#------------------------------------------------------------------------------ #$Date: 2012-09-11 12:26:43 +0300 (Tue, 11 Sep 2012) $ #$Revision: 66590 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/42/2234259.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2234259_Fobs loop_ _publ_author_name 'Li, Yan' 'Guo, Zhenghua' 'Dong, Jianfang' 'Li, Lianzhi' _publ_section_title ; Bis[\m-N-(3-methoxy-2-oxidobenzylidene-1:2\k^2^O^2^:O^2^)-L-isoleucinato-2\k^2^N,O]bis(1,10-phenanthroline-1\k^2^N,N')dinickel(II) methanol tetrasolvate trihydrate ; _journal_coeditor_code HY2519 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m371 _journal_page_last m372 _journal_volume 68 _journal_year 2012 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 14.1827 _cell_length_b 14.3876 _cell_length_c 28.7870 _exptl_crystal_F_000 2504.00 _reflns_d_resolution_high 0.8403 _[local]_cod_data_source_file hy2519Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 090427c in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 509.31 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 67.26 -46.45 30.97 o 4 0 0 259397.38 271641.97 9765.60 o 6 0 0 346.53 285.77 73.07 o 8 0 0 915.29 1142.81 128.76 o 10 0 0 1383.06 1673.33 156.74 o 12 0 0 9292.44 9053.62 452.83 o 14 0 0 110.61 -35.59 125.23 o 16 0 0 1882.48 2174.51 264.04 o 1 1 0 81572.13 78198.71 1573.90 o 2 1 0 613.20 565.29 23.06 o 3 1 0 8668.41 8952.12 199.34 o 4 1 0 610.81 458.99 44.26 o 5 1 0 65074.75 69967.68 2000.79 o 6 1 0 35211.00 37544.80 995.37 o 7 1 0 8664.69 8625.69 381.93 o 8 1 0 2120.75 2313.72 115.23 o 9 1 0 5848.38 6255.98 227.22 o 10 1 0 4521.67 5247.96 208.48 o 11 1 0 2915.45 3246.77 161.75 o 12 1 0 3.20 77.96 65.70 o 13 1 0 81.49 70.13 76.16 o 14 1 0 1504.43 1460.72 148.02 o 15 1 0 177.91 228.32 102.75 o 16 1 0 0.91 -11.16 90.98 o 0 2 0 52.95 39.93 18.34 o 1 2 0 27003.22 36879.66 923.35 o 2 2 0 334.84 937.56 100.55 o 3 2 0 376.84 632.05 27.81 o 4 2 0 32.89 -6.09 24.01 o 5 2 0 19588.55 20787.79 450.76 o 6 2 0 8224.72 9716.58 418.06 o 7 2 0 1161.68 1108.86 80.32 o 8 2 0 1330.84 1105.72 87.10 o 9 2 0 476.95 489.44 74.07 o 10 2 0 1967.27 1698.87 113.33 o 11 2 0 2344.44 2590.60 144.19 o 12 2 0 324.61 341.73 85.05 o 13 2 0 85.15 76.91 75.97 o 14 2 0 73.50 -85.25 94.12 o 15 2 0 2605.71 2641.98 247.06 o 16 2 0 221.93 304.24 152.94 o 1 3 0 492.00 288.87 21.03 o 2 3 0 5147.22 4270.83 135.15 o 3 3 0 16288.68 20398.23 463.56 o 4 3 0 363.88 504.07 32.74 o 5 3 0 61.01 33.11 28.11 o 6 3 0 21031.90 23573.27 1166.80 o 