#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:36:36 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181261 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/39/2233916.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2233916_Fobs loop_ _publ_author_name 'Chaithanya, U.' 'Foro, Sabine' 'Gowda, B. Thimme' _publ_section_title ; N-(4-Methyl-2-nitrophenyl)succinamic acid ; _journal_coeditor_code KP2388 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o819 _journal_volume 68 _journal_year 2012 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 69.590 _cell_angle_beta 78.770 _cell_angle_gamma 83.620 _cell_length_a 4.8531 _cell_length_b 11.0150 _cell_length_c 11.7870 _exptl_crystal_F_000 264.00 _reflns_d_resolution_high 0.8001 _cod_data_source_file kp2388Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' CS18 P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 108.57 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 245.70 242.60 2.39 o 2 0 0 30.43 30.73 0.55 o 3 0 0 315.00 336.33 1.61 o 4 0 0 0.12 -0.28 0.58 o 5 0 0 37.43 36.74 1.24 o -5 1 0 50.08 48.07 1.35 o -4 1 0 4.48 7.48 0.49 o -3 1 0 21.80 43.61 0.60 o -2 1 0 1445.24 1508.31 2.18 o -1 1 0 14.55 21.54 0.25 o 1 1 0 242.79 241.38 2.95 o 2 1 0 1001.86 1051.42 3.41 o 3 1 0 30.13 24.67 0.34 o 4 1 0 11.83 12.79 0.80 o 5 1 0 6.67 7.35 0.81 o -5 2 0 51.92 54.00 1.41 o -4 2 0 0.36 1.61 0.45 o -3 2 0 22.85 23.50 0.78 o -2 2 0 510.36 572.93 1.69 o -1 2 0 13.37 16.28 0.20 o 0 2 0 290.56 273.79 1.32 o 1 2 0 2019.24 2100.76 4.89 o 2 2 0 124.53 121.44 2.26 o 3 2 0 126.31 131.60 1.00 o 4 2 0 16.45 15.48 0.89 o 5 2 0 59.38 62.45 1.57 o -5 3 0 16.45 14.03 0.54 o -4 3 0 73.62 65.97 0.99 o -3 3 0 4.11 6.23 0.27 o -2 3 0 31.84 38.13 0.66 o -1 3 0 26.53 20.07 0.46 o 0 3 0 817.48 745.41 1.67 o 1 3 0 387.35 377.95 1.01 o 2 3 0 82.68 71.61 1.25 o 3 3 0 98.37 88.64 0.96 o 4 3 0 98.01 97.64 1.69 o 5 3 0 74.58 78.83 1.79 o -5 4 0 18.06 16.13 0.57 o -4 4 0 1.39 2.37 0.35 o -3 4 0 12.89 12.20 0.33 o -2 4 0 8.40 8.95 0.21 o -1 4 0 172.45 167.46 2.15 o 0 4 0 224.82 204.69 0.91 o 1 4 0 33.23 42.81 1.13 o 2 4 0 601.05 592.74 1.92 o 3 4 0 178.02 193.32 1.28 o 4 4 0 154.52 