#------------------------------------------------------------------------------ #$Date: 2012-09-11 12:26:43 +0300 (Tue, 11 Sep 2012) $ #$Revision: 66590 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/42/2234260.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2234260_Fobs loop_ _publ_author_name 'Wang, Guo-Ming' 'Li, Zeng-Xin' 'Wang, Pei' _publ_section_title ; Tris(ethylenediamine-\k^2^N,N')cadmium hexafluoridogermanate ; _journal_coeditor_code HY2520 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m396 _journal_page_last m397 _journal_volume 68 _journal_year 2012 _space_group_IT_number 163 _symmetry_space_group_name_Hall '-P 3 2c' _symmetry_space_group_name_H-M 'P -3 1 c' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 120.000 _cell_length_a 9.5422 _cell_length_b 9.5422 _cell_length_c 9.9977 _exptl_crystal_F_000 472.00 _reflns_d_resolution_high 0.7975 _[local]_cod_data_source_file hy2520Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 1 in P-31c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 192.57 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-y, x-y, z' '-x+y, -x, z' '-y, -x, -z+1/2' '-x+y, y, -z+1/2' 'x, x-y, -z+1/2' '-x, -y, -z' 'y, -x+y, -z' 'x-y, x, -z' 'y, x, z-1/2' 'x-y, -y, z-1/2' '-x, -x+y, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status -1 2 0 18944.46 19245.00 169.97 o 0 2 0 13072.48 13089.78 72.48 o -1 3 0 1150.07 1129.46 6.08 o 0 3 0 4456.62 4289.02 22.83 o -2 4 0 10183.13 10009.00 61.24 o -1 4 0 2045.63 1973.86 15.60 o 0 4 0 2858.37 2928.45 20.80 o -2 5 0 867.44 826.95 6.87 o -1 5 0 9034.10 9102.64 46.71 o 0 5 0 2917.83 2934.69 23.75 o -3 6 0 7041.18 7154.88 46.57 o -2 6 0 1661.92 1645.30 19.08 o -1 6 0 3068.11 3007.53 18.46 o 0 6 0 8154.29 8245.82 55.54 o -3 7 0 2087.61 2066.42 15.35 o -2 7 0 4720.93 4733.42 27.22 o -1 7 0 998.93 1012.18 10.61 o 0 7 0 103.61 107.03 9.33 o -4 8 0 3656.97 3649.81 34.83 o -3 8 0 542.01 542.48 8.41 o -2 8 0 1054.61 989.12 11.16 o -1 8 0 2744.40 2754.43 24.59 o 0 8 0 751.83 774.36 26.40 o -4 9 0 334.49 333.85 7.62 o -3 9 0 2205.89 2178.60 20.51 o -2 9 0 764.89 747.34 12.87 o -1 9 0 431.08 444.44 11.97 o 0 9 0 785.46 810.81 22.30 o -5 10 0 1452.12 1408.10 25.34 o -4 10 0 321.91 296.84 9.24 o -3 10 0 482.00 481.05 11.81 o -2 10 0 1275.19 1225.25 20.70 o -1 10 0 137.19 165.23 11.06 o 0 10 0 256.05 270.53 18.67 o -5 11 0 261.97 259.01 18.17 