#------------------------------------------------------------------------------ #$Date: 2012-09-11 12:26:43 +0300 (Tue, 11 Sep 2012) $ #$Revision: 66590 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/40/2234055.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2234055_Fobs loop_ _publ_author_name 'Li, Hong-Qi' 'Ramachandran, G.' 'Satheesh, V.' 'Sathiyanarayanan, K.' 'Rathore, R. S.' _publ_section_title ; 1,1'-[(2-Bromophenyl)methylene]dipyrrolidin-2-one ; _journal_coeditor_code XU5471 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o768 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 91.859 _cell_angle_gamma 90.000 _cell_length_a 7.9734 _cell_length_b 11.0788 _cell_length_c 15.9456 _exptl_crystal_F_000 688.00 _reflns_d_resolution_high 0.6991 _[local]_cod_data_source_file xu5471Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' bs_br1_0m in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 143.86 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 11.39 11.03 3.10 o 6 0 0 701.55 639.49 18.51 o 8 0 0 719.05 676.04 30.08 o 10 0 0 271.95 283.43 24.22 o 1 1 0 46.90 36.88 2.03 o 3 1 0 2918.75 2984.98 33.53 o 4 1 0 4042.99 4082.62 50.09 o 5 1 0 105.76 92.83 4.27 o 6 1 0 11.54 5.99 3.41 o 7 1 0 40.88 49.26 6.37 o 8 1 0 1163.19 1191.69 21.84 o 9 1 0 504.63 489.78 16.65 o 10 1 0 848.78 918.04 24.35 o 11 1 0 107.47 116.42 19.73 o 1 2 0 1703.67 1772.83 20.27 o 2 2 0 8.41 9.99 1.16 o 3 2 0 283.46 349.84 5.62 o 4 2 0 275.49 266.27 5.19 o 5 2 0 3112.50 3147.20 36.53 o 6 2 0 2913.09 2860.81 34.26 o 7 2 0 5225.30 5288.53 66.15 o 8 2 0 77.35 82.88 10.79 o 9 2 0 490.47 489.11 16.83 o 10 2 0 44.53 58.91 10.40 o 11 2 0 64.96 77.55 24.03 o 1 3 0 775.59 736.94 8.91 o 2 3 0 872.42 929.37 12.25 o 3 3 0 11925.21 11748.36 140.86 o 4 3 0 358.19 406.47 10.25 o 5 3 0 2200.32 2094.65 25.67 o 6 3 0 14.34 8.61 3.57 o 7 3 0 24.10 31.87 7.36 o 8 3 0 18.58 8.19 7.26 o 9 3 0 1099.18 1068.34 25.03 o 10 3 0 0.66 3.25 13.96 o 11 3 0 150.82 122.09 27.15 o 0 4 0 653.64 610.68 9.08 o 1 4 0 8680.77 8490.18 90.09 o 2 4 0 2046.04 2254.33 24.71 o 3 4 0 112.14 127.73 5.14 o 4 4 0 78.97 53.02 5.10 o 5 4 0 1447.92 1398.72 23.81 o 6 4 0 1189.54 1191.01 26.37 o 7 4 0 1196.02 1132.81 24.98 o 8 4 0 168.78 162.40 11.46 o 9 4 0 316.87 346.44 20.61 o 10 4 0 123.20 95.52 24.81 o 11 4 0 72.06 84.19 26.96 o 1 5 0 1053.95 1042.86 11.16 o 2 5 0 3189.32 3177.37 49.43 o 3 5 0 4181.45 4359.19 71.72 o 4 5 0 4328.38 4299.56 61.48 o 5 5 0 418.28 462.56 12.53 o 6 5 0 22.94 28.74 