#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:36:57 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181262 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/40/2234038.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2234038_Fobs loop_ _publ_author_name 'Hu, Xiao-Lei' 'Wang, Zhong-Xia' 'Wang, Fang-Ming' 'Han, Guang-Fan' _publ_section_title ; 2-Amino-4-(2-chlorophenyl)-7,7-dimethyl-5-oxo-5,6,7,8-tetrahydro-4H-chromene-3-carbonitrile hemihydrate ; _journal_coeditor_code XU5439 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o823 _journal_volume 68 _journal_year 2012 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 111.240 _cell_angle_gamma 90.000 _cell_length_a 31.4310 _cell_length_b 9.3230 _cell_length_c 25.0790 _exptl_crystal_F_000 2832.00 _reflns_d_resolution_high 0.8298 _cod_data_source_file xu5439Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 358.81 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 6 0 0 4528.03 3823.26 54.88 o 8 0 0 13520.89 15508.10 268.17 o 10 0 0 1386.25 1940.32 249.24 o 12 0 0 2135.81 2485.25 79.11 o 14 0 0 75511.23 70793.13 259.10 o 16 0 0 17712.86 19146.32 505.35 o 18 0 0 2057.79 2333.75 190.43 o 20 0 0 1275.03 1225.53 162.35 o 22 0 0 2835.44 2863.26 222.38 o 24 0 0 537.61 681.26 179.11 o 26 0 0 756.35 1021.65 243.94 o 28 0 0 392.24 370.44 82.32 o 30 0 0 150.48 242.38 420.74 o 32 0 0 3713.45 3507.70 338.42 o 34 0 0 660.29 553.37 18.29 o 7 1 0 18726.69 17228.25 564.83 o 11 1 0 240.79 255.41 53.67 o 13 1 0 665.58 535.71 104.48 o 15 1 0 1081.15 857.33 90.48 o 17 1 0 250.26 171.50 102.31 o 19 1 0 2546.27 2024.44 123.22 o 21 1 0 0.65 0.00 64.68 o 23 1 0 156.81 56.72 28.51 o 25 1 0 107.03 96.37 112.12 o 27 1 0 619.45 826.09 245.30 o 29 1 0 1215.76 1346.44 78.49 o 31 1 0 1622.95 1737.74 64.03 o 33 1 0 214.13 288.51 88.30 o 35 1 0 24.02 19.30 235.80 o 0 2 0 6535.82 6997.11 274.40 o 2 2 0 468.18 620.85 37.95 o 4 2 0 261.82 265.75 44.73 o 8 2 0 28246.59 26803.97 73.17 o 10 2 0 88.91 76.09 84.49 o 12 2 0 2219.80 2166.26 86.24 o 14 2 0 155.34 53.29 108.71 o 16 2 0 2600.74 2701.30 158.20 o 18 2 0 697.77 1132.77 141.92 o 20 2 0 86.20 0.00 156.03 o 22 2 0 1019.01 924.20 234.22 o 24 2 0 7.65 0.00 22.54 o 26 2 0 237.96 201.71 63.10 o 28 2 0 2783.42 2907.01 134.73 o 30 2 0 1256.78 1265.19 103.86 o 32 2 0 1055.39 1752.46 263.68 o 34 2 0 104.32 342.00 207.78 o 1 3 0 633.51 1091.10 246.77 o 3 3 0 1706.19 1493.00 83.03 o 5 3 0 13389.35 14076.90 549.75 o 7 3 0 560.53 888.78 189.66 o 9 3 0 6248.44 6457.52 253.82 o 11 3 0 580.72 426.92 117.30 o 13 3 0 104.09 95.61 73.39 o 15 3 0 234.46 173.12 