#------------------------------------------------------------------------------ #$Date: 2012-09-11 12:26:43 +0300 (Tue, 11 Sep 2012) $ #$Revision: 66590 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/42/2234238.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2234238_Fobs loop_ _publ_author_name 'Asiri, Abdullah M.' 'Faidallah, Hassan M.' 'Alamry, Khalid A.' 'Ng, Seik Weng' 'Tiekink, Edward R. T.' _publ_section_title ; 4-[5-(Furan-2-yl)-3-trifluoromethyl-1H-pyrazol-1-yl]benzenesulfonamide ; _journal_coeditor_code HB6693 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1168 _journal_page_last o1169 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 110.728 _cell_angle_gamma 90.000 _cell_length_a 16.0536 _cell_length_b 4.8173 _cell_length_c 20.6202 _exptl_crystal_F_000 728.00 _reflns_d_resolution_high 0.7680 _[local]_cod_data_source_file hb6693Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P21/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 169.22 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1517.18 1695.77 41.21 o 4 0 0 3115.85 2659.87 73.21 o 6 0 0 102.68 84.12 16.83 o 8 0 0 19.83 15.84 9.51 o 10 0 0 0.10 -2.89 10.22 o 12 0 0 57.91 33.39 13.33 o 14 0 0 224.88 174.88 34.10 o 16 0 0 218.10 275.02 46.74 o 18 0 0 8.23 34.41 20.40 o 1 1 0 1607.18 1541.87 20.89 o 2 1 0 7540.45 8407.93 78.05 o 3 1 0 3388.33 3495.33 35.45 o 4 1 0 3460.25 3263.74 37.68 o 5 1 0 128.70 184.40 9.32 o 6 1 0 2969.20 3337.39 44.77 o 7 1 0 349.92 404.93 21.16 o 8 1 0 779.23 779.22 31.16 o 9 1 0 48.99 61.84 8.82 o 10 1 0 403.17 417.48 31.84 o 11 1 0 33.19 41.97 13.76 o 12 1 0 913.38 785.03 59.10 o 13 1 0 325.41 337.48 32.93 o 14 1 0 13.68 8.67 24.07 o 15 1 0 70.48 37.60 37.84 o 16 1 0 78.72 57.48 19.11 o 17 1 0 0.01 10.06 11.99 o 18 1 0 74.88 55.11 17.01 o 19 1 0 97.35 126.11 48.57 o 0 2 0 7418.31 8303.68 325.50 o 1 2 0 1302.78 1178.97 29.09 o 2 2 0 2.52 1.81 2.46 o 3 2 0 0.52 1.62 3.26 o 4 2 0 3226.18 3319.54 57.65 o 5 2 0 213.15 191.18 10.54 o 6 2 0 300.75 249.05 14.52 o 7 2 0 3136.28 3537.90 58.68 o 8 2 0 350.98 239.62 17.05 o 9 2 0 0.06 1.92 8.51 o 10 2 0 34.76 23.67 11.04 o 11 2 0 304.03 253.70 27.33 o 12 2 0 440.12 427.18 36.96 o 13 2 0 214.05 167.40 24.70 o 14 2 0 216.35 224.92 29.71 o 15 2 0 44.50 58.17 17.42 o 16 2 0 87.76 116.68 24.80 o 17 2 0 11.64 -1.28 17.27 o 18 2 