#------------------------------------------------------------------------------ #$Date: 2012-09-11 12:26:43 +0300 (Tue, 11 Sep 2012) $ #$Revision: 66590 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/42/2234248.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2234248_Fobs loop_ _publ_author_name 'Dinake, Pogisego' 'Prokhorova, Polina E.' 'Talanov, Vladimir S.' 'Butcher, Ray J.' 'Talanova, Galina G.' _publ_section_title ; Aqua(\m-cone-26,28-dibutoxy-25,27-bis{N-[5-(dimethylamino)naphthalene-1-sulfonyl]carbamoylmethoxy}-5,11,17,23-tetrakis(1,1-dimethylethyl)calix[4]arene(2{-}))disodium acetonitrile tetrasolvate ; _journal_coeditor_code HG5188 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m460 _journal_page_last m461 _journal_volume 68 _journal_year 2012 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 81.799 _cell_angle_beta 87.108 _cell_angle_gamma 64.007 _cell_length_a 18.92640 _cell_length_b 19.3850 _cell_length_c 26.0062 _exptl_crystal_F_000 3176.00 _reflns_d_resolution_high 0.7709 _[local]_cod_data_source_file hg5188Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' dinake10 ' _shelx_refln_list_code 4 _shelx_f_calc_maximum 500.08 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz x,y,z -x,-y,-z loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status _refln_sint/lambda 2 0 0 59462.78 48502.84 635.87 o 0.05879 3 0 0 9009.62 5609.72 71.71 o 0.08818 6 0 0 1896.36 1202.93 28.48 o 0.17636 7 0 0 1747.99 1659.45 47.34 o 0.20576 8 0 0 3956.79 5336.53 106.24 o 0.23515 9 0 0 458.88 434.28 25.95 o 0.26454 10 0 0 26.97 20.28 10.77 o 0.29394 11 0 0 2101.37 2172.02 89.15 o 0.32333 12 0 0 1582.33 1407.51 73.46 o 0.35273 13 0 0 158.21 129.04 12.17 o 0.38212 14 0 0 9.96 7.09 8.49 o 0.41151 15 0 0 57.40 41.75 10.76 o 0.44091 16 0 0 336.54 302.58 20.39 o 0.47030 17 0 0 222.19 171.19 16.27 o 0.49969 18 0 0 57.54 50.62 12.26 o 0.52909 19 0 0 16.39 15.95 10.18 o 0.55848 20 0 0 142.03 144.99 16.03 o 0.58788 20 -1 0 1.98 9.45 10.39 o 0.60107 19 -1 0 24.89 10.13 10.21 o 0.57170 18 -1 0 16.78 7.43 10.77 o 0.54234 17 -1 0 641.98 608.04 32.44 o 0.51298 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274.18 18.70 o 0.52502 17 18 2 678.00 704.24 28.61 o 0.53928 18 18 2 130.14 130.65 15.87 o 0.55474 19 18 2 189.77 180.41 26.45 o 0.57129 20 18 2 10.01 12.28 14.17 o 0.58884 21 18 2 14.27 17.00 12.28 o 0.60731 22 18 2 27.77 19.84 9.45 o 0.62662 -4 19 2 652.69 674.40 24.04 o 0.60713 -3 19 2 23.29 14.90 9.95 o 0.59033 -2 19 2 250.35 310.81 24.47 o 0.57454 -1 19 2 773.33 894.66 43.65 o 0.55985 0 19 2 8.62 5.19 12.69 o 0.54634 1 19 