53.00 o 17 3 0 1178.38 982.50 89.33 o 19 3 0 2618.72 2991.73 142.35 o 21 3 0 2738.29 2975.30 147.75 o 23 3 0 2725.23 3096.76 258.88 o 25 3 0 56.73 69.51 116.70 o 27 3 0 3628.98 3476.68 92.87 o 29 3 0 335.13 401.35 64.93 o 31 3 0 215.52 179.94 36.59 o 33 3 0 671.23 648.64 171.18 o 0 4 0 46.96 265.11 306.75 o 2 4 0 2398.78 2659.64 149.56 o 4 4 0 9384.99 8148.44 235.98 o 6 4 0 197.16 254.97 46.23 o 8 4 0 4302.06 4546.39 133.84 o 10 4 0 619.39 682.78 101.78 o 12 4 0 101.77 37.05 15.05 o 14 4 0 591.55 706.02 68.46 o 16 4 0 603.51 623.98 39.02 o 18 4 0 397.05 424.26 52.75 o 20 4 0 665.85 612.00 71.78 o 22 4 0 1070.84 1130.88 129.21 o 24 4 0 881.98 868.04 48.09 o 26 4 0 352.76 485.83 182.63 o 28 4 0 67.64 36.29 140.03 o 30 4 0 446.11 381.55 240.47 o 32 4 0 0.02 4.57 255.47 o 1 5 0 1676.47 2054.39 202.36 o 3 5 0 596.16 528.20 67.33 o 5 5 0 133.19 97.07 111.70 o 7 5 0 1311.61 1455.23 37.13 o 9 5 0 3547.26 3528.47 318.11 o 11 5 0 347.60 347.65 37.69 o 13 5 0 393.43 421.70 84.87 o 15 5 0 829.71 1713.01 184.07 o 17 5 0 481.17 404.15 90.14 o 19 5 0 247.96 187.63 34.46 o 21 5 0 228.20 389.73 125.57 o 23 5 0 16.85 1.11 41.22 o 25 5 0 1562.92 1706.40 322.17 o 27 5 0 416.64 415.90 144.53 o 29 5 0 531.18 556.01 84.47 o 31 5 0 1.05 36.59 420.74 o 0 6 0 1286.77 1342.59 246.96 o 2 6 0 52.58 51.84 89.33 o 4 6 0 964.07 731.89 71.90 o 6 6 0 314.47 457.79 186.01 o 8 6 0 1168.20 1086.11 86.48 o 10 6 0 6251.75 5769.45 83.10 o 12 6 0 0.68 0.00 72.65 o 14 6 0 3326.29 3115.18 184.85 o 16 6 0 307.15 329.54 92.64 o 18 6 0 379.34 327.91 53.14 o 20 6 0 341.03 309.66 41.27 o 22 6 0 96.37 146.07 202.47 o 24 6 0 4.21 0.00 25.22 o 26 6 0 238.53 160.06 86.89 o 28 6 0 125.87 210.37 146.34 o 1 7 0 1590.28 2129.87 141.47 o 3 7 0 161.03 198.48 94.43 o 5 7 0 30.86 52.11 86.61 o 7 7 0 26.11 0.00 80.33 o 9 7 0 5162.20 4823.80 97.98 o 11 7 0 1754.85 1984.56 139.13 o 13 7 0 119.41 73.25 123.94 o 15 7 0 219.74 274.51 49.56 o 17 7 0 931.18 773.26 98.00 o 19 7 0 0.09 0.00 25.80 o 21 7 0 0.04 0.00 45.02 o 23 7 0 389.47 553.37 384.16 o 25 7 0 431.38 384.16 375.01 o 27 7 0 48.68 96.04 137.20 o 0 8 0 95.81 133.22 53.30 o 2 8 0 2121.77 1994.34 152.57 o 4 8 0 2339.64 2181.37 266.27 o 6 8 0 427.11 466.50 91.62 o 8 8 0 2727.53 3003.57 289.14 o 10 8 0 11.04 0.00 22.79 o 12 8 0 545.45 588.36 102.59 o 14 8 0 1600.08 1816.54 203.00 o 16 8 0 1349.39 1452.76 353.93 o 18 8 0 240.11 139.42 53.28 o 20 8 0 22.23 9.15 320.13 o 22 8 0 96.10 96.04 333.85 o 24 8 0 188.06 365.86 393.30 o 1 9 0 1436.97 1271.31 108.81 o 3 9 0 1258.78 1244.90 29.33 o 5 9 0 217.57 149.06 75.53 o 7 9 0 1230.73 1054.81 187.94 