141.63 2.00 o 5 4 0 13.43 13.97 0.98 o -5 5 0 7.72 9.15 0.69 o -4 5 0 64.48 67.32 0.95 o -3 5 0 179.03 173.95 4.02 o -2 5 0 0.32 0.16 0.19 o -1 5 0 66.41 70.67 1.22 o 0 5 0 128.69 132.66 2.27 o 1 5 0 5.88 7.02 0.31 o 2 5 0 223.54 204.20 1.22 o 3 5 0 175.63 176.29 4.05 o 4 5 0 9.89 10.50 0.81 o 5 5 0 0.00 0.11 0.68 o -5 6 0 8.68 9.55 0.81 o -4 6 0 19.31 18.53 0.92 o -3 6 0 74.38 71.63 1.41 o -2 6 0 155.88 143.04 3.55 o -1 6 0 71.09 63.84 2.02 o 0 6 0 109.63 108.28 2.50 o 1 6 0 1.66 2.39 0.15 o 2 6 0 74.85 76.82 3.07 o 3 6 0 1.50 1.35 0.35 o 4 6 0 11.70 10.31 0.77 o 5 6 0 0.18 0.63 0.67 o -4 7 0 1.17 1.31 0.65 o -3 7 0 0.03 -0.66 0.66 o -2 7 0 275.69 277.42 1.85 o -1 7 0 0.89 0.78 0.29 o 0 7 0 121.21 120.09 0.96 o 1 7 0 254.94 260.37 1.26 o 2 7 0 1.81 1.10 0.32 o 3 7 0 0.84 -0.16 0.36 o 4 7 0 1.18 1.37 0.66 o 5 7 0 4.08 4.16 0.75 o -4 8 0 21.30 24.75 1.17 o -3 8 0 19.05 19.84 0.95 o -2 8 0 14.36 13.18 0.80 o -1 8 0 146.65 147.81 1.22 o 0 8 0 47.39 45.01 0.77 o 1 8 0 159.37 168.27 1.92 o 2 8 0 16.06 15.58 0.48 o 3 8 0 3.36 4.43 0.42 o 4 8 0 15.62 16.06 0.94 o -4 9 0 52.34 59.54 1.69 o -3 9 0 1.06 1.80 0.62 o -2 9 0 0.51 0.22 0.44 o -1 9 0 112.47 103.07 1.34 o 0 9 0 15.76 13.65 0.81 o 1 9 0 64.17 66.00 1.37 o 2 9 0 0.01 -0.25 0.61 o 3 9 0 3.78 4.72 1.51 o 4 9 0 3.16 2.54 0.72 o -3 10 0 1.77 1.29 0.64 o -2 10 0 5.98 4.52 0.48 o -1 10 0 18.26 17.52 0.59 o 0 10 0 1.37 0.92 0.66 o 1 10 0 6.15 7.77 0.74 o 2 10 0 2.73 1.19 0.68 o 3 10 0 18.26 16.67 0.85 o -2 11 0 4.48 5.42 0.78 o -1 11 0 2.23 2.19 0.58 o 0 11 0 0.46 2.98 0.61 o 1 11 0 0.29 0.08 0.71 o 2 11 0 1.39 1.88 0.76 o 3 11 0 4.94 3.14 0.55 o -1 12 0 1.16 0.00 0.87 o 0 12 0 1.52 2.41 0.63 o 1 12 0 11.44 11.95 0.95 o 2 12 0 1.83 3.70 0.76 o -1 -12 1 3.67 3.16 0.75 o 0 -12 1 2.99 5.13 0.69 o 1 -12 1 3.50 1.92 0.62 o -2 -11 1 12.30 10.64 0.88 o -1 -11 1 37.59 45.56 1.41 o 0 -11 1 11.27 10.22 0.85 o 1 -11 1 15.90 15.89 0.85 o 2 -11 1 0.51 -0.39 0.63 o -3 -10 1 47.45 51.99 1.37 o -2 -10 1 7.90 7.88 0.79 o -1 -10 1 14.89 14.72 0.93 o 0 -10 1 44.31 43.57 1.23 o 1 -10 1 0.23 -0.04 0.61 o 2 -10 1 8.30 7.99 0.75 o 3 -10 1 0.52 2.02 0.77 o -4 -9 1 1.39 -0.47 0.47 o -3 -9 1 75.90 79.41 1.62 