7 3 0 12337.34 12207.38 418.41 o 8 3 0 4220.62 3739.64 496.97 o 9 3 0 1712.89 1717.04 107.78 o 10 3 0 2672.10 2419.67 136.77 o 11 3 0 1025.41 1060.42 118.30 o 12 3 0 2256.70 2120.79 138.01 o 13 3 0 52.44 81.25 76.01 o 14 3 0 171.20 70.08 127.94 o 15 3 0 81.65 135.99 86.66 o 16 3 0 172.08 136.09 148.05 o 0 4 0 31556.97 38330.93 1260.70 o 1 4 0 12798.28 14706.38 282.14 o 2 4 0 152.81 219.52 22.30 o 3 4 0 146.30 113.39 22.20 o 4 4 0 540.40 644.02 30.40 o 5 4 0 220.91 264.66 45.50 o 6 4 0 1691.57 1744.01 140.42 o 7 4 0 3398.08 3563.90 120.68 o 8 4 0 2863.92 3171.03 126.41 o 9 4 0 5360.80 5542.33 258.74 o 10 4 0 345.15 233.51 53.93 o 11 4 0 492.04 342.29 149.54 o 12 4 0 4125.58 4727.03 321.76 o 13 4 0 320.95 365.53 90.38 o 14 4 0 313.72 296.58 141.93 o 15 4 0 149.16 189.41 94.58 o 16 4 0 714.54 835.03 203.19 o 1 5 0 11.92 38.95 13.67 o 2 5 0 1664.86 1514.16 54.63 o 3 5 0 303.58 222.18 35.34 o 4 5 0 18.96 4.39 20.31 o 5 5 0 1192.56 1120.74 43.14 o 6 5 0 815.65 855.25 54.62 o 7 5 0 4434.39 4466.02 172.36 o 8 5 0 7287.23 7644.77 278.07 o 9 5 0 105.60 89.95 39.49 o 10 5 0 301.28 230.02 72.43 o 11 5 0 498.11 416.93 104.45 o 12 5 0 969.07 1265.19 121.40 o 13 5 0 528.34 617.74 105.79 o 14 5 0 392.59 324.05 93.03 o 15 5 0 334.84 539.43 114.36 o 16 5 0 18.20 -70.63 139.90 o 0 6 0 7309.08 6950.85 199.57 o 1 6 0 21348.02 22932.95 419.29 o 2 6 0 1403.15 1247.18 53.74 o 3 6 0 2799.52 3035.52 102.34 o 4 6 0 1773.54 1546.83 72.01 o 5 6 0 5199.14 5149.67 131.03 o 6 6 0 4698.85 4343.29 168.36 o 7 6 0 322.99 349.59 51.86 o 8 6 0 5.21 19.29 47.64 o 9 6 0 58.66 26.86 45.53 o 10 6 0 97.31 40.14 49.06 o 11 6 0 3.02 -49.08 64.34 o 12 6 0 70.92 19.58 67.80 o 13 6 0 1053.52 1240.87 276.13 o 14 6 0 806.69 776.62 114.77 o 15 6 0 77.63 -115.15 118.03 o 1 7 0 1593.84 1334.57 45.92 o 2 7 0 6.89 -5.41 20.89 o 3 7 0 6358.50 6636.40 169.18 o 4 7 0 339.18 345.47 42.12 o 5 7 0 158.26 137.03 46.19 o 6 7 0 1881.59 1658.37 77.91 o 7 7 0 7227.04 7482.92 201.32 o 8 7 0 341.05 579.59 60.86 o 9 7 0 675.97 912.01 77.07 o 10 7 0 1112.37 1137.81 89.40 o 11 7 0 3.83 -13.78 51.57 o 12 7 0 214.93 233.90 110.83 o 13 7 0 405.56 740.24 113.51 o 14 7 0 109.90 94.43 91.96 o 15 7 0 359.98 354.22 159.45 o 0 8 0 442.07 462.52 48.95 o 1 8 0 8056.41 9334.64 189.27 o 2 8 0 19377.73 20735.43 387.91 o 3 8 0 1137.61 1258.56 65.10 o 4 8 0 130.78 100.87 36.47 o 5 8 0 2945.51 3387.01 163.04 o 6 8 0 2643.75 2614.95 151.71 o 7 8 0 392.74 347.18 56.14 o 8 8 0 2.21 53.18 46.45 o 9 8 0 494.77 501.49 67.01 o 10 8 0 656.21 688.34 