#------------------------------------------------------------------------------ #$Date: 2012-09-11 12:26:43 +0300 (Tue, 11 Sep 2012) $ #$Revision: 66590 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/42/2234241.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2234241_Fobs loop_ _publ_author_name 'Roy, Tapashi G.' 'Palit, Debashis' 'Nath, Babul Chandra' 'Ng, Seik Weng' 'Tiekink, Edward R. T.' _publ_section_title ; cis-(Acetato-\k^2^O,O')(5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane-\k^4^N,N',N'',N''')nickel(II) perchlorate monohydrate ; _journal_coeditor_code HB6703 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m525 _journal_page_last m526 _journal_volume 68 _journal_year 2012 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 96.534 _cell_angle_gamma 90.000 _cell_length_a 9.4041 _cell_length_b 15.9593 _cell_length_c 16.0721 _exptl_crystal_F_000 1112.00 _reflns_d_resolution_high 0.7924 _[local]_cod_data_source_file hb6703Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' C2/c 15.9(6)% twin' _shelx_refln_list_code 4 _shelx_f_calc_maximum 286.47 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 17805.70 20091.02 473.74 o 4 0 0 56415.84 55954.44 252.63 o 6 0 0 10.06 9.30 5.81 o 8 0 0 545.13 692.14 25.64 o 10 0 0 233.18 155.45 14.08 o 1 1 0 13014.99 12871.36 68.96 o 3 1 0 7515.87 6255.74 46.62 o 5 1 0 9186.71 9940.06 88.04 o 7 1 0 915.57 782.79 31.16 o 9 1 0 548.84 563.15 16.42 o 11 1 0 80.13 65.57 9.45 o 0 2 0 20418.06 19490.60 80.60 o 2 2 0 259.46 264.57 14.85 o 4 2 0 10312.30 10640.08 68.77 o 6 2 0 15.58 9.22 4.54 o 8 2 0 502.80 561.07 14.99 o 10 2 0 83.01 50.37 5.96 o 1 3 0 67.62 95.49 8.82 o 3 3 0 75.79 189.30 35.44 o 5 3 0 1244.20 1353.87 33.64 o 7 3 0 0.86 -0.75 2.68 o 9 3 0 164.98 163.60 8.85 o 11 3 0 33.88 32.31 6.23 o 0 4 0 82063.55 73322.21 229.06 o 2 4 0 1440.57 1741.73 46.25 o 4 4 0 1525.25 1386.78 50.83 o 6 4 0 41.74 90.12 14.44 o 8 4 0 45.34 65.76 7.70 o 10 4 0 93.12 88.10 6.96 o 1 5 0 267.27 357.88 20.94 o 3 5 0 86.41 86.60 13.00 o 5 5 0 829.31 831.35 77.42 o 7 5 0 693.39 635.90 15.25 o 9 5 0 265.66 227.70 11.11 o 11 5 0 114.33 70.81 7.23 o 0 6 0 535.12 645.60 26.81 o 2 6 0 581.09 669.65 33.75 o 4 6 0 3347.50 3439.04 91.15 o 6 6 0 667.77 620.67 37.79 o 8 6 0 429.23 461.28 16.35 o 10 6 0 416.67 390.95 13.27 o 1 7 0 8434.75 7872.25 113.01 o 3 7 0 5692.91 5470.06 111.59 o 5 7 0 3732.65 4051.43 94.55 o 7 7 0 1005.51 1094.04 26.66 o 9 7 0 604.47 633.89 19.31 o 2 8 0 5101.15 5374.98 110.60 o 