o -2 -9 1 9.74 8.31 0.76 o -1 -9 1 29.54 27.46 1.01 o 0 -9 1 34.99 36.13 1.08 o 1 -9 1 28.27 28.15 1.22 o 2 -9 1 11.43 9.79 0.53 o 3 -9 1 0.42 0.24 0.64 o -4 -8 1 0.01 -0.83 0.83 o -3 -8 1 13.99 11.71 0.53 o -2 -8 1 16.38 16.18 0.79 o -1 -8 1 76.49 74.27 1.38 o 0 -8 1 4.89 6.41 0.44 o 1 -8 1 0.02 -0.04 0.35 o 2 -8 1 237.10 246.47 1.67 o 3 -8 1 52.40 55.61 1.38 o 4 -8 1 1.24 1.06 0.62 o -4 -7 1 20.80 17.34 0.94 o -3 -7 1 16.53 15.09 1.41 o -2 -7 1 32.94 38.08 0.88 o -1 -7 1 21.74 27.91 0.87 o 0 -7 1 10.84 12.25 0.41 o 1 -7 1 127.43 122.82 1.06 o 2 -7 1 227.13 226.74 1.51 o 3 -7 1 4.52 3.83 0.62 o 4 -7 1 0.32 -0.17 0.64 o -5 -6 1 3.16 5.81 0.94 o -4 -6 1 36.98 37.61 1.19 o -3 -6 1 27.52 28.15 0.64 o -2 -6 1 5.62 3.18 0.33 o -1 -6 1 97.50 104.20 1.91 o 0 -6 1 176.10 183.39 4.13 o 1 -6 1 163.97 167.59 1.22 o 2 -6 1 140.59 137.66 1.10 o 3 -6 1 235.98 237.40 2.66 o 4 -6 1 6.51 5.96 0.74 o 5 -6 1 0.70 -0.55 0.71 o -5 -5 1 6.98 8.64 0.97 o -4 -5 1 7.87 8.45 0.79 o -3 -5 1 22.51 26.69 0.89 o -2 -5 1 66.13 71.95 0.85 o -1 -5 1 89.17 99.91 2.21 o 0 -5 1 588.07 568.65 5.61 o 1 -5 1 211.73 221.26 1.20 o 2 -5 1 25.29 26.95 0.50 o 3 -5 1 26.01 28.08 2.21 o 4 -5 1 74.79 69.29 1.53 o -5 -4 1 19.25 22.16 1.19 o -4 -4 1 81.54 87.22 1.69 o -3 -4 1 43.26 40.04 0.69 o -2 -4 1 135.61 153.14 1.77 o -1 -4 1 482.93 486.04 3.35 o 0 -4 1 109.90 112.86 2.79 o 1 -4 1 584.56 556.58 1.68 o 2 -4 1 6.80 6.02 0.20 o 3 -4 1 1.42 0.93 0.35 o 4 -4 1 0.18 0.57 0.34 o 5 -4 1 3.72 4.04 0.44 o -5 -3 1 23.67 27.28 1.29 o -4 -3 1 11.03 10.72 0.83 o -3 -3 1 0.43 0.35 0.39 o -2 -3 1 125.15 138.00 1.47 o -1 -3 1 58.06 57.03 0.34 o 0 -3 1 903.19 840.76 3.30 o 1 -3 1 843.17 823.87 4.72 o 2 -3 1 6.03 9.74 0.22 o 3 -3 1 35.16 31.06 0.45 o 4 -3 1 14.77 14.53 0.59 o 5 -3 1 69.44 62.03 0.97 o -5 -2 1 29.44 26.24 1.21 o -4 -2 1 99.45 97.99 1.71 o -3 -2 1 6.66 8.04 0.38 o -2 -2 1 32.11 36.79 1.34 o -1 -2 1 103.73 97.79 0.58 o 0 -2 1 133.76 133.31 0.57 o 1 -2 1 266.10 282.53 1.55 o 2 -2 1 25.88 27.84 0.26 o 3 -2 1 17.27 15.58 0.61 o 4 -2 1 84.86 87.99 0.82 o 5 -2 1 1.16 2.62 0.64 o -5 -1 1 1.79 2.26 0.78 o -4 -1 1 10.32 12.64 0.84 o -3 -1 1 214.94 222.79 2.07 o -2 -1 1 303.33 