#------------------------------------------------------------------------------ #$Date: 2012-09-11 12:26:43 +0300 (Tue, 11 Sep 2012) $ #$Revision: 66590 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/42/2234280.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2234280_Fobs loop_ _publ_author_name 'Farag, Abeer Mohamed' 'Guan, Teoh Siang' 'Osman, Hasnah' 'Hemamalini, Madhukar' 'Fun, Hoong-Kun' _publ_section_title ; catena-Poly[[[aquamanganese(III)]-\m-(E)-5-bromo-N-[2-(5-bromo-2-oxidobenzylideneamino)-4-nitrophenyl]-2-oxidobenzamidato] N,N-dimethylfomamide monosolvate] ; _journal_coeditor_code IS5080 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m365 _journal_page_last m366 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 114.658 _cell_angle_gamma 90.000 _cell_length_a 11.0746 _cell_length_b 24.9781 _cell_length_c 9.5563 _exptl_crystal_F_000 1344.00 _reflns_d_resolution_high 0.6741 _[local]_cod_data_source_file is5080Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' anbrmnm in P2(1)/c (100K)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 369.15 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1560.22 1846.91 36.09 o 3 0 0 50646.84 50168.48 891.48 o 4 0 0 131.95 180.69 9.44 o 5 0 0 15997.77 16231.37 238.36 o 6 0 0 16267.08 17198.84 253.32 o 7 0 0 3189.40 3041.89 57.32 o 8 0 0 269.00 252.28 28.71 o 9 0 0 9.96 46.33 28.41 o 10 0 0 3456.40 3561.79 83.83 o 11 0 0 97.78 114.09 39.88 o 12 0 0 1550.29 1702.55 80.37 o 13 0 0 4190.36 4233.80 142.53 o 14 0 0 166.00 131.09 49.15 o 2 1 0 15872.67 16815.89 300.46 o 3 1 0 221.03 232.02 8.01 o 4 1 0 9.32 -4.86 4.86 o 5 1 0 732.40 634.31 17.73 o 6 1 0 5612.49 5836.53 81.23 o 7 1 0 4745.56 4799.20 55.09 o 8 1 0 39.23 79.37 13.94 o 9 1 0 704.56 732.45 31.27 o 10 1 0 357.07 383.30 21.56 o 11 1 0 4.15 31.78 25.17 o 12 1 0 70.70 132.15 29.96 o 13 1 0 21.40 60.79 30.01 o 14 1 0 7.83 70.53 35.63 o 1 2 0 6870.18 7539.96 193.70 o 2 2 0 17928.22 18384.76 328.18 o 3 2 0 26333.78 27644.33 493.27 o 4 2 0 175.28 204.37 7.54 o 5 2 0 45034.11 44580.23 454.87 o 6 2 0 1592.97 1573.05 29.06 o 7 2 0 3565.68 3718.73 80.80 o 8 2 0 14562.34 14281.64 185.82 o 9 2 0 2.73 46.91 14.67 o 10 2 0 4379.71 4388.80 68.72 o 11 2 0 618.65 570.59 28.96 o 12 2 0 337.27 374.84 62.35 o 13 2 0 147.44 219.63 34.24 o 14 2 0 572.91 610.54 45.45 o 1 3 0 2741.10 2854.56 53.15 o 2 3 0 10462.24 11120.98 163.46 o 3 3 0 3449.86 3710.21 86.60 o 4 3 0 52.94 107.36 7.96 o 5 3 0 601.18 524.54 13.41 o 6 3 0 4228.49 4335.00 49.56 o 7 3 0 2766.29 2779.35 47.71 o 8 3 0 1183.88 1266.35 63.35 o 9 3 0 8.67 15.67 12.83 o 10 3 0 1559.47 1654.46 34.25 o 11 3 0 0.67 8.36 33.64 o 12 3 0 5.57 71.39 40.85 o 13 3 0 471.61 645.60 75.16 o 14 3 0 117.07 164.87 36.07 o 0 4 0 25059.61 26879.71 685.70 o 1 4 0 39.17 36.35 3.83 o 2 4 0 20269.90 21938.84 319.28 o 3 4 0 16720.68 16649.31 244.66 o 4 4 0 2894.20 2613.26 37.40 o 5 4 0 4721.36 4527.56 62.36 o 6 4 0 165.99 149.38 9.79 o 7 4 0 3493.57 3529.18 55.88 