#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:36:36 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181261 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/39/2233967.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2233967_Fobs loop_ _publ_author_name 'El-Azab, Adel S.' 'Abdel-Aziz, Alaa A.-M.' 'Ng, Seik Weng' 'Tiekink, Edward R. T.' _publ_section_title ; 6-Methyl-3-phenyl-2-sulfanylidene-1,2,3,4-tetrahydroquinazolin-4-one ; _journal_coeditor_code QM2054 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o862 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 91.814 _cell_angle_gamma 90.000 _cell_length_a 12.7770 _cell_length_b 5.1384 _cell_length_c 19.0973 _exptl_crystal_F_000 560.00 _reflns_d_resolution_high 0.7924 _cod_data_source_file qm2054Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P21/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 141.16 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1611.27 1606.42 12.63 o 4 0 0 734.89 698.20 7.03 o 6 0 0 2.31 6.20 1.09 o 8 0 0 773.49 762.06 21.43 o 10 0 0 322.55 342.64 11.65 o 12 0 0 8.90 1.31 4.05 o 14 0 0 180.15 174.35 11.27 o 16 0 0 235.14 201.69 7.34 o 1 1 0 963.60 912.50 9.68 o 2 1 0 405.08 453.36 4.00 o 3 1 0 19926.29 18745.20 36.47 o 4 1 0 1355.32 1362.86 9.57 o 5 1 0 360.15 369.78 7.68 o 6 1 0 2889.32 3001.42 24.53 o 7 1 0 1929.09 1939.58 29.72 o 8 1 0 493.97 570.25 13.25 o 9 1 0 576.40 527.22 13.78 o 10 1 0 1.79 3.70 1.53 o 11 1 0 2.63 0.66 2.59 o 12 1 0 39.98 36.18 4.44 o 13 1 0 812.55 840.24 18.26 o 14 1 0 5.84 1.54 2.16 o 15 1 0 496.01 453.79 19.23 o 0 2 0 1518.76 1405.10 19.58 o 1 2 0 788.74 816.39 8.67 o 2 2 0 152.49 151.05 4.05 o 3 2 0 576.64 612.09 7.53 o 4 2 0 2944.81 3299.15 18.96 o 5 2 0 1098.69 1310.37 21.75 o 6 2 0 148.47 131.49 7.95 o 7 2 0 0.24 1.21 1.46 o 8 2 0 767.13 764.93 22.63 o 9 2 0 31.28 21.30 2.63 o 10 2 0 0.58 -3.16 5.31 o 11 2 0 66.49 50.08 3.67 o 12 2 0 0.74 1.41 1.62 o 13 2 0 13.15 13.07 2.57 o 14 2 0 67.30 69.27 4.08 o 15 2 0 7.20 10.30 2.40 o 1 3 0 993.95 942.72 17.33 o 2 3 0 1097.40 1249.36 26.97 o 3 3 0 363.85 377.12 15.83 o 4 3 0 215.89 176.07 11.66 o 5 3 0 49.28 40.41 6.48 o 6 3 0 13.73 9.15 3.90 o 7 3 0 1439.41 1499.84 37.97 o 8 3 0 232.82 183.90 12.85 o 9 3 0 826.66 760.98 19.98 o 10 3 0 80.00 77.81 6.30 o 11 3 0 41.87 41.83 5.20 o 12 3 0 120.46 120.62 5.75 o 13 3 0 53.14 61.36 3.44 o 14 3 0 13.37 7.43 2.04 o 0 4 0 651.86 648.02 19.57 o 1 4 0 1330.46 1422.83 27.99 o 2 4 0 51.10 41.38 4.95 o 3 4 0 283.22 