295.82 1.91 o -1 -1 1 503.73 485.32 0.97 o 0 -1 1 1096.43 1074.05 1.91 o 1 -1 1 3302.49 3017.08 21.76 o 2 -1 1 21.61 14.75 0.20 o 3 -1 1 181.64 189.67 0.97 o 4 -1 1 37.53 31.66 0.52 o 5 -1 1 18.46 19.89 0.97 o -5 0 1 6.45 6.15 0.84 o -4 0 1 116.52 101.79 1.67 o -3 0 1 383.71 403.75 2.68 o -2 0 1 141.33 151.27 1.34 o -1 0 1 380.66 339.89 0.89 o 1 0 1 1661.01 1616.13 3.02 o 2 0 1 92.05 83.73 0.57 o 3 0 1 72.88 79.32 1.16 o 4 0 1 0.78 1.31 0.35 o 5 0 1 13.65 15.92 0.94 o 6 0 1 3.90 3.47 0.89 o -5 1 1 0.29 0.00 0.63 o -4 1 1 86.87 85.35 0.96 o -3 1 1 55.87 53.56 1.03 o -2 1 1 916.75 865.65 12.81 o -1 1 1 2236.73 2155.06 11.24 o 1 1 1 14.09 15.42 0.23 o 2 1 1 343.21 330.95 1.23 o 3 1 1 82.18 77.00 1.36 o 4 1 1 13.51 10.03 0.80 o 5 1 1 0.01 -0.19 0.70 o 6 1 1 0.28 0.24 0.76 o -5 2 1 10.51 13.43 0.94 o -4 2 1 11.55 13.24 0.49 o -3 2 1 24.76 26.45 0.61 o -2 2 1 158.08 173.62 1.63 o -1 2 1 17.04 17.13 0.25 o 0 2 1 2959.90 2898.30 13.93 o 1 2 1 874.74 837.95 1.74 o 2 2 1 13.95 12.81 0.36 o 3 2 1 1.01 1.80 0.24 o 4 2 1 3.53 2.83 0.67 o 5 2 1 6.00 2.97 0.76 o -5 3 1 5.61 8.12 0.82 o -4 3 1 0.06 -0.27 0.27 o -3 3 1 0.48 1.06 0.19 o -2 3 1 96.55 97.43 0.58 o -1 3 1 394.18 393.95 2.28 o 0 3 1 1187.16 1167.27 2.73 o 1 3 1 92.60 98.79 0.71 o 2 3 1 231.38 256.53 1.11 o 3 3 1 50.76 48.47 0.60 o 4 3 1 4.35 6.78 0.71 o 5 3 1 23.50 23.49 1.09 o -5 4 1 2.53 2.40 0.53 o -4 4 1 1.48 1.45 0.30 o -3 4 1 11.27 8.74 0.30 o -2 4 1 127.68 137.15 1.30 o -1 4 1 97.57 73.29 0.65 o 0 4 1 913.06 857.06 2.09 o 1 4 1 1214.23 1166.14 3.89 o 2 4 1 213.17 227.91 2.35 o 3 4 1 59.14 63.72 0.73 o 4 4 1 1.36 0.69 0.63 o 5 4 1 87.37 81.87 1.77 o -5 5 1 0.28 -0.54 0.54 o -4 5 1 22.54 21.13 0.94 o -3 5 1 2.38 2.02 0.70 o -2 5 1 83.19 81.14 0.51 o -1 5 1 43.22 46.71 1.44 o 0 5 1 144.04 147.17 1.45 o 1 5 1 15.12 15.82 0.59 o 2 5 1 19.22 21.03 0.37 o 3 5 1 2.72 4.38 0.40 o 4 5 1 24.62 25.32 0.99 o 5 5 1 0.00 -0.55 0.71 o -5 6 1 1.84 1.15 0.45 o -4 6 1 0.75 2.42 0.66 o -3 6 1 11.21 12.38 0.79 o -2 6 1 47.59 48.01 0.85 o -1 6 1 37.39 40.73 0.63 o 0 6 1 13.36 15.14 0.38 o 1 6 1 4.23 3.49 0.15 o 2 6 1 5.02 5.53 0.28 o 3 6 1 21.13 24.00 1.43 o 4 6 1 74.42 72.09 1.49 o 5 6 1 1.65 0.84 