4 8 0 1697.59 1444.25 58.90 o 6 8 0 791.10 611.28 23.25 o 8 8 0 622.83 565.96 18.90 o 10 8 0 233.75 162.99 10.58 o 5 9 0 1966.06 1749.10 47.31 o 7 9 0 319.39 344.41 18.05 o 9 9 0 34.67 46.27 5.00 o 2 10 0 2829.26 2938.56 71.50 o 4 10 0 1174.27 1212.15 77.98 o 6 10 0 179.29 251.88 19.75 o 8 10 0 10.51 20.64 4.02 o 10 10 0 4.81 17.69 4.31 o 1 11 0 72.94 102.04 16.02 o 3 11 0 42.62 62.24 14.22 o 5 11 0 600.38 702.13 30.43 o 7 11 0 57.00 77.40 8.62 o 9 11 0 117.29 116.35 8.26 o 0 12 0 885.04 666.47 43.40 o 2 12 0 866.31 850.07 33.99 o 4 12 0 154.04 137.88 14.31 o 6 12 0 6.33 11.68 6.04 o 8 12 0 290.18 303.33 11.17 o 1 13 0 411.80 412.16 19.41 o 3 13 0 104.34 356.79 87.21 o 5 13 0 866.63 817.07 26.54 o 7 13 0 126.57 137.68 12.15 o 0 14 0 5930.87 6133.38 128.63 o 2 14 0 15.22 30.89 14.04 o 4 14 0 1891.81 2116.23 54.93 o 6 14 0 97.81 118.28 8.92 o 8 14 0 110.57 108.92 9.91 o 1 15 0 1031.38 1161.22 38.86 o 3 15 0 256.58 258.54 19.01 o 5 15 0 575.07 673.30 49.21 o 7 15 0 94.51 80.63 6.66 o 0 16 0 3585.04 3998.44 98.85 o 2 16 0 806.41 880.91 48.71 o 4 16 0 2312.72 2084.55 48.08 o 6 16 0 496.90 415.10 13.91 o 1 17 0 270.55 210.29 14.57 o 3 17 0 413.37 479.31 32.01 o 5 17 0 306.55 331.28 15.67 o 0 18 0 249.62 240.38 19.54 o 2 18 0 65.89 69.12 11.66 o 4 18 0 29.83 23.11 5.91 o 1 19 0 115.20 95.75 10.83 o 3 19 0 83.87 113.59 11.26 o -11 1 1 1.80 1.77 2.68 o -9 1 1 14.35 17.70 3.26 o -7 1 1 30.46 28.94 7.13 o -5 1 1 293.98 324.85 15.88 o -3 1 1 11.72 45.60 4.63 o -1 1 1 27668.94 24715.07 85.16 o 1 1 1 6007.30 6870.77 59.80 o 3 1 1 713.70 687.83 11.34 o 5 1 1 703.22 748.53 19.50 o 7 1 1 21.12 28.44 3.53 o 9 1 1 7.18 35.26 14.51 o 11 1 1 6.49 5.17 2.64 o -10 2 1 439.72 391.54 13.55 o -8 2 1 788.27 707.60 16.42 o -6 2 1 115.69 204.79 14.54 o -4 2 1 1085.42 999.85 23.48 o -2 2 1 22376.76 22939.04 144.15 o 0 2 1 8629.32 8975.02 56.99 o 2 2 1 4482.59 4711.33 111.01 o 4 2 1 12031.81 13903.76 77.20 o 6 2 1 194.22 149.07 34.09 o 8 2 1 46.19 57.54 5.18 o 10 2 1 408.01 436.77 15.94 o -11 3 1 89.18 87.65 7.96 o -9 3 1 940.19 1034.28 21.69 o -7 3 1 1369.06 1277.89 21.24 o -5 3 1 15081.76 16103.08 131.83 o -3 3 1 4792.77 5259.94 65.56 o -1 3 1 25864.10 24012.55 94.29 o 1 3 1 454.34 607.03 13.02 o 3 3 1 780.16 659.28 19.98 o 5 3 1 1898.19 1999.36 44.53 o 7 3 1 374.82 415.92 12.17 o 9 3 1 605.07 700.39 19.60 o 11 3 1 133.88 92.64 10.59 o -10 4 1 989.82 949.43 22.14 o -8 4 1 2410.24 2593.68 37.59 o -6 4 1 1792.06 1827.40 104.85 o -4 4 1 4974.21 4503.46 131.39 o -2 4 1 