o -4 11 0 791.81 782.42 20.78 o -3 11 0 186.39 216.84 16.93 o -2 11 0 95.36 140.39 15.28 o 0 2 1 2017.44 1975.85 13.81 o 1 2 1 1020.72 1051.47 6.55 o -1 3 1 2813.97 2948.77 12.18 o 0 3 1 7.41 15.33 1.73 o 1 3 1 1724.20 1686.55 10.56 o 2 3 1 1455.22 1431.47 11.43 o -1 4 1 647.52 689.07 5.60 o 0 4 1 551.89 560.12 6.44 o 1 4 1 71.71 65.67 2.63 o 2 4 1 603.16 547.69 6.01 o 3 4 1 39.65 52.39 3.71 o -2 5 1 177.18 175.99 3.54 o -1 5 1 378.62 385.68 5.11 o 0 5 1 961.81 951.03 8.57 o 1 5 1 66.74 66.33 3.86 o 2 5 1 267.56 269.05 5.16 o 3 5 1 8.08 17.23 4.02 o 4 5 1 2.34 11.72 5.16 o -2 6 1 129.57 141.86 3.94 o -1 6 1 64.30 70.49 4.93 o 0 6 1 5.36 8.63 3.45 o 1 6 1 1.55 3.91 2.72 o 2 6 1 0.48 9.98 4.11 o 3 6 1 31.27 39.58 7.74 o 4 6 1 46.93 71.53 10.10 o 5 6 1 133.15 137.27 11.05 o -3 7 1 115.33 117.08 4.44 o -2 7 1 98.73 105.77 4.41 o -1 7 1 17.14 28.84 5.60 o 0 7 1 10.45 11.94 3.91 o 1 7 1 84.70 89.08 5.64 o 2 7 1 142.50 141.27 6.87 o 3 7 1 69.90 81.87 7.83 o 4 7 1 5.42 10.11 7.77 o -3 8 1 164.10 166.51 6.79 o -2 8 1 21.21 24.99 5.28 o -1 8 1 28.18 32.32 4.75 o 0 8 1 0.58 4.75 4.12 o 1 8 1 72.87 74.49 7.60 o 2 8 1 2.66 33.68 9.77 o 3 8 1 48.25 58.03 9.64 o -4 9 1 122.75 133.30 5.98 o -3 9 1 2.18 19.84 6.65 o -2 9 1 321.44 283.93 8.11 o -1 9 1 75.17 72.87 6.57 o 0 9 1 40.96 51.56 7.30 o 1 9 1 49.41 79.01 9.78 o 2 9 1 27.97 33.23 10.07 o -4 10 1 107.55 114.88 7.27 o -3 10 1 71.25 68.91 7.45 o -2 10 1 2.27 14.51 7.23 o -1 10 1 17.79 18.52 6.70 o 0 10 1 18.90 30.00 9.07 o -5 11 1 12.14 5.74 7.46 o -4 11 1 7.83 25.89 9.55 o -3 11 1 13.29 2.57 8.25 o -2 11 1 31.21 44.22 9.38 o 0 0 2 37083.52 36400.04 149.68 o 0 1 2 3976.04 4089.04 14.74 o 1 1 2 8129.93 8229.46 36.92 o -1 2 2 27112.49 27741.37 266.90 o 0 2 2 5811.59 5781.30 37.83 o 1 2 2 1255.24 1214.47 11.75 o 2 2 2 3030.14 3059.33 24.36 o -1 3 2 8406.52 8241.44 28.30 o 0 3 2 10649.05 10600.22 40.50 o 1 3 2 441.99 406.48 4.98 o 2 3 2 1307.24 1263.12 10.76 o 3 3 2 6452.37 6472.88 50.60 o -2 4 2 30873.30 31328.64 165.07 o -1 4 2 4806.39 4803.73 21.36 o 0 4 2 2759.62 2726.81 20.85 o 1 4 2 5843.23 5892.24 36.50 o 2 4 2 1017.96 990.82 8.49 o 3 4 2 1650.48 1609.53 12.75 o 4 4 2 3705.75 3675.74 36.69 o -2 5 2 1176.33 1117.55 9.04 o -1 5 2 8736.20 8553.53 47.27 o 0 5 2 2278.86 2263.40 18.90 o 1 5 2 2559.18 2561.81 18.41 o 2 5 2 5119.32 5090.01 36.27 o 3 5 2 1067.00 1015.11 12.59 o 4 5 2 292.70 254.91 9.44 