0.77 o -4 7 1 11.39 9.19 0.81 o -3 7 1 116.85 118.07 1.86 o -2 7 1 54.48 51.41 0.80 o -1 7 1 50.54 49.65 0.70 o 0 7 1 2.29 2.40 0.64 o 1 7 1 44.09 42.68 0.65 o 2 7 1 1.15 2.47 0.25 o 3 7 1 19.75 19.26 0.59 o 4 7 1 4.14 5.25 0.72 o 5 7 1 0.04 0.74 0.80 o -4 8 1 9.31 7.15 0.70 o -3 8 1 4.40 3.79 0.73 o -2 8 1 124.44 121.51 1.22 o -1 8 1 0.01 0.16 0.35 o 0 8 1 2.85 3.07 0.35 o 1 8 1 22.08 27.73 0.90 o 2 8 1 0.57 0.23 0.31 o 3 8 1 1.19 2.31 0.63 o 4 8 1 2.69 1.66 0.67 o 5 8 1 3.48 4.61 0.88 o -4 9 1 10.57 15.25 0.99 o -3 9 1 0.33 0.01 0.64 o -2 9 1 22.52 20.66 0.67 o -1 9 1 102.68 99.49 1.11 o 0 9 1 108.28 102.88 2.26 o 1 9 1 40.66 40.23 1.10 o 2 9 1 82.91 94.46 1.59 o 3 9 1 0.16 0.05 0.59 o 4 9 1 1.60 1.57 0.62 o -3 10 1 3.06 5.19 0.69 o -2 10 1 14.15 14.97 0.64 o -1 10 1 125.31 135.70 1.35 o 0 10 1 0.40 0.79 0.57 o 1 10 1 6.53 6.53 0.72 o 2 10 1 2.75 4.51 0.74 o 3 10 1 0.02 -0.58 0.58 o 4 10 1 2.55 3.35 0.67 o -3 11 1 3.23 5.55 0.85 o -2 11 1 1.64 2.17 0.52 o -1 11 1 44.73 40.78 2.12 o 0 11 1 13.31 12.14 0.93 o 1 11 1 65.62 76.03 1.64 o 2 11 1 7.97 9.39 0.81 o 3 11 1 3.99 7.61 0.68 o -2 12 1 0.75 -0.10 0.42 o -1 12 1 0.95 2.75 0.81 o 0 12 1 1.28 0.31 0.70 o 1 12 1 16.25 18.17 1.08 o 0 13 1 1.77 1.27 0.70 o 1 13 1 6.91 7.59 0.83 o 0 -12 2 0.48 0.03 0.66 o -2 -11 2 2.82 1.57 0.51 o -1 -11 2 0.98 0.50 0.65 o 0 -11 2 15.21 15.78 0.98 o 1 -11 2 0.20 1.26 0.55 o 2 -11 2 0.41 -0.63 0.63 o -3 -10 2 2.33 1.41 0.67 o -2 -10 2 6.24 9.63 0.87 o -1 -10 2 0.03 -0.76 0.76 o 0 -10 2 0.05 0.56 0.69 o 1 -10 2 0.01 -0.09 0.38 o 2 -10 2 4.50 4.74 0.69 o 3 -10 2 0.53 -0.28 0.67 o -3 -9 2 5.33 4.40 0.73 o -2 -9 2 22.30 21.75 0.98 o -1 -9 2 0.02 0.50 0.58 o 0 -9 2 39.60 39.35 1.17 o 1 -9 2 6.22 7.06 0.48 o 2 -9 2 13.96 11.40 0.70 o 3 -9 2 3.58 2.71 0.69 o -4 -8 2 0.02 0.91 1.57 o -3 -8 2 2.92 4.18 0.71 o -2 -8 2 2.03 1.43 0.63 o -1 -8 2 22.15 23.01 0.94 o 0 -8 2 14.50 14.42 0.49 o 1 -8 2 0.94 0.78 0.36 o 2 -8 2 13.43 11.56 0.48 o 3 -8 2 10.36 9.38 0.84 o 4 -8 2 2.25 1.32 0.72 o -4 -7 2 0.29 0.96 0.68 o -3 -7 2 21.22 22.49 0.65 o -2 -7 2 1.19 0.47 0.59 o -1 -7 2 50.00 43.05 1.08 o 0 -7 2 35.18 38.48 0.62 o 1 -7 2 56.78 58.89 1.28 o 2 -7 2 151.11 137.39 