0 139.31 190.82 45.36 o 1 3 0 34.13 46.48 7.48 o 2 3 0 760.19 830.14 26.05 o 3 3 0 56.10 86.85 8.83 o 4 3 0 1103.99 1270.78 30.94 o 5 3 0 289.64 370.92 17.14 o 6 3 0 354.75 370.50 19.85 o 7 3 0 314.96 307.64 22.35 o 8 3 0 29.23 40.55 10.65 o 9 3 0 679.38 690.02 44.23 o 10 3 0 52.03 17.86 29.79 o 11 3 0 27.59 -9.89 14.13 o 12 3 0 176.92 153.93 23.52 o 13 3 0 0.03 -7.41 10.79 o 14 3 0 21.48 13.52 10.74 o 15 3 0 58.05 33.36 14.99 o 16 3 0 9.08 19.29 20.10 o 17 3 0 1.41 43.49 16.16 o 0 4 0 169.05 227.88 31.89 o 1 4 0 61.52 41.47 8.11 o 2 4 0 128.19 133.82 13.77 o 3 4 0 512.60 604.99 27.52 o 4 4 0 237.27 273.36 16.77 o 5 4 0 206.17 204.76 16.82 o 6 4 0 168.91 204.40 17.32 o 7 4 0 551.77 612.87 44.97 o 8 4 0 289.83 335.53 34.47 o 9 4 0 132.62 125.45 23.23 o 10 4 0 180.60 203.70 29.65 o 11 4 0 46.06 24.80 15.96 o 12 4 0 40.05 48.31 21.59 o 13 4 0 15.98 20.71 15.44 o 14 4 0 124.02 161.62 41.80 o 15 4 0 48.01 85.25 33.51 o 1 5 0 175.79 182.65 23.39 o 2 5 0 41.27 22.66 11.71 o 3 5 0 186.05 219.38 21.95 o 4 5 0 146.15 138.01 17.35 o 5 5 0 58.62 98.68 19.12 o 6 5 0 14.79 14.60 10.41 o 7 5 0 289.76 339.14 37.69 o 8 5 0 3.11 1.63 23.63 o 9 5 0 19.11 18.98 10.51 o 10 5 0 98.34 83.41 21.23 o 11 5 0 2.00 -5.27 19.54 o 2 6 0 158.15 216.13 39.91 o 3 6 0 29.35 18.17 13.63 o 4 6 0 6.93 -15.44 15.44 o -19 0 1 131.44 144.51 36.61 o -17 0 1 0.01 -2.30 14.24 o -15 0 1 0.64 1.79 16.51 o -13 0 1 1566.13 1561.71 96.66 o -11 0 1 111.39 96.73 23.92 o -9 0 1 37.11 42.24 15.79 o -7 0 1 7113.65 7741.92 167.54 o -5 0 1 1374.40 1246.21 52.43 o -3 0 1 17846.75 17279.69 222.78 o 3 0 1 28636.67 29862.27 363.99 o 5 0 1 49.85 120.95 19.40 o 7 0 1 732.47 674.89 47.44 o 9 0 1 6.35 -13.54 13.54 o 11 0 1 220.90 195.78 32.70 o 13 0 1 27.75 48.91 19.20 o 15 0 1 600.65 585.05 67.69 o 17 0 1 25.41 -0.95 11.66 o 19 0 1 185.49 176.70 44.63 o -19 1 1 0.72 6.23 12.74 o -18 1 1 0.57 1.58 12.27 o -17 1 1 66.31 85.40 27.85 o -16 1 1 87.23 86.43 20.91 o -15 1 1 1441.48 1370.82 71.18 o -14 1 1 17.21 3.59 9.05 o -13 1 1 31.83 11.43 9.56 o -12 1 1 6.76 24.95 13.25 o -11 1 1 252.00 213.09 24.36 o -10 1 1 198.77 236.04 19.45 o -9 1 1 628.25 758.90 26.89 o -8 1 1 8.63 4.19 3.71 o -7 1 1 1563.69 1263.00 31.00 o -6 1 1 13.99 32.42 5.75 o -5 1 1 55.25 67.61 6.42 o -4 1 1 3144.57 3402.12 37.47 o -3 1 1 11662.85 12739.90 184.80 o -2 1 1 56.21 61.53 