2 367.22 371.84 31.05 o 0.53412 2 19 2 90.48 49.80 16.54 o 0.52326 3 19 2 59.22 89.73 28.34 o 0.51385 4 19 2 35.10 47.23 21.72 o 0.50598 5 19 2 2.89 6.61 17.95 o 0.49972 6 19 2 810.60 864.98 41.93 o 0.49513 7 19 2 834.20 792.41 40.88 o 0.49225 8 19 2 1343.56 1429.08 56.00 o 0.49112 9 19 2 92.47 110.81 16.66 o 0.49174 10 19 2 585.01 601.37 35.38 o 0.49412 11 19 2 446.70 319.03 25.71 o 0.49822 12 19 2 20.14 41.56 18.89 o 0.50400 13 19 2 42.83 55.73 20.78 o 0.51142 14 19 2 668.84 666.88 34.35 o 0.52039 15 19 2 54.88 43.92 10.25 o 0.53083 16 19 2 648.27 521.15 24.38 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718.00 638.89 33.49 o 0.56799 -4 6 27 554.72 535.55 43.45 o 0.55750 -3 6 27 1.19 0.94 15.11 o 0.54838 -2 6 27 0.81 0.00 15.11 o 0.54071 -1 6 27 219.71 221.02 34.00 o 0.53454 0 6 27 273.67 204.02 34.00 o 0.52994 1 6 27 278.96 299.42 37.78 o 0.52694 2 6 27 136.21 119.01 26.45 o 0.52557 3 6 27 0.31 0.82 9.95 o 0.52584 4 6 27 326.13 378.14 27.36 o 0.52774 5 6 27 20.70 1.50 11.67 o 0.53128 6 6 27 360.46 416.82 28.38 o 0.53640 7 6 27 37.84 9.45 16.06 o 0.54306 8 6 27 146.63 108.62 25.50 o 0.55122 9 6 27 195.36 258.80 33.06 o 0.56080 10 6 27 24.70 38.08 11.12 o 0.57173 11 6 27 77.29 86.10 13.39 o 0.58394 12 6 27 15.47 39.88 9.95 o 0.59734 13 6 27 68.02 106.72 11.67 o 0.61187 8 -7 -27 48.35 69.13 10.44 o 0.61740 -7 7 27 169.29 166.92 14.51 o 0.60286 -6 7 27 35.61 17.08 9.67 o 0.58943 -5 7 27 112.18 118.13 15.32 o 0.57719 -4 7 27 3.09 0.00 14.17 o 0.56621 -3 7 27 141.32 131.29 24.56 o 0.55657 -2 7 27 0.10 0.00 17.95 o 0.54833 -1 7 27 550.50 440.15 42.50 o 0.54157 0 7 27 180.73 186.07 29.28 o 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196.46 28.34 o 0.54758 8 8 27 4.51 55.73 19.84 o 0.55433 9 8 27 10.15 9.45 15.11 o 0.56254 10 8 27 31.47 27.39 17.95 o 0.57214 11 8 27 612.55 675.34 46.28 o 0.58307 12 8 27 88.69 165.88 15.68 o 0.59525 13 8 27 177.83 201.80 15.68 o 0.60861 -6 9 27 522.35 624.95 25.55 o 0.61239 -5 9 27 511.84 492.11 25.66 o 0.59937 -4 9 27 82.43 110.25 15.19 o 0.58755 -3 9 27 440.37 426.93 37.78 o 0.57697 -2 9 27 349.85 442.04 39.67 o 0.56773 -1 9 27 0.82 0.94 15.11 o 0.55988 0 9 27 260.70 210.63 31.17 o 0.55347 1 9 27 229.49 179.46 28.34 o 0.54858 2 9 27 82.23 94.45 23.61 o 0.54522 3 9 27 216.17 188.91 29.28 o 0.54343 4 9 27 54.76 50.17 11.97 o 0.54324 5 9 27 2.88 4.72 10.02 o 0.54463 6 9 27 42.79 21.75 11.80 o 0.54759 7 9 27 297.76 393.87 37.78 o 0.55211 8 9 27 140.70 144.51 24.56 o 0.55814 9 9 27 790.76 790.57 52.89 o 0.56564 10 9 27 97.02 85.95 20.78 o 0.57455 11 9 27 1.77 0.94 15.11 o 0.58479 12 9 27 1035.21 