#------------------------------------------------------------------------------ #$Date: 2012-09-11 12:26:43 +0300 (Tue, 11 Sep 2012) $ #$Revision: 66590 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/39/2233996.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2233996_Fobs loop_ _publ_author_name 'Jothi, L.' 'Vasuki, G.' 'Babu, R. Ramesh' 'Ramamurthi, K.' _publ_section_title ; 4-Bromo-N-(4-hydroxybenzylidene)aniline ; _journal_coeditor_code SJ5193 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o772 _journal_volume 68 _journal_year 2012 _space_group_IT_number 60 _symmetry_space_group_name_Hall '-P 2n 2ab' _symmetry_space_group_name_H-M 'P b c n' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 21.9588 _cell_length_b 11.0866 _cell_length_c 9.3132 _exptl_crystal_F_000 1104.00 _reflns_d_resolution_high 0.8410 _[local]_cod_data_source_file sj5193Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' BHBA in Pbcn' _shelx_refln_list_code 4 _shelx_f_calc_maximum 393.88 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y+1/2, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y, -z+1/2' '-x, -y, -z' 'x-1/2, y-1/2, -z-1/2' '-x-1/2, y-1/2, z' 'x, -y, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 3585.97 1044.38 46.13 o 4 0 0 11050.76 11009.20 182.68 o 6 0 0 22886.85 22712.15 372.80 o 8 0 0 41177.37 44837.35 803.68 o 10 0 0 1527.87 1537.40 47.98 o 12 0 0 12573.48 15477.55 365.18 o 14 0 0 4506.82 5130.89 131.20 o 16 0 0 3051.13 3975.58 107.52 o 18 0 0 854.35 1136.65 51.48 o 20 0 0 72.08 35.79 31.04 o 22 0 0 603.83 710.08 45.05 o 24 0 0 193.17 227.22 53.34 o 26 0 0 582.52 529.49 65.35 o 1 1 0 734.00 372.31 19.29 o 3 1 0 17862.29 17326.69 200.24 o 5 1 0 25714.93 26370.09 333.96 o 7 1 0 14022.43 14465.81 167.64 o 9 1 0 811.00 805.60 20.94 o 11 1 0 5031.90 5760.44 93.23 o 13 1 0 536.98 591.48 22.47 o 15 1 0 165.96 219.98 22.24 o 17 1 0 42.44 21.53 24.07 o 19 1 0 57.71 45.52 22.73 o 21 1 0 162.03 138.61 24.50 o 23 1 0 395.27 408.31 34.45 o 25 1 0 54.72 56.14 28.64 o 0 2 0 15465.88 16934.64 303.42 o 2 2 0 32900.10 35303.19 446.13 o 4 2 0 9754.90 11013.48 127.70 o 6 2 0 2436.24 2634.30 37.49 o 8 2 0 14516.61 15814.66 201.71 o 10 2 0 1275.95 1527.07 24.14 o 12 2 0 1115.38 1207.05 36.02 o 14 2 0 6026.02 6559.36 99.84 o 16 2 0 1651.59 1770.79 49.37 o 18 2 0 265.15 312.10 33.97 o 20 2 0 46.87 88.85 23.86 o 22 2 0 234.34 281.17 29.48 o 24 2 0 112.79 167.91 37.14 o 1 3 0 47157.18 47220.55 595.48 o 3 3 0 21478.00 20811.02 294.12 o 5 3 0 30715.45 30068.94 379.82 o 7 3 0 23024.27 22933.47 290.39 o 9 3 0 13848.52 14144.99 190.91 o 11 3 0 14301.18 14333.61 184.27 o 13 3 0 4949.75 5371.71 78.11 o 15 3 0 28.73 18.84 12.79 o 17 3 0 65.53 64.19 11.20 o 19 3 0 1176.61 1224.59 40.85 o 21 3 0 304.72 316.04 28.41 o 23 3 0 540.88 458.76 39.40 o 25 3 0 261.96 277.30 35.38 o 0 4 0 9326.60 11112.62 222.92 o 2 4 0 17574.08 16140.43 228.28 o 4 4 0 11398.35 10024.33 142.72 o 6 4 0 2231.11 1954.38 27.61 o 8 4 0 1638.68 1701.39 25.62 o 10 4 0 150.55 255.45 10.95 o 12 4 0 145.46 140.17 12.12 o 14 4 0 0.93 