o 5 5 2 1591.09 1586.08 35.84 o -3 6 2 6190.06 6146.09 44.29 o -2 6 2 2932.73 2984.50 20.66 o -1 6 2 813.20 799.86 9.62 o 0 6 2 5658.57 5754.66 36.00 o 1 6 2 946.51 929.72 11.48 o 2 6 2 703.67 693.19 11.20 o 3 6 2 1919.88 1928.99 24.12 o 4 6 2 445.80 438.84 14.25 o 5 6 2 252.68 264.79 13.06 o -3 7 2 1130.32 1144.98 11.72 o -2 7 2 3194.17 3272.96 22.25 o -1 7 2 661.48 630.42 10.80 o 0 7 2 564.92 554.21 9.55 o 1 7 2 2933.53 2946.34 27.20 o 2 7 2 655.01 660.94 14.09 o 3 7 2 305.81 349.56 19.10 o 4 7 2 723.90 713.56 19.40 o -4 8 2 3221.51 3252.27 34.14 o -3 8 2 567.19 559.94 9.34 o -2 8 2 876.33 872.18 11.85 o -1 8 2 2167.77 2180.90 22.69 o 0 8 2 448.21 437.37 10.70 o 1 8 2 434.19 431.36 12.67 o 2 8 2 1091.05 1040.20 18.47 o 3 8 2 108.96 128.61 11.96 o -4 9 2 432.80 427.11 9.20 o -3 9 2 1851.52 1839.85 19.51 o -2 9 2 378.04 378.17 10.58 o -1 9 2 431.13 461.52 11.27 o 0 9 2 1033.48 1051.01 24.95 o 1 9 2 179.91 176.76 11.56 o 2 9 2 172.79 185.12 14.78 o -5 10 2 1407.78 1406.34 27.27 o -4 10 2 223.35 224.78 9.49 o -3 10 2 377.81 364.61 11.63 o -2 10 2 973.19 975.26 24.19 o -1 10 2 291.28 300.58 13.31 o 0 10 2 170.91 194.36 13.83 o -5 11 2 280.26 296.89 13.83 o -4 11 2 856.76 853.62 21.71 o -3 11 2 230.93 227.21 11.90 o -2 11 2 62.89 93.40 10.72 o 0 1 3 271.19 269.60 2.78 o 0 2 3 1570.76 1568.70 8.62 o 1 2 3 817.82 788.41 7.17 o -1 3 3 332.31 383.89 3.65 o 0 3 3 457.89 467.43 4.28 o 1 3 3 676.65 635.17 9.74 o 2 3 3 591.07 517.13 5.56 o -1 4 3 2.85 8.98 1.93 o 0 4 3 25.57 50.58 3.06 o 1 4 3 35.34 45.45 3.95 o 2 4 3 330.26 292.38 8.15 o 3 4 3 167.29 148.09 5.53 o -2 5 3 164.43 159.87 4.14 o -1 5 3 127.82 141.26 3.63 o 0 5 3 27.02 27.52 3.72 o 1 5 3 128.55 145.81 5.18 o 2 5 3 15.66 8.75 3.20 o 3 5 3 4.20 17.80 4.20 o 4 5 3 18.03 10.17 9.43 o -2 6 3 62.21 82.40 5.23 o -1 6 3 139.55 132.96 4.32 o 0 6 3 0.60 3.11 3.60 o 1 6 3 177.11 186.40 7.63 o 2 6 3 46.21 56.36 5.43 o 3 6 3 33.27 47.16 7.35 o 4 6 3 5.63 25.18 9.91 o 5 6 3 87.38 108.18 10.88 o -3 7 3 392.54 362.27 8.91 o -2 7 3 11.83 20.71 3.71 o -1 7 3 197.61 189.40 8.21 o 0 7 3 115.65 131.57 6.61 o 1 7 3 4.08 4.86 4.22 o 2 7 3 4.32 16.53 5.29 o 3 7 3 2.57 8.57 6.62 o 4 7 3 0.41 5.29 7.68 o -3 8 3 277.90 257.13 7.40 o -2 8 3 212.16 199.03 7.74 o -1 8 3 38.79 50.35 5.60 o 0 8 3 146.91 137.27 7.53 o 1 8 3 18.89 21.93 8.17 o 2 8 3 0.86 4.55 7.46 o 3 8 3 22.60 56.28 11.55 o -4 9 3 138.80 136.44 