0 2928.35 2868.50 53.24 o 15 5 0 8.12 -3.95 3.95 o 17 5 0 247.25 262.01 13.29 o 19 5 0 11.38 5.99 3.13 o 21 5 0 2434.79 2563.41 52.90 o 23 5 0 3373.98 3414.55 58.31 o 25 5 0 721.47 699.84 22.32 o 0 6 0 283.84 266.72 24.84 o 2 6 0 541.61 554.08 25.27 o 4 6 0 955.30 1068.95 35.22 o 6 6 0 772.09 830.98 25.45 o 8 6 0 97.85 92.42 11.31 o 10 6 0 2.17 3.40 5.08 o 12 6 0 0.67 3.10 3.08 o 14 6 0 0.37 0.34 7.72 o 16 6 0 0.60 2.45 5.62 o 18 6 0 87.13 89.64 12.44 o 20 6 0 210.63 202.24 10.21 o 22 6 0 351.18 317.18 13.84 o 1 7 0 58.44 72.44 7.58 o 3 7 0 9.08 12.89 3.62 o 5 7 0 308.01 318.06 15.02 o 7 7 0 196.33 226.50 16.28 o 9 7 0 3238.38 3447.93 70.87 o 11 7 0 937.95 998.57 33.75 o 13 7 0 230.35 227.13 14.16 o 15 7 0 71.61 75.44 7.60 o 17 7 0 288.21 259.13 12.27 o 19 7 0 509.32 538.14 19.97 o 0 8 0 146.40 153.93 10.85 o 2 8 0 172.73 168.24 9.51 o 4 8 0 948.82 918.77 21.61 o 6 8 0 701.87 619.41 17.21 o 8 8 0 94.75 74.00 7.58 o 10 8 0 671.01 623.32 17.27 o 12 8 0 8.42 16.24 3.14 o 14 8 0 169.59 160.13 9.72 o -31 1 1 3312.19 3607.11 46.78 o -29 1 1 264.66 302.59 11.37 o -27 1 1 111.45 92.97 8.68 o -25 1 1 2572.22 2537.34 46.27 o -23 1 1 1169.37 1121.30 37.27 o -21 1 1 22.53 26.14 4.49 o -19 1 1 183.56 205.84 20.42 o -17 1 1 3585.61 3421.96 78.79 o -15 1 1 9851.77 9713.95 125.52 o -13 1 1 12414.34 12899.19 64.51 o -11 1 1 14577.79 14896.26 82.56 o -9 1 1 148.24 113.70 5.16 o -7 1 1 3851.41 4232.92 40.71 o -5 1 1 2308.14 2473.02 23.61 o -3 1 1 13616.68 12281.62 38.10 o -1 1 1 1353.49 1422.47 18.56 o 1 1 1 15230.24 14475.37 64.16 o 3 1 1 1321.17 1296.03 22.45 o 5 1 1 2423.53 2444.41 20.94 o 7 1 1 77.77 67.55 5.83 o 9 1 1 319.00 303.10 17.28 o 11 1 1 766.43 727.22 16.65 o 13 1 1 1996.76 2165.33 34.39 o 15 1 1 931.99 842.65 19.33 o 17 1 1 834.02 783.79 26.30 o 19 1 1 8730.93 8455.34 92.14 o 21 1 1 13623.19 12636.32 116.81 o 23 1 1 1483.07 1444.07 43.85 o 25 1 1 1358.63 1382.32 32.78 o 27 1 1 854.90 849.21 23.66 o 29 1 1 970.02 1017.22 21.57 o 31 1 1 157.68 159.39 12.90 o -30 2 1 93.97 85.09 5.77 o -28 2 1 610.11 601.55 16.33 o -26 2 1 449.74 467.01 23.43 o -24 2 1 29.24 24.19 6.40 o -22 2 1 7.93 5.78 4.64 o -20 2 1 2799.91 2912.39 84.01 o -18 2 1 85.72 69.67 12.62 o -16 2 1 1.73 15.50 6.26 o -14 2 1 22.25 29.42 5.15 o -12 2 1 260.53 175.60 11.14 o -10 2 1 730.20 776.64 12.41 o -8 2 1 4247.05 4654.74 80.98 o -6 2 1 2166.82 2310.39 76.82 o -4 2 1 617.71 543.92 9.54 o -2 2 1 29069.18 28144.12 148.90 o 0 2 1 15470.35 15888.75 43.68 o 2 2 1 19983.27 20112.28 103.65 