8.99 11.81 o 16 4 0 18.39 12.93 16.07 o 18 4 0 461.75 535.99 28.79 o 20 4 0 4.12 6.23 36.20 o 22 4 0 1693.48 1875.34 88.74 o 24 4 0 76.26 64.57 46.21 o 1 5 0 3593.59 3863.63 56.51 o 3 5 0 9192.57 9368.53 133.61 o 5 5 0 5940.09 5950.19 83.58 o 7 5 0 3575.95 3518.12 50.03 o 9 5 0 1309.95 1216.11 21.39 o 11 5 0 6643.24 6231.95 87.63 o 13 5 0 920.94 760.07 20.09 o 15 5 0 2613.84 2315.42 50.60 o 17 5 0 1360.47 1104.48 40.91 o 19 5 0 216.36 177.99 25.26 o 21 5 0 174.83 200.86 39.00 o 23 5 0 346.82 383.40 71.33 o 0 6 0 6942.59 6886.01 140.31 o 2 6 0 4101.04 3843.18 56.85 o 4 6 0 14623.68 14236.79 202.39 o 6 6 0 11081.32 10767.21 154.08 o 8 6 0 1895.95 1628.66 25.65 o 10 6 0 8094.90 7543.61 98.96 o 12 6 0 2759.60 2286.90 40.77 o 14 6 0 174.47 330.56 20.62 o 16 6 0 380.47 248.00 23.41 o 18 6 0 843.16 685.57 31.32 o 20 6 0 65.62 129.37 31.37 o 22 6 0 3.97 -0.15 49.73 o 1 7 0 627.87 760.43 16.03 o 3 7 0 3623.08 4218.17 62.75 o 5 7 0 30.74 21.43 5.08 o 7 7 0 367.56 428.27 13.80 o 9 7 0 378.91 345.88 12.88 o 11 7 0 45.16 54.16 13.33 o 13 7 0 1163.64 1046.60 35.34 o 15 7 0 532.28 520.71 25.95 o 17 7 0 249.47 289.67 27.65 o 19 7 0 439.45 566.94 68.14 o 21 7 0 263.54 336.18 76.27 o 0 8 0 1199.16 1066.54 27.37 o 2 8 0 368.54 246.36 10.02 o 4 8 0 1084.84 752.02 16.47 o 6 8 0 2097.67 1589.97 27.53 o 8 8 0 3577.55 3096.14 49.70 o 10 8 0 23.50 71.73 15.27 o 12 8 0 1628.06 1231.40 37.81 o 14 8 0 181.89 102.51 26.07 o 16 8 0 1450.93 1131.29 56.17 o 18 8 0 170.20 126.24 50.47 o 20 8 0 512.38 443.40 83.50 o 1 9 0 1241.01 1448.30 24.71 o 3 9 0 2863.30 3080.76 43.82 o 5 9 0 1636.01 1713.92 28.24 o 7 9 0 61.41 65.16 14.40 o 9 9 0 25.85 6.34 21.87 o 11 9 0 827.75 701.90 30.20 o 13 9 0 561.87 452.30 29.61 o 15 9 0 39.79 46.28 34.56 o 17 9 0 63.85 22.65 46.73 o 19 9 0 359.07 211.92 58.51 o 0 10 0 312.45 590.04 44.91 o 2 10 0 47.23 255.62 21.06 o 4 10 0 5.40 47.55 19.08 o 6 10 0 113.47 13.73 19.40 o 8 10 0 965.58 1203.16 40.41 o 10 10 0 44.16 -14.17 22.52 o 12 10 0 41.77 3.83 29.56 o 14 10 0 23.91 30.72 41.70 o 16 10 0 46.22 67.28 65.46 o 1 11 0 95.65 24.27 21.49 o 3 11 0 101.76 44.87 21.69 o 5 11 0 99.21 21.11 22.49 o 7 11 0 833.53 561.32 29.54 o 9 11 0 344.66 443.94 31.73 o 11 11 0 921.57 762.69 50.18 o 13 11 0 29.62 -7.05 95.84 o 0 12 0 1253.82 1431.67 66.72 o 2 12 0 14.60 0.35 25.82 o 4 12 0 51.85 65.79 24.18 o 6 12 0 3.71 12.56 37.22 o 8 12 0 450.58 498.02 72.70 o 10 12 0 4.14 -7.65 40.38 o 1 13 0 72.23 286.16 48.64 o 3 13 0 27.96 15.79 38.72 o 1 1 1 52.33 30.84 2.55 o 2 1 1 1145.18 1071.12 9.28 o 3 1 1 1996.96 2042.45 16.61 o 4 1 1 24617.66 24001.41 197.35 o 5 1 1 9746.81 10078.83 82.15 o 6 1 1 10214.68 9696.11 82.82 o 7 1 1 4934.58 5383.64 47.01 o 8 1 1 3907.22 3516.35 33.41 o 9 1 1 7.85 -0.12 4.93 o 10 1 1 2817.44 2267.50 24.10 o 11 1 1 156.53 147.33 8.04 o 12 1 1 4667.79 4367.85 46.15 o 13 1 1 347.35 417.39 17.61 o 14 1 1 2351.71 2078.27 32.81 o 15 1 1 13.54 18.07 12.16 o 16 1 1 3897.71 3881.34 50.73 o 17 1 1 30.89 62.92 13.84 o 18 1 1 3100.87 3072.48 47.47 o 19 1 1 0.89 57.64 15.31 o 20 1 1 1815.84 1793.37 39.96 