300.32 10.66 o 4 4 0 32.11 37.59 2.75 o 5 4 0 37.35 33.33 3.99 o 6 4 0 693.30 664.82 18.49 o 7 4 0 38.63 30.47 4.90 o 8 4 0 13.03 19.51 3.15 o 9 4 0 293.07 285.07 9.47 o 10 4 0 124.17 135.27 6.45 o 11 4 0 90.04 98.47 10.59 o 12 4 0 26.16 24.74 2.08 o 1 5 0 4.55 4.85 1.75 o 2 5 0 33.15 40.55 3.04 o 3 5 0 168.16 180.33 6.52 o 4 5 0 256.37 293.33 13.60 o 5 5 0 0.23 3.47 2.72 o 6 5 0 56.34 59.41 6.00 o 7 5 0 61.09 68.66 4.06 o 8 5 0 7.93 10.32 2.30 o 9 5 0 106.26 116.52 5.87 o 10 5 0 55.21 57.39 3.36 o 0 6 0 33.55 33.06 2.88 o 1 6 0 41.73 36.38 2.23 o 2 6 0 129.35 117.01 3.84 o 3 6 0 264.85 237.49 5.30 o 4 6 0 0.41 2.15 0.88 o 5 6 0 196.81 191.03 6.35 o -15 0 1 109.76 105.19 7.56 o -13 0 1 129.10 119.74 10.36 o -11 0 1 293.16 301.13 16.31 o -9 0 1 95.27 121.09 9.36 o -7 0 1 792.70 736.16 18.71 o -5 0 1 1637.24 1590.22 17.25 o -3 0 1 14.00 8.27 0.68 o -1 0 1 9096.87 7688.42 20.04 o 1 0 1 1862.28 1786.15 10.67 o 3 0 1 3700.52 3524.83 24.95 o 5 0 1 31.78 30.82 1.95 o 7 0 1 128.45 101.36 4.02 o 9 0 1 3778.60 3827.36 51.97 o 11 0 1 187.46 168.91 12.13 o 13 0 1 40.88 38.87 6.79 o 15 0 1 388.81 386.17 13.82 o -15 1 1 177.96 173.82 6.33 o -14 1 1 328.62 319.70 10.28 o -13 1 1 2.06 1.85 2.51 o -12 1 1 989.43 999.36 21.00 o -11 1 1 112.88 108.82 7.25 o -10 1 1 47.87 48.72 3.39 o -9 1 1 17.90 20.78 3.53 o -8 1 1 344.50 338.75 10.12 o -7 1 1 38.90 35.90 3.25 o -6 1 1 2072.41 2195.33 20.79 o -5 1 1 599.99 626.56 7.56 o -4 1 1 775.61 733.57 8.49 o -3 1 1 2106.62 2091.18 13.96 o -2 1 1 1163.21 1158.05 7.79 o -1 1 1 7360.14 6648.66 40.22 o 0 1 1 19.81 21.19 1.29 o 1 1 1 2141.87 1977.46 10.26 o 2 1 1 9175.02 9088.08 16.75 o 3 1 1 17704.85 16765.40 39.07 o 4 1 1 928.43 941.57 10.87 o 5 1 1 1490.76 1594.41 16.13 o 6 1 1 647.51 661.35 16.78 o 7 1 1 14.74 20.28 2.69 o 8 1 1 42.86 34.41 3.61 o 9 1 1 17.43 20.11 3.12 o 10 1 1 152.31 147.50 5.58 o 11 1 1 71.82 67.86 5.75 o 12 1 1 369.69 376.47 12.85 o 13 1 1 0.91 5.45 2.75 o 14 1 1 154.66 144.30 7.20 o 15 1 1 1.53 -1.79 1.79 o -15 2 1 328.00 321.61 10.14 o -14 2 1 392.83 368.35 13.99 o -13 2 1 208.77 214.24 5.91 o -12 2 1 2.40 -0.58 1.81 o -11 2 1 11.39 8.15 1.94 o -10 2 1 171.45 173.03 6.97 o -9 2 1 71.68 66.30 3.44 o -8 2 1 524.30 568.26 19.29 o -7 2 1 273.57 258.35 12.01 o -6 2 1 65.33 64.05 5.60 o -5 2 1 1069.12 1076.77 10.10 o -4 2 1 0.92 0.56 0.75 o -3 2 1 4149.89 4545.93 21.96 o -2 2 1 148.60 161.86 4.85 o -1 2 1 0.93 0.52 0.96 o 0 2 1 63.73 63.29 3.10 o 1 2 1 863.13 792.51 10.05 o 2 2 1 137.87 158.38 3.28 