7.02 o -3 9 3 1.25 18.17 7.10 o -2 9 3 65.42 85.14 8.09 o -1 9 3 28.96 52.64 10.68 o 0 9 3 0.19 5.78 6.01 o 1 9 3 13.20 25.78 9.43 o -4 10 3 21.07 37.83 9.04 o -3 10 3 1.68 20.14 8.41 o -2 10 3 5.72 31.96 11.41 o -1 10 3 2.78 19.90 7.97 o 0 10 3 37.42 20.93 10.18 o -5 11 3 0.45 4.00 6.91 o -4 11 3 1.35 -0.20 8.90 o -3 11 3 0.23 4.37 7.18 o 0 0 4 259.99 326.39 7.98 o 0 1 4 1155.26 1132.91 6.82 o 1 1 4 10883.02 11127.10 48.89 o -1 2 4 10762.33 10755.03 48.82 o 0 2 4 1588.49 1567.17 9.67 o 1 2 4 3816.76 3879.98 16.89 o 2 2 4 9240.35 9235.66 61.95 o -1 3 4 5130.13 5226.34 25.19 o 0 3 4 14419.43 14431.40 58.14 o 1 3 4 2318.45 2300.08 18.24 o 2 3 4 1617.67 1545.25 14.12 o 3 3 4 4881.15 4765.52 53.24 o -2 4 4 14067.02 14412.33 121.11 o -1 4 4 2636.21 2562.36 13.25 o 0 4 4 1744.79 1745.05 14.15 o 1 4 4 4731.40 4809.58 29.20 o 2 4 4 1359.75 1333.17 12.53 o 3 4 4 636.36 629.81 12.69 o 4 4 4 2969.02 2957.06 45.58 o -2 5 4 2361.45 2303.98 14.44 o -1 5 4 6427.00 6454.63 39.75 o 0 5 4 1095.40 1092.70 12.08 o 1 5 4 592.72 607.19 9.42 o 2 5 4 3192.88 3130.48 26.98 o 3 5 4 888.89 867.39 16.33 o 4 5 4 535.38 556.98 15.44 o 5 5 4 1257.70 1252.59 39.25 o -3 6 4 5462.97 5589.19 42.92 o -2 6 4 1417.22 1436.94 12.99 o -1 6 4 578.40 603.90 9.64 o 0 6 4 2497.20 2496.74 22.25 o 1 6 4 585.15 547.29 10.09 o 2 6 4 540.58 528.00 14.14 o 3 6 4 1548.59 1552.39 28.29 o 4 6 4 281.02 299.80 13.28 o 5 6 4 163.31 186.08 12.87 o -3 7 4 666.33 702.46 10.12 o -2 7 4 2831.76 2855.66 25.23 o -1 7 4 535.98 501.32 9.93 o 0 7 4 1166.01 1135.95 16.35 o 1 7 4 2000.87 1945.16 24.36 o 2 7 4 232.64 226.88 11.62 o 3 7 4 215.94 216.21 12.15 o 4 7 4 668.40 639.85 19.49 o -4 8 4 2001.97 2053.10 30.13 o -3 8 4 767.25 724.32 12.84 o -2 8 4 328.60 343.48 9.44 o -1 8 4 1750.34 1727.46 21.05 o 0 8 4 244.68 229.99 9.60 o 1 8 4 289.01 289.77 11.32 o 2 8 4 801.64 791.04 20.32 o -4 9 4 363.33 356.07 10.97 o -3 9 4 1396.51 1372.22 19.60 o -2 9 4 288.21 302.81 10.54 o -1 9 4 345.45 350.85 12.48 o 0 9 4 1250.41 1204.93 20.87 o 1 9 4 288.73 296.13 14.66 o -5 10 4 1324.74 1341.25 32.11 o -4 10 4 300.70 343.80 16.67 o -3 10 4 186.64 200.64 11.80 o -2 10 4 790.10 819.31 17.16 o -1 10 4 311.36 304.10 13.58 o -5 11 4 258.64 246.42 12.99 o -4 11 4 859.99 892.04 22.05 o 0 1 5 1124.23 1097.33 7.92 o 0 2 5 1724.17 1739.73 10.41 o 1 2 5 192.56 201.07 3.22 o -1 3 5 153.87 147.24 3.11 o 0 3 5 3.10 10.74 2.96 o 