4.92 o -1 1 1 5389.83 4935.49 55.42 o 0 1 1 5314.79 5082.05 168.08 o 1 1 1 723.90 709.12 55.72 o 2 1 1 43.33 65.60 4.34 o 3 1 1 7141.26 6935.68 125.38 o 4 1 1 2277.06 2127.67 30.32 o 5 1 1 1788.21 2025.30 36.71 o 6 1 1 100.32 133.38 10.49 o 7 1 1 1301.97 1402.74 39.46 o 8 1 1 966.59 907.97 34.45 o 9 1 1 721.22 669.32 33.11 o 10 1 1 248.66 276.42 27.13 o 11 1 1 57.57 44.46 14.30 o 12 1 1 118.28 132.55 22.54 o 13 1 1 109.63 96.96 36.42 o 14 1 1 3.29 -1.50 8.19 o 15 1 1 2.36 -2.41 11.37 o 16 1 1 9.29 2.13 20.23 o 17 1 1 99.75 149.67 26.28 o 18 1 1 24.65 15.90 13.49 o 19 1 1 150.96 144.02 41.38 o -18 2 1 73.86 165.36 30.22 o -17 2 1 3.45 21.80 12.29 o -16 2 1 80.75 120.54 23.89 o -15 2 1 119.33 116.29 22.75 o -14 2 1 202.04 169.75 25.43 o -13 2 1 114.90 114.43 19.79 o -12 2 1 101.73 113.72 19.51 o -11 2 1 44.90 46.49 14.34 o -10 2 1 67.89 70.99 14.11 o -9 2 1 118.00 157.58 13.74 o -8 2 1 334.13 366.31 19.26 o -7 2 1 2077.58 2208.86 45.07 o -6 2 1 2477.61 2582.48 46.21 o -5 2 1 18.55 1.89 2.63 o -4 2 1 565.84 639.75 19.61 o -3 2 1 5409.45 5673.37 144.03 o -2 2 1 134.10 149.73 8.93 o -1 2 1 106.29 88.79 8.05 o 0 2 1 116.31 175.28 9.68 o 1 2 1 431.25 457.83 21.79 o 2 2 1 1399.27 1858.64 32.55 o 3 2 1 2265.93 2547.66 35.74 o 4 2 1 694.55 656.53 18.42 o 5 2 1 1556.63 1516.65 34.43 o 6 2 1 537.27 502.58 20.66 o 7 2 1 74.36 82.40 9.19 o 8 2 1 132.18 171.55 13.59 o 9 2 1 427.82 377.34 24.09 o 10 2 1 138.62 155.15 21.42 o 11 2 1 522.75 543.69 54.20 o 12 2 1 44.32 68.85 17.27 o 13 2 1 318.26 348.98 35.43 o 14 2 1 403.86 401.76 39.86 o 15 2 1 269.79 263.93 33.68 o 16 2 1 0.32 25.78 13.81 o 17 2 1 22.56 21.69 12.45 o 18 2 1 90.94 121.36 31.51 o -17 3 1 27.21 6.15 15.53 o -16 3 1 0.40 -7.78 12.60 o -15 3 1 96.27 117.92 23.56 o -14 3 1 39.29 47.61 16.35 o -13 3 1 113.24 108.96 21.00 o -12 3 1 139.70 164.50 24.52 o -11 3 1 47.26 22.56 19.73 o -10 3 1 0.03 7.73 12.37 o -9 3 1 641.00 686.33 43.50 o -8 3 1 644.52 675.36 33.06 o -7 3 1 835.42 863.94 31.19 o -6 3 1 287.82 300.27 17.82 o -5 3 1 1340.08 1491.51 34.58 o -4 3 1 184.01 195.52 13.47 o -3 3 1 149.31 137.35 10.95 o -2 3 1 89.32 121.99 9.97 o -1 3 1 11.23 1.50 4.68 o 0 3 1 414.22 367.01 27.36 o 1 3 1 2153.72 2535.77 53.77 o 2 3 1 44.62 61.26 7.31 o 3 3 1 144.43 152.21 10.42 o 4 3 1 54.95 40.23 5.99 o 5 3 1 343.88 370.84 17.12 o 6 3 1 115.49 102.72 