o 4 2 1 1805.03 2024.74 57.25 o 6 2 1 7706.19 7839.62 74.72 o 8 2 1 6977.02 7173.01 69.22 o 10 2 1 80.91 110.00 13.37 o 12 2 1 298.45 326.90 14.07 o 14 2 1 4251.18 4210.69 99.88 o 16 2 1 846.67 850.08 28.86 o 18 2 1 2838.82 2861.13 46.15 o 20 2 1 117.93 115.28 18.50 o 22 2 1 5402.77 5375.87 84.51 o 24 2 1 41.99 45.66 6.38 o 26 2 1 297.79 302.97 14.11 o 28 2 1 473.80 488.32 32.84 o 30 2 1 30.60 29.52 3.03 o -29 3 1 295.15 342.64 15.97 o -27 3 1 634.08 608.59 16.83 o -25 3 1 10.52 13.58 4.25 o -23 3 1 157.44 144.47 14.11 o -21 3 1 807.68 795.91 44.83 o -19 3 1 565.20 539.98 36.10 o -17 3 1 102.99 126.48 12.39 o -15 3 1 2867.19 3004.30 84.60 o -13 3 1 7612.64 7976.84 85.27 o -11 3 1 2912.95 3195.17 39.09 o -9 3 1 2286.85 2325.79 38.55 o -7 3 1 103.06 122.40 8.81 o -5 3 1 23.59 32.14 7.99 o -3 3 1 469.64 572.39 17.40 o -1 3 1 302.29 279.93 6.73 o 1 3 1 2535.47 2757.61 32.71 o 3 3 1 1233.10 1528.47 20.62 o 5 3 1 463.52 463.70 16.19 o 7 3 1 1759.00 1742.94 24.53 o 9 3 1 372.38 320.72 11.13 o 11 3 1 6.22 3.12 3.77 o 13 3 1 302.75 327.18 16.34 o 15 3 1 1654.35 1719.87 53.05 o 17 3 1 1871.22 1968.25 48.34 o 19 3 1 3894.35 3745.85 103.68 o 21 3 1 5043.32 5208.14 80.81 o 23 3 1 760.23 829.22 31.45 o 25 3 1 271.35 289.45 17.04 o 27 3 1 910.80 947.74 18.80 o 29 3 1 7.47 7.00 1.70 o -28 4 1 11.88 11.72 2.02 o -26 4 1 63.47 51.08 5.74 o -24 4 1 318.53 332.48 15.97 o -22 4 1 2171.38 2302.23 45.33 o -20 4 1 432.54 454.17 24.60 o -18 4 1 47.42 48.91 7.21 o -16 4 1 6.58 0.41 4.34 o -14 4 1 617.95 589.24 16.96 o -12 4 1 462.66 445.33 27.17 o -10 4 1 481.27 556.39 28.16 o -8 4 1 1738.57 1982.59 32.69 o -4 4 1 12625.64 13804.01 371.74 o -2 4 1 18519.94 19566.64 120.36 o 0 4 1 2917.27 2902.35 90.45 o 2 4 1 823.83 966.46 26.04 o 4 4 1 2300.76 2684.21 42.61 o 6 4 1 4578.82 4732.23 83.94 o 8 4 1 6021.22 6357.31 71.59 o 10 4 1 1333.92 1476.93 24.76 o 12 4 1 124.92 124.79 11.82 o 14 4 1 1026.87 1081.99 26.17 o 16 4 1 6336.26 6297.86 123.09 o 18 4 1 3174.15 3301.80 68.85 o 20 4 1 1381.03 1411.14 34.40 o 22 4 1 2921.83 3065.92 46.81 o 24 4 1 434.96 472.19 17.63 o 26 4 1 651.42 668.95 13.34 o 28 4 1 423.48 433.91 19.46 o -25 5 1 93.43 110.61 9.02 o -23 5 1 874.23 918.80 30.85 o -21 5 1 172.83 174.91 9.55 o -19 5 1 79.61 68.20 8.15 o -17 5 1 236.13 261.39 15.58 o -15 5 1 56.75 50.81 10.10 o -13 5 1 208.99 205.94 18.16 o -11 5 1 2574.59 2816.94 41.53 o -9 5 1 1394.21 1481.46 25.26 o -7 5 1 72.26 96.03 10.40 o -5 5 1 1686.02 1946.91 53.45 o -3 5 1 260.23 273.43 17.98 o -1 5 1 3170.87 3551.27 44.57 o 1 5 1 99.84 117.61 9.58 o 3 5 1 218.73 224.40 13.01 o 5 5 1 15.60 26.90 5.03 o 7 5 1 1111.62 1153.67 23.17 o 9 5 1 186.36 202.44 8.76 o 11 5 1 21.69 27.99 4.90 o 13 5 1 129.38 154.07 10.55 o 15 5 1 1360.03 1313.77 36.69 o 17 5 1 1298.69 1402.41 30.15 o 19 5 1 1218.63 1321.70 27.95 o 21 5 1 577.25 596.70 20.12 o 23 5 1 36.19 45.52 4.52 o 25 5 1 92.61 94.31 6.69 o -24 6 1 1197.34 1170.98 28.50 o -22 6 1 1860.72 1679.39 126.20 o -20 6 1 162.84 156.71 11.09 o -18 6 1 158.46 165.60 14.51 o -16 6 1 358.66 372.24 22.79 o -14 6 1 350.16 312.23 27.64 o -12 6 1 692.72 668.49 45.01 o -10 6 1 469.59 516.81 25.42 o -8 6 1 105.66 110.54 9.52 o -6 6 1 98.08 100.61 9.04 o -4 6 1 10150.09 10484.79 110.66 o -2 6 1 10205.76 10634.44 110.14 o 0 6 1 12.72 9.59 6.24 o 2 6 1 33.91 47.74 12.21 o 4 6 1 2381.36 2535.18 56.55 o 6 6 1 2980.42 3045.05 81.76 o 8 6 1 1723.27 1833.11 49.47 o 10 6 1 785.16 841.59 26.85 o 12 6 1 5.58 5.71 3.67 o 14 6 1 386.97 384.88 22.95 o 16 6 1 6157.01 5840.42 182.89 o 18 6 1 432.67 418.36 21.27 o 20 6 1 416.74 403.16 11.48 o 22 6 1 579.06 562.51 16.95 o -19 7 1 266.35 246.27 11.13 o -17 7 1 21.19 20.83 4.53 o -15 7 1 19.04 19.27 7.53 o -13 7 1 89.75 70.14 8.24 o -11 7 1 47.42 58.70 12.26 o -9 7 1 1259.88 1256.29 27.96 o -7 7 1 1550.06 1681.95 33.61 o -5 7 1 114.39 120.20 9.41 o -3 7 1 0.91 -1.46 3.79 o -1 7 1 951.82 976.16 35.26 o 1 7 1 613.20 620.74 27.29 o 3 7 1 135.26 135.27 13.18 o 5 7 1 194.96 202.93 15.70 o 7 7 1 130.09 129.27 12.74 o 9 7 1 357.00 372.29 20.44 o 11 7 1 24.73 29.13 9.90 o 13 7 1 344.41 313.33 26.25 o 15 7 1 6.41 0.83 4.87 o 17 7 1 1005.96 914.34 21.73 o 19 7 1 358.69 354.90 16.96 o -14 8 1 920.97 960.72 24.41 o -12 8 1 24.02 25.89 2.91 o -10 8 1 1.13 2.78 1.84 o -8 8 1 140.03 106.68 8.49 o -6 8 1 1342.39 1356.16 24.04 o -4 8 1 3159.10 3133.32 32.04 o -2 8 1 920.14 923.07 21.60 o 0 8 1 283.61 298.34 12.67 o 2 8 1 154.98 161.92 9.49 o 4 8 1 853.38 858.94 21.15 o 6 8 1 395.91 395.32 16.88 o 8 8 1 522.06 515.59 26.80 o 10 8 1 509.00 424.21 27.61 o 12 8 1 1.21 4.32 3.01 o -32 0 2 580.82 581.88 24.02 o -30 0 2 211.01 200.57 19.22 o -28 0 2 1504.21 1378.09 56.73 o -26 0 2 1984.14 2016.82 60.21 o -24 0 2 117.22 74.50 9.63 o -22 0 2 10.83 13.36 5.37 o -20 0 2 528.87 562.64 36.68 o -18 0 2 2307.34 2104.11 57.22 o -16 0 2 406.04 496.91 17.52 o -14 0 2 410.88 269.51 12.46 o -12 0 2 33.66 46.83 5.01 o -10 0 2 3855.66 4088.21 104.03 o -8 0 2 3473.74 3505.97 35.32 o -6 0 2 30452.96 29113.24 245.03 