140.35 o 11 8 0 32.82 65.30 55.13 o 12 8 0 227.40 303.91 74.74 o 13 8 0 377.19 517.27 105.24 o 14 8 0 1081.62 1090.87 232.39 o 1 9 0 1840.74 1752.58 74.67 o 2 9 0 33.85 6.36 32.64 o 3 9 0 601.77 743.09 70.33 o 4 9 0 1840.82 1890.49 112.66 o 5 9 0 30.67 0.44 37.84 o 6 9 0 448.19 435.19 57.14 o 7 9 0 808.56 1010.50 134.97 o 8 9 0 4790.48 4760.55 294.46 o 9 9 0 1.89 -68.88 46.81 o 10 9 0 146.35 124.68 58.88 o 11 9 0 180.80 128.59 85.69 o 12 9 0 564.28 593.11 110.60 o 13 9 0 1.34 26.52 64.52 o 14 9 0 1.29 14.88 84.82 o 0 10 0 678.06 600.06 98.61 o 1 10 0 1809.09 1857.08 78.04 o 2 10 0 385.60 670.56 59.60 o 3 10 0 5802.99 5565.13 160.02 o 4 10 0 345.43 513.22 68.47 o 5 10 0 1834.79 1495.00 90.50 o 6 10 0 17.28 36.73 48.22 o 7 10 0 995.01 1017.20 81.90 o 8 10 0 565.05 636.35 76.29 o 9 10 0 991.34 1260.80 95.59 o 10 10 0 0.33 -54.85 66.59 o 11 10 0 6.23 -83.87 55.91 o 12 10 0 85.37 85.53 67.79 o 13 10 0 1109.39 1309.04 114.23 o 1 11 0 994.60 1337.75 138.40 o 2 11 0 1282.71 1350.57 98.51 o 3 11 0 396.76 581.84 64.51 o 4 11 0 567.27 712.22 66.33 o 5 11 0 2236.99 2401.82 137.86 o 6 11 0 3.67 -51.73 67.07 o 7 11 0 1643.75 1536.49 98.10 o 8 11 0 530.27 677.57 80.13 o 9 11 0 311.00 263.26 69.30 o 10 11 0 361.49 311.29 72.38 o 11 11 0 92.54 -0.26 62.04 o 12 11 0 427.48 445.84 84.28 o 0 12 0 2457.06 2893.28 193.68 o 1 12 0 575.39 550.50 114.36 o 2 12 0 415.52 427.45 75.39 o 3 12 0 10.96 76.39 60.24 o 4 12 0 549.74 618.68 79.22 o 5 12 0 791.68 757.28 106.08 o 6 12 0 41.33 -46.90 50.55 o 7 12 0 134.04 30.21 57.24 o 8 12 0 31.63 -12.47 58.68 o 9 12 0 5.29 6.13 61.10 o 10 12 0 577.12 536.10 82.89 o 11 12 0 111.39 -4.64 67.80 o 12 12 0 206.59 150.94 97.02 o 1 13 0 1131.91 1181.81 105.51 o 2 13 0 927.35 773.64 95.21 o 3 13 0 434.51 447.56 108.52 o 4 13 0 1160.24 1284.41 111.91 o 5 13 0 35.72 81.07 69.49 o 6 13 0 615.57 692.56 197.35 o 7 13 0 268.63 211.56 68.57 o 8 13 0 87.31 118.29 67.24 o 9 13 0 93.71 6.96 65.65 o 10 13 0 223.68 129.01 138.68 o 0 14 0 862.06 1519.30 173.58 o 1 14 0 425.64 462.78 82.87 o 2 14 0 1.81 87.15 66.92 o 3 14 0 1442.75 1522.44 121.58 o 4 14 0 1788.89 1808.38 126.30 o 5 14 0 120.23 201.82 81.84 o 6 14 0 1.84 -25.09 112.60 o 7 14 0 213.91 186.44 85.18 o 8 14 0 41.90 -9.51 78.41 o 9 14 0 141.03 84.81 68.34 o 1 15 0 69.02 116.59 78.51 o 2 15 0 18.54 -67.69 71.87 o 3 15 0 184.56 158.21 81.63 o 4 15 0 624.73 657.16 144.79 o 5 15 0 962.37 942.59 117.58 o 6 15 0 2.82 84.06 76.83 o 7 15 0 496.33 442.98 263.22 o 8 15 0 128.56 122.15 96.43 o 0 16 0 1518.17 1738.25 