12.69 o 7 3 1 453.62 455.26 29.37 o 8 3 1 719.63 654.82 43.81 o 9 3 1 15.88 23.70 11.32 o 10 3 1 574.48 535.81 41.15 o 11 3 1 264.82 270.71 30.62 o 12 3 1 17.43 10.78 9.63 o 13 3 1 87.38 59.95 15.54 o 14 3 1 159.97 109.61 22.50 o 15 3 1 0.01 31.09 15.58 o 16 3 1 5.04 -1.36 22.95 o -15 4 1 21.41 7.52 21.04 o -14 4 1 0.54 -27.96 27.96 o -13 4 1 13.93 26.04 20.77 o -12 4 1 25.69 1.79 17.55 o -11 4 1 10.52 -14.97 22.05 o -10 4 1 268.20 302.30 48.96 o -9 4 1 128.59 130.39 23.49 o -8 4 1 329.57 349.73 46.37 o -7 4 1 51.76 54.87 9.76 o -6 4 1 575.48 611.48 28.90 o -5 4 1 845.38 1037.62 39.65 o -4 4 1 10.02 7.05 5.04 o -3 4 1 276.60 351.82 23.20 o -2 4 1 308.29 352.92 29.22 o -1 4 1 215.01 244.56 16.81 o 0 4 1 333.02 367.45 28.23 o 1 4 1 310.30 299.16 18.54 o 2 4 1 425.50 455.77 23.49 o 3 4 1 584.51 731.88 31.58 o 4 4 1 577.76 569.57 24.15 o 5 4 1 28.83 52.72 8.15 o 6 4 1 100.91 103.40 23.47 o 7 4 1 861.27 883.05 53.81 o 8 4 1 19.14 18.03 10.41 o 9 4 1 54.68 48.74 16.03 o 10 4 1 427.83 380.46 38.54 o 11 4 1 0.82 10.35 17.14 o 12 4 1 167.98 185.45 42.95 o 13 4 1 1.17 14.18 20.42 o 14 4 1 41.07 56.15 33.55 o -12 5 1 75.68 46.34 36.91 o -11 5 1 72.74 62.02 47.07 o -10 5 1 525.82 668.12 56.63 o -9 5 1 44.79 64.49 24.92 o -8 5 1 1.72 7.10 12.95 o -7 5 1 7.29 1.30 7.32 o -6 5 1 0.02 8.14 7.98 o -5 5 1 149.09 153.99 19.06 o -4 5 1 534.48 566.01 36.49 o -3 5 1 4.81 15.41 8.36 o -2 5 1 16.02 22.44 9.33 o -1 5 1 2.51 -3.78 6.09 o 0 5 1 208.40 231.23 26.53 o 1 5 1 8.40 -11.44 12.14 o 2 5 1 59.87 55.47 12.72 o 3 5 1 0.49 -2.93 10.31 o 4 5 1 39.19 53.75 11.21 o 5 5 1 54.36 64.97 12.62 o 6 5 1 24.53 23.70 16.42 o 7 5 1 256.71 272.39 33.12 o 8 5 1 32.53 44.81 19.48 o 9 5 1 40.99 41.10 28.12 o 10 5 1 20.37 18.33 10.82 o 11 5 1 83.01 81.79 22.31 o -3 6 1 12.86 57.79 19.93 o -2 6 1 0.05 -16.26 16.26 o -1 6 1 20.60 2.87 9.24 o 0 6 1 118.36 160.00 34.20 o 1 6 1 19.34 50.48 16.92 o 2 6 1 348.24 501.80 62.52 o 3 6 1 89.66 33.52 18.49 o 4 6 1 1.18 11.19 17.54 o 5 6 1 15.42 -14.29 14.29 o -20 0 2 102.84 68.73 29.19 o -18 0 2 6.04 4.44 13.93 o -16 0 2 461.91 345.08 50.95 o -14 0 2 109.47 109.42 27.59 o -12 0 2 7.42 8.76 14.40 o -10 0 2 15.67 22.46 14.40 o -8 0 2 1080.60 1052.98 59.71 o -6 0 2 1291.72 1355.34 58.09 o -4 0 2 602.53 576.43 31.37 o -2 0 2 2050.82 1968.24 40.39 o 2 0 2 14292.62 14115.06 192.39 o 4 0 