1 3 5 7.54 11.55 2.04 o 2 3 5 8.38 7.38 2.57 o -1 4 5 0.94 5.26 1.94 o 0 4 5 24.53 29.76 4.15 o 1 4 5 43.08 47.49 3.82 o 2 4 5 2.43 1.15 3.62 o 3 4 5 82.56 84.07 6.91 o -2 5 5 10.76 14.39 3.35 o -1 5 5 104.33 122.06 6.91 o 0 5 5 1.27 8.87 4.19 o 1 5 5 109.98 111.73 5.40 o 2 5 5 134.61 128.82 6.94 o 3 5 5 110.59 103.86 8.62 o 4 5 5 83.97 88.14 9.23 o -2 6 5 610.78 554.17 8.83 o -1 6 5 146.03 147.94 7.54 o 0 6 5 2.75 7.12 3.79 o 1 6 5 197.51 208.40 9.23 o 2 6 5 114.18 119.60 9.04 o 3 6 5 25.23 21.76 6.87 o 4 6 5 17.67 32.16 8.36 o -3 7 5 118.21 96.70 5.43 o -2 7 5 7.81 9.26 4.52 o -1 7 5 274.62 252.61 8.33 o 0 7 5 114.76 123.62 9.45 o 1 7 5 22.41 24.17 7.17 o 2 7 5 2.78 0.49 6.10 o 3 7 5 5.51 5.06 7.48 o -3 8 5 36.08 29.50 5.22 o -2 8 5 117.15 117.58 7.84 o -1 8 5 20.78 34.64 6.21 o 0 8 5 94.20 98.24 8.42 o 1 8 5 6.81 6.91 7.24 o 2 8 5 2.40 -4.16 7.29 o -4 9 5 4.26 10.57 6.50 o -3 9 5 5.54 2.18 5.75 o -2 9 5 5.49 30.33 9.76 o -1 9 5 6.54 13.89 6.42 o 0 9 5 18.33 48.63 9.21 o -4 10 5 2.37 5.49 6.69 o -3 10 5 1.63 11.07 7.14 o -2 10 5 0.81 10.33 7.15 o 0 0 6 1821.10 1726.13 27.99 o 0 1 6 1777.09 1747.67 11.97 o 1 1 6 9710.62 9854.72 55.81 o -1 2 6 4731.38 4823.23 40.85 o 0 2 6 978.06 985.23 8.50 o 1 2 6 2362.69 2351.96 15.50 o 2 2 6 8270.78 8175.60 55.51 o -1 3 6 907.93 923.41 8.89 o 0 3 6 7672.50 7783.11 36.36 o 1 3 6 2705.87 2683.40 18.62 o 2 3 6 1696.98 1679.50 18.12 o 3 3 6 3133.64 3241.48 45.96 o -2 4 6 1992.88 2119.51 28.90 o -1 4 6 940.19 943.31 9.36 o 0 4 6 1102.53 1080.31 13.78 o 1 4 6 4662.74 4656.58 31.62 o 2 4 6 766.96 759.15 13.00 o 3 4 6 325.80 341.69 11.17 o 4 4 6 1447.72 1471.42 36.57 o -2 5 6 1826.83 1769.68 14.75 o -1 5 6 4150.80 4248.22 30.47 o 0 5 6 526.72 535.96 9.57 o 1 5 6 381.09 370.79 9.59 o 2 5 6 1859.83 1831.84 24.73 o 3 5 6 280.04 285.70 12.81 o 4 5 6 576.75 564.17 16.55 o 5 5 6 705.96 746.97 28.89 o -3 6 6 3073.10 3185.46 40.79 o -2 6 6 312.70 334.34 8.65 o -1 6 6 769.43 768.93 12.17 o 0 6 6 1571.81 1534.82 18.04 o 1 6 6 531.28 491.02 12.96 o 2 6 6 393.78 399.50 13.62 o 3 6 6 1217.32 1216.59 23.35 o 4 6 6 155.00 151.23 12.15 o -3 7 6 480.49 498.78 10.72 o -2 7 6 2434.00 2441.84 24.71 o -1 7 6 653.33 612.98 12.16 o 0 7 6 531.49 516.05 13.05 o 1 7 6 1119.52 1171.95 21.97 o 2 7 6 144.94 186.21 16.68 o 3 7 6 194.23 207.60 13.74 o -4 8 6 1287.07 1309.20 29.90 o -3 8 6 496.47 487.91 12.88 o -2 8 6 206.95 225.40 