7.84 o 7 5 0 90.51 74.10 9.63 o 8 5 0 743.15 724.49 21.69 o 9 5 0 438.90 401.48 33.60 o 10 5 0 762.42 702.04 44.15 o 0 6 0 10434.06 10440.08 125.80 o 1 6 0 75.71 65.96 2.85 o 2 6 0 7282.26 7567.55 77.86 o 3 6 0 454.64 549.25 11.59 o 4 6 0 315.99 316.67 9.54 o 5 6 0 20.57 30.63 7.55 o 6 6 0 2399.97 2480.42 45.87 o 7 6 0 100.60 76.96 10.57 o 8 6 0 351.23 359.92 16.26 o 9 6 0 37.29 28.41 11.87 o 10 6 0 259.85 189.87 30.08 o 1 7 0 2.39 1.89 2.55 o 2 7 0 1386.63 1411.88 16.27 o 3 7 0 9.39 9.81 3.34 o 4 7 0 3575.21 3475.30 60.34 o 5 7 0 343.64 322.17 13.67 o 6 7 0 351.60 342.89 15.02 o 7 7 0 85.99 89.65 11.43 o 8 7 0 545.07 522.43 31.42 o 9 7 0 217.89 189.53 15.17 o 10 7 0 650.34 645.59 45.12 o 0 8 0 1136.98 1119.39 16.99 o 1 8 0 2312.13 2378.11 23.95 o 2 8 0 1117.44 1103.23 13.94 o 3 8 0 657.52 602.96 11.94 o 4 8 0 479.18 457.94 15.20 o 5 8 0 397.12 361.99 15.24 o 6 8 0 723.49 751.91 22.03 o 7 8 0 1133.33 1153.71 28.64 o 8 8 0 211.04 193.55 15.20 o 9 8 0 1.08 8.17 15.65 o 1 9 0 2176.92 2173.42 27.69 o 2 9 0 116.90 117.61 6.01 o 3 9 0 2356.41 2402.17 34.68 o 4 9 0 117.51 81.32 10.07 o 5 9 0 1138.68 1099.82 33.26 o 6 9 0 71.94 57.57 11.39 o 7 9 0 453.68 455.22 29.67 o 8 9 0 40.37 24.97 13.13 o 9 9 0 438.07 430.76 26.27 o 0 10 0 20.37 23.72 14.75 o 1 10 0 3800.04 3907.28 46.74 o 2 10 0 814.27 849.01 16.03 o 3 10 0 177.84 180.62 10.22 o 4 10 0 1607.54 1563.21 39.94 o 5 10 0 691.09 650.94 21.17 o 6 10 0 305.97 276.37 16.19 o 7 10 0 515.69 527.89 21.78 o 8 10 0 252.33 239.12 18.20 o 1 11 0 835.21 879.22 26.39 o 2 11 0 868.55 797.29 25.42 o 3 11 0 750.98 761.37 26.19 o 4 11 0 536.83 509.32 19.05 o 5 11 0 556.04 576.52 21.11 o 6 11 0 139.22 152.53 14.74 o 7 11 0 258.81 282.16 18.64 o 8 11 0 191.38 235.61 23.19 o 0 12 0 175.46 191.82 21.10 o 1 12 0 32.30 29.57 10.75 o 2 12 0 399.26 428.28 20.05 o 3 12 0 40.59 39.72 13.09 o 4 12 0 149.70 101.69 18.95 o 5 12 0 120.23 102.26 16.55 o 6 12 0 681.54 650.90 30.32 o 7 12 0 317.07 341.56 29.82 o 1 13 0 14.78 29.11 19.53 o 2 13 0 763.70 738.18 40.24 o 3 13 0 24.25 24.81 19.73 o 4 13 0 536.99 495.29 25.07 o 5 13 0 32.61 37.32 15.56 o 6 13 0 384.76 385.70 25.47 o 0 14 0 1281.87 1249.57 52.35 o 1 14 0 1327.86 1310.90 55.28 o 2 14 0 588.34 630.54 37.70 o 3 14 0 3.48 30.47 23.64 o 4 14 0 2.00 -13.48 23.64 o 5 14 0 380.04 395.16 25.08 o 1 15 0 284.26 305.70 31.45 o 2 15 0 1.83 -0.78 22.66 o 3 15 0 654.07 586.20 42.19 o -9 0 1 2548.30 2537.32 56.91 o -7 0 1 2619.29 2536.21 44.81 o -5 0 1 32.92 59.09 6.08 o -3 0 1 6766.35 