o 9 9 0 21.26 19.51 217.53 o 11 9 0 132.13 130.81 87.11 o 13 9 0 1398.47 1694.22 228.66 o 15 9 0 243.11 411.59 265.25 o 17 9 0 179.76 375.01 260.68 o 19 9 0 70.99 45.73 146.34 o 21 9 0 178.98 320.13 411.59 o 2 10 0 671.81 796.64 181.44 o 4 10 0 211.43 146.34 283.54 o 6 10 0 0.22 0.00 32.01 o 8 10 0 463.64 393.46 75.46 o 10 10 0 340.71 205.91 80.03 o 12 10 0 13.28 0.00 9.15 o 14 10 0 254.92 379.58 237.81 o 16 10 0 7.44 0.00 45.73 o 1 11 0 27.49 0.00 51.18 o 3 11 0 74.34 0.00 184.00 o 5 11 0 74.04 68.60 109.81 o 7 11 0 2.21 0.00 13.72 o -35 1 1 162.13 366.89 174.16 o -33 1 1 30.53 0.00 69.94 o -31 1 1 68.18 74.47 260.09 o -29 1 1 1342.35 1834.84 155.74 o -27 1 1 273.11 282.03 111.33 o -25 1 1 157.68 257.10 105.95 o -23 1 1 1157.30 1230.89 54.10 o -21 1 1 6533.65 6884.67 201.94 o -19 1 1 1394.35 1206.47 57.68 o -17 1 1 2441.26 2574.22 89.93 o -15 1 1 3849.00 3919.80 211.09 o -13 1 1 2035.02 1734.46 265.68 o -11 1 1 9832.27 9845.51 124.69 o -9 1 1 64509.03 62424.72 862.23 o -7 1 1 2495.44 2247.56 60.17 o -5 1 1 34506.29 34903.46 585.38 o 3 1 1 59.91 20.53 68.66 o 5 1 1 177.78 112.28 224.21 o 7 1 1 3625.93 3933.89 163.45 o 9 1 1 5213.95 5588.67 194.66 o 11 1 1 20931.73 19299.32 790.77 o 13 1 1 6890.32 6406.66 94.26 o 15 1 1 14982.12 14351.51 371.75 o 17 1 1 3756.29 4020.09 143.19 o 19 1 1 533.46 515.27 77.20 o 21 1 1 430.66 433.61 33.91 o 23 1 1 4900.23 4699.55 87.80 o 25 1 1 582.58 528.14 100.80 o 27 1 1 5.03 0.00 136.07 o 29 1 1 879.28 759.55 50.31 o 31 1 1 1636.15 1781.32 81.28 o 33 1 1 238.17 183.99 68.60 o -34 2 1 12.05 6.72 130.22 o -32 2 1 556.13 371.65 82.21 o -30 2 1 931.86 1750.59 271.87 o -28 2 1 347.73 310.11 111.96 o -26 2 1 3686.17 3602.42 63.76 o -24 2 1 283.06 286.01 52.81 o -22 2 1 1749.76 1850.91 40.27 o -20 2 1 136.86 344.08 98.45 o -18 2 1 2095.86 2325.52 114.80 o -16 2 1 165.53 65.78 45.57 o -14 2 1 5909.43 6186.91 253.03 o -12 2 1 3585.87 3668.30 203.97 o -10 2 1 3334.17 3731.41 141.71 o -6 2 1 1984.01 1708.84 110.69 o -4 2 1 5474.53 5243.69 139.82 o -2 2 1 46181.30 44591.29 215.51 o 0 2 1 44593.19 41982.67 50.31 o 2 2 1 12067.06 12183.01 640.24 o 4 2 1 4626.90 4599.19 224.87 o 6 2 1 12297.79 11895.09 164.64 o 8 2 1 1952.92 2083.80 81.37 o 10 2 1 712.23 601.91 137.31 o 12 2 1 935.31 1214.92 108.05 o 14 2 1 51.36 107.98 80.86 o 16 2 1 105.49 256.52 113.33 o 18 2 1 276.03 171.07 39.32 o 20 2 1 1163.88 1453.45 83.83 o 22 2 1 421.45 515.71 93.98 o 24 2 1 411.38 576.03 158.22 o 26 2 1 216.74 130.28 65.23 o 28 2 1 165.73 310.82 105.56 o 30 2 1 24.84 0.00 93.10 o 32 2 1 2.38 0.00 67.64 o 34 2 1 32.55 12.28 174.25 o -33 3 1 