1038.03 1277.80 39.94 o 0 4 1 8029.38 8259.83 76.05 o 2 4 1 339.70 318.31 12.72 o 4 4 1 414.33 469.13 19.20 o 6 4 1 434.89 447.90 31.16 o 8 4 1 1018.00 1065.70 22.69 o 10 4 1 540.28 499.64 16.03 o -11 5 1 272.23 282.59 19.18 o -9 5 1 1712.57 1794.27 41.20 o -7 5 1 1349.65 986.25 18.57 o -5 5 1 9007.99 8362.78 114.76 o -3 5 1 717.04 603.31 32.99 o -1 5 1 2821.94 2814.07 34.99 o 1 5 1 4353.44 4585.00 73.30 o 3 5 1 19.31 96.66 18.41 o 5 5 1 3583.60 3902.28 57.84 o 7 5 1 1134.40 1069.27 21.62 o 9 5 1 1616.84 1668.65 29.63 o 11 5 1 315.61 241.09 14.04 o -10 6 1 247.25 212.40 11.35 o -8 6 1 659.50 771.40 22.41 o -6 6 1 1592.16 1880.15 65.93 o -4 6 1 1731.78 1540.98 52.94 o -2 6 1 579.78 459.32 38.86 o 0 6 1 1019.36 1495.07 41.71 o 2 6 1 365.96 302.71 21.46 o 4 6 1 194.77 237.18 26.78 o 6 6 1 721.62 734.11 40.84 o 8 6 1 1260.49 1307.72 26.39 o 10 6 1 157.61 161.85 8.51 o -11 7 1 167.50 147.11 11.47 o -9 7 1 117.27 113.89 7.37 o -7 7 1 183.19 188.50 13.77 o -5 7 1 686.94 555.44 34.63 o -1 7 1 84.33 150.51 12.79 o 1 7 1 1114.61 1203.10 45.37 o 3 7 1 52.52 221.49 25.91 o 5 7 1 459.89 422.17 21.43 o 7 7 1 82.39 74.69 7.37 o 9 7 1 144.17 120.09 8.44 o -10 8 1 2.17 4.31 6.55 o -8 8 1 27.47 21.62 4.45 o -6 8 1 92.71 58.73 7.53 o -4 8 1 6.33 6.43 4.35 o 0 8 1 2371.29 2504.36 62.98 o 2 8 1 1737.24 1819.77 38.45 o 4 8 1 7.72 10.13 7.59 o 6 8 1 84.96 66.91 8.19 o 8 8 1 9.17 11.48 3.24 o 10 8 1 133.93 110.08 7.15 o -9 9 1 221.08 249.32 9.60 o -7 9 1 169.09 228.90 12.36 o -5 9 1 539.03 477.11 20.59 o -3 9 1 1629.78 2025.16 74.82 o 1 9 1 3312.29 3533.07 58.57 o 3 9 1 6.99 21.05 16.36 o 5 9 1 187.31 167.19 10.61 o 7 9 1 383.77 310.40 17.21 o 9 9 1 233.98 234.44 12.38 o -10 10 1 113.96 65.32 8.33 o -8 10 1 146.22 151.64 9.29 o -6 10 1 185.34 207.99 17.86 o -4 10 1 1823.33 1755.30 72.00 o -2 10 1 1094.82 1021.74 52.65 o 0 10 1 2292.92 2007.04 67.35 o 2 10 1 1313.91 1376.05 63.15 o 4 10 1 2035.56 2085.97 133.53 o 6 10 1 220.46 250.46 19.72 o 8 10 1 364.26 386.36 15.00 o -9 11 1 535.18 538.56 19.61 o -7 11 1 81.73 116.57 10.14 o -5 11 1 1019.43 1059.08 31.31 o -3 11 1 5.72 24.02 7.37 o -1 11 1 4667.37 5002.61 117.41 o 1 11 1 1118.87 1216.96 52.11 o 3 11 1 1015.16 1112.20 37.58 o 5 11 1 595.36 627.41 25.39 o 7 11 1 291.88 307.69 16.56 o 9 11 1 129.95 176.17 9.94 o -8 12 1 842.02 791.51 17.98 o -6 12 1 469.38 390.84 18.48 o -4 12 1 2644.76 2406.04 84.92 o -2 12 1 292.84 441.50 92.02 o 0 12 1 5285.32 5380.98 121.49 o 2 12 1 14.64 8.16 5.22 o 4 12 1 3055.69 2886.62 