o 21 1 1 12.48 51.64 16.77 o 22 1 1 1787.29 1787.47 38.11 o 23 1 1 19.65 66.60 22.82 o 24 1 1 328.23 343.45 21.43 o 25 1 1 6.94 18.09 24.37 o 0 2 1 13515.04 14300.01 183.74 o 1 2 1 12004.57 12768.42 107.09 o 2 2 1 96.61 102.48 2.11 o 3 2 1 1937.16 1794.71 15.21 o 4 2 1 2678.75 2964.43 26.18 o 5 2 1 357.68 217.57 4.84 o 6 2 1 1104.68 1049.32 11.29 o 7 2 1 5937.28 5418.35 50.95 o 8 2 1 1296.51 1461.19 16.06 o 9 2 1 3972.86 3428.22 34.87 o 10 2 1 213.70 274.24 9.83 o 11 2 1 17866.20 18707.73 176.36 o 12 2 1 310.04 416.58 18.71 o 13 2 1 5211.84 4850.34 66.22 o 14 2 1 417.68 419.76 13.97 o 15 2 1 6149.28 6225.87 91.90 o 16 2 1 77.84 83.03 10.88 o 17 2 1 2518.51 2484.60 41.47 o 18 2 1 0.36 6.23 14.89 o 19 2 1 1782.95 1987.05 37.50 o 20 2 1 48.21 112.29 17.55 o 21 2 1 479.88 531.59 21.49 o 22 2 1 14.18 21.65 18.94 o 23 2 1 416.85 479.13 22.92 o 24 2 1 2.68 8.51 20.01 o 25 2 1 430.56 437.18 25.75 o 1 3 1 312.18 348.47 4.65 o 2 3 1 0.85 2.24 2.18 o 3 3 1 1282.11 1164.77 11.07 o 4 3 1 593.83 508.37 6.67 o 5 3 1 363.16 383.34 6.47 o 6 3 1 715.90 677.74 8.85 o 7 3 1 1477.70 1675.40 17.93 o 8 3 1 126.28 88.94 5.02 o 9 3 1 2247.46 2773.00 28.32 o 10 3 1 262.03 277.65 10.67 o 11 3 1 2606.92 2768.71 29.87 o 12 3 1 388.74 411.76 9.91 o 13 3 1 25.60 39.04 7.98 o 14 3 1 50.28 74.52 8.26 o 15 3 1 548.34 659.60 22.25 o 16 3 1 6.07 12.92 8.37 o 17 3 1 134.61 164.46 10.43 o 18 3 1 99.42 140.75 14.07 o 19 3 1 283.86 260.66 18.17 o 20 3 1 127.75 151.72 17.66 o 21 3 1 23.34 27.68 19.64 o 22 3 1 243.18 170.01 19.34 o 23 3 1 86.77 151.95 21.88 o 24 3 1 41.28 61.90 29.81 o 25 3 1 24.80 21.47 24.72 o 0 4 1 2037.96 2308.55 30.75 o 1 4 1 526.83 595.75 7.29 o 2 4 1 3.72 9.98 2.92 o 3 4 1 2850.95 3079.68 28.72 o 4 4 1 677.83 588.87 7.85 o 5 4 1 92.25 107.15 4.18 o 6 4 1 1679.82 1710.68 17.56 o 7 4 1 1322.28 1326.22 14.74 o 8 4 1 49.79 36.22 4.20 o 9 4 1 3632.16 3838.76 37.82 o 10 4 1 3.69 1.28 6.53 o 11 4 1 2436.03 2544.77 28.36 o 12 4 1 438.15 450.25 16.11 o 13 4 1 2856.77 2969.79 33.26 o 14 4 1 192.81 210.75 12.63 o 15 4 1 2385.46 2342.40 44.14 o 16 4 1 235.08 264.10 12.92 o 17 4 1 2690.49 2609.50 48.24 o 18 4 1 250.63 274.52 18.09 o 19 4 1 440.99 399.42 19.91 o 20 4 1 202.49 154.87 19.01 o 21 4 1 1316.60 1229.26 30.89 o 22 4 1 8.91 10.97 24.29 o 23 4 1 583.22 585.83 28.61 o 24 4 1 96.06 79.12 32.96 o 1 5 1 2.14 2.99 3.51 o 2 5 1 337.34 310.71 5.84 o 3 5 1 1691.40 1625.75 16.41 o 4 5 1 21.67 35.02 4.04 o 5 5 1 173.28 247.23 5.61 o 6 5 1 5623.28 5918.73 54.47 o 7 5 1 1258.42 1405.58 15.35 o 8 5 1 1579.50 1607.55 17.74 o 9 5 1 78.44 50.27 6.05 o 10 5 1 8794.38 9116.61 85.91 o 11 5 1 470.06 438.08 10.28 o 12 5 1 1185.10 1378.97 19.45 o 13 5 1 0.06 -2.11 10.52 o 14 5 1 4923.01 5332.35 70.81 o 15 5 1 85.05 110.28 15.10 o 16 5 1 1441.68 1518.11 32.49 o 17 5 1 83.75 108.04 15.85 o 18 5 1 2689.58 2844.06 66.42 o 19 5 1 2.54 -8.91 17.48 o 20 5 1 257.12 330.71 26.07 o 21 5 1 15.76 2.65 21.56 o 22 5 1 1159.57 1196.18 43.27 o 23 5 1 24.03 37.44 34.60 o 24 5 1 56.82 38.82 41.42 o 0 6 1 2068.05 2242.68 31.07 o 1 6 1 2634.64 2953.02 