261.35 361.98 181.80 o -31 3 1 907.19 978.56 308.51 o -29 3 1 32.38 0.00 49.55 o -27 3 1 1518.64 1703.94 122.44 o -25 3 1 19.47 0.00 109.81 o -23 3 1 159.27 260.12 64.56 o -21 3 1 158.13 243.49 152.70 o -19 3 1 47.66 0.00 27.09 o -17 3 1 4131.57 3956.42 193.91 o -15 3 1 5148.22 4513.37 112.35 o -13 3 1 28095.83 26387.05 603.54 o -11 3 1 12916.20 11888.83 427.60 o -9 3 1 14748.60 14081.12 173.78 o -7 3 1 10152.90 10838.97 321.38 o -5 3 1 1301.58 1540.30 260.33 o -3 3 1 74.56 0.00 22.27 o -1 3 1 24532.40 23462.23 257.72 o 1 3 1 37402.77 34825.49 128.05 o 3 3 1 55.10 0.00 33.66 o 5 3 1 15.47 0.00 64.38 o 7 3 1 61.83 9.34 48.16 o 9 3 1 10977.62 11436.67 301.00 o 11 3 1 256.88 187.37 55.14 o 13 3 1 1734.60 2451.34 150.82 o 15 3 1 214.74 99.07 121.38 o 17 3 1 2355.08 2453.03 171.85 o 19 3 1 507.58 554.87 83.37 o 21 3 1 1691.74 1916.58 123.99 o 23 3 1 6305.49 5746.38 184.85 o 25 3 1 2503.35 2986.72 171.16 o 27 3 1 587.13 668.76 140.16 o 29 3 1 178.00 255.86 70.91 o 31 3 1 679.31 689.13 108.81 o 33 3 1 33.51 0.00 29.73 o -32 4 1 71.69 0.00 215.35 o -30 4 1 847.60 731.90 96.04 o -28 4 1 193.19 265.05 125.88 o -26 4 1 1863.37 1746.40 178.00 o -24 4 1 185.89 152.21 29.41 o -22 4 1 334.22 239.36 87.92 o -20 4 1 1820.34 1817.95 212.87 o -18 4 1 538.29 570.32 74.32 o -16 4 1 146.89 197.40 52.59 o -14 4 1 550.42 550.68 86.59 o -12 4 1 268.32 206.76 28.88 o -10 4 1 5042.20 4611.49 74.78 o -8 4 1 5006.96 4726.40 124.12 o -6 4 1 1645.06 1180.43 242.76 o -4 4 1 3321.88 3507.70 164.64 o 0 4 1 12014.20 13242.33 335.87 o 2 4 1 427.40 478.59 55.69 o 4 4 1 32.55 183.54 140.73 o 6 4 1 474.76 852.00 84.48 o 8 4 1 2.10 173.69 112.68 o 10 4 1 6655.11 6152.53 120.97 o 12 4 1 5571.83 5663.05 132.45 o 14 4 1 1948.64 1737.63 59.29 o 16 4 1 415.28 383.24 50.49 o 18 4 1 1594.59 1972.18 96.06 o 20 4 1 2411.51 2390.42 283.17 o 22 4 1 217.58 359.65 128.55 o 24 4 1 11.83 0.00 55.83 o 26 4 1 143.27 402.23 267.47 o 28 4 1 1783.53 1654.65 258.91 o 30 4 1 399.61 538.15 225.89 o 32 4 1 707.28 630.71 62.76 o -31 5 1 105.34 114.33 310.98 o -29 5 1 13.30 0.00 170.36 o -27 5 1 2215.09 2045.62 182.93 o -25 5 1 2616.22 2446.20 395.59 o -23 5 1 136.32 129.58 38.45 o -21 5 1 494.28 471.22 84.95 o -19 5 1 1567.55 2142.07 184.97 o -17 5 1 3866.18 3355.65 126.22 o -15 5 1 167.45 296.59 64.26 o -13 5 1 432.26 260.55 44.26 o -11 5 1 179.94 207.90 44.54 o -9 5 1 12283.09 12849.28 376.72 o -7 5 1 14687.57 14399.57 306.77 o -5 5 1 2731.11 2483.12 79.92 o -3 5 1 4116.10 4358.68 242.82 o -1 5 1 6674.82 6698.53 171.33 o 1 5 1 4826.42 4664.60 115.61 o 3 5 1 438.28 647.57 44.53 o 5 5 1 44.90 0.00 