1011.60 53.84 o 0.59632 13 9 27 68.87 73.94 10.88 o 0.60904 14 9 27 39.59 8.50 8.50 o 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251.73 355.14 28.34 o 0.60215 10 14 27 131.75 155.85 19.84 o 0.60747 11 14 27 27.03 4.72 9.45 o 0.61416 12 14 27 1.19 4.72 8.50 o 0.62217 2 15 27 15.49 35.89 10.39 o 0.62019 3 15 27 16.19 7.56 8.50 o 0.61501 4 15 27 74.57 45.34 10.39 o 0.61120 8 15 27 102.17 85.01 14.17 o 0.61006 9 15 27 385.67 506.27 30.23 o 0.61330 10 15 27 433.00 401.43 26.45 o 0.61793 11 15 27 3.33 5.67 9.45 o 0.62391 8 8 -28 11.51 8.50 10.39 o 0.62266 7 8 -28 2.68 0.94 11.33 o 0.61734 -6 -8 28 3.75 0.00 7.26 o 0.61339 -5 -8 28 2.34 10.96 6.80 o 0.61084 -4 -8 28 164.15 116.36 12.23 o 0.60969 -3 -8 28 34.60 17.95 11.33 o 0.60995 -2 -8 28 1.19 0.00 11.33 o 0.61163 -1 -8 28 79.24 60.45 15.11 o 0.61472 9 7 -28 176.93 169.07 19.84 o 0.62120 8 7 -28 90.00 87.84 17.00 o 0.61387 -7 -7 28 10.85 11.39 6.99 o 0.60787 -6 -7 28 102.83 99.82 12.48 o 0.60324 -5 -7 28 457.41 383.73 22.59 o 0.60002 -4 -7 28 86.40 80.76 12.02 o 0.59823 -3 -7 28 17.14 18.96 9.00 o 0.59788 -2 -7 28 82.43 91.62 18.89 o 0.59898 -1 -7 28 131.98 116.01 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42.50 12.28 o 0.61767 10 0 -28 1.87 17.95 10.39 o 0.61477 9 0 -28 0.19 16.83 8.33 o 0.60163 -8 0 28 43.18 32.36 7.29 o 0.58966 -7 0 28 616.49 663.76 24.65 o 0.57894 -6 0 28 1048.06 942.79 39.81 o 0.56954 -5 0 28 209.46 261.92 22.01 o 0.56152 -4 0 28 35.00 26.93 11.80 o 0.55495 -3 0 28 88.16 76.51 20.78 o 0.54987 -2 0 28 22.17 0.00 19.84 o 0.54632 -1 0 28 1.18 0.94 17.00 o 0.54434 0 0 28 0.56 0.00 18.89 o 0.54395 1 0 28 32.30 14.62 11.33 o 0.54514 2 0 28 175.81 197.75 20.65 o 0.54790 3 0 28 1.34 2.91 11.12 o 0.55223 4 0 28 10.71 14.51 9.95 o 0.55806 5 0 28 51.64 47.56 12.64 o 0.56537 6 0 28 112.38 85.95 14.03 o 0.57409 7 0 28 84.20 34.00 16.06 o 0.58416 8 0 28 846.10 979.48 56.67 o 0.59552 9 0 28 462.89 489.27 35.89 o 0.60808 10 -1 -28 5.08 10.39 11.33 o 0.61804 9 -1 -28 79.49 95.60 11.67 o 0.60436 -8 1 28 0.66 7.02 6.27 o 0.59182 -7 1 28 134.57 92.34 10.88 o 0.58050 -6 1 28 143.39 142.13 13.28 o 0.57047 -5 1 28 5.81 6.14 10.02 o 0.56181 -4 1 28 1000.37 1189.17 46.08 o 0.55457 -3 1 28 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11.00 o 0.54808 5 2 28 218.87 189.79 20.00 o 0.55418 6 2 28 449.66 445.44 28.33 o 0.56175 7 2 28 522.24 644.17 49.12 o 0.57074 8 2 28 379.90 329.64 35.89 o 0.58108 9 2 28 2.38 0.00 16.06 o 0.59270 10 2 28 58.62 104.35 13.01 o 0.60552 10 -3 -28 13.61 23.61 9.45 o 0.62854 9 -3 -28 0.27 8.34 6.99 o 0.61389 -8 3 28 3.20 0.00 7.69 o 0.60031 -7 