11.08 o -1 8 6 1280.03 1257.31 21.13 o 0 8 6 296.35 309.37 12.67 o 1 8 6 136.86 151.27 11.82 o -4 9 6 401.84 402.43 17.01 o -3 9 6 1281.95 1339.67 22.74 o -2 9 6 275.40 301.43 12.53 o -1 9 6 200.93 186.22 12.80 o 0 9 6 865.89 829.86 22.54 o -5 10 6 907.02 929.81 30.78 o -4 10 6 275.91 290.61 15.28 o -3 10 6 157.24 162.03 11.97 o 0 1 7 288.29 284.59 5.00 o 0 2 7 140.18 133.93 3.91 o 1 2 7 13.07 18.19 4.03 o -1 3 7 1.23 3.17 2.95 o 0 3 7 249.58 236.59 5.36 o 1 3 7 13.47 23.87 4.47 o 2 3 7 1.78 11.38 4.91 o -1 4 7 113.11 111.71 4.68 o 0 4 7 452.51 412.36 8.13 o 1 4 7 0.00 3.03 3.55 o 2 4 7 49.65 60.32 6.77 o 3 4 7 1.04 5.29 6.27 o -2 5 7 300.26 278.39 6.22 o -1 5 7 66.01 71.72 5.10 o 0 5 7 48.17 53.73 4.95 o 1 5 7 41.59 57.38 6.44 o 2 5 7 5.62 -4.59 6.21 o 3 5 7 127.64 110.80 9.70 o 4 5 7 39.55 33.25 8.92 o -2 6 7 479.28 435.20 9.68 o -1 6 7 53.11 64.07 5.71 o 0 6 7 0.42 3.70 4.98 o 1 6 7 33.01 36.04 7.23 o 2 6 7 41.63 51.68 8.80 o 3 6 7 50.41 99.97 10.62 o -3 7 7 7.12 20.16 6.24 o -2 7 7 0.31 4.88 5.12 o -1 7 7 19.23 21.01 5.71 o 0 7 7 21.08 38.61 9.62 o 1 7 7 0.39 11.13 7.37 o 2 7 7 11.41 21.01 10.40 o -3 8 7 3.27 6.29 5.54 o -2 8 7 6.66 17.75 6.64 o -1 8 7 2.50 10.62 6.46 o 0 8 7 0.90 21.24 8.67 o 1 8 7 10.14 23.76 8.39 o -4 9 7 0.32 8.01 6.58 o -3 9 7 9.80 38.86 10.41 o -2 9 7 0.54 4.66 8.64 o -1 9 7 8.04 14.33 9.63 o 0 0 8 7428.89 7367.42 97.27 o 0 1 8 1777.86 1746.98 14.43 o 1 1 8 4499.24 4579.50 38.97 o -1 2 8 4197.12 4276.42 37.05 o 0 2 8 834.01 832.78 13.98 o 1 2 8 591.31 602.25 8.85 o 2 2 8 2378.60 2363.19 30.00 o -1 3 8 376.83 380.62 6.82 o 0 3 8 2758.85 2784.35 21.23 o 1 3 8 802.08 782.09 12.36 o 2 3 8 1069.54 1018.72 17.40 o 3 3 8 1934.79 1920.14 36.95 o -2 4 8 1129.19 1162.08 18.76 o -1 4 8 642.93 632.32 9.26 o 0 4 8 552.08 566.94 10.36 o 1 4 8 2846.74 2841.20 29.54 o 2 4 8 285.45 270.38 11.45 o 3 4 8 289.59 306.61 12.75 o 4 4 8 685.40 661.30 25.49 o -2 5 8 654.84 631.73 11.09 o -1 5 8 2140.73 2148.63 21.74 o 0 5 8 357.49 356.56 10.29 o 1 5 8 515.43 519.66 14.61 o 2 5 8 1348.43 1335.73 23.41 o 3 5 8 155.84 158.66 13.17 o 4 5 8 227.90 236.50 14.23 o -3 6 8 1465.23 1391.03 30.02 o -2 6 8 257.72 254.94 9.10 o -1 6 8 437.66 415.47 10.64 o 0 6 8 1375.17 1380.06 23.92 o 1 6 8 441.42 429.99 14.39 o 2 6 8 171.02 199.82 15.05 o 3 6 8 714.58 694.90 20.83 o -3 7 8 314.59 317.72 12.84 o -2 7 8 1560.08 1561.53 28.98 o -1 7 8 459.48 441.55 