70.13 o 7 5 1 3.19 2.09 153.17 o 9 5 1 2731.93 2819.07 202.09 o 11 5 1 1132.18 1120.14 56.86 o 13 5 1 300.41 387.60 60.40 o 15 5 1 875.73 955.47 93.04 o 17 5 1 12784.70 13205.96 809.92 o 19 5 1 3286.19 3262.43 139.73 o 21 5 1 16.58 0.00 148.28 o 23 5 1 135.83 80.75 51.68 o 25 5 1 432.33 606.08 193.00 o 27 5 1 479.33 453.10 164.10 o 29 5 1 419.10 507.28 119.13 o 31 5 1 793.74 841.48 288.12 o -30 6 1 297.48 283.54 137.20 o -28 6 1 1140.44 891.79 370.44 o -26 6 1 145.02 297.26 164.64 o -24 6 1 1470.54 1321.86 233.24 o -22 6 1 1532.68 2023.52 144.17 o -20 6 1 17.38 0.00 107.45 o -18 6 1 7874.24 6998.54 381.25 o -16 6 1 301.39 349.51 53.44 o -14 6 1 88.52 103.92 129.34 o -12 6 1 6850.86 7124.96 136.85 o -10 6 1 1338.50 1766.25 179.55 o -8 6 1 1555.46 1308.08 204.59 o -6 6 1 22.04 0.00 56.62 o -4 6 1 186.67 129.59 99.23 o -2 6 1 296.92 411.46 114.22 o 0 6 1 30.71 224.21 123.38 o 2 6 1 111.43 134.43 38.11 o 4 6 1 5861.62 5494.10 206.81 o 6 6 1 1540.44 1889.14 145.11 o 8 6 1 8885.89 9394.67 450.52 o 10 6 1 3.56 116.15 89.36 o 12 6 1 114.04 130.64 39.33 o 14 6 1 1157.48 1030.03 78.46 o 16 6 1 3403.65 3449.63 89.14 o 18 6 1 3216.40 3779.10 202.56 o 20 6 1 282.50 215.94 46.12 o 22 6 1 988.15 1502.91 162.37 o 24 6 1 836.49 887.68 132.41 o 26 6 1 62.98 86.89 448.18 o 28 6 1 738.55 695.14 91.47 o -27 7 1 591.56 658.55 105.19 o -25 7 1 3.32 0.00 233.24 o -23 7 1 258.74 375.01 274.40 o -21 7 1 1.59 9.15 370.44 o -19 7 1 139.45 103.76 183.74 o -17 7 1 222.60 371.93 105.75 o -15 7 1 5383.16 4781.57 73.79 o -13 7 1 4228.37 4032.10 96.30 o -11 7 1 505.40 1218.96 151.28 o -9 7 1 531.95 593.68 106.02 o -7 7 1 5.23 121.45 101.30 o -5 7 1 567.37 480.34 56.95 o -3 7 1 69.23 42.91 87.57 o -1 7 1 8649.02 8344.32 89.66 o 1 7 1 194.52 111.66 165.08 o 3 7 1 2280.58 2515.07 145.95 o 5 7 1 106.27 288.19 153.35 o 7 7 1 4975.18 5140.80 187.34 o 9 7 1 35.56 0.00 78.39 o 11 7 1 4104.13 4110.21 153.55 o 13 7 1 108.37 166.91 128.47 o 15 7 1 1137.58 1339.73 106.81 o 17 7 1 12.07 0.00 33.99 o 19 7 1 155.83 182.11 64.85 o 21 7 1 2325.54 2398.04 242.84 o 23 7 1 2979.12 3242.45 425.31 o 25 7 1 232.78 375.01 246.96 o 27 7 1 144.23 283.54 146.34 o -24 8 1 1312.92 1536.62 420.74 o -22 8 1 1006.47 1088.44 352.14 o -20 8 1 831.97 987.83 265.25 o -18 8 1 259.71 205.80 32.01 o -16 8 1 19.44 0.41 176.25 o -14 8 1 1051.50 952.50 109.65 o -12 8 1 502.74 470.24 153.26 o -10 8 1 2907.80 2876.59 68.69 o -8 8 1 571.20 739.08 144.46 o -6 8 1 852.80 966.12 73.03 o -4 8 1 828.86 641.27 46.58 o -2 8 1 1159.50 940.05 154.60 o 0 8 1 892.31 879.00 40.13 o 2 8 1 1451.23 1992.73 116.53 o 4 8 1 234.90 