28.19 o 2 6 1 113.32 107.77 4.74 o 3 6 1 9.46 25.42 4.59 o 4 6 1 163.66 229.41 5.73 o 5 6 1 348.71 396.32 7.67 o 6 6 1 32.49 36.64 5.24 o 7 6 1 414.48 412.13 8.20 o 8 6 1 831.64 818.23 12.00 o 9 6 1 369.13 339.64 7.90 o 10 6 1 9.64 13.27 5.46 o 11 6 1 109.85 118.61 8.45 o 12 6 1 241.87 216.11 9.61 o 13 6 1 952.86 1018.75 21.43 o 14 6 1 460.24 492.89 16.90 o 15 6 1 9.40 4.06 14.56 o 16 6 1 59.65 75.80 15.41 o 17 6 1 25.32 55.48 17.05 o 18 6 1 6.22 16.44 18.55 o 19 6 1 13.90 41.10 20.31 o 20 6 1 7.61 -18.23 21.34 o 21 6 1 2.04 -4.41 36.67 o 22 6 1 99.76 81.79 31.04 o 23 6 1 11.11 -16.79 32.44 o 1 7 1 1.71 -1.54 5.04 o 2 7 1 7.59 3.47 5.19 o 3 7 1 646.72 575.69 9.86 o 4 7 1 26.54 51.88 5.54 o 5 7 1 810.79 729.96 11.12 o 6 7 1 37.71 78.50 6.26 o 7 7 1 219.48 238.35 7.34 o 8 7 1 181.96 255.31 7.81 o 9 7 1 1266.21 1326.04 17.02 o 10 7 1 2327.72 2562.31 27.97 o 11 7 1 2795.44 2646.62 31.92 o 12 7 1 454.10 530.87 14.26 o 13 7 1 75.87 74.45 13.09 o 14 7 1 1715.10 1782.66 37.40 o 15 7 1 503.74 492.86 24.94 o 16 7 1 414.42 416.54 19.28 o 17 7 1 39.15 27.23 18.61 o 18 7 1 281.26 309.16 22.87 o 19 7 1 108.24 135.78 24.70 o 20 7 1 269.97 279.57 31.27 o 21 7 1 96.18 123.11 35.52 o 22 7 1 537.71 493.23 46.77 o 0 8 1 273.99 301.74 10.35 o 1 8 1 2.86 0.92 5.89 o 2 8 1 108.18 97.51 6.32 o 3 8 1 582.71 718.98 11.55 o 4 8 1 0.00 0.13 6.27 o 5 8 1 1132.86 1358.95 16.52 o 6 8 1 443.61 434.27 9.32 o 7 8 1 1157.66 1423.17 18.57 o 8 8 1 178.18 168.03 8.95 o 9 8 1 1376.13 1652.36 21.59 o 10 8 1 311.49 309.14 12.11 o 11 8 1 519.82 716.67 17.61 o 12 8 1 165.16 187.74 14.06 o 13 8 1 31.16 92.42 14.62 o 14 8 1 48.77 61.83 16.06 o 15 8 1 1748.20 2042.87 40.73 o 16 8 1 39.81 25.24 22.21 o 17 8 1 455.58 553.26 28.32 o 18 8 1 50.84 60.23 29.59 o 19 8 1 888.99 942.13 43.34 o 20 8 1 2.84 -47.05 38.28 o 1 9 1 14.78 4.30 7.26 o 2 9 1 231.41 279.74 8.88 o 3 9 1 318.94 268.18 9.91 o 4 9 1 107.34 166.53 9.44 o 5 9 1 3.48 -2.21 8.76 o 6 9 1 152.88 110.83 9.41 o 7 9 1 216.98 229.20 10.73 o 8 9 1 524.21 672.55 17.10 o 9 9 1 53.17 27.47 11.22 o 10 9 1 4.84 21.32 12.66 o 11 9 1 558.97 533.26 18.03 o 12 9 1 163.79 238.32 16.91 o 13 9 1 65.86 67.66 17.78 o 14 9 1 366.81 435.19 24.13 o 15 9 1 88.31 67.90 24.64 o 16 9 1 29.80 30.05 28.68 o 17 9 1 30.45 19.38 33.34 o 18 9 1 45.33 19.26 37.00 o 0 10 1 203.07 214.37 15.91 o 1 10 1 13.21 15.28 9.35 o 2 10 1 3.97 5.19 9.59 o 3 10 1 324.45 346.95 12.20 o 4 10 1 380.18 398.46 14.87 o 5 10 1 2.09 9.40 11.88 o 6 10 1 805.17 754.44 28.36 o 7 10 1 341.88 380.93 16.09 o 8 10 1 0.24 4.08 13.55 o 9 10 1 213.15 171.45 16.94 o 10 10 1 18.64 12.17 16.64 o 11 10 1 504.77 486.53 21.00 o 12 10 1 68.98 57.92 18.37 o 13 10 1 50.36 55.60 19.39 o 14 10 1 39.37 59.51 27.60 o 15 10 1 39.13 69.75 31.51 o 16 10 1 7.93 4.42 32.97 o 1 11 1 10.49 -0.98 15.26 o 2 11 1 1.34 -16.46 15.01 o 3 11 1 17.29 -0.60 14.97 o 4 11 1 16.09 -20.93 15.14 o 5 11 1 1.77 -7.39 15.62 o 6 11 1 207.94 331.79 18.26 o 7 11 1 19.79 11.20 16.60 o 8 11 1 91.70 178.52 17.76 o 9 11 1 81.16 89.60 18.06 o 10 11 1 80.29 175.22 20.08 o 11 11 1 237.25 