203.19 o 1 16 0 802.26 1023.36 117.76 o 2 16 0 360.52 306.47 94.27 o 3 16 0 99.66 63.02 96.16 o 4 16 0 87.83 26.83 84.00 o 5 16 0 196.95 390.98 98.97 o 6 16 0 1.08 68.20 87.74 o 1 17 0 25.47 -63.24 75.78 o 2 17 0 144.91 20.41 81.15 o 1 0 1 16562.31 20465.11 753.81 o 2 0 1 6443.53 8190.40 226.92 o 3 0 1 1825.25 2622.44 89.89 o 4 0 1 86957.34 93434.91 2395.51 o 5 0 1 1062.26 1359.93 160.13 o 6 0 1 69292.28 74527.42 1930.99 o 7 0 1 9915.19 11005.68 331.78 o 8 0 1 10165.30 10347.75 322.41 o 9 0 1 150.70 223.34 60.68 o 10 0 1 10479.99 10363.61 338.93 o 11 0 1 1803.56 1961.27 125.24 o 12 0 1 434.34 626.27 93.93 o 13 0 1 261.18 254.14 88.67 o 14 0 1 749.67 789.52 119.33 o 15 0 1 513.37 518.65 115.34 o 16 0 1 99.58 67.91 99.98 o -16 1 1 219.77 99.15 138.81 o -15 1 1 1387.62 1346.60 149.61 o -14 1 1 445.31 506.26 107.53 o -13 1 1 1570.34 1553.19 138.94 o -12 1 1 588.01 780.61 101.64 o -11 1 1 3627.27 3726.65 177.06 o -10 1 1 2339.47 2486.89 132.70 o -9 1 1 2763.16 2909.72 140.02 o -8 1 1 880.72 1068.17 88.25 o -7 1 1 3682.93 4198.73 159.42 o -6 1 1 12595.67 12725.47 445.50 o -5 1 1 1327.00 1166.50 156.47 o -4 1 1 31020.81 35366.07 926.21 o -3 1 1 11606.36 11761.90 304.83 o -2 1 1 1449.73 2123.19 67.22 o -1 1 1 39376.77 36346.34 736.20 o 0 1 1 116793.17 101092.72 2461.14 o 1 1 1 38632.24 33954.32 850.80 o 2 1 1 1785.47 2528.15 63.80 o 3 1 1 11861.63 12031.18 263.18 o 4 1 1 31025.33 34321.16 898.97 o 5 1 1 1868.77 1788.96 181.19 o 6 1 1 13224.46 13826.96 536.23 o 7 1 1 3369.74 3749.61 159.32 o 8 1 1 733.83 799.85 78.91 o 9 1 1 3070.71 3343.51 149.59 o 10 1 1 2744.74 2683.46 137.82 o 11 1 1 3596.24 3586.52 170.91 o 12 1 1 612.32 814.72 191.64 o 13 1 1 1551.67 1458.76 134.39 o 14 1 1 466.74 366.16 105.82 o 15 1 1 1431.22 1396.72 150.31 o 16 1 1 273.16 305.93 165.16 o -16 2 1 621.61 668.79 182.27 o -15 2 1 228.47 384.65 153.75 o -14 2 1 35.67 -100.78 106.76 o -13 2 1 229.06 203.06 86.58 o -12 2 1 889.96 1081.28 117.02 o -11 2 1 1257.84 1374.51 112.72 o -10 2 1 72.70 154.11 59.84 o -9 2 1 4421.35 4122.04 169.96 o -8 2 1 998.83 977.10 165.43 o -7 2 1 7125.82 7977.77 471.30 o -6 2 1 873.39 901.63 86.38 o -5 2 1 12346.68 13474.53 302.65 o -4 2 1 9378.53 10087.92 197.45 o -3 2 1 4296.69 4074.11 100.56 o -2 2 1 234.87 345.02 20.57 o -1 2 1 2421.89 5190.04 186.83 o 0 2 1 27396.00 29407.56 522.59 o 1 2 1 2599.41 5462.85 120.74 o 2 2 1 221.25 289.93 14.35 o 3 2 1 4602.51 4189.91 79.26 o 4 2 1 10551.05 11162.59 247.42 o 5 2 1 11705.28 12678.11 287.02 o 6 2 1 842.70 802.76 70.76 o 