3 28 51.45 34.68 9.28 o 0.58790 -6 3 28 49.37 47.78 11.53 o 0.57671 -5 3 28 13.75 11.09 11.00 o 0.56683 -4 3 28 95.50 110.62 15.86 o 0.55833 -3 3 28 76.29 82.17 22.67 o 0.55126 -2 3 28 68.19 21.72 16.06 o 0.54569 -1 3 28 38.86 47.23 18.89 o 0.54166 0 3 28 76.52 89.73 22.67 o 0.53920 1 3 28 5.10 0.00 17.00 o 0.53833 2 3 28 551.07 404.41 27.84 o 0.53908 3 3 28 242.82 248.99 22.37 o 0.54141 4 3 28 16.07 2.51 10.34 o 0.54533 5 3 28 94.99 91.34 15.68 o 0.55079 6 3 28 0.68 6.14 10.69 o 0.55774 7 3 28 12.50 18.89 17.00 o 0.56614 8 3 28 0.38 1.89 16.06 o 0.57592 9 3 28 368.39 480.77 40.61 o 0.58701 10 3 28 27.91 7.56 14.17 o 0.59933 11 3 28 180.04 145.09 12.91 o 0.61282 9 -4 -28 8.78 5.66 6.58 o 0.62063 8 -4 -28 6.84 8.00 8.61 o 0.60659 -7 4 28 24.71 35.65 9.53 o 0.59368 -6 4 28 23.77 27.41 9.67 o 0.58197 -5 4 28 109.30 106.84 15.60 o 0.57154 -4 4 28 1.82 17.76 9.95 o 0.56244 -3 4 28 6.30 0.00 14.17 o 0.55476 -2 4 28 468.18 504.38 44.39 o 0.54854 -1 4 28 270.39 252.19 32.11 o 0.54385 0 4 28 5.79 4.72 17.00 o 0.54072 1 4 28 357.79 306.97 36.84 o 0.53917 2 4 28 4.84 23.73 11.30 o 0.53922 3 4 28 30.33 40.93 12.34 o 0.54087 4 4 28 18.89 17.40 11.56 o 0.54411 5 4 28 1654.14 1738.02 59.43 o 0.54890 6 4 28 1.13 11.33 10.44 o 0.55521 7 4 28 1.81 3.78 16.06 o 0.56299 8 4 28 21.28 27.39 17.00 o 0.57217 9 4 28 16.39 38.73 17.00 o 0.58270 10 4 28 0.41 0.00 15.11 o 0.59449 11 4 28 15.41 0.94 12.28 o 0.60747 12 4 28 22.89 20.78 11.33 o 0.62158 8 -5 -28 72.39 41.53 9.26 o 0.61418 -7 5 28 506.81 476.56 23.53 o 0.60081 -6 5 28 44.38 57.65 11.33 o 0.58861 -5 5 28 102.23 136.70 16.27 o 0.57765 -4 5 28 64.23 40.21 12.34 o 0.56800 -3 5 28 152.25 116.18 23.61 o 0.55973 -2 5 28 48.82 63.28 20.78 o 0.55290 -1 5 28 216.40 242.75 32.11 o 0.54757 0 5 28 95.63 118.07 25.50 o 0.54377 1 5 28 19.20 14.17 15.11 o 0.54155 2 5 28 19.04 15.11 16.06 o 0.54092 3 5 28 153.44 105.70 15.68 o 0.54188 4 5 28 15.36 21.31 11.97 o 0.54443 5 5 28 849.02 890.29 40.40 o 0.54854 6 5 28 31.57 12.43 10.30 o 0.55419 7 5 28 46.90 109.57 22.67 o 0.56132 8 5 28 327.99 315.47 34.95 o 0.56988 9 5 28 202.58 183.24 27.39 o 0.57980 10 5 28 8.50 0.00 14.17 o 0.59102 11 5 28 204.96 222.91 25.50 o 0.60347 12 5 28 48.52 27.39 12.28 o 0.61706 8 -6 -28 21.01 15.26 7.49 o 0.62301 -7 6 28 73.44 39.20 8.68 o 0.60923 -6 6 28 734.03 829.42 33.21 o 0.59658 -5 6 28 117.87 96.79 13.98 o 0.58514 -4 6 28 1.00 3.21 9.95 o 0.57497 -3 6 28 108.27 122.79 23.61 o 0.56615 -2 6 28 205.25 192.68 29.28 o 0.55873 -1 6 28 196.95 231.41 31.17 o 0.55278 0 6 28 214.67 249.36 33.06 o 0.54835 1 6 28 327.00 336.25 36.84 o 0.54546 2 6 