6669.40 79.74 o -1 0 1 343.78 327.72 4.05 o 1 0 1 8082.10 7459.86 346.04 o 3 0 1 3590.68 3593.78 43.76 o 5 0 1 9819.96 9226.76 396.22 o 7 0 1 127.18 134.86 10.33 o 9 0 1 476.24 484.08 20.41 o -11 1 1 159.73 172.09 21.10 o -10 1 1 153.87 145.83 14.11 o -9 1 1 54.45 73.80 9.69 o -8 1 1 3.13 -3.36 6.02 o -7 1 1 823.52 820.22 15.61 o -6 1 1 1950.40 1922.61 33.69 o -5 1 1 6247.79 6293.60 72.97 o -4 1 1 355.03 353.52 6.12 o -3 1 1 4038.47 4134.18 42.54 o -2 1 1 4791.55 5075.25 52.01 o -1 1 1 34.24 31.02 1.31 o 0 1 1 3802.78 3840.41 33.63 o 1 1 1 7032.07 7265.75 86.82 o 2 1 1 854.04 879.61 9.12 o 3 1 1 1299.18 1254.42 15.08 o 4 1 1 615.26 642.26 10.00 o 5 1 1 308.05 277.92 6.80 o 6 1 1 204.79 217.70 6.88 o 7 1 1 4694.73 4689.71 66.63 o 8 1 1 1376.00 1358.67 24.05 o 9 1 1 294.96 308.07 13.92 o 10 1 1 12.23 15.11 9.91 o 11 1 1 58.91 54.69 18.17 o -11 2 1 38.19 19.53 23.44 o -10 2 1 445.28 449.16 17.32 o -9 2 1 310.69 323.30 14.20 o -8 2 1 1113.78 1137.33 24.61 o -7 2 1 351.57 332.18 8.87 o -6 2 1 71.74 71.64 4.32 o -5 2 1 11.62 33.17 4.23 o -4 2 1 1970.08 1886.32 22.33 o -3 2 1 2732.65 2662.74 30.46 o -2 2 1 16384.56 15800.91 211.53 o -1 2 1 1128.29 1255.10 14.67 o 0 2 1 2999.16 3024.99 23.56 o 1 2 1 6208.43 6217.04 75.05 o 2 2 1 279.47 252.90 5.39 o 3 2 1 3222.46 3346.15 32.43 o 4 2 1 8787.77 8557.43 94.11 o 5 2 1 4795.15 4884.37 55.36 o 6 2 1 803.93 763.05 12.06 o 7 2 1 305.10 298.16 8.88 o 8 2 1 122.25 127.35 9.45 o 9 2 1 7.16 -0.86 8.60 o 10 2 1 838.88 872.17 29.84 o 11 2 1 57.90 60.55 24.22 o -11 3 1 25.59 27.15 23.64 o -10 3 1 134.07 134.47 27.54 o -9 3 1 8.60 14.58 8.02 o -8 3 1 1036.02 1027.09 22.91 o -7 3 1 70.39 79.19 8.54 o -6 3 1 5175.74 5245.10 59.69 o -5 3 1 276.04 268.48 5.81 o -4 3 1 3398.63 3501.84 50.44 o -3 3 1 141.27 153.87 6.07 o -2 3 1 46.88 53.99 2.81 o -1 3 1 255.24 267.17 4.14 o 0 3 1 5299.83 5325.86 41.41 o 1 3 1 3077.77 3301.19 30.12 o 2 3 1 6281.53 6243.01 66.73 o 3 3 1 286.10 318.22 6.46 o 4 3 1 776.26 813.58 18.46 o 5 3 1 122.52 130.49 4.74 o 6 3 1 3794.64 3809.38 44.54 o 7 3 1 867.86 838.40 16.98 o 8 3 1 2409.31 2399.70 37.62 o 9 3 1 123.84 94.28 17.85 o 10 3 1 52.70 71.72 15.65 o 11 3 1 26.34 4.69 23.05 o -11 4 1 1.74 15.82 22.46 o -10 4 1 539.04 560.03 37.70 o -9 4 1 310.50 311.76 20.18 o -8 4 1 1477.59 1515.70 31.66 o -7 4 1 478.28 477.27 15.76 o -6 4 1 43.90 29.00 6.21 o -5 4 1 20.76 16.73 5.14 o -4 4 1 3826.91 3916.40 55.60 o -3 4 1 1614.75 1607.02 22.40 o -2 4 1 8998.34 9198.47 101.65 o -1 4 1 481.27 484.87 5.74 o 