o -4 0 2 1491.61 1330.74 25.42 o -2 0 2 2690.47 2380.03 29.02 o 0 0 2 3487.16 3462.09 40.71 o 2 0 2 27010.94 23307.63 72.45 o 4 0 2 14155.59 13404.76 176.21 o 6 0 2 25718.35 25095.73 132.37 o 8 0 2 1310.75 1376.22 34.68 o 10 0 2 7738.25 8348.51 95.03 o 12 0 2 6025.29 5481.22 82.38 o 14 0 2 14328.30 13955.25 142.07 o 16 0 2 532.17 543.02 29.97 o 18 0 2 214.07 215.59 13.65 o 20 0 2 7471.43 7132.18 224.11 o 22 0 2 2426.52 2324.36 74.60 o 24 0 2 32.12 30.06 8.53 o 26 0 2 1707.14 1707.49 38.84 o 28 0 2 354.68 363.02 17.54 o 30 0 2 2004.93 1959.12 47.33 o -31 1 2 2.61 -2.25 2.25 o -29 1 2 166.53 165.86 13.13 o -27 1 2 14.17 12.82 3.47 o -25 1 2 946.05 932.57 28.41 o -23 1 2 5.20 14.12 5.20 o -21 1 2 346.71 343.52 14.82 o -19 1 2 2.60 14.58 5.96 o -17 1 2 1011.33 973.81 42.79 o -15 1 2 1102.03 1228.87 54.29 o -13 1 2 739.30 728.96 21.75 o -11 1 2 3053.39 3223.35 158.26 o -9 1 2 728.48 785.64 19.80 o -7 1 2 11.51 16.53 2.15 o -5 1 2 7391.46 6754.28 43.28 o -3 1 2 7549.02 7360.50 60.64 o -1 1 2 210.06 247.71 7.61 o 1 1 2 2663.01 2629.86 26.17 o 3 1 2 7194.76 7168.08 37.15 o 5 1 2 27.03 25.47 3.37 o 7 1 2 4926.11 4941.39 57.35 o 9 1 2 177.53 189.33 10.04 o 11 1 2 162.60 151.86 7.41 o 13 1 2 890.48 912.32 24.59 o 15 1 2 943.39 1034.58 43.38 o 17 1 2 85.99 94.18 9.73 o 19 1 2 1066.98 995.55 24.53 o 21 1 2 213.59 214.29 16.54 o 23 1 2 333.00 336.41 20.27 o 25 1 2 32.79 30.30 5.17 o 27 1 2 87.59 84.95 7.20 o 29 1 2 180.62 185.11 7.51 o 31 1 2 246.97 226.71 13.18 o -30 2 2 282.97 274.27 12.40 o -28 2 2 950.07 964.31 18.62 o -26 2 2 1329.40 1389.77 32.05 o -24 2 2 11.59 16.70 8.16 o -22 2 2 122.98 135.62 13.94 o -20 2 2 154.56 132.47 8.16 o -18 2 2 1136.77 1054.84 28.38 o -16 2 2 462.49 424.04 14.31 o -14 2 2 265.46 377.23 12.69 o -12 2 2 314.44 336.92 11.24 o -10 2 2 2342.50 2668.04 39.31 o -8 2 2 779.08 737.72 11.68 o -6 2 2 1674.48 1696.74 47.36 o -4 2 2 18.67 19.55 4.83 o -2 2 2 859.05 909.19 14.76 o 0 2 2 10809.12 10574.49 64.56 o 2 2 2 9924.66 9597.29 48.36 o 4 2 2 3921.21 3719.53 39.87 o 6 2 2 12538.90 12659.62 74.09 o 8 2 2 4685.98 4652.39 77.68 o 10 2 2 6.52 4.79 2.70 o 12 2 2 505.01 403.17 16.95 o 14 2 2 3896.81 3724.24 52.66 o 16 2 2 769.96 747.62 37.40 o 18 2 2 3875.95 3987.89 63.83 o 20 2 2 2538.40 2546.94 107.90 o 22 2 2 190.83 179.38 22.30 o 24 2 2 907.84 966.94 25.25 o 26 2 2 226.05 222.27 11.38 o 28 2 2 443.58 436.46 14.23 o 30 2 2 535.78 508.19 11.33 o -29 3 2 476.28 466.58 23.60 o -27 3 2 88.61 95.29 5.87 o -25 3 2 2842.76 2944.03 48.12 