28 465.69 446.76 42.50 o 0.54415 3 6 28 104.16 70.24 12.91 o 0.54443 4 6 28 439.64 404.51 26.99 o 0.54628 5 6 28 19.04 14.98 11.67 o 0.54971 6 6 28 0.01 5.69 9.53 o 0.55468 7 6 28 267.59 274.86 32.11 o 0.56114 8 6 28 60.79 84.06 19.84 o 0.56905 9 6 28 12.43 38.73 17.00 o 0.57835 10 6 28 135.70 91.85 12.71 o 0.58896 11 6 28 19.85 8.89 7.51 o 0.60083 12 6 28 69.58 101.07 17.00 o 0.61388 7 -7 -28 3.79 6.84 6.99 o 0.61890 -6 7 28 96.29 84.87 11.80 o 0.60584 -5 7 28 119.04 104.86 13.98 o 0.59395 -4 7 28 2.47 0.57 9.53 o 0.58329 -3 7 28 65.71 81.23 19.84 o 0.57395 -2 7 28 659.89 783.96 52.89 o 0.56598 -1 7 28 10.98 18.89 17.00 o 0.55945 0 7 28 75.49 70.84 20.78 o 0.55440 1 7 28 37.90 37.78 17.00 o 0.55087 2 7 28 8.80 12.28 16.06 o 0.54890 3 7 28 3.78 21.00 10.44 o 0.54849 4 7 28 20.94 9.01 10.21 o 0.54966 5 7 28 117.08 111.67 15.68 o 0.55240 6 7 28 2.07 0.00 10.34 o 0.55667 7 7 28 0.31 0.00 14.17 o 0.56245 8 7 28 0.70 0.94 14.17 o 0.56969 9 7 28 3.58 37.78 17.00 o 0.57834 10 7 28 296.33 290.58 19.74 o 0.58833 11 7 28 264.23 174.31 14.97 o 0.59959 12 7 28 41.87 52.89 15.11 o 0.61206 13 7 28 184.42 231.41 19.84 o 0.62566 -6 8 28 147.41 126.17 11.53 o 0.61631 -5 8 28 110.83 99.21 12.91 o 0.60401 -4 8 28 29.37 42.98 10.69 o 0.59292 -3 8 28 451.57 594.11 42.50 o 0.58309 -2 8 28 0.21 13.22 14.17 o 0.57461 -1 8 28 35.62 50.06 17.95 o 0.56752 0 8 28 224.25 178.52 26.45 o 0.56188 1 8 28 241.77 266.36 33.06 o 0.55773 2 8 28 342.47 253.13 32.11 o 0.55511 3 8 28 271.20 182.29 28.34 o 0.55404 4 8 28 345.39 259.01 21.03 o 0.55453 5 8 28 35.45 21.25 10.69 o 0.55658 6 8 28 35.46 26.83 10.44 o 0.56016 7 8 28 41.96 51.00 17.95 o 0.56525 8 8 28 112.28 110.51 20.78 o 0.57180 9 8 28 80.79 62.34 18.89 o 0.57978 10 8 28 12.79 46.28 17.00 o 0.58911 11 8 28 260.41 272.04 18.14 o 0.59974 12 8 28 11.51 25.65 7.86 o 0.61160 13 8 28 20.99 26.45 10.39 o 0.62462 -5 9 28 1.89 3.74 6.80 o 0.61528 -4 9 28 134.45 131.99 14.35 o 0.60378 -3 9 28 345.91 373.09 33.06 o 0.59351 -2 9 28 81.15 132.23 22.67 o 0.58454 -1 9 28 4.41 11.33 13.22 o 0.57693 0 9 28 19.29 22.67 14.17 o 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24.56 o 0.59492 11 10 28 8.32 17.00 14.17 o 0.60422 12 10 28 181.72 190.43 14.26 o 0.61479 13 10 28 306.11 269.19 21.72 o 0.62656 -3 11 28 3.35 3.62 6.99 o 0.61789 -2 11 28 97.73 114.29 13.36 o 0.60806 -1 11 28 39.97 46.28 16.06 o 0.59951 0 11 28 79.64 51.95 16.06 o 0.59230 1 11 28 60.99 40.61 17.00 o 0.58647 2 11 28 103.98 90.68 19.84 o 0.58207 3 11 28 182.61 168.13 23.61 o 0.57913 4 11 28 359.19 364.59 32.11 o 0.57767 5 11 28 418.70 348.23 21.03 o 0.57771 6 