#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:36:36 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181261 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/39/2233938.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2233938_Fobs loop_ _publ_author_name 'Beack, Hyun Jin' 'Yoo, Seung Mee' 'Kim, Jae Eun' 'Sim, Wonbo' 'Lee, Jai Young' _publ_section_title ; 6,7-Bis(bromomethyl)-2,11,18,21,24,27-hexaoxatetracyclo[26.4.0.0^4,9^.0^12,17^]dotriaconta-1(28),4,6,8,12(17),13,15,29,31-nonaene dichloromethane monosolvate ; _journal_coeditor_code LX2226 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o720 _journal_volume 68 _journal_year 2012 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 66.116 _cell_angle_beta 85.263 _cell_angle_gamma 77.080 _cell_length_a 9.1331 _cell_length_b 12.1909 _cell_length_c 15.0379 _exptl_crystal_F_000 716.00 _reflns_d_resolution_high 0.7490 _cod_data_source_file lx2226Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' sss in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 231.60 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 462.37 457.57 13.21 o 2 0 0 17594.08 20667.45 328.85 o 3 0 0 13.57 21.38 11.11 o 4 0 0 512.76 513.32 33.31 o 5 0 0 806.85 777.59 40.23 o 6 0 0 2.29 10.66 23.77 o 7 0 0 255.77 297.45 70.74 o 8 0 0 582.12 779.30 102.63 o 9 0 0 381.35 281.80 86.97 o 10 0 0 53.33 159.45 86.40 o 11 0 0 62.13 251.07 104.95 o -11 1 0 37.54 54.50 99.73 o -10 1 0 19.76 -12.18 66.10 o -9 1 0 131.31 120.61 67.26 o -8 1 0 4.09 54.50 52.18 o -7 1 0 219.59 189.03 62.04 o -6 1 0 689.59 747.38 59.57 o -5 1 0 6838.58 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25.91 85.82 74.22 o -6 9 0 108.90 139.36 52.83 o -5 9 0 0.78 51.93 35.66 o -4 9 0 189.07 72.48 54.50 o -3 9 0 254.72 216.86 65.52 o -2 9 0 131.85 233.06 43.42 o -1 9 0 609.33 542.14 85.82 o 0 9 0 2016.63 1872.86 128.14 o 1 9 0 395.86 355.31 45.08 o 2 9 0 2903.05 3573.42 376.02 o 3 9 0 275.55 260.39 43.78 o 4 9 0 11.91 -9.23 24.66 o 5 9 0 142.89 137.65 42.33 o 6 9 0 56.47 84.18 39.28 o 7 9 0 2.20 -34.54 34.54 o 8 9 0 0.35 38.44 42.49 o 9 9 0 97.34 30.55 73.06 o 10 9 0 279.84 167.10 210.77 o -7 10 0 97.28 126.54 55.71 o -6 10 0 170.05 182.65 58.15 o -5 10 0 199.26 248.08 56.54 o -4 10 0 96.30 128.14 71.90 o -3 10 0 294.96 401.82 87.55 o -2 10 0 360.52 407.62 90.45 o -1 10 0 101.66 115.39 52.76 o 0 10 0 97.69 71.32 49.29 o 1 10 0 246.25 367.03 78.28 o 2 10 0 84.54 12.41 47.26 o 3 10 0 1.17 42.14 31.61 o 4 10 0 6.20 -28.62 28.62 o 5 10 0 683.54 722.80 71.17 o 6 10 0 176.31 279.63 80.31 o 7 10 0 2.17 -18.27 42.04 o 8 10 0 165.62 154.38 77.70 o 9 10 0 73.75 16.37 38.98 o 10 10 0 94.78 -15.89 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