215.95 23.85 o 12 11 1 428.93 592.49 35.62 o 13 11 1 0.44 12.88 30.49 o 14 11 1 89.88 128.24 33.68 o 0 12 1 0.30 -9.45 23.81 o 1 12 1 0.03 -1.79 17.36 o 2 12 1 10.44 -0.90 16.74 o 3 12 1 195.42 218.88 18.43 o 4 12 1 39.08 15.06 18.63 o 5 12 1 110.52 34.90 20.14 o 6 12 1 56.29 64.48 20.94 o 7 12 1 322.65 431.88 26.95 o 8 12 1 3.13 4.55 27.30 o 9 12 1 101.01 80.80 28.86 o 10 12 1 89.49 114.18 30.37 o 1 13 1 12.83 64.82 26.41 o 2 13 1 3.77 47.17 26.39 o 3 13 1 71.34 93.85 26.93 o 0 0 2 45213.94 42390.48 1136.73 o 1 0 2 3672.75 3602.63 37.63 o 2 0 2 34835.67 32921.28 373.69 o 3 0 2 14900.91 15593.72 184.81 o 4 0 2 155145.34 145929.98 2021.59 o 5 0 2 324.79 321.34 10.66 o 6 0 2 6825.79 7021.29 93.68 o 7 0 2 1210.01 1237.04 19.17 o 8 0 2 4622.28 4801.16 62.69 o 9 0 2 1350.28 1450.74 24.04 o 10 0 2 8157.54 8476.91 108.39 o 11 0 2 1640.07 1633.85 26.38 o 12 0 2 12771.82 14650.41 185.28 o 13 0 2 329.15 333.69 13.23 o 14 0 2 709.13 751.30 20.18 o 15 0 2 61.37 39.33 13.00 o 16 0 2 2176.59 2498.37 69.88 o 17 0 2 666.50 584.46 26.52 o 18 0 2 836.13 923.28 42.40 o 19 0 2 92.50 91.49 22.94 o 20 0 2 921.22 965.32 35.39 o 21 0 2 4.21 47.29 25.40 o 22 0 2 325.32 318.50 29.05 o 23 0 2 60.80 96.85 26.95 o 24 0 2 705.43 769.71 36.78 o 25 0 2 76.87 14.11 41.57 o 1 1 2 20136.55 18955.17 182.15 o 2 1 2 375.12 380.36 4.35 o 3 1 2 1056.77 1342.78 11.46 o 4 1 2 10014.32 10546.97 89.35 o 5 1 2 19560.24 19697.01 173.32 o 6 1 2 189.07 172.26 4.54 o 7 1 2 15891.91 16418.25 148.45 o 8 1 2 735.25 788.31 10.35 o 9 1 2 2150.93 2047.27 20.43 o 10 1 2 29.01 35.70 5.34 o 11 1 2 1435.14 1574.62 18.40 o 12 1 2 841.53 895.59 13.81 o 13 1 2 343.84 425.20 11.89 o 14 1 2 77.12 99.20 7.88 o 15 1 2 107.30 144.79 10.30 o 16 1 2 28.53 28.58 10.46 o 17 1 2 121.54 138.85 12.72 o 18 1 2 87.65 77.11 12.22 o 19 1 2 294.55 275.05 17.46 o 20 1 2 32.68 39.54 16.79 o 21 1 2 1.51 13.99 17.89 o 22 1 2 334.50 345.65 23.42 o 23 1 2 43.89 80.19 18.93 o 24 1 2 5.33 29.11 21.52 o 25 1 2 29.44 58.01 24.74 o 0 2 2 736.69 900.28 15.41 o 1 2 2 9959.41 10372.71 110.34 o 2 2 2 7975.25 8505.32 77.71 o 3 2 2 8070.60 8258.25 67.42 o 4 2 2 29713.80 30935.72 248.99 o 5 2 2 3461.08 3864.89 32.98 o 6 2 2 6990.56 7838.43 67.13 o 7 2 2 291.86 359.48 6.65 o 8 2 2 2285.09 2471.58 24.40 o 9 2 2 530.18 421.95 8.37 o 10 2 2 2404.19 2575.78 27.73 o 11 2 2 1651.48 1657.23 20.42 o 12 2 2 2793.27 2865.77 35.52 o 13 2 2 111.99 81.07 7.88 o 14 2 2 1332.69 1396.46 21.77 o 15 2 2 113.88 91.04 10.47 o 16 2 2 294.72 329.84 16.37 o 17 2 2 418.40 352.76 15.89 o 18 2 2 2111.15 2046.97 37.76 o 19 2 2 488.97 521.07 17.72 o 20 2 2 53.61 74.76 17.22 o 21 2 2 483.05 422.76 20.82 o 22 2 2 1.39 25.60 19.19 o 23 2 2 11.90 -0.92 24.12 o 24 2 2 67.65 65.04 22.75 o 25 2 2 10.06 52.35 32.87 o 1 3 2 18121.02 17451.98 168.44 o 2 3 2 527.14 550.32 7.26 o 3 3 2 48088.69 48567.16 430.25 o 4 3 2 106.95 108.74 3.47 o 5 3 2 8237.75 7897.97 67.79 o 6 3 2 3535.35 3845.77 35.82 o 7 3 2 24656.16 24972.11 227.00 o 8 3 2 304.51 299.51 8.09 o 9 3 2 16337.76 16513.33 159.77 o 10 3 2 451.83 445.22 14.43 o 11 3 