11 28 115.29 157.82 14.65 o 0.57924 7 11 28 38.35 37.78 17.00 o 0.58226 8 11 28 615.47 719.73 44.39 o 0.58673 9 11 28 443.64 435.43 34.00 o 0.59263 10 11 28 9.87 12.28 11.33 o 0.59991 11 11 28 223.89 208.74 22.67 o 0.60852 12 11 28 133.42 151.13 18.89 o 0.61842 -2 12 28 467.68 492.14 21.64 o 0.62151 -1 12 28 278.12 217.24 22.67 o 0.61254 0 12 28 113.30 139.79 19.84 o 0.60487 1 12 28 21.52 0.00 11.33 o 0.59855 2 12 28 44.40 86.90 17.00 o 0.59361 3 12 28 181.39 289.97 28.34 o 0.59010 4 12 28 66.89 41.56 13.22 o 0.58804 5 12 28 37.49 80.29 16.06 o 0.58745 6 12 28 6.57 12.28 12.28 o 0.58832 7 12 28 166.79 240.86 24.56 o 0.59066 8 12 28 159.48 196.46 22.67 o 0.59445 9 12 28 254.39 315.47 28.34 o 0.59965 10 12 28 0.17 0.00 13.22 o 0.60624 11 12 28 6.38 0.00 10.39 o 0.61416 12 12 28 112.11 133.18 16.06 o 0.62337 -1 13 28 74.76 119.01 15.11 o 0.62665 0 13 28 273.33 416.54 28.34 o 0.61855 1 13 28 125.74 102.95 16.06 o 0.61176 2 13 28 139.34 192.68 20.78 o 0.60632 3 13 28 39.84 33.06 11.33 o 0.60227 4 13 28 35.94 61.39 13.22 o 0.59963 5 13 28 28.86 45.34 11.33 o 0.59843 6 13 28 93.28 110.51 14.17 o 0.59867 7 13 28 149.65 171.91 18.89 o 0.60035 8 13 28 280.01 309.81 25.50 o 0.60346 9 13 28 16.49 48.17 14.17 o 0.60798 10 13 28 16.23 42.50 12.28 o 0.61387 11 13 28 28.24 11.33 10.39 o 0.62110 2 14 28 2.47 0.00 7.56 o 0.62012 3 14 28 132.67 133.18 16.06 o 0.61556 4 14 28 47.16 29.28 8.50 o 0.61237 8 14 28 310.86 331.53 22.67 o 0.61371 9 14 28 59.79 13.22 9.45 o 0.61755 10 14 28 15.91 9.45 8.50 o 0.62275 7 7 -29 59.78 21.72 10.39 o 0.62607 6 7 -29 253.55 235.19 22.67 o 0.62159 -5 -7 29 7.32 18.63 6.80 o 0.61848 -4 -7 29 15.52 1.89 8.50 o 0.61675 -3 -7 29 217.43 221.97 21.72 o 0.61643 -2 -7 29 36.72 40.61 13.22 o 0.61750 -1 -7 29 1.29 0.00 9.45 o 0.61997 0 -7 29 59.36 63.28 13.22 o 0.62381 8 6 -29 77.70 69.90 14.17 o 0.62445 7 6 -29 0.21 0.00 11.33 o 0.61796 -6 -6 29 17.08 40.81 8.56 o 0.61282 -5 -6 29 119.51 109.16 12.41 o 0.60905 -4 -6 29 28.02 26.59 9.28 o 0.60669 -3 -6 29 496.56 438.05 23.35 o 0.60575 -2 -6 29 512.68 549.72 37.78 o 0.60623 -1 -6 29 104.06 88.79 17.00 o 0.60813 0 -6 29 33.28 29.28 14.17 o 0.61144 1 -6 29 28.95 8.69 6.80 o 0.61614 9 5 -29 19.30 9.45 9.45 o 0.62673 8 5 -29 12.88 0.00 10.39 o 0.61828 7 5 -29 23.57 14.17 12.28 o 0.61112 -6 -5 29 7.30 5.52 7.93 o 0.60531 -5 -5 29 205.16 151.82 15.66 o 0.60088 -4 -5 29 53.57 50.57 10.88 o 0.59786 -3 -5 29 3.10 2.03 9.00 o 0.59628 -2 -5 29 29.23 31.14 9.75 o 0.59615 -1 -5 29 0.72 4.12 6.80 o 0.59746 0 -5 29 1.02 1.74 8.33 o 0.60021 1 -5 29 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