o 3 2 1 571.53 698.84 6.80 o 4 2 1 1446.13 1675.09 51.33 o 5 2 1 3148.81 3526.72 35.61 o 6 2 1 2065.78 2108.84 31.18 o 7 2 1 242.97 242.05 11.89 o 8 2 1 403.29 400.45 16.31 o 9 2 1 702.62 672.61 11.53 o 10 2 1 2.30 1.88 2.29 o 11 2 1 844.60 817.85 12.07 o 12 2 1 5.13 0.78 1.76 o 13 2 1 150.17 139.55 6.73 o 14 2 1 8.19 6.85 1.85 o 15 2 1 33.17 28.70 3.34 o -14 3 1 70.47 65.62 4.58 o -13 3 1 15.54 14.74 2.00 o -12 3 1 81.72 91.52 5.07 o -11 3 1 594.87 573.31 12.97 o -10 3 1 28.29 22.12 2.98 o -9 3 1 1.30 -0.22 1.79 o -8 3 1 484.59 449.52 14.95 o -7 3 1 79.85 83.73 5.67 o -6 3 1 977.87 946.47 29.65 o -5 3 1 83.45 90.16 8.81 o -4 3 1 474.63 453.25 18.22 o -3 3 1 20.01 27.17 4.56 o -2 3 1 1386.31 1459.83 16.98 o -1 3 1 341.93 328.13 9.63 o 0 3 1 35.56 34.30 2.88 o 1 3 1 283.16 293.84 12.89 o 2 3 1 907.66 958.71 24.25 o 3 3 1 375.59 357.21 15.65 o 4 3 1 259.75 221.13 13.08 o 5 3 1 653.89 665.26 23.72 o 6 3 1 363.34 391.75 19.23 o 7 3 1 305.64 300.95 10.27 o 8 3 1 377.30 358.42 13.87 o 9 3 1 76.36 65.57 4.68 o 10 3 1 112.53 138.80 11.30 o 11 3 1 0.94 -0.80 2.68 o 12 3 1 3.89 0.97 1.64 o 13 3 1 73.34 80.99 3.74 o 14 3 1 118.12 112.05 5.66 o -12 4 1 52.17 56.22 4.23 o -11 4 1 157.28 164.25 6.08 o -10 4 1 200.39 213.58 7.98 o -9 4 1 66.84 68.36 4.93 o -8 4 1 282.59 249.44 17.42 o -7 4 1 371.47 339.65 11.77 o -6 4 1 256.81 218.75 9.28 o -5 4 1 107.47 96.28 6.31 o -4 4 1 25.72 21.73 2.12 o -3 4 1 114.05 102.87 4.70 o -2 4 1 95.42 87.83 4.95 o -1 4 1 52.73 55.22 5.64 o 0 4 1 74.67 81.25 5.02 o 1 4 1 1739.48 1712.70 31.50 o 2 4 1 234.89 238.59 8.69 o 3 4 1 376.45 355.89 8.99 o 4 4 1 666.13 665.90 10.68 o 5 4 1 198.63 217.00 9.10 o 6 4 1 280.28 287.23 20.62 o 7 4 1 0.58 2.03 1.88 o 8 4 1 3.28 6.74 2.46 o 9 4 1 155.26 158.87 7.10 o 10 4 1 234.72 240.19 6.28 o 11 4 1 5.41 1.42 1.43 o 12 4 1 231.22 230.74 5.49 o -10 5 1 15.43 15.62 1.41 o -9 5 1 67.18 71.45 4.60 o -8 5 1 2.41 0.21 1.29 o -7 5 1 48.88 55.65 3.68 o -6 5 1 17.88 19.27 2.50 o -5 5 1 0.35 3.29 2.51 o -4 5 1 57.76 51.61 5.92 o -3 5 1 1268.33 1363.35 29.65 o -2 5 1 46.75 41.98 3.05 o -1 5 1 121.50 131.28 4.41 o 0 5 1 57.95 56.55 2.99 o 1 5 1 0.67 2.19 1.40 o 2 5 1 25.12 24.28 2.50 o 3 5 1 49.51 57.07 3.47 o 4 5 1 300.60 311.00 14.21 o 5 5 1 7.27 11.33 3.44 o 6 5 1 44.71 38.43 5.05 o 7 5 1 352.03 370.27 13.12 o 8 5 1 206.15 216.15 6.33 o 9 5 1 4.15 3.71 1.93 o 10 5 1 131.50 170.50 5.54 o -5 6 1 82.59 77.97 4.00 o -4 6 1 149.86 140.07 4.05 o -3 6 1 0.05 2.51 0.92 o -2 6 1 74.64 72.52 3.15 o -1 6 1 