14.59 o 0 7 8 204.75 226.25 12.04 o 1 7 8 701.43 717.61 19.76 o -4 8 8 1096.78 1106.44 32.00 o -3 8 8 207.39 228.84 12.34 o -2 8 8 294.10 307.21 16.66 o -1 8 8 823.44 858.74 24.05 o -4 9 8 350.62 372.17 15.42 o -3 9 8 902.65 921.42 24.86 o 0 1 9 0.75 9.16 3.90 o 0 2 9 13.84 29.81 4.03 o 1 2 9 7.87 5.75 3.93 o -1 3 9 198.97 190.34 7.46 o 0 3 9 34.28 55.58 5.90 o 1 3 9 42.01 55.79 6.56 o 2 3 9 31.73 35.22 9.06 o -1 4 9 114.38 110.07 6.50 o 0 4 9 151.58 145.18 7.77 o 1 4 9 45.77 50.33 8.12 o 2 4 9 142.77 146.73 9.86 o 3 4 9 3.88 29.38 11.43 o -2 5 9 130.08 125.31 7.61 o -1 5 9 8.68 14.91 5.80 o 0 5 9 18.05 18.22 6.04 o 1 5 9 11.26 20.34 7.23 o 2 5 9 7.02 34.26 8.55 o 3 5 9 15.13 22.83 8.10 o -2 6 9 0.98 16.72 9.73 o -1 6 9 5.82 2.41 5.42 o 0 6 9 0.00 12.35 7.71 o 1 6 9 9.17 4.61 7.06 o 2 6 9 6.44 4.23 8.00 o -3 7 9 1.10 12.68 6.68 o -2 7 9 9.13 16.46 9.22 o -1 7 9 0.41 25.12 8.97 o 0 7 9 2.34 12.47 12.31 o -3 8 9 18.17 49.32 10.13 o -2 8 9 1.38 0.45 8.50 o 0 0 10 2859.07 2891.00 100.20 o 0 1 10 631.57 621.17 10.23 o 1 1 10 1678.07 1694.27 26.91 o -1 2 10 2523.12 2501.36 30.79 o 0 2 10 462.86 450.05 9.55 o 1 2 10 319.15 323.49 9.35 o 2 2 10 863.18 891.64 26.21 o -1 3 10 497.83 475.26 10.84 o 0 3 10 1373.56 1356.18 18.66 o 1 3 10 161.21 160.14 9.45 o 2 3 10 309.69 273.36 12.19 o 3 3 10 947.57 920.30 29.94 o -2 4 10 1702.26 1743.61 31.12 o -1 4 10 416.61 423.29 11.05 o 0 4 10 273.19 300.57 11.93 o 1 4 10 1028.89 1005.50 20.21 o 2 4 10 222.12 240.30 13.82 o 3 4 10 199.04 214.15 13.66 o -2 5 10 212.68 221.34 11.40 o -1 5 10 947.56 965.73 18.26 o 0 5 10 265.01 277.56 14.81 o 1 5 10 258.92 211.44 12.70 o 2 5 10 846.13 821.03 21.33 o -3 6 10 891.15 865.65 26.58 o -2 6 10 349.50 346.32 14.22 o -1 6 10 151.30 140.41 18.25 o 0 6 10 934.44 936.73 24.27 o -3 7 10 171.13 186.78 12.87 o -2 7 10 762.52 743.55 22.06 o 0 1 11 5.09 2.94 4.35 o 0 2 11 28.27 30.99 7.00 o 1 2 11 52.40 56.89 7.32 o -1 3 11 64.48 64.13 7.54 o 0 3 11 30.84 53.49 8.41 o 1 3 11 84.58 89.83 9.75 o 2 3 11 27.09 52.68 9.48 o -1 4 11 22.76 23.66 7.72 o 0 4 11 0.55 5.15 7.53 o 1 4 11 1.05 14.51 8.22 o -2 5 11 2.14 9.99 7.86 o -1 5 11 5.09 5.87 7.07 o 0 0 12 714.04 675.03 38.33 o 0 1 12 154.56 140.12 10.37 o 1 1 12 789.90 718.26 34.82 o -1 2 12 794.32 656.56 103.21 o 0 2 12 226.04 229.38 11.64 o 1 2 12 246.33 246.07 13.41 o -1 3 12 258.25 288.56 17.67 o 0 3 12 733.91 726.73 21.28 o