0 4 1 2886.80 2955.56 24.76 o 1 4 1 45.27 42.70 2.08 o 2 4 1 410.37 568.16 9.49 o 3 4 1 1161.73 1185.84 15.24 o 4 4 1 2550.05 2441.12 36.78 o 5 4 1 14.78 31.22 3.98 o 6 4 1 620.90 601.05 16.62 o 7 4 1 8.57 7.13 7.78 o 8 4 1 523.30 536.82 18.02 o 9 4 1 65.76 28.30 13.88 o 10 4 1 1935.18 1883.82 71.49 o 11 4 1 231.86 226.20 32.43 o -10 5 1 222.43 235.18 31.06 o -9 5 1 146.47 147.39 16.97 o -8 5 1 191.41 188.52 12.85 o -7 5 1 685.81 675.86 19.12 o -6 5 1 1389.22 1315.86 27.85 o -5 5 1 4334.83 4183.95 60.81 o -4 5 1 427.32 392.59 9.66 o -3 5 1 5.22 12.93 3.72 o -2 5 1 3464.98 3820.38 38.04 o -1 5 1 1191.68 1214.94 13.34 o 0 5 1 2599.23 2732.25 24.33 o 1 5 1 4287.82 4206.49 41.24 o 2 5 1 1209.09 1159.98 13.05 o 3 5 1 142.18 111.10 5.68 o 4 5 1 156.30 139.62 7.16 o 5 5 1 173.74 150.28 8.54 o 6 5 1 28.63 41.82 8.27 o 7 5 1 1183.55 1157.04 26.37 o 8 5 1 621.46 655.37 20.42 o 9 5 1 679.52 709.54 28.48 o 10 5 1 162.37 165.84 27.54 o -10 6 1 56.97 97.47 27.54 o -9 6 1 1244.30 1368.31 32.96 o -8 6 1 13.66 23.74 10.77 o -7 6 1 1089.58 1103.57 33.08 o -6 6 1 17.77 11.63 8.30 o -5 6 1 227.49 213.37 11.05 o -4 6 1 3.49 0.32 4.63 o -3 6 1 3541.78 3489.92 47.68 o -2 6 1 3.35 5.70 2.10 o -1 6 1 3301.08 3258.61 31.01 o 0 6 1 145.15 149.04 3.51 o 1 6 1 342.88 375.55 5.51 o 2 6 1 60.51 70.49 3.43 o 3 6 1 9310.59 9240.38 94.72 o 4 6 1 111.40 99.81 6.19 o 5 6 1 2602.61 2700.84 48.16 o 6 6 1 12.56 11.32 8.19 o 7 6 1 203.57 217.23 13.53 o 8 6 1 18.33 25.82 10.46 o 9 6 1 97.49 102.08 13.12 o 10 6 1 177.99 191.43 30.08 o -10 7 1 24.94 5.66 24.03 o -9 7 1 140.05 152.31 17.60 o -8 7 1 5.45 -8.27 10.96 o -7 7 1 1162.30 1205.97 28.66 o -6 7 1 153.33 151.99 12.44 o -5 7 1 1706.47 1704.46 29.69 o -4 7 1 532.58 511.89 13.69 o -3 7 1 2009.21 2064.51 23.82 o -2 7 1 379.89 428.94 6.94 o -1 7 1 126.80 113.59 3.95 o 0 7 1 2410.00 2434.87 22.53 o 1 7 1 8806.58 8631.81 74.67 o 2 7 1 1644.69 1735.06 20.53 o 3 7 1 1867.08 1983.63 25.49 o 4 7 1 49.23 48.98 6.58 o 5 7 1 2074.25 1759.99 34.91 o 6 7 1 938.64 843.80 37.26 o 7 7 1 1736.74 1753.47 42.14 o 8 7 1 6.98 11.02 11.06 o 9 7 1 308.60 309.41 18.17 o 10 7 1 84.11 80.87 26.76 o -9 8 1 408.22 361.62 23.25 o -8 8 1 811.37 768.68 34.06 o -7 8 1 356.61 360.75 17.14 o -6 8 1 1012.81 916.70 24.14 o -5 8 1 622.15 643.71 19.38 o -4 8 1 299.15 306.21 11.54 o -3 8 1 1410.26 1430.71 22.72 o -2 8 1 2555.04 2531.80 25.42 o -1 8 1 899.64 922.26 19.44 o 0 8 1 251.96 242.65 4.89 o 1 8 1 110.45 109.58 3.94 o 2 8 1 3364.40 3327.97 34.54 o 3 8 1 3813.76 