2 1837.33 1781.23 63.19 o 6 0 2 1446.09 1469.09 66.76 o 8 0 2 955.24 1143.36 67.09 o 10 0 2 295.12 283.03 37.52 o 12 0 2 1072.72 862.59 72.48 o 14 0 2 849.44 819.13 77.21 o 16 0 2 49.05 51.14 23.91 o 18 0 2 261.46 281.04 53.64 o -19 1 2 0.15 27.85 14.28 o -18 1 2 127.21 164.90 28.09 o -17 1 2 48.59 63.99 24.50 o -16 1 2 17.92 4.12 17.87 o -15 1 2 7.54 22.77 13.51 o -14 1 2 298.23 319.32 32.94 o -13 1 2 207.83 243.57 27.69 o -12 1 2 321.27 292.87 47.48 o -11 1 2 553.82 417.67 32.00 o -10 1 2 656.57 637.84 30.67 o -9 1 2 325.53 369.40 22.39 o -8 1 2 1.00 3.48 5.36 o -7 1 2 3005.25 3009.46 56.62 o -6 1 2 3512.85 3495.04 57.07 o -5 1 2 384.41 439.94 17.50 o -4 1 2 281.21 244.86 14.85 o -3 1 2 7069.76 7022.72 65.96 o -2 1 2 4216.46 3882.95 133.89 o -1 1 2 10547.03 10256.91 558.33 o 0 1 2 10330.83 11093.80 187.06 o 1 1 2 10676.11 11036.23 66.03 o 2 1 2 4353.99 4241.99 47.29 o 3 1 2 3547.88 3477.95 49.87 o 4 1 2 1606.30 1817.39 69.30 o 5 1 2 1136.62 1331.84 30.40 o 6 1 2 4145.12 4239.21 60.58 o 7 1 2 80.85 45.50 21.33 o 8 1 2 571.71 653.54 29.98 o 9 1 2 703.08 710.65 33.51 o 10 1 2 30.73 42.30 13.40 o 11 1 2 110.02 133.24 20.56 o 12 1 2 449.01 448.59 37.88 o 13 1 2 191.54 142.00 22.50 o 14 1 2 777.76 730.02 90.60 o 15 1 2 78.33 83.83 20.18 o 16 1 2 19.15 43.78 16.47 o 17 1 2 7.80 4.42 9.71 o 18 1 2 0.32 15.98 13.00 o -19 2 2 20.00 15.22 20.16 o -18 2 2 27.64 33.69 15.33 o -17 2 2 2.19 -9.75 11.33 o -16 2 2 109.59 97.85 20.99 o -15 2 2 16.13 1.31 9.32 o -14 2 2 31.05 30.29 13.02 o -13 2 2 93.86 72.05 16.24 o -12 2 2 287.07 219.88 25.69 o -11 2 2 19.36 10.04 11.88 o -10 2 2 187.47 180.90 17.55 o -9 2 2 180.55 210.20 18.45 o -8 2 2 106.39 140.91 12.55 o -7 2 2 185.50 209.99 13.71 o -6 2 2 102.69 113.54 8.63 o -5 2 2 64.27 51.74 7.34 o -4 2 2 1771.76 1985.47 34.51 o -3 2 2 508.59 525.16 19.28 o -2 2 2 71.73 93.18 11.49 o -1 2 2 1360.02 1665.97 60.62 o 0 2 2 416.80 422.24 15.03 o 1 2 2 169.76 205.98 11.55 o 2 2 2 466.83 525.10 14.87 o 3 2 2 3345.08 3558.52 45.43 o 4 2 2 2096.73 2395.11 47.28 o 5 2 2 38.98 27.99 5.39 o 6 2 2 431.90 554.31 21.94 o 7 2 2 2634.78 2758.67 67.56 o 8 2 2 163.02 138.75 12.74 o 9 2 2 16.62 32.32 25.61 o 10 2 2 31.79 38.09 12.93 o 11 2 2 49.55 43.23 15.04 o 12 2 2 426.66 393.89 44.11 o 13 2 2 37.00 21.64 13.00 o 14 2 2 23.81 26.78 16.18 o 15 2 2 29.20 41.92 15.81 o 16 