247.15 238.17 7.94 o 0 6 1 500.82 532.18 11.54 o 1 6 1 108.24 105.47 5.50 o 2 6 1 8.54 6.29 1.78 o 3 6 1 1.45 0.18 1.24 o 4 6 1 174.40 153.86 6.31 o 5 6 1 19.81 16.29 2.15 o -16 0 2 10.20 6.80 1.73 o -14 0 2 425.21 436.03 17.43 o -12 0 2 167.53 144.92 11.61 o -10 0 2 658.12 651.15 16.61 o -8 0 2 0.88 1.72 2.52 o -6 0 2 2102.90 2026.84 27.31 o -4 0 2 215.59 206.21 6.84 o -2 0 2 780.12 754.53 8.97 o 0 0 2 691.21 718.74 6.15 o 2 0 2 11668.64 10726.15 38.15 o 4 0 2 2242.65 2404.34 24.90 o 6 0 2 973.60 964.49 30.57 o 8 0 2 7248.81 7620.42 68.95 o 10 0 2 18.71 19.80 3.36 o 12 0 2 87.09 94.47 9.79 o 14 0 2 0.11 -2.26 3.39 o 16 0 2 2.94 0.77 1.20 o -15 1 2 15.14 10.11 2.07 o -14 1 2 150.28 142.98 16.81 o -13 1 2 104.31 101.28 6.73 o -12 1 2 11.27 15.86 3.56 o -11 1 2 256.36 248.64 10.69 o -10 1 2 35.57 36.89 2.53 o -9 1 2 14.98 32.62 15.69 o -8 1 2 2.21 3.61 1.92 o -7 1 2 68.77 76.74 4.49 o -6 1 2 197.05 257.50 7.12 o -5 1 2 1396.94 1372.26 11.30 o -4 1 2 197.92 198.72 7.04 o -3 1 2 2473.91 2402.65 13.55 o -2 1 2 152.08 150.48 2.89 o -1 1 2 341.07 337.99 2.98 o 0 1 2 713.80 690.48 11.04 o 1 1 2 2560.09 2465.50 7.72 o 2 1 2 14808.74 14372.08 36.68 o 3 1 2 877.43 839.42 23.40 o 4 1 2 8.62 13.38 1.64 o 5 1 2 769.79 924.03 27.36 o 6 1 2 0.06 1.34 1.69 o 7 1 2 1052.94 1175.11 17.70 o 8 1 2 48.69 45.14 10.00 o 9 1 2 226.44 199.90 8.81 o 10 1 2 101.47 102.09 4.73 o 11 1 2 1678.97 1591.62 58.21 o 12 1 2 236.56 254.94 10.56 o 13 1 2 245.08 245.50 9.90 o 14 1 2 17.48 14.15 2.87 o 15 1 2 26.89 26.76 2.76 o -15 2 2 3.09 2.57 1.48 o -14 2 2 28.72 24.55 4.33 o -13 2 2 2.81 4.48 1.72 o -12 2 2 127.10 146.38 6.77 o -11 2 2 83.18 82.19 5.63 o -10 2 2 40.88 37.18 3.90 o -9 2 2 241.70 236.10 7.15 o -8 2 2 28.41 35.35 5.18 o -7 2 2 338.70 359.36 14.02 o -6 2 2 34.06 20.71 2.11 o -5 2 2 4.26 5.16 1.16 o -4 2 2 1862.54 1919.45 16.07 o -3 2 2 1166.79 1355.34 18.13 o -2 2 2 463.75 455.79 10.89 o -1 2 2 144.85 133.51 4.53 o 0 2 2 200.54 178.68 4.99 o 1 2 2 2790.70 2826.62 17.79 o 2 2 2 1611.70 1689.06 10.39 o 3 2 2 1613.40 1828.35 15.75 o 4 2 2 4163.00 4472.71 44.40 o 5 2 2 3714.70 3953.83 32.08 o 6 2 2 1461.11 1550.61 20.94 o 7 2 2 102.45 123.71 6.95 o 8 2 2 136.01 148.80 7.79 o 9 2 2 4.45 4.44 1.48 o 10 2 2 638.09 619.53 15.58 o 11 2 2 164.82 147.38 7.90 o 12 2 2 150.51 149.04 5.45 o 13 2 2 144.72 125.07 6.36 o 14 2 2 0.89 4.39 3.06 o 15 2 2 130.85 122.17 6.16 o -14 3 2 0.48 2.67 1.65 o -13 3 2 30.66 26.68 2.47 o -12 3 2 0.48 2.60 2.05 o -11 3 2 687.21 688.65 14.42 o -10 3 2 73.14 74.35 5.41 o -9 3 2 63.80 76.55 5.34 o -8 3 2 229.23 212.19 8.53 o -7 3 2 135.51 127.78 6.85 o -6 3 2 296.75 294.93 16.99 o -5 3 2 651.81 619.54 22.92 o -4 3 2 3.59 2.74 2.31 o -3 3 2 221.77 212.74 6.71 o -2 3 2 1222.10 1273.74 27.12 o -1 3 2 685.05 736.69 12.47 o 0 3 2 1381.23 1474.13 27.24 o 1 3 2 707.17 766.91 21.16 o 2 3 2 228.67 201.91 11.52 o 3 3 2 109.37 99.81 8.62 o 4 3 2 77.60 68.55 7.71 o 5 3 2 17.43 17.23 4.57 o 6 3 2 359.49 403.98 19.68 o 7 3 2 146.22 158.44 6.05 o 8 3 2 2013.50 2022.40 24.48 o 9 3 2 29.59 22.67 3.00 o 10 3 2 141.44 100.64 8.92 o 11 3 2 2.36 8.33 3.03 o 12 3 2 75.07 74.13 5.09 o 13 3 2 30.77 29.21 3.94 o 14 3 2 123.21 127.32 5.62 o -12 4 2 250.34 258.00 6.03 o -11 4 2 2.07 6.64 1.84 o -10 4 2 33.18 35.10 3.65 o -9 4 2 122.65 137.66 5.45 o -8 4 2 10.40 9.13 2.65 o -7 4 2 98.38 121.19 6.98 o -6 4 2 301.31 277.89 10.38 o -5 4 2 90.00 91.35 6.09 o -4 4 2 314.12 299.66 10.52 o -3 4 2 206.74 209.83 8.64 o -2 4 2 1.86 5.66 2.84 o -1 4 2 252.29 223.65 11.05 o 0 4 2 525.33 575.47 19.11 o 1 4 2 198.11 201.71 8.06 o 2 4 2 51.24 48.68 4.20 o 3 4 2 136.69 136.92 5.69 o 4 4 2 779.41 784.97 13.52 o 5 4 2 571.27 611.14 11.51 o 6 4 2 424.54 410.76 12.88 o 7 4 2 246.30 286.10 10.28 o 8 4 2 70.95 79.30 8.63 o 9 4 2 67.18 63.21 6.51 o 10 4 2 638.30 621.97 11.82 o 11 4 2 53.42 51.99 3.49 o 12 4 2 27.01 24.23 3.52 o -10 5 2 279.50 259.87 4.87 o -9 5 2 539.25 537.78 11.68 o -8 5 2 109.43 119.54 4.69 o -7 5 2 2.36 2.14 1.45 o -6 5 2 71.24 60.91 3.94 o -5 5 2 4.45 7.31 1.83 o -4 5 2 61.73 58.88 6.22 o -3 5 2 115.09 112.99 9.37 o -2 5 2 536.96 554.65 13.14 o -1 5 2 50.68 55.59 4.33 o 0 5 2 419.95 435.27 16.76 o 1 5 2 220.83 235.61 6.84 o 2 5 2 0.38 1.98 1.58 o 3 5 2 1550.91 1690.39 17.92 o 4 5 2 149.63 158.09 10.58 o 5 5 2 159.86 189.13 10.94 o 6 5 2 110.31 114.65 8.12 o 7 5 2 38.14 32.66 4.13 o 8 5 2 209.72 229.17 9.02 o 9 5 2 11.85 11.36 2.32 o 10 5 2 287.10 305.50 7.20 o -5 6 2 53.66 45.23 3.16 o -4 6 2 22.77 22.57 1.77 o -3 6 2 119.14 92.93 3.45 o -2 6 2 39.20 39.72 3.63 o -1 6 2 160.27 173.88 7.16 o 0 6 2 1.49 2.12 1.04 o 1 6 2 98.26 92.61 5.30 o 2 6 2 103.46 92.55 5.37 o 3 6 2 7.64 7.21 1.91 o 4 6 2 2.65 3.10 1.58 o 5 6 2 65.70 66.17 3.90 o -15 0 3 1.36 2.92 2.55 o -13 0 3 3745.24 3750.54 55.54 o -11 0 3 1946.51 1861.05 40.09 o -9 0 3 16.16 15.98 3.88 o -7 0 3 52.47 63.02 5.65 o -5 0 3 3.48 3.72 1.78 o -3 0 3 2024.05 1965.03 18.11 o -1 0 3 1560.75 1470.25 11.55 o 1 0 3 5856.92 5431.68 21.63 o 3 0 3 14.31 14.95 2.34 