64.79 o 6 12 1 524.02 652.68 34.01 o 8 12 1 535.95 523.57 12.80 o -7 13 1 691.48 716.17 26.26 o -5 13 1 2572.91 2699.66 62.28 o -3 13 1 2113.83 2164.85 55.33 o -1 13 1 4776.07 4674.41 58.54 o 1 13 1 2916.71 2972.22 52.32 o 3 13 1 2881.48 2798.34 63.62 o 5 13 1 1328.45 1372.81 43.54 o 7 13 1 216.87 230.62 13.49 o -8 14 1 379.76 343.10 18.54 o -6 14 1 275.73 315.21 14.49 o -4 14 1 249.35 271.77 19.97 o -2 14 1 142.66 162.93 16.06 o 0 14 1 24.92 27.46 9.04 o 2 14 1 206.12 185.94 16.92 o 4 14 1 60.53 76.33 10.75 o 6 14 1 109.04 118.37 8.87 o 8 14 1 342.93 246.09 13.36 o -7 15 1 220.59 173.73 11.51 o -5 15 1 340.41 298.03 18.51 o -3 15 1 177.53 245.65 18.26 o -1 15 1 37.80 37.37 7.60 o 1 15 1 110.98 94.17 11.09 o 3 15 1 0.39 3.11 4.57 o 5 15 1 101.17 82.10 48.62 o 7 15 1 130.21 112.10 7.87 o -6 16 1 181.88 158.15 10.96 o -4 16 1 30.52 30.11 6.07 o -2 16 1 14.39 99.45 22.64 o 0 16 1 1802.40 1940.62 48.63 o 2 16 1 41.22 107.95 21.74 o 4 16 1 684.70 715.72 38.93 o 6 16 1 17.66 24.73 5.53 o -5 17 1 346.38 308.77 15.70 o -3 17 1 441.67 488.25 32.51 o -1 17 1 1044.05 1061.62 32.49 o 1 17 1 1127.21 1124.87 32.80 o 3 17 1 781.87 758.60 39.48 o 5 17 1 420.32 350.03 13.99 o -4 18 1 418.76 442.67 16.21 o -2 18 1 24.60 26.19 8.19 o 0 18 1 615.42 572.41 21.13 o 2 18 1 29.26 54.03 10.86 o 4 18 1 215.88 237.84 16.56 o -3 19 1 367.80 376.18 19.21 o -1 19 1 335.98 363.38 20.37 o 1 19 1 228.57 216.37 16.13 o 3 19 1 270.92 257.31 15.59 o -10 0 2 916.71 784.60 24.28 o -8 0 2 1148.21 1089.73 24.15 o -6 0 2 149.12 78.79 12.90 o -4 0 2 823.75 678.37 25.55 o -2 0 2 9883.82 9348.59 59.23 o 2 0 2 22849.03 23746.77 82.39 o 4 0 2 25613.43 26575.33 304.14 o 6 0 2 2148.11 2286.88 69.57 o 8 0 2 238.87 311.45 17.62 o 10 0 2 85.32 307.69 26.91 o -11 1 2 96.26 83.38 12.77 o -9 1 2 609.30 560.41 15.83 o -7 1 2 35.16 70.82 9.44 o -5 1 2 3136.29 2932.78 46.78 o -3 1 2 56.11 30.62 2.57 o -1 1 2 9800.93 10419.24 31.72 o 1 1 2 42.38 154.52 4.17 o 3 1 2 15187.38 15906.81 65.86 o 5 1 2 2255.43 2253.01 41.40 o 7 1 2 1843.92 1732.92 23.57 o 9 1 2 331.05 309.62 12.36 o 11 1 2 216.24 175.70 10.82 o -10 2 2 330.76 321.35 12.04 o -8 2 2 6.66 63.76 18.13 o -6 2 2 1902.15 1838.06 42.61 o -4 2 2 1839.84 1879.96 30.02 o -2 2 2 8599.24 8249.52 57.56 o 0 2 2 6991.88 6981.15 56.56 o 2 2 2 10977.58 11282.56 42.64 o 4 2 2 4472.30 4307.51 63.39 o 6 2 2 1428.74 1429.69 39.57 o 8 2 2 293.81 348.33 12.08 o 10 2 2 47.63 96.67 8.87 o -11 3 2 5.70 4.03 2.49 o -9 3 2 83.03 140.15 8.01 o -7 3 2 36.15 21.61 3.37 