#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:36:57 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181262 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/40/2234047.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2234047_Fobs loop_ _publ_author_name 'Zhao, Qun' _publ_section_title ; 1-[(4-Bromophenyl)(morpholin-4-yl)methyl]naphthalen-2-ol ; _journal_coeditor_code XU5461 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o812 _journal_volume 68 _journal_year 2012 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 82.320 _cell_angle_beta 89.430 _cell_angle_gamma 88.670 _cell_length_a 10.5140 _cell_length_b 10.7000 _cell_length_c 34.0020 _exptl_crystal_F_000 1631.76 _reflns_d_resolution_high 0.8410 _cod_data_source_file xu5461Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 1 P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 347.83 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 6157.61 6740.70 159.08 o 3 0 0 5216.89 6495.12 435.38 o 4 0 0 54.38 53.97 22.16 o 5 0 0 2607.72 2723.62 126.60 o 6 0 0 1348.85 1647.08 171.77 o 7 0 0 582.44 576.07 64.18 o 8 0 0 20.06 83.30 108.86 o 9 0 0 859.78 899.96 112.25 o 10 0 0 160.46 293.06 102.25 o 11 0 0 176.32 200.62 211.89 o 12 0 0 206.68 97.20 235.61 o -12 1 0 30.60 -15.16 155.13 o -11 1 0 8.82 -111.33 113.16 o -10 1 0 31.14 197.51 225.89 o -9 1 0 2658.70 2363.10 207.39 o -8 1 0 852.88 819.32 87.82 o -7 1 0 2.96 2.28 24.38 o -6 1 0 4048.65 3966.53 175.89 o -5 1 0 645.23 676.55 99.72 o -4 1 0 25791.52 26038.26 871.50 o -3 1 0 23365.48 21918.30 1522.62 o -2 1 0 27824.42 25631.91 825.43 o 2 1 0 11845.27 10694.65 657.19 o 3 1 0 312.76 267.50 68.04 o 4 1 0 248.62 345.97 106.01 o 5 1 0 90.12 84.63 30.84 o 6 1 0 7345.27 7452.58 373.00 o 7 1 0 5142.11 5209.60 297.03 o 8 1 0 253.75 343.72 83.05 o 9 1 0 950.32 875.32 252.71 o 10 1 0 749.08 926.09 177.27 o 11 1 0 9.50 -42.38 193.62 o 12 1 0 94.53 123.64 204.89 o -12 2 0 168.17 172.62 252.71 o -11 2 0 505.66 470.05 255.05 o -10 2 0 120.99 346.80 205.28 o -9 2 0 113.13 197.68 94.25 o -8 2 0 402.12 634.90 132.91 o -7 2 0 20.04 40.63 34.04 o -6 2 0 440.06 475.20 56.88 o -5 2 0 1782.57 1860.02 70.09 o -4 2 0 10951.16 10930.83 636.92 o -3 2 0 2325.69 2328.57 122.95 o -2 2 0 34417.91 27157.94 1377.67 o -1 2 0 7742.27 7785.48 182.50 o 0 2 0 12601.71 10413.58 560.16 o 1 2 0 26344.09 25187.84 969.76 o 2 2 0 22168.72 20814.25 1086.45 o 3 2 0 3694.84 3649.56 125.26 o 4 2 0 7244.13 8309.02 372.63 o 5 2 0 67.91 123.83 89.42 o 6 2 0 33.80 94.12 180.20 o 7 2 0 2765.11 2809.90 187.43 o 8 2 0 4800.99 4952.50 428.96 o 9 2 0 577.71 702.32 183.12 o 10 2 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4 0 1111.93 1036.74 137.44 o -5 4 0 225.09 323.67 70.85 o -4 4 0 2056.75 2263.21 197.56 o -3 4 0 714.87 731.48 39.26 o -2 4 0 3685.71 3926.85 200.34 o -1 4 0 1434.59 1980.13 115.93 o 0 4 0 667.61 739.08 89.62 o 1 4 0 25284.38 21977.10 2838.63 o 2 4 0 3560.98 3534.95 131.43 o 3 4 0 8172.19 7952.40 520.71 o 4 4 0 3552.61 3556.60 178.80 o 5 4 0 163.07 209.96 83.75 o 6 4 0 423.39 408.33 51.84 o 7 4 0 594.36 654.88 78.17 o 8 4 0 208.58 156.83 52.33 o 9 4 0 5.55 -36.94 173.79 o 10 4 0 2.18 108.08 178.46 o 11 4 0 108.19 538.86 353.41 o -11 5 0 18.99 172.62 174.96 o -10 5 0 168.68 250.34 126.73 o -9 5 0 49.41 226.28 190.90 o -8 5 0 1310.67 1338.91 213.44 o -7 5 0 250.29 382.29 118.56 o -6 5 0 