254.21 50.72 o 6 8 1 1834.50 1798.47 201.30 o 8 8 1 231.19 473.99 201.51 o 10 8 1 873.03 880.26 97.39 o 12 8 1 29.23 35.58 77.16 o 14 8 1 426.97 587.95 210.27 o 16 8 1 2229.75 2435.75 122.23 o 18 8 1 286.98 188.14 117.01 o 20 8 1 52.35 41.16 269.82 o 22 8 1 1333.37 1211.92 288.12 o 24 8 1 74.70 123.48 100.61 o -21 9 1 809.71 905.51 448.18 o -19 9 1 1.29 0.00 64.03 o -17 9 1 8.67 0.00 132.62 o -15 9 1 732.43 768.31 402.45 o -13 9 1 508.48 542.60 89.33 o -11 9 1 46.02 23.22 135.42 o -9 9 1 1218.18 1109.68 41.85 o -7 9 1 1920.54 2139.48 172.66 o -5 9 1 505.14 445.54 83.69 o -3 9 1 9.26 0.00 16.16 o -1 9 1 599.34 666.83 98.42 o 1 9 1 1164.10 1147.92 95.71 o 3 9 1 2384.32 2545.88 268.74 o 5 9 1 307.78 264.15 104.82 o 7 9 1 1219.67 1063.08 524.46 o 9 9 1 544.42 481.41 21.27 o 11 9 1 33.09 0.00 13.68 o 13 9 1 1113.03 1331.40 176.07 o 15 9 1 80.68 45.73 9.15 o 17 9 1 57.82 41.16 196.65 o 19 9 1 222.43 160.06 22.87 o -16 10 1 31.10 4.57 343.00 o -14 10 1 405.13 416.17 347.57 o -12 10 1 861.66 832.34 416.17 o -10 10 1 190.40 155.49 260.68 o -8 10 1 450.28 298.54 93.86 o -6 10 1 759.00 701.39 290.88 o -4 10 1 485.92 627.02 136.15 o -2 10 1 794.01 725.01 70.89 o 0 10 1 400.73 345.23 48.02 o 2 10 1 74.18 20.22 59.18 o 4 10 1 100.54 4.57 58.93 o 6 10 1 3.54 0.00 67.16 o 8 10 1 389.68 575.73 185.59 o 10 10 1 586.48 658.96 174.18 o 12 10 1 11.40 32.01 411.59 o 14 10 1 161.64 475.62 397.87 o -7 11 1 39.14 50.31 384.16 o -5 11 1 313.99 489.34 343.00 o -3 11 1 56.43 0.00 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110.15 106.31 219.92 o -19 1 28 359.58 461.78 176.59 o -17 1 28 200.20 319.48 208.54 o -15 1 28 412.99 367.20 116.84 o -13 1 28 32.05 138.29 205.50 o -11 1 28 263.75 328.54 132.24 o -9 1 28 170.13 199.03 19.39 o -7 1 28 66.96 0.00 144.06 o -5 1 28 590.81 675.00 130.76 o -3 1 28 42.24 84.18 107.47 o -1 1 28 31.46 131.86 265.85 o -24 2 28 427.57 365.86 36.59 o -22 2 28 494.01 626.10 164.21 o -20 2 28 227.94 343.00 200.50 o -18 2 28 96.96 43.10 58.10 o -16 2 28 411.02 392.75 39.19 o -14 2 28 410.39 370.30 76.37 o -12 2 28 52.39 115.21 173.49 o -10 2 28 331.61 248.64 22.42 o -8 2 28 592.49 526.12 142.98 o -6 2 28 68.92 207.76 227.52 o -4 2 28 248.07 440.35 186.48 o -2 2 28 83.80 71.65 77.72 o -21 3 28 17.89 36.59 361.29 o -19 3 28 545.67 683.53 171.57 o -17 3 28 349.01 691.43 287.61 o -15 3 28 60.83 88.19 198.72 o -13 3 28 152.47 324.01 169.93 o -11 3 28 405.25 349.09 162.05 o -9 3 28 224.04 148.22 109.76 o -7 3 28 333.40 514.75 271.41 o -5 3 28 187.23 317.21 130.44 o -16 4 28 63.59 4.57 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