o -23 3 2 32.98 35.96 7.69 o -21 3 2 853.34 840.07 36.57 o -19 3 2 408.81 393.66 30.77 o -17 3 2 4894.83 5384.19 80.48 o -15 3 2 5283.85 5545.63 84.72 o -13 3 2 557.71 515.86 22.69 o -11 3 2 2399.96 2691.79 35.96 o -9 3 2 6603.95 6831.38 56.65 o -7 3 2 2470.95 2535.44 55.52 o -5 3 2 793.73 716.22 30.32 o -3 3 2 936.94 1071.20 24.92 o -1 3 2 75.23 60.67 2.92 o 1 3 2 1630.37 1501.17 15.86 o 3 3 2 2790.25 2899.09 24.02 o 5 3 2 12.26 23.38 4.39 o 7 3 2 502.72 514.74 13.92 o 9 3 2 2480.14 2592.12 55.12 o 11 3 2 1602.92 1563.13 29.95 o 13 3 2 24.96 15.46 3.04 o 15 3 2 6.80 5.45 2.94 o 17 3 2 482.58 465.27 16.78 o 19 3 2 1126.29 1202.24 58.80 o 21 3 2 16.07 21.65 5.84 o 23 3 2 1800.72 1906.08 36.22 o 25 3 2 423.95 431.67 13.40 o 27 3 2 1.51 1.60 1.44 o 29 3 2 318.59 321.06 11.41 o -28 4 2 718.85 722.47 15.43 o -26 4 2 158.77 149.83 11.66 o -24 4 2 207.20 219.43 13.07 o -22 4 2 131.42 116.31 8.29 o -20 4 2 411.58 414.08 16.32 o -18 4 2 79.44 70.05 8.55 o -16 4 2 814.58 794.42 27.22 o -14 4 2 1.29 1.63 5.71 o -12 4 2 215.02 254.16 23.58 o -10 4 2 119.29 112.66 10.06 o -8 4 2 371.32 345.50 24.29 o -6 4 2 92.37 94.51 13.32 o -4 4 2 536.63 516.85 30.99 o -2 4 2 7670.01 8093.71 87.28 o 0 4 2 2346.95 2499.40 93.77 o 2 4 2 111.38 97.04 9.51 o 4 4 2 6593.32 7389.95 51.73 o 6 4 2 3.52 2.25 1.89 o 8 4 2 806.93 799.22 21.30 o 10 4 2 52.40 111.42 10.90 o 12 4 2 88.49 86.17 7.12 o 14 4 2 16.52 15.91 3.14 o 16 4 2 97.11 87.14 9.03 o 18 4 2 2203.35 2370.41 58.93 o 20 4 2 9.10 4.55 3.96 o 22 4 2 5.65 6.77 3.19 o 24 4 2 492.58 503.14 12.69 o 26 4 2 150.64 162.89 6.85 o -25 5 2 83.16 103.23 12.80 o -23 5 2 655.61 687.94 18.96 o -21 5 2 193.20 207.05 12.34 o -19 5 2 4302.82 4256.71 60.48 o -17 5 2 1861.84 1838.46 40.67 o -15 5 2 4045.64 4104.58 61.65 o -13 5 2 1281.31 1298.96 44.57 o -11 5 2 1468.80 1644.93 32.57 o -9 5 2 6362.22 6797.32 60.07 o -7 5 2 1586.13 1617.94 29.75 o -5 5 2 7.62 6.51 4.82 o -3 5 2 1102.14 1146.75 52.78 o -1 5 2 308.64 268.11 17.00 o 1 5 2 2458.09 2503.85 67.06 o 3 5 2 506.57 526.95 24.68 o 5 5 2 928.77 1017.25 24.27 o 7 5 2 44.40 71.88 5.57 o 9 5 2 2590.44 2698.90 36.52 o 11 5 2 1861.28 1866.74 35.60 o 13 5 2 79.81 100.17 10.14 o 15 5 2 323.59 297.77 17.35 o 17 5 2 1453.02 1551.21 32.66 o 19 5 2 429.38 468.27 16.16 o 21 5 2 262.09 258.99 9.74 o 23 5 2 1400.44 1392.58 25.68 o 25 5 2 901.21 875.80 19.22 o -24 6 2 79.56 73.73 5.94 o -22 6 2 513.76 491.49 15.64 o -20 6 2 100.46 93.05 8.75 o 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