1532.39 1742.98 216.81 o -5 5 0 279.83 435.56 106.07 o -4 5 0 394.65 415.10 26.70 o -3 5 0 88.45 132.91 37.68 o -2 5 0 132.45 167.60 37.49 o -1 5 0 2138.55 2144.26 151.49 o 0 5 0 214.19 429.33 58.53 o 1 5 0 699.61 659.72 51.23 o 2 5 0 275.42 266.66 50.02 o 3 5 0 14515.71 15387.03 632.71 o 4 5 0 825.37 859.88 59.06 o 5 5 0 336.90 340.36 37.21 o 6 5 0 0.66 85.53 92.53 o 7 5 0 699.92 677.03 85.74 o 8 5 0 363.13 425.73 262.43 o 9 5 0 152.44 191.38 271.57 o 10 5 0 498.59 850.67 358.47 o 11 5 0 3.24 215.00 229.00 o -10 6 0 282.24 353.41 245.33 o -9 6 0 15.51 -107.34 107.34 o -8 6 0 126.63 165.62 171.46 o -7 6 0 11.75 -55.60 107.70 o -6 6 0 167.02 101.49 95.45 o -5 6 0 40.47 179.62 100.70 o -4 6 0 37.61 246.56 75.19 o -3 6 0 2322.38 2480.45 128.60 o -2 6 0 4370.60 4345.24 300.33 o -1 6 0 3861.76 4128.89 211.31 o 0 6 0 3339.96 3428.39 177.93 o 1 6 0 789.89 900.77 175.13 o 2 6 0 153.18 190.34 52.92 o 3 6 0 2889.43 2861.11 125.74 o 4 6 0 193.32 165.94 27.33 o 5 6 0 180.00 341.77 101.09 o 6 6 0 447.66 443.60 106.06 o 7 6 0 1010.78 923.38 317.64 o 8 6 0 210.79 788.08 284.60 o 9 6 0 388.63 530.70 281.10 o 10 6 0 283.45 2.72 166.40 o 11 6 0 34.72 175.73 240.66 o -10 7 0 21.08 407.84 247.27 o -9 7 0 118.98 266.32 207.61 o -8 7 0 37.41 -114.69 135.69 o -7 7 0 2.00 138.80 129.08 o -6 7 0 471.11 663.91 140.55 o -5 7 0 147.07 17.76 111.58 o -4 7 0 1390.15 1252.81 178.30 o -3 7 0 6.23 22.95 53.70 o -2 7 0 1598.83 1518.66 228.56 o -1 7 0 37.42 27.45 68.40 o 0 7 0 1660.57 1374.96 105.78 o 1 7 0 32.65 81.42 89.95 o 2 7 0 598.11 563.08 58.71 o 3 7 0 615.34 588.99 123.06 o 4 7 0 25.57 54.02 74.84 o 5 7 0 613.58 976.64 246.49 o 6 7 0 14.79 31.49 108.86 o 7 7 0 2.99 76.34 83.82 o 8 7 0 20.45 -8.94 166.40 o 9 7 0 121.84 445.17 276.82 o 10 7 0 16.11 -191.67 293.93 o -9 8 0 3.83 46.65 173.40 o -8 8 0 1.35 -30.19 94.82 o -7 8 0 0.15 22.94 148.91 o -6 8 0 1643.46 1377.10 310.64 o -5 8 0 118.87 -30.09 80.87 o -4 8 0 295.50 481.71 155.52 o -3 8 0 2509.47 2626.62 185.68 o -2 8 0 533.64 765.19 133.24 o -1 8 0 348.58 505.25 153.91 o 0 8 0 1306.82 1270.80 211.45 o 1 8 0 125.22 79.23 69.81 o 2 8 0 336.26 396.62 77.61 o 3 8 0 137.21 53.68 72.11 o 4 8 0 253.70 273.81 265.54 o 5 8 0 1008.03 979.36 261.27 o 6 8 0 169.73 351.86 235.22 o 7 8 0 168.34 363.52 265.93 o 8 8 0 3.87 115.81 103.39 o 9 8 0 74.39 -141.29 150.85 o -8 9 0 22.01 10.50 130.63 o -7 9 0 174.19 -20.22 125.19 o -6 9 0 101.81 23.33 111.19 o -5 9 0 264.31 247.45 104.53 o -4 9 0 301.97 203.63 106.12 o -3 9 0 389.94 543.53 213.45 o -2 9 0 808.23 1284.57 363.52 o -1 9 0 350.93 589.01 99.61 o 0 9 0 173.99 172.11 56.12 o 1 9 0 3.45 19.43 99.52 o 2 9 0 28.28 21.22 67.85 o 3 9 0 380.31 477.16 116.87 o 4 9 0 554.57 942.01 187.79 o 5 9 0 22.28 217.33 210.72 o 6 9 0 27.88 181.86 253.88 o 7 9 0 26.90 -256.99 256.99 o 8 9 0 0.24 29.81 110.22 o -7 10 0 40.27 219.67 221.61 o -6 10 0 42.71 -156.29 156.29 o -5 10 0 121.68 213.84 198.28 o -4 10 0 455.77 286.15 239.50 o -3 10 0 290.68 242.61 174.18 o -2 10 0 317.92 444.78 223.94 o -1 10 0 539.63 507.78 120.58 o 0 10 0 27.54 -27.67 78.54 o 1 10 0 211.73 169.95 76.14 o 2 10 0 1936.15 1763.94 412.12 o 3 10 0 1.18 -12.44 145.41 o 4 10 0 362.63 332.81 256.60 o 5 10 0 65.94 436.22 254.27 o 6 10 0 1.43 148.91 217.72 o 7 10 0 2.07 132.00 122.27 o -5 11 0 168.86 74.26 188.56 o -4 11 0 34.97 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