2 4022.29 3893.01 42.87 o 12 3 2 59.87 81.00 7.98 o 13 3 2 1663.44 1661.21 23.79 o 14 3 2 52.30 42.35 8.72 o 15 3 2 2585.97 2762.39 45.00 o 16 3 2 364.82 350.82 11.72 o 17 3 2 8.95 -5.44 10.41 o 18 3 2 163.15 173.56 12.23 o 19 3 2 492.52 503.24 18.13 o 20 3 2 263.16 221.82 18.85 o 21 3 2 23.88 0.96 18.46 o 22 3 2 17.24 24.25 20.99 o 23 3 2 11.25 11.75 26.39 o 24 3 2 31.10 -12.63 39.99 o 0 4 2 18617.47 17208.67 241.75 o 1 4 2 17.09 5.59 4.11 o 2 4 2 5036.24 4475.73 45.99 o 3 4 2 1571.12 1748.00 17.78 o 4 4 2 295.96 183.35 4.69 o 5 4 2 950.99 1125.39 12.87 o 6 4 2 1810.29 1515.68 16.43 o 7 4 2 1306.98 1318.89 15.22 o 8 4 2 2999.24 2803.33 29.16 o 9 4 2 17.98 4.27 6.11 o 10 4 2 63.94 91.50 7.14 o 11 4 2 206.43 283.74 10.11 o 12 4 2 240.40 285.18 9.95 o 13 4 2 103.32 130.90 9.69 o 14 4 2 219.22 262.62 11.90 o 15 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12 4 13.46 25.36 23.42 o 2 12 4 79.31 113.40 24.37 o 3 12 4 81.92 82.69 30.85 o 4 12 4 24.44 34.63 25.07 o 5 12 4 41.06 28.40 25.01 o 1 1 5 1726.76 1774.19 19.93 o 2 1 5 659.66 665.32 9.18 o 3 1 5 2306.12 2482.57 26.59 o 4 1 5 4.75 8.00 4.40 o 5 1 5 1874.88 2095.32 21.02 o 6 1 5 1870.73 1827.47 18.91 o 7 1 5 4120.60 4466.37 43.17 o 8 1 5 90.67 95.82 6.18 o 9 1 5 2315.84 2516.62 26.67 o 10 1 5 1540.55 1527.08 18.52 o 11 1 5 269.44 307.38 9.10 o 12 1 5 492.22 521.10 13.06 o 13 1 5 268.76 297.77 9.94 o 14 1 5 4512.41 4614.72 50.04 o 15 1 5 426.68 477.60 14.94 o 16 1 5 377.36 423.92 14.99 o 17 1 5 175.42 154.97 14.34 o 18 1 5 391.45 428.39 20.42 o 19 1 5 8.23 -10.59 17.93 o 20 1 5 77.95 58.10 20.99 o 21 1 5 58.46 48.03 33.90 o 22 1 5 306.39 418.50 69.04 o 23 1 5 1.94 -74.59 58.23 o 0 2 5 2292.45 2432.06 43.92 o 1 2 5 1.19 -4.52 3.48 o 2 2 5 4217.03 4342.99 52.34 o 3 2 5 1558.50 1439.13 20.38 o 4 2 5 121.16 84.25 5.95 o 5 2 5 126.43 109.15 6.23 o 6 2 5 780.28 737.04 12.51 o 7 2 5 1174.63 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5 152.11 136.27 33.98 o 22 3 5 6.39 -57.54 38.36 o 0 4 5 3153.20 3131.46 58.88 o 1 4 5 226.79 240.08 9.54 o 2 4 5 1510.37 1345.85 21.33 o 3 4 5 693.42 745.18 15.86 o 4 4 5 5399.96 5253.01 61.12 o 5 4 5 4.60 -0.29 7.64 o 6 4 5 41.71 23.96 8.03 o 7 4 5 1248.71 1350.05 20.38 o 8 4 5 3014.16 3103.73 39.13 o 9 4 5 110.54 159.24 12.18 o 10 4 5 675.43 691.88 14.88 o 11 4 5 679.28 748.31 16.42 o 12 4 5 212.68 230.42 11.82 o 13 4 5 70.43 111.16 9.75 o 14 4 5 44.95 53.17 9.78 o 15 4 5 137.88 178.93 13.71 o 16 4 5 284.53 354.70 16.03 o 17 4 5 505.87 521.82 20.95 o 18 4 5 0.69 21.72 20.20 o 19 4 5 1031.64 952.76 29.90 o 20 4 5 53.85 17.26 28.34 o 21 4 5 4.00 -49.30 32.87 o 1 5 5 9.82 5.19 10.71 o 2 5 5 135.45 132.08 11.26 o 3 5 5 999.28 919.31 21.47 o 4 5 5 1052.85 961.65 18.36 o 5 5 5 348.59 239.30 11.57 o 6 5 5 1360.92 1358.73 25.46 o 7 5 5 15.79 26.08 10.66 o 8 5 5 664.33 671.36 20.90 o 9 5 5 47.27 -0.62 12.87 o 10 5 5 699.91 686.62 18.36 o 11 5 5 21.73 -8.27 11.10 o 12 5 5 1547.44 1524.63 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6 3768.04 3576.39 46.70 o 7 0 6 1085.28 1286.51 21.83 o 8 0 6 81.00 