o 8 4 0 20.10 36.37 14.69 o 9 4 0 28.01 41.26 14.86 o 10 4 0 2000.68 2063.24 38.60 o 11 4 0 152.39 199.22 23.66 o 12 4 0 1053.63 1149.15 76.35 o 13 4 0 186.92 264.62 36.49 o 14 4 0 15.54 7.16 33.62 o 1 5 0 1639.38 2001.85 38.48 o 2 5 0 733.60 809.69 20.71 o 3 5 0 2788.32 3012.63 41.86 o 4 5 0 317.73 355.78 16.38 o 5 5 0 1355.01 1442.88 29.62 o 6 5 0 3346.71 3389.86 50.36 o 7 5 0 913.07 965.49 41.97 o 8 5 0 61.67 106.14 12.57 o 9 5 0 284.18 338.07 17.09 o 10 5 0 109.06 112.03 16.46 o 11 5 0 693.33 674.24 31.34 o 12 5 0 23.54 48.43 28.45 o 13 5 0 11.17 67.13 51.46 o 14 5 0 24.61 29.59 34.55 o 0 6 0 8609.89 10307.44 265.70 o 1 6 0 8441.60 8943.42 161.51 o 2 6 0 731.62 814.81 21.13 o 3 6 0 410.11 420.00 9.50 o 4 6 0 14053.87 14512.19 183.56 o 5 6 0 11720.88 11889.48 151.83 o 6 6 0 614.61 564.85 18.70 o 7 6 0 18.23 33.74 13.69 o 8 6 0 1244.16 1226.25 35.14 o 9 6 0 2919.37 2847.79 44.54 o 10 6 0 1257.11 1345.64 59.58 o 11 6 0 290.68 347.65 31.12 o 12 6 0 180.01 247.74 33.53 o 13 6 0 61.24 55.12 32.76 o 14 6 0 269.22 314.30 58.85 o 1 7 0 4120.95 4535.79 84.35 o 2 7 0 400.90 423.96 10.86 o 3 7 0 42.97 75.05 12.78 o 4 7 0 17.01 18.57 6.69 o 5 7 0 109.85 86.43 9.49 o 6 7 0 42.70 51.34 11.74 o 7 7 0 41.36 73.71 16.67 o 8 7 0 701.49 715.32 18.58 o 9 7 0 5.81 32.26 14.00 o 10 7 0 693.88 685.54 25.68 o 11 7 0 108.58 167.30 42.65 o 12 7 0 97.10 77.58 30.09 o 13 7 0 167.57 216.24 76.12 o 14 7 0 4.10 8.99 46.49 o 0 8 0 502.58 488.22 14.54 o 1 8 0 17550.25 18991.83 339.89 o 2 8 0 1459.95 1577.50 30.87 o 3 8 0 42.90 42.00 6.69 o 4 8 0 18310.19 17943.44 203.19 o 5 8 0 3702.44 3614.09 46.87 o 6 8 0 19009.70 18895.54 217.81 o 7 8 0 254.28 266.00 21.37 o 8 8 0 57.72 63.21 11.23 o 9 8 0 2939.92 2911.15 45.75 o 10 8 0 154.72 212.11 35.11 o 11 8 0 760.86 824.15 34.75 o 12 8 0 171.84 206.35 39.33 o 13 8 0 18.90 60.86 50.04 o 14 8 0 182.78 250.71 56.87 o 1 9 0 1053.61 1013.28 24.33 o 2 9 0 5836.44 6078.01 79.12 o 3 9 0 1852.12 2414.81 35.40 o 4 9 0 1484.78 1613.78 24.57 o 5 9 0 562.50 564.02 18.66 o 6 9 0 66.63 92.94 9.23 o 7 9 0 604.35 639.80 32.56 o 8 9 0 138.33 153.18 12.30 o 9 9 0 639.31 701.96 26.34 o 10 9 0 1435.20 1625.76 116.69 o 11 9 0 487.55 489.39 30.03 o 12 9 0 258.26 283.78 53.21 o 13 9 0 42.43 112.20 47.84 o 14 9 0 16.21 52.43 51.46 o 0 10 0 9440.79 10894.39 197.83 o 1 10 0 47753.87 49914.69 722.09 o 2 10 0 2524.21 2589.03 32.22 o 3 10 0 2172.28 2476.95 32.81 o 4 10 0 14582.29 13901.72 159.11 o 5 10 0 360.00 333.07 13.97 o 6 10 0 6051.38 6088.46 84.33 o 7 10 0 1741.79 1664.32 34.75 o 8 10 0 2693.12 2734.35 38.40 o 9 10 0 3798.85 3882.31 103.23 o 10 10 0 870.46 938.49 50.38 o 11 10 0 3388.05 3543.90 90.37 o 12 10 0 143.51 69.82 47.51 o 13 10 0 180.09 223.07 53.92 o 14 10 0 784.42 788.78 71.54 o 1 11 0 5591.44 5548.66 73.04 o 2 11 0 1941.51 2646.07 30.41 o 3 11 0 8290.27 8718.76 101.35 o 4 11 0 1289.87 1434.61 23.42 o 5 11 0 71.77 90.92 15.77 o 6 11 0 2633.63 2764.47 40.53 o 7 11 0 3147.79 3073.09 45.15 o 8 11 0 26.11 