1.19 o 3 -7 2 2.63 3.75 0.69 o 4 -7 2 15.84 15.63 0.94 o -5 -6 2 2.50 3.38 0.90 o -4 -6 2 0.14 0.34 0.65 o -3 -6 2 21.65 20.20 1.56 o -2 -6 2 11.63 8.69 0.41 o -1 -6 2 42.88 41.72 0.57 o 0 -6 2 98.46 90.76 1.03 o 1 -6 2 16.74 16.48 0.45 o 2 -6 2 88.13 83.20 0.88 o 3 -6 2 39.25 35.16 0.87 o 4 -6 2 9.20 9.23 0.51 o 5 -6 2 9.23 11.36 0.81 o -5 -5 2 22.94 24.35 1.20 o -4 -5 2 0.52 0.43 0.72 o -3 -5 2 1.67 4.50 0.42 o -2 -5 2 38.56 38.15 0.64 o -1 -5 2 14.31 12.70 0.74 o 0 -5 2 232.19 241.34 1.94 o 1 -5 2 0.05 0.07 0.27 o 2 -5 2 74.09 71.81 0.80 o 3 -5 2 140.08 142.86 1.25 o 4 -5 2 46.09 49.70 0.88 o 5 -5 2 17.32 21.49 0.68 o -5 -4 2 1.17 1.73 0.78 o -4 -4 2 13.55 15.55 0.94 o -3 -4 2 4.09 4.27 0.45 o -2 -4 2 97.39 100.66 1.00 o -1 -4 2 2.14 2.97 0.17 o 0 -4 2 105.85 124.78 2.51 o 1 -4 2 86.45 75.02 0.67 o 2 -4 2 238.99 244.99 1.51 o 3 -4 2 370.60 342.02 3.31 o 4 -4 2 0.34 0.54 0.82 o 5 -4 2 10.39 10.31 0.54 o -5 -3 2 29.18 34.44 1.35 o -4 -3 2 0.49 -0.54 0.69 o -3 -3 2 110.92 116.76 1.10 o -2 -3 2 194.79 210.36 2.91 o -1 -3 2 76.82 83.16 0.84 o 0 -3 2 54.00 52.80 1.42 o 1 -3 2 1622.93 1631.44 4.40 o 2 -3 2 1.07 1.78 0.29 o 3 -3 2 6.22 6.04 0.36 o 4 -3 2 37.90 38.30 0.74 o 5 -3 2 3.60 2.35 0.41 o -5 -2 2 42.36 41.02 1.48 o -4 -2 2 99.92 101.59 1.79 o -3 -2 2 15.68 14.99 0.47 o -2 -2 2 1421.21 1519.53 3.24 o -1 -2 2 846.52 871.04 3.62 o 0 -2 2 24.42 28.14 0.33 o 1 -2 2 2343.62 2170.32 4.99 o 2 -2 2 15.22 12.57 0.54 o 3 -2 2 32.84 31.87 0.44 o 4 -2 2 27.54 25.06 0.72 o 5 -2 2 4.11 3.11 0.64 o -5 -1 2 39.46 37.73 1.33 o -4 -1 2 354.78 380.22 3.24 o -3 -1 2 2.53 1.59 0.53 o -2 -1 2 0.17 0.55 0.42 o -1 -1 2 122.81 114.22 2.16 o 0 -1 2 203.32 204.74 1.18 o 1 -1 2 1420.49 1406.00 2.98 o 2 -1 2 0.01 -0.01 0.16 o 3 -1 2 121.76 130.28 0.80 o 4 -1 2 1.82 1.31 0.28 o 5 -1 2 55.42 50.02 0.90 o -5 0 2 6.67 3.52 0.73 o -4 0 2 112.91 115.69 1.85 o -3 0 2 29.68 33.16 0.92 o -2 0 2 2.80 2.60 0.41 o -1 0 2 361.75 358.46 1.16 o 0 0 2 749.79 727.70 1.52 o 1 0 2 11.74 8.36 0.28 o 2 0 2 215.61 213.37 0.80 o 3 0 2 326.66 337.09 2.01 o 4 0 2 20.86 21.71 0.58 o 5 0 2 5.78 5.21 0.48 o 6 0 2 9.20 11.99 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