50.56 9.36 o 9 0 6 784.59 839.13 18.43 o 10 0 6 3749.19 3544.59 47.84 o 11 0 6 233.87 259.81 12.61 o 12 0 6 2968.16 2952.00 42.34 o 13 0 6 3205.34 3489.09 54.03 o 14 0 6 105.63 121.20 17.44 o 15 0 6 31.04 51.07 19.10 o 16 0 6 116.31 97.30 22.68 o 17 0 6 37.52 51.55 25.89 o 18 0 6 203.07 230.69 37.81 o 19 0 6 326.87 294.96 40.23 o 20 0 6 42.31 92.91 41.71 o 21 0 6 102.80 25.33 66.83 o 1 1 6 2140.02 1967.06 27.54 o 2 1 6 24.15 24.47 5.65 o 3 1 6 1090.93 914.73 12.84 o 4 1 6 17.11 16.36 6.38 o 5 1 6 323.77 266.01 7.96 o 6 1 6 688.88 789.67 11.70 o 7 1 6 1226.64 1205.63 15.21 o 8 1 6 2.23 1.90 5.96 o 9 1 6 268.90 277.47 8.27 o 10 1 6 777.66 854.32 13.31 o 11 1 6 1033.31 1096.58 16.60 o 12 1 6 355.94 326.06 10.60 o 13 1 6 171.35 167.98 10.47 o 14 1 6 19.63 35.36 12.09 o 15 1 6 215.75 239.90 14.88 o 16 1 6 185.36 206.52 18.34 o 17 1 6 35.81 22.44 17.07 o 18 1 6 296.61 317.60 25.09 o 19 1 6 21.96 5.36 25.40 o 20 1 6 0.47 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25.81 o 15 5 7 10.46 43.28 25.09 o 16 5 7 182.62 183.78 18.70 o 17 5 7 33.94 62.41 26.10 o 0 6 7 241.56 254.98 28.34 o 1 6 7 24.66 18.07 18.12 o 2 6 7 582.81 576.78 22.61 o 3 6 7 50.64 42.89 18.40 o 4 6 7 491.31 475.69 22.73 o 5 6 7 5.21 -15.92 17.89 o 6 6 7 595.94 570.08 23.62 o 7 6 7 212.50 168.33 17.57 o 8 6 7 164.29 198.34 18.33 o 9 6 7 13.52 3.71 21.08 o 10 6 7 355.37 408.04 23.88 o 11 6 7 342.92 319.21 24.06 o 12 6 7 184.24 219.49 23.50 o 13 6 7 394.21 404.75 29.15 o 14 6 7 126.00 215.65 28.63 o 15 6 7 65.96 96.22 29.66 o 16 6 7 45.25 126.29 28.21 o 1 7 7 1839.88 1629.95 40.52 o 2 7 7 135.03 100.45 20.80 o 3 7 7 49.03 16.14 15.54 o 4 7 7 444.89 473.54 20.90 o 5 7 7 140.31 127.04 17.88 o 6 7 7 20.23 19.98 17.67 o 7 7 7 493.45 474.06 22.87 o 8 7 7 214.40 160.40 19.89 o 9 7 7 340.86 333.16 22.84 o 10 7 7 143.48 201.68 22.08 o 11 7 7 42.08 36.96 32.64 o 12 7 7 1.63 2.72 23.14 o 13 7 7 180.92 213.48 25.49 o 14 7 7 9.55 52.83 29.11 o 0 8 7 7.28 -8.41 29.09 o 1 8 7 7.66 2.05 20.93 o 2 8 7 0.90 15.12 21.93 o 3 8 7 10.14 19.07 21.65 o 4 8 7 93.62 43.78 21.66 o 5 8 7 1.23 6.03 21.09 o 6 8 7 1.78 1.98 22.58 o 7 8 7 150.53 199.83 23.24 o 8 8 7 56.38 24.50 19.99 o 9 8 7 34.53 72.79 21.49 o 10 8 7 81.66 132.97 23.32 o 11 8 7 209.32 250.71 24.58 o 12 8 7 69.18 87.79 27.09 o 1 9 7 109.25 83.70 24.44 o 2 9 7 31.33 19.43 25.40 o 3 9 7 79.51 79.63 24.75 o 4 9 7 146.50 154.37 24.52 o 5 9 7 165.56 167.44 24.55 o 6 9 7 24.73 29.59 24.30 o 7 9 7 178.45 170.21 26.52 o 8 9 7 130.49 139.24 27.22 o 9 9 7 287.95 311.41 27.96 o 0 10 7 382.34 429.68 39.35 o 1 10 7 82.40 68.37 26.86 o 2 10 7 65.35 38.20 25.56 o 3 10 7 16.28 56.59 33.26 o 4 10 7 135.96 126.23 35.08 o 0 0 8 2611.11 2442.06 123.45 o 1 0 8 646.98 647.42 21.11 o 2 0 8 101.72 57.96 20.17 o 3 0 8 13.69 12.36 16.58 o 4 0 8 277.59 234.67 16.87 o 5 0 8 458.60 549.92 22.58 o 6 0 8 627.59 554.79 21.67 o 7 0 8 102.29 97.13 18.64 o 8 0 8 1349.70 1217.05 43.00 o 9 0 8 438.96 583.45 26.33 o 10 0 8 369.99 313.36 23.62 o 11 0 8 664.71 826.51 52.12 o 12 0 8 4.66 2.87 26.90 o 13 0 8 3.90 69.59 28.65 o 14 