o -5 3 2 4657.92 4627.99 83.48 o -3 3 2 191.95 238.54 10.51 o -1 3 2 37071.53 34696.84 122.02 o 1 3 2 4259.41 4750.75 37.83 o 3 3 2 3033.84 2875.00 39.67 o 5 3 2 148.23 180.16 10.74 o 7 3 2 310.16 315.24 10.94 o 9 3 2 5.97 10.72 3.13 o 11 3 2 1.07 -0.81 2.34 o -10 4 2 2.25 5.88 3.13 o -8 4 2 716.92 945.17 33.03 o -6 4 2 236.61 189.47 14.42 o -4 4 2 478.55 545.81 18.91 o -2 4 2 937.89 1026.37 45.13 o 0 4 2 10862.90 11273.38 143.42 o 2 4 2 7.46 64.33 42.82 o 4 4 2 1526.70 1615.69 35.58 o 6 4 2 75.54 110.03 55.38 o 8 4 2 107.71 90.07 7.51 o 10 4 2 0.39 27.40 4.94 o -11 5 2 11.02 7.53 2.86 o -9 5 2 125.70 118.45 14.80 o -7 5 2 6.88 5.02 2.23 o -5 5 2 452.96 361.42 24.30 o -3 5 2 1619.02 1357.48 44.20 o -1 5 2 1882.81 2374.03 32.24 o 1 5 2 2742.83 2685.22 49.29 o 3 5 2 126.10 151.31 17.05 o 5 5 2 221.25 239.73 16.51 o 7 5 2 31.13 25.04 3.84 o 9 5 2 341.70 361.24 13.73 o 11 5 2 41.22 50.84 6.48 o -10 6 2 427.76 477.43 22.09 o -8 6 2 516.62 549.18 18.93 o -6 6 2 2755.49 2799.16 81.93 o -4 6 2 3733.29 3715.03 82.80 o -2 6 2 177.63 165.61 10.55 o 0 6 2 1919.98 1877.46 47.49 o 2 6 2 966.69 1033.86 173.11 o 4 6 2 3463.86 3319.28 106.36 o 6 6 2 1255.83 1260.32 25.30 o 8 6 2 686.00 775.27 20.87 o 10 6 2 193.80 243.07 11.93 o -11 7 2 19.25 5.88 2.67 o -9 7 2 936.90 1042.27 23.53 o -7 7 2 239.26 327.97 14.36 o -5 7 2 12107.00 10486.55 150.71 o -3 7 2 2172.90 1558.07 56.10 o -1 7 2 25083.28 25970.12 132.33 o 1 7 2 10247.60 9839.43 84.64 o 3 7 2 3583.29 3535.17 93.71 o 5 7 2 3676.19 3846.90 67.86 o 7 7 2 506.23 490.01 18.57 o 9 7 2 723.15 713.50 19.58 o -10 8 2 344.70 315.38 17.55 o -8 8 2 261.54 207.50 10.18 o -6 8 2 603.85 418.53 16.28 o -4 8 2 1110.65 955.19 48.08 o -2 8 2 2423.43 2565.30 74.07 o 0 8 2 6476.98 7120.48 108.61 o 2 8 2 2491.31 2644.49 135.60 o 4 8 2 4135.84 4229.38 115.21 o 6 8 2 1927.07 1853.18 40.17 o 8 8 2 1337.53 1301.69 29.29 o 10 8 2 313.99 352.21 12.29 o -9 9 2 370.74 363.79 18.16 o -7 9 2 63.93 96.51 9.92 o -5 9 2 2164.05 2096.79 52.35 o -3 9 2 517.73 512.62 36.57 o -1 9 2 3730.57 3446.17 55.39 o 1 9 2 3115.65 2551.82 50.01 o 3 9 2 6075.64 5730.32 132.46 o 5 9 2 3899.66 3935.61 57.40 o 7 9 2 248.94 229.89 19.21 o 9 9 2 160.93 139.14 9.43 o -10 10 2 83.26 82.47 9.27 o -8 10 2 19.50 37.11 5.66 o -6 10 2 643.76 547.20 28.89 o -4 10 2 923.57 826.02 33.59 o -2 10 2 1398.44 1209.87 57.18 o 0 10 2 11193.57 11481.09 112.62 o 2 10 2 2973.76 3415.51 101.95 o 4 10 2 1958.72 1981.83 51.35 o 6 10 2 52.37 82.90 11.36 o 8 10 2 0.49 -2.59 2.59 