3788.08 49.06 o 4 8 1 3061.59 2949.08 55.66 o 5 8 1 1781.64 1691.66 44.81 o 6 8 1 312.89 290.10 15.21 o 7 8 1 368.08 370.08 17.52 o 8 8 1 334.87 349.60 18.34 o 9 8 1 20.13 18.53 16.29 o -9 9 1 71.89 56.81 29.40 o -8 9 1 71.36 83.24 14.49 o -7 9 1 202.94 205.02 15.46 o -6 9 1 2672.53 2572.47 49.76 o -5 9 1 437.59 444.66 17.28 o -4 9 1 3077.25 2902.76 45.74 o -3 9 1 291.87 288.39 19.74 o -2 9 1 64.64 68.30 5.41 o -1 9 1 283.48 296.35 8.35 o 0 9 1 3092.99 3139.33 32.27 o 1 9 1 21.77 25.34 4.61 o 2 9 1 836.49 823.01 19.13 o 3 9 1 1.72 3.19 5.96 o 4 9 1 20.33 27.58 8.83 o 5 9 1 372.04 305.53 14.84 o 6 9 1 1546.44 1467.96 33.64 o 7 9 1 471.13 424.57 19.10 o 8 9 1 421.02 399.59 24.02 o 9 9 1 189.39 230.65 24.71 o -8 10 1 227.96 242.12 18.05 o -7 10 1 15.18 4.22 12.51 o -6 10 1 80.45 62.19 12.21 o -5 10 1 221.01 198.46 11.95 o -4 10 1 1421.18 1398.74 26.95 o -3 10 1 1011.22 1046.94 29.20 o -2 10 1 3318.89 3359.97 44.87 o -1 10 1 488.85 491.11 10.81 o 0 10 1 1910.27 1905.23 31.61 o 1 10 1 279.42 291.81 9.26 o 2 10 1 908.92 906.70 16.60 o 3 10 1 346.31 355.02 13.11 o 4 10 1 1062.12 1106.36 32.87 o 5 10 1 20.36 31.91 11.01 o 6 10 1 207.09 160.07 14.18 o 7 10 1 4.99 22.55 19.54 o 8 10 1 373.93 368.00 20.56 o -8 11 1 174.39 214.13 22.58 o -7 11 1 289.51 282.07 18.42 o -6 11 1 293.24 307.62 17.78 o -5 11 1 313.92 331.05 16.89 o -4 11 1 408.35 368.62 21.51 o -3 11 1 124.20 111.78 11.19 o -2 11 1 39.91 42.39 10.40 o -1 11 1 1605.02 1603.73 30.86 o 0 11 1 2549.87 2557.40 55.87 o 1 11 1 279.77 297.66 15.61 o 2 11 1 1285.61 1281.27 33.25 o 3 11 1 260.31 245.76 16.37 o 4 11 1 6.68 0.39 14.60 o 5 11 1 204.86 203.03 19.22 o 6 11 1 244.47 268.67 17.25 o 7 11 1 493.07 489.88 22.24 o 8 11 1 15.86 -4.95 17.61 o -7 12 1 528.33 514.68 23.80 o -6 12 1 22.01 21.54 17.05 o -5 12 1 6.26 18.81 14.64 o -4 12 1 115.16 97.99 33.60 o -3 12 1 1141.91 1145.48 46.88 o -2 12 1 274.98 269.47 16.38 o -1 12 1 733.23 783.61 26.19 o 0 12 1 140.88 157.81 16.41 o 1 12 1 90.23 82.88 12.59 o 2 12 1 1.92 7.23 17.78 o 3 12 1 970.38 973.07 30.91 o 4 12 1 62.36 82.60 14.57 o 5 12 1 822.79 798.36 30.47 o 6 12 1 152.08 167.30 21.49 o 7 12 1 40.38 42.02 17.65 o -6 13 1 13.74 27.40 16.65 o -5 13 1 577.95 530.58 56.26 o -4 13 1 14.35 5.40 15.04 o -3 13 1 188.12 213.70 26.57 o -2 13 1 0.94 22.27 20.71 o -1 13 1 1233.56 1261.87 51.96 o 0 13 1 185.73 198.68 16.18 o 1 13 1 451.47 474.12 22.21 o 2 13 1 644.44 594.02 36.72 o 3 13 1 606.42 606.91 37.11 o 4 13 1 28.59 30.68 16.51 o 5 13 1 203.03 194.15 19.82 