0 8 156.08 145.98 30.19 o 15 0 8 706.13 719.55 38.01 o 16 0 8 25.44 43.90 30.66 o 17 0 8 47.28 68.75 39.37 o 18 0 8 0.83 5.39 41.12 o 1 1 8 297.37 258.67 11.10 o 2 1 8 36.66 39.88 9.80 o 3 1 8 154.65 140.39 9.30 o 4 1 8 0.44 6.40 9.24 o 5 1 8 650.35 584.58 15.36 o 6 1 8 96.25 125.59 10.73 o 7 1 8 234.03 245.00 10.46 o 8 1 8 324.03 364.05 14.56 o 9 1 8 229.77 221.58 12.51 o 10 1 8 33.28 9.52 12.27 o 11 1 8 638.65 648.43 21.01 o 12 1 8 2.42 -17.70 16.46 o 13 1 8 32.39 24.60 20.37 o 14 1 8 78.73 98.34 20.87 o 15 1 8 45.55 21.20 21.11 o 16 1 8 3.82 5.74 21.61 o 17 1 8 39.50 16.44 26.80 o 0 2 8 323.74 283.25 18.85 o 1 2 8 91.88 102.60 9.78 o 2 2 8 106.83 114.93 9.89 o 3 2 8 67.53 57.38 9.96 o 4 2 8 104.84 83.39 12.31 o 5 2 8 348.10 349.55 16.66 o 6 2 8 276.94 232.26 16.34 o 7 2 8 170.99 179.83 18.60 o 8 2 8 395.51 358.73 18.25 o 9 2 8 3.62 -17.42 19.22 o 10 2 8 248.37 278.76 25.70 o 11 2 8 4.02 -9.61 16.17 o 12 2 8 140.16 95.59 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4 8 5.74 33.27 30.37 o 15 4 8 2.39 12.12 30.84 o 16 4 8 2.11 3.72 31.37 o 1 5 8 24.53 47.79 21.50 o 2 5 8 25.25 20.37 20.07 o 3 5 8 93.53 103.09 20.50 o 4 5 8 0.33 -10.85 19.75 o 5 5 8 108.49 148.98 21.21 o 6 5 8 10.15 4.39 20.57 o 7 5 8 89.82 97.28 21.16 o 8 5 8 47.60 35.70 23.48 o 9 5 8 184.27 198.82 25.23 o 10 5 8 293.40 250.93 28.07 o 11 5 8 137.46 72.88 27.50 o 12 5 8 255.81 237.36 31.88 o 13 5 8 5.19 1.28 26.05 o 14 5 8 27.89 49.48 28.50 o 15 5 8 58.86 42.03 30.51 o 0 6 8 1215.46 1330.09 63.68 o 1 6 8 398.51 373.07 25.05 o 2 6 8 54.44 82.35 22.63 o 3 6 8 2.54 -24.12 22.75 o 4 6 8 872.13 926.39 37.54 o 5 6 8 451.46 460.68 28.72 o 6 6 8 5.92 6.36 24.11 o 7 6 8 246.97 271.55 27.95 o 8 6 8 246.61 253.05 28.41 o 9 6 8 21.76 24.40 28.49 o 10 6 8 214.29 355.26 32.22 o 11 6 8 435.85 456.72 31.36 o 12 6 8 509.88 561.61 35.60 o 13 6 8 136.58 234.19 32.62 o 1 7 8 262.74 313.57 26.31 o 2 7 8 10.11 2.83 23.92 o 3 7 8 102.12 115.28 28.01 o 4 7 8 39.08 28.62 26.67 o 5 7 8 287.36 343.69 29.79 o 6 7 8 1.62 -7.39 27.86 o 7 7 8 360.31 368.19 31.51 o 8 7 8 262.50 300.28 35.18 o 9 7 8 16.44 86.02 30.59 o 10 7 8 26.98 0.15 35.78 o 11 7 8 141.97 175.24 35.80 o 0 8 8 29.10 -7.39 33.93 o 1 8 8 68.05 48.86 23.16 o 2 8 8 14.44 45.11 29.74 o 3 8 8 24.22 25.23 25.66 o 4 8 8 33.19 21.55 32.86 o 5 8 8 0.87 -31.01 28.37 o 6 8 8 14.57 21.35 28.39 o 7 8 8 46.19 40.90 30.46 o 8 8 8 1.17 8.63 31.43 o 1 9 8 26.29 61.98 36.00 o 2 9 8 0.42 -13.83 26.26 o 1 1 9 866.47 953.04 52.41 o 2 1 9 4.40 7.80 15.96 o 3 1 9 278.24 306.42 22.83 o 4 1 9 5.43 0.67 16.73 o 5 1 9 150.67 173.58 18.00 o 6 1 9 34.57 -6.87 19.43 o 7 1 9 380.44 392.36 27.87 o 8 1 9 12.09 -8.09 24.95 o 9 1 9 30.34 24.75 23.45 o 10 1 9 5.65 -0.26 17.73 o 11 1 9 263.93 233.02 20.85 o 12 1 9 68.70 66.91 19.55 o 13 1 9 16.60 -8.75 20.42 o 14 1 9 192.27 229.58 23.32 o 15 1 9 50.39 16.44 23.26 o 0 2 9 635.13 712.60 69.86 o 1 2 9 7.75 1.99 22.93 o 2 2 9 235.14 253.88 25.22 o 3 2 9 54.37 56.81 24.29 o 4 2 9 140.27 194.22 25.68 o 5 2 9 78.54 72.97 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