2 2 80.74 88.35 21.62 o 17 2 2 0.02 -2.03 33.91 o -17 3 2 0.23 35.02 16.70 o -16 3 2 4.93 2.23 21.62 o -15 3 2 10.67 39.54 13.72 o -14 3 2 0.48 6.26 9.63 o -13 3 2 72.91 82.87 26.28 o -12 3 2 14.67 11.29 17.85 o -11 3 2 0.10 -0.10 6.85 o -10 3 2 0.28 4.37 7.95 o -9 3 2 35.92 69.01 12.07 o -8 3 2 0.24 9.99 6.68 o -7 3 2 211.52 291.16 20.60 o -6 3 2 285.33 328.39 18.22 o -5 3 2 1189.68 1356.08 35.66 o -4 3 2 178.18 161.84 11.95 o -3 3 2 739.52 760.82 24.80 o -2 3 2 1361.62 1585.18 44.68 o -1 3 2 1240.58 1335.91 77.12 o 0 3 2 2899.70 3327.41 68.02 o 1 3 2 4.83 8.38 4.91 o 2 3 2 39.81 42.23 5.79 o 3 3 2 362.14 342.25 15.38 o 4 3 2 94.63 132.73 10.25 o 5 3 2 351.10 389.45 20.27 o 6 3 2 243.33 275.48 17.97 o 7 3 2 26.82 43.08 11.78 o 8 3 2 33.52 19.95 16.19 o 9 3 2 2.05 -7.19 8.62 o 10 3 2 12.82 -2.18 8.18 o 11 3 2 114.11 104.92 20.52 o 12 3 2 30.07 14.17 12.20 o 13 3 2 38.41 39.47 13.81 o 14 3 2 315.27 324.69 37.36 o 15 3 2 0.01 -10.24 15.26 o 16 3 2 145.71 215.61 34.45 o -15 4 2 43.12 6.02 21.48 o -14 4 2 0.90 -17.95 17.95 o -13 4 2 38.29 68.86 27.78 o -12 4 2 206.33 264.52 49.55 o -11 4 2 90.58 142.02 35.86 o -10 4 2 3.20 3.96 15.12 o -9 4 2 5.53 23.56 18.77 o -8 4 2 104.43 131.23 17.06 o -7 4 2 47.04 48.52 9.58 o -6 4 2 434.07 502.20 25.78 o -5 4 2 308.44 347.53 23.49 o -4 4 2 61.35 71.17 12.66 o -3 4 2 1261.87 1433.15 62.24 o -2 4 2 1.61 -6.08 6.32 o -1 4 2 941.92 1132.74 39.41 o 0 4 2 2.97 13.00 6.78 o 1 4 2 45.55 47.32 7.91 o 2 4 2 21.11 29.80 6.25 o 3 4 2 152.33 133.85 13.07 o 4 4 2 101.55 104.19 13.11 o 5 4 2 5.85 11.74 9.29 o 6 4 2 0.73 4.28 7.87 o 7 4 2 243.81 313.68 32.58 o 8 4 2 393.88 406.38 37.99 o 9 4 2 33.96 57.88 16.38 o 10 4 2 864.06 772.94 55.92 o 11 4 2 45.89 45.59 13.16 o 12 4 2 1.12 -19.14 19.14 o 13 4 2 82.45 81.00 31.33 o 14 4 2 69.57 87.03 35.54 o -12 5 2 3.81 41.12 17.22 o -11 5 2 19.45 19.64 13.87 o -10 5 2 3.63 -11.76 25.26 o -9 5 2 118.20 149.27 27.02 o -8 5 2 430.82 509.07 43.94 o -7 5 2 47.21 35.92 13.82 o -6 5 2 20.71 40.52 10.81 o -5 5 2 0.73 -0.68 7.29 o -4 5 2 235.67 258.53 35.56 o -3 5 2 74.81 99.05 17.49 o -2 5 2 49.18 61.65 37.03 o -1 5 2 491.04 565.58 57.27 o 0 5 2 7.37 3.38 9.59 o 1 5 2 24.21 5.81 6.04 o 2 5 2 145.13 139.07 16.10 o 3 5 2 58.35 92.35 14.06 o 4 5 2 98.37 134.57 16.43 o 5 5 2 85.44 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