o -9 11 2 58.31 41.54 4.46 o -7 11 2 85.44 133.84 10.67 o -5 11 2 2882.54 3027.34 56.33 o -3 11 2 553.25 664.06 47.52 o -1 11 2 1427.30 1373.70 61.27 o 1 11 2 23.49 22.97 6.11 o 3 11 2 213.81 147.99 12.18 o 5 11 2 887.71 886.72 32.94 o 7 11 2 6.35 6.68 3.21 o 9 11 2 4.01 1.56 1.60 o -8 12 2 28.88 111.88 28.60 o -6 12 2 187.85 175.58 12.63 o -4 12 2 353.90 416.95 24.84 o -2 12 2 18.42 29.58 7.06 o 0 12 2 505.57 540.61 26.14 o 2 12 2 133.69 154.71 20.63 o 4 12 2 5.64 4.11 4.36 o 6 12 2 68.09 89.24 11.83 o 8 12 2 231.05 275.59 14.01 o -7 13 2 60.11 87.37 11.49 o -5 13 2 1327.52 1267.47 42.77 o -3 13 2 268.86 699.90 151.14 o -1 13 2 2121.31 2043.45 37.41 o 1 13 2 186.62 134.16 13.28 o 3 13 2 1097.16 1211.44 78.68 o 5 13 2 396.64 397.41 33.92 o 7 13 2 75.97 70.68 8.94 o -8 14 2 186.14 192.46 10.72 o -6 14 2 58.61 74.40 7.13 o -4 14 2 752.63 733.15 32.39 o -2 14 2 266.76 257.39 17.93 o 0 14 2 1986.37 2158.68 53.91 o 2 14 2 296.03 290.62 47.45 o 4 14 2 1008.97 1108.93 40.66 o 6 14 2 69.90 87.63 10.38 o 8 14 2 92.01 130.22 9.61 o -7 15 2 112.20 122.91 9.79 o -5 15 2 191.05 213.78 25.15 o -3 15 2 1.55 6.83 3.97 o -1 15 2 164.97 188.08 16.07 o 1 15 2 56.00 101.93 12.64 o 3 15 2 609.75 707.56 43.92 o 5 15 2 257.97 296.60 23.35 o 7 15 2 314.04 297.56 12.43 o -6 16 2 608.44 577.92 15.86 o -4 16 2 1629.09 1688.56 42.49 o -2 16 2 955.47 954.03 31.69 o 0 16 2 1684.43 1778.67 46.30 o 2 16 2 388.43 411.69 32.48 o 4 16 2 357.74 304.50 24.80 o 6 16 2 149.87 119.85 11.92 o -5 17 2 531.90 499.19 18.27 o -3 17 2 255.09 368.42 29.04 o -1 17 2 451.08 409.16 20.12 o 1 17 2 209.79 188.16 13.26 o 3 17 2 150.42 163.84 18.42 o 5 17 2 130.35 91.29 7.27 o -4 18 2 1.36 1.08 1.91 o -2 18 2 142.11 145.76 16.02 o 0 18 2 9.32 4.88 3.03 o 2 18 2 150.51 140.79 15.58 o 4 18 2 20.65 27.22 5.81 o -3 19 2 126.93 157.68 12.48 o -1 19 2 290.37 265.85 25.75 o 1 19 2 260.39 186.98 14.90 o 3 19 2 159.44 149.11 11.46 o -11 1 3 23.88 31.95 7.88 o -9 1 3 207.64 181.46 8.19 o -7 1 3 132.25 160.31 13.86 o -5 1 3 182.36 237.71 13.29 o -3 1 3 2555.30 2516.71 43.90 o -1 1 3 437.08 394.31 14.36 o 1 1 3 133.79 199.77 5.45 o 3 1 3 741.55 543.21 11.36 o 5 1 3 647.56 874.48 22.27 o 7 1 3 5.64 19.03 3.08 o 9 1 3 28.98 45.88 5.16 o 11 1 3 0.14 9.51 4.43 o -10 2 3 430.44 385.11 18.34 o -8 2 3 863.02 840.82 19.33 o -6 2 3 55.76 171.63 23.83 o -4 2 3 298.39 224.80 37.77 o -2 2 3 20344.51 17685.00 68.99 o 0 2 3 17105.76 17572.78 98.96 o 2 2 3 4704.85 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