o 5 0 3 552.53 470.84 8.05 o 7 0 3 68.19 50.58 3.24 o 9 0 3 74.51 63.25 7.23 o 11 0 3 446.70 399.10 18.80 o 13 0 3 561.47 555.35 21.05 o 15 0 3 20.49 24.67 4.10 o -15 1 3 72.93 59.18 3.75 o -14 1 3 32.66 33.24 3.74 o -13 1 3 20.76 21.71 3.64 o -12 1 3 40.26 40.74 4.88 o -11 1 3 8.59 11.29 2.49 o -10 1 3 1085.72 1082.45 12.16 o -9 1 3 0.90 -0.90 1.87 o -8 1 3 869.14 827.56 22.95 o -7 1 3 497.50 480.98 10.76 o -6 1 3 525.35 520.24 7.90 o -5 1 3 1.77 1.91 0.92 o -4 1 3 2102.68 1975.70 47.72 o -3 1 3 467.73 473.18 6.27 o -2 1 3 2354.04 2397.78 20.54 o -1 1 3 797.00 736.58 11.60 o 0 1 3 176.49 154.91 5.79 o 1 1 3 572.91 541.28 11.05 o 2 1 3 15524.84 14166.28 66.64 o 3 1 3 1081.25 1147.20 10.56 o 4 1 3 486.29 487.39 8.44 o 5 1 3 95.62 119.29 4.81 o 6 1 3 849.96 891.22 14.31 o 7 1 3 792.18 879.16 15.72 o 8 1 3 25.97 33.42 3.78 o 9 1 3 40.49 35.63 4.15 o 10 1 3 668.72 659.08 12.76 o 11 1 3 126.22 129.56 8.66 o 12 1 3 201.32 203.39 9.35 o 13 1 3 352.89 346.49 11.49 o 14 1 3 138.94 138.58 6.64 o 15 1 3 0.84 -0.51 4.10 o -15 2 3 202.14 169.11 6.58 o -14 2 3 363.56 371.29 14.20 o -13 2 3 22.39 16.27 2.48 o -12 2 3 112.08 107.42 5.91 o -11 2 3 237.64 223.02 8.88 o -10 2 3 80.58 75.49 5.53 o -9 2 3 119.85 120.28 5.43 o -8 2 3 9.47 12.25 3.63 o -7 2 3 209.13 233.01 7.29 o -6 2 3 74.30 78.07 4.02 o -5 2 3 394.27 427.25 8.61 o -4 2 3 202.35 177.03 7.09 o -3 2 3 596.75 621.90 13.15 o -2 2 3 271.23 281.82 9.10 o -1 2 3 101.00 87.50 3.75 o 0 2 3 576.36 531.34 13.97 o 1 2 3 2.67 2.26 0.71 o 2 2 3 81.56 58.38 5.31 o 3 2 3 1607.75 1530.25 28.66 o 4 2 3 126.63 135.00 5.78 o 5 2 3 10338.01 10420.59 49.02 o 6 2 3 131.42 136.15 6.38 o 7 2 3 16.86 11.91 2.57 o 8 2 3 41.40 39.51 4.26 o 9 2 3 4.32 2.70 1.61 o 10 2 3 191.04 180.78 8.52 o 11 2 3 235.02 222.78 9.44 o 12 2 3 6.31 10.29 2.57 o 13 2 3 226.30 235.92 8.31 o 14 2 3 562.58 520.23 10.02 o 15 2 3 7.91 6.30 1.77 o -14 3 3 12.33 9.57 1.99 o -13 3 3 29.02 35.09 4.65 o -12 3 3 369.30 380.29 9.87 o -11 3 3 485.32 495.12 12.64 o -10 3 3 249.45 241.47 9.35 o -9 3 3 153.86 117.84 5.26 o -8 3 3 261.19 220.08 12.83 o -7 3 3 619.16 616.00 17.18 o -6 3 3 26.85 25.46 2.75 o -5 3 3 969.37 1065.35 30.16 o -4 3 3 759.86 784.03 13.42 o -3 3 3 6.32 3.57 1.38 o -2 3 3 1529.55 1589.15 20.41 o -1 3 3 1200.61 1238.89 16.12 o 0 3 3 608.03 657.68 18.76 o 1 3 3 846.70 907.12 23.54 o 2 3 3 335.60 329.56 14.93 o 3 3 3 377.31 362.29 16.26 o 4 3 3 325.90 287.30 15.30 o 5 3 3 203.78 192.59 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