7 2 1 7183.28 8013.58 360.06 o 8 2 1 1202.61 1100.68 89.77 o 9 2 1 3877.44 3561.67 156.86 o 10 2 1 58.39 82.06 60.48 o 11 2 1 1407.68 1538.11 115.05 o 12 2 1 910.91 1165.12 248.42 o 13 2 1 191.14 262.58 107.57 o 14 2 1 44.73 -89.41 109.34 o 15 2 1 227.21 371.14 106.59 o 16 2 1 689.68 463.15 170.05 o -16 3 1 710.54 501.73 173.85 o -15 3 1 826.09 1170.78 202.92 o -14 3 1 381.88 371.63 109.34 o -13 3 1 879.88 870.08 169.23 o -12 3 1 1407.36 1260.70 180.64 o -11 3 1 634.71 752.91 95.87 o -10 3 1 133.25 197.91 67.47 o -9 3 1 810.03 870.69 87.51 o -8 3 1 272.19 230.70 82.85 o -7 3 1 303.20 317.90 35.99 o -6 3 1 7095.41 7172.19 316.73 o -5 3 1 6808.98 7656.47 184.42 o -4 3 1 1172.09 1149.05 46.98 o -3 3 1 99.94 207.82 62.56 o -2 3 1 12005.54 14761.27 311.79 o -1 3 1 10671.99 9991.41 213.61 o 0 3 1 4334.90 3597.13 73.27 o 1 3 1 9917.42 8838.35 165.59 o 2 3 1 12045.36 15102.96 276.91 o 3 3 1 20.42 116.02 32.97 o 4 3 1 953.65 1069.36 73.47 o 5 3 1 7141.94 7988.09 146.46 o 6 3 1 6954.80 7013.06 177.63 o 7 3 1 303.70 282.90 42.52 o 8 3 1 400.06 403.05 63.04 o 9 3 1 977.61 1002.51 92.21 o 10 3 1 151.80 119.01 62.49 o 11 3 1 481.31 483.16 86.62 o 12 3 1 1484.63 1737.05 132.38 o 13 3 1 764.59 677.95 82.55 o 14 3 1 377.00 265.68 98.95 o 15 3 1 785.01 1120.80 199.39 o 16 3 1 752.80 720.94 182.54 o -16 4 1 432.04 325.16 161.63 o -15 4 1 848.45 898.33 199.39 o -14 4 1 187.50 192.75 88.54 o -13 4 1 905.84 1173.99 138.95 o -12 4 1 86.70 213.51 78.13 o -11 4 1 262.06 229.09 73.20 o -10 4 1 1373.53 1342.40 102.22 o -9 4 1 936.28 922.91 88.37 o -8 4 1 906.26 946.21 110.68 o -7 4 1 599.32 754.69 55.95 o -6 4 1 12042.14 12521.52 295.76 o -5 4 1 3574.35 3701.53 107.07 o -4 4 1 4045.54 4276.35 227.01 o -3 4 1 3663.46 3386.82 138.29 o -2 4 1 9081.03 8516.81 190.61 o -1 4 1 20181.40 18542.51 422.41 o 0 4 1 395.61 553.82 29.72 o 1 4 1 19095.41 17703.05 322.94 o 2 4 1 8465.17 8264.89 188.28 o 3 4 1 4340.83 4296.31 92.52 o 4 4 1 3350.46 3546.78 92.38 o 5 4 1 3451.85 3798.13 123.73 o 6 4 1 12146.01 12951.79 229.21 o 7 4 1 530.55 673.95 41.05 o 8 4 1 699.72 815.57 74.26 o 9 4 1 968.21 1006.64 62.99 o 10 4 1 1629.53 1515.94 72.98 o 11 4 1 254.69 247.90 51.68 o 12 4 1 63.75 123.19 57.75 o 13 4 1 953.20 1018.48 139.35 o 14 4 1 167.86 162.78 87.22 o 15 4 1 845.25 1131.53 268.11 o 16 4 1 405.13 245.29 158.64 o -15 5 1 694.64 715.78 180.91 o -14 5 1 921.45 1172.28 129.31 o -13 5 1 70.18 79.19 71.39 o -12 5 1 631.97 604.17 94.07 o -11 5 1 42.15 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