#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:37:37 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181264 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/42/2234201.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2234201_Fobs loop_ _publ_author_name 'Wang, Ying-Chun' _publ_section_title ; trans-Tetrakis[N-(adamantan-1-yl)pyridine-4-carboxamide]dichloridomanganese(II)--N-(adamantan-1-yl)pyridine-4-carboxamide (1/2) ; _journal_coeditor_code GW2114 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m408 _journal_volume 68 _journal_year 2012 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 86.122 _cell_angle_beta 83.605 _cell_angle_gamma 84.094 _cell_length_a 11.1890 _cell_length_b 11.5710 _cell_length_c 16.9210 _exptl_crystal_F_000 886.85 _reflns_d_resolution_high 0.7699 _cod_data_source_file gw2114Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 1 in P1 P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 150.53 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 16765.62 15477.97 120.34 o 3 0 0 1096.18 1096.46 17.43 o 4 0 0 942.54 899.32 17.05 o 5 0 0 0.66 7.17 5.88 o 6 0 0 733.81 688.12 53.86 o 7 0 0 68.70 62.90 11.93 o 8 0 0 114.42 130.77 44.18 o 9 0 0 75.16 64.12 10.31 o 10 0 0 379.43 460.79 37.02 o 11 0 0 295.75 336.38 333.47 o 12 0 0 318.17 288.30 65.51 o 13 0 0 20.23 26.26 32.58 o -14 1 0 85.64 67.24 25.23 o -13 1 0 16.34 30.66 21.62 o -12 1 0 9.99 29.97 18.12 o -11 1 0 498.25 454.07 87.18 o -10 1 0 11.39 110.78 27.84 o -9 1 0 592.41 602.15 21.75 o -8 1 0 173.71 169.49 14.47 o -7 1 0 301.84 261.71 15.68 o -6 1 0 1638.74 1813.65 40.58 o -5 1 0 2628.95 2666.07 33.14 o -4 1 0 1668.10 1674.47 30.84 o -3 1 0 181.69 151.13 4.16 o -2 1 0 741.03 731.24 32.34 o 2 1 0 7984.56 7772.92 190.68 o 3 1 0 1329.54 1272.82 27.76 o 4 1 0 773.60 723.39 16.56 o 5 1 0 254.80 261.59 7.29 o 6 1 0 688.54 688.98 34.05 o 7 1 0 1215.94 1227.67 24.24 o 8 1 0 288.74 323.21 38.52 o 9 1 0 131.29 180.00 29.39 o 10 1 0 1201.50 1124.95 79.85 o 11 1 0 127.41 87.92 22.71 o 12 1 0 204.46 224.22 48.13 o 14 1 0 75.85 105.94 29.08 o -14 2 0 0.12 27.50 19.65 o -13 2 0 0.06 57.86 35.25 o -12 2 0 18.09 17.67 13.03 o -11 2 0 142.64 69.80 34.75 o -10 2 0 73.72 69.31 19.15 o -9 2 0 447.89 598.96 46.85 o -8 2 0 315.80 289.97 27.15 o -7 2 0 271.03 243.52 31.46 o -5 2 0 20.85 45.71 22.51 o -4 2 0 17.08 32.29 19.50 o -3 2 0 891.66 931.79 40.33 o -2 2 0 1036.07 1048.22 24.01 o -1 2 0 1131.75 1063.15 16.41 o 0 2 0 20601.54 18845.77 147.56 o 1 2 0 15582.54 15309.37 163.98 o 2 2 0 3674.28 3559.19 24.28 o 3 2 0 2753.60 2579.77 41.32 o 4 2 0 834.37 849.28 25.67 o 5 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16.77 o 12 7 0 26.94 13.18 23.65 o 13 7 0 84.63 69.56 39.30 o -11 8 0 21.50 91.18 49.07 o -10 8 0 36.26 23.40 40.58 o -9 8 0 83.70 77.16 34.75 o -8 8 0 28.03 37.72 28.93 o -7 8 0 16.89 -44.78 44.78 o -6 8 0 234.97 184.48 43.84 o -5 8 0 440.70 433.24 76.22 o -4 8 0 1239.33 1215.16 63.68 o -3 8 0 1334.37 1313.63 75.01 o -2 8 0 159.57 166.62 33.00 o -1 8 0 128.89 131.33 19.21 o 0 8 0 871.33 896.34 31.85 o 1 8 0 160.12 161.66 28.96 o 2 8 0 167.45 195.50 35.90 o 3 8 0 1188.66 1283.70 56.57 o 4 8 0 363.81 330.13 51.36 o 5 8 0 544.68 591.70 21.32 o 6 8 0 282.32 250.12 32.29 o 7 8 0 379.27 417.23 44.44 o 8 8 0 333.78 272.56 40.98 o 9 8 0 198.43 163.86 30.01 o 10 8 0 7.53 16.38 28.31 o 11 8 0 30.17 17.23 13.33 o 12 8 0 22.35 26.47 16.55 o -10 9 0 139.39 120.90 53.71 o -9 9 0 25.38 22.76 25.42 o -8 9 0 17.36 -19.10 33.32 o -7 9 0 4.26 -2.76 43.44 o -6 9 0 180.26 174.91 37.17 o -5 9 0 16.49 44.28 22.17 o -4 9 0 865.13 953.51 60.98 o -3 9 0 1123.12 1214.15 102.56 o -2 9 0 1343.50 1388.03 61.37 o 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