o 6 13 1 2.61 -5.17 16.84 o -5 14 1 88.78 92.33 18.86 o -4 14 1 378.27 305.31 33.79 o -3 14 1 715.25 792.48 45.71 o -2 14 1 153.72 105.09 23.83 o -1 14 1 212.11 218.97 26.37 o 0 14 1 3.31 8.19 13.86 o 1 14 1 30.33 71.30 20.31 o 2 14 1 520.25 519.01 36.72 o 3 14 1 267.43 261.95 29.69 o 4 14 1 249.73 257.84 30.86 o 5 14 1 223.62 203.66 20.65 o -3 15 1 80.58 81.06 27.74 o -2 15 1 14.62 63.87 25.20 o -1 15 1 86.56 47.47 24.03 o 0 15 1 385.31 342.81 32.23 o 1 15 1 87.31 57.62 24.42 o 2 15 1 235.67 271.32 31.25 o 3 15 1 55.02 42.19 25.78 o -10 0 2 1389.70 1341.76 51.57 o -8 0 2 592.90 541.69 19.53 o -6 0 2 4557.63 4761.71 77.33 o -4 0 2 10936.92 11402.99 288.64 o -2 0 2 1246.21 1298.01 18.71 o 0 0 2 228.59 244.63 10.33 o 2 0 2 20695.81 18844.67 716.20 o 4 0 2 980.06 963.16 41.35 o 6 0 2 2531.38 2498.42 52.61 o 8 0 2 2681.26 2732.05 59.73 o 10 0 2 158.38 216.24 23.05 o -11 1 2 134.21 157.64 20.71 o -10 1 2 7.98 6.48 9.60 o -9 1 2 405.96 422.06 17.89 o -8 1 2 1882.11 1850.13 30.28 o -7 1 2 839.64 839.52 15.17 o -6 1 2 1376.11 1433.73 18.62 o -5 1 2 646.01 631.54 9.61 o -4 1 2 3669.87 3967.98 44.61 o -3 1 2 1894.76 2222.11 23.51 o -1 1 2 2131.98 2143.11 20.67 o 1 1 2 145.84 156.97 2.47 o 2 1 2 115.02 126.17 3.64 o 3 1 2 3001.56 3108.90 38.51 o 4 1 2 4038.70 3890.33 48.19 o 5 1 2 3098.70 3074.99 39.23 o 6 1 2 1525.67 1495.87 21.31 o 7 1 2 105.04 101.75 7.58 o 8 1 2 354.55 361.61 12.35 o 9 1 2 3.12 2.13 8.66 o 10 1 2 355.31 371.93 16.22 o -10 2 2 667.44 665.94 20.28 o -9 2 2 729.07 711.76 19.54 o -8 2 2 57.48 57.74 8.09 o -7 2 2 80.05 85.39 6.89 o -6 2 2 195.59 197.73 6.01 o -5 2 2 2459.61 2316.34 29.34 o -4 2 2 3983.84 4145.83 46.62 o -3 2 2 2251.59 2258.93 26.37 o -2 2 2 961.65 1001.33 10.72 o -1 2 2 2554.30 2730.29 28.31 o 0 2 2 2012.73 2061.30 17.87 o 2 2 2 3050.60 3074.70 32.17 o 3 2 2 8286.47 8159.90 89.61 o 4 2 2 36.98 52.20 3.15 o 5 2 2 13.70 18.43 4.41 o 6 2 2 522.69 540.97 10.08 o 7 2 2 503.65 494.91 11.12 o 8 2 2 830.54 797.68 25.06 o 9 2 2 605.19 614.01 19.07 o 10 2 2 389.16 392.25 16.83 o 11 2 2 15.70 -17.19 21.49 o -11 3 2 7.55 -0.59 22.27 o -10 3 2 76.08 44.44 15.39 o -9 3 2 816.17 830.07 21.21 o -8 3 2 0.53 6.01 6.73 o -7 3 2 3023.12 3010.90 69.56 o -6 3 2 206.44 211.24 6.08 o -5 3 2 215.80 257.10 5.60 o -4 3 2 214.21 216.94 10.46 o -3 3 2 5328.24 5186.47 63.92 o -2 3 2 47.13 45.80 3.12 o -1 3 2 13808.41 13479.39 146.98 o 0 3 2 2154.39 2371.81 21.45 o 1 3 2 948.53 895.47 9.73 o 2 3 2 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