65.25 17.84 o 9 11 0 1773.87 1837.80 39.52 o 10 11 0 2322.67 2381.54 69.04 o 11 11 0 1416.08 1555.72 60.05 o 12 11 0 372.41 490.60 58.45 o 13 11 0 404.32 445.28 60.73 o 14 11 0 102.26 134.68 52.01 o 0 12 0 8377.12 8968.96 134.40 o 1 12 0 25143.04 26348.37 330.52 o 2 12 0 7125.95 7649.61 75.38 o 3 12 0 6209.31 5853.50 70.26 o 4 12 0 14876.24 14491.42 166.13 o 5 12 0 2340.73 2358.95 39.67 o 6 12 0 15749.35 15646.49 181.03 o 7 12 0 1148.68 1140.17 26.73 o 8 12 0 100.16 144.98 14.53 o 9 12 0 3459.10 3306.76 66.61 o 10 12 0 247.27 288.92 48.54 o 11 12 0 517.07 564.98 41.55 o 12 12 0 1348.28 1431.46 60.43 o 13 12 0 279.50 317.64 57.02 o 14 12 0 383.47 406.01 62.82 o 1 13 0 8839.68 9303.89 120.35 o 2 13 0 4835.86 4968.55 50.72 o 3 13 0 11.53 35.70 6.94 o 4 13 0 256.66 270.56 10.99 o 5 13 0 5228.95 5188.70 89.35 o 6 13 0 1313.94 1450.52 27.52 o 7 13 0 1335.90 1358.77 29.31 o 8 13 0 2.34 40.39 15.20 o 9 13 0 331.81 336.86 30.36 o 10 13 0 1.71 -6.90 27.37 o 11 13 0 628.75 585.03 41.23 o 12 13 0 42.95 43.43 34.54 o 13 13 0 403.12 340.55 58.52 o 0 14 0 14354.89 14130.63 209.31 o 1 14 0 29593.89 30609.46 384.13 o 2 14 0 8671.00 8759.48 86.47 o 3 14 0 2045.52 2081.94 32.87 o 4 14 0 12426.76 11911.13 176.07 o 5 14 0 2415.53 2419.80 41.35 o 6 14 0 5266.18 5173.68 75.20 o 7 14 0 1339.22 1211.35 31.24 o 8 14 0 671.25 696.08 28.60 o 9 14 0 2067.11 1978.60 71.95 o 10 14 0 16.36 76.00 29.01 o 11 14 0 3510.98 3444.33 89.73 o 12 14 0 19.47 58.75 35.31 o 13 14 0 2.35 71.90 53.00 o 1 15 0 1274.82 1373.69 22.18 o 2 15 0 789.95 826.31 14.65 o 3 15 0 902.42 897.55 18.18 o 4 15 0 2141.28 2101.30 31.88 o 5 15 0 2621.84 2553.30 43.90 o 6 15 0 2269.81 2237.69 41.24 o 7 15 0 3781.38 3819.43 61.25 o 8 15 0 1.67 14.66 16.57 o 9 15 0 32.83 42.88 18.36 o 10 15 0 212.37 218.24 32.48 o 11 15 0 76.99 113.77 64.42 o 12 15 0 0.53 8.75 34.96 o 13 15 0 153.25 160.23 57.52 o 0 16 0 2111.89 2114.59 40.14 o 1 16 0 9365.44 9593.70 125.16 o 2 16 0 12.98 26.41 6.37 o 3 16 0 7234.59 7510.03 101.85 o 4 16 0 5005.03 5029.39 72.59 o 5 16 0 4562.35 4550.77 68.28 o 6 16 0 10729.99 10561.80 142.09 o 7 16 0 137.87 125.84 16.74 o 8 16 0 706.46 648.47 30.56 o 9 16 0 3927.01 3872.33 83.80 o 10 16 0 23.76 52.14 36.92 o 11 16 0 61.70 83.77 47.96 o 12 16 0 244.61 287.07 40.21 o 13 16 0 457.53 436.20 67.90 o 1 17 0 4603.50 4786.79 66.45 o 2 17 0 4999.46 5239.66 71.95 o 3 17 0 699.84 764.64 25.17 o 4 17 0 381.36 417.27 33.53 o 5 17 0 3298.90 3255.44 53.43 o 6 17 0 566.63 601.51 23.04 o 7 17 0 36.23 19.22 15.84 o 8 17 0 28.55 79.44 22.46 o 9 17 0 1439.18 1422.84 39.03 o 10 17 0 744.77 697.63 44.50 o 11 17 0 60.87 61.03 36.19 o 12 17 0 1107.14 995.52 98.01 o 13 17 0 214.58 299.84 63.20 o 0 18 0 10584.82 11113.84 168.09 o 1 18 0 5440.93 5622.66 77.16 o 2 18 0 544.28 558.25 30.76 o 3 18 0 6339.61 6363.07 89.16 o 4 18 0 8854.21 8530.92 116.39 o 5 18 0 431.54 414.89 19.39 o 6 18 0 912.76 846.97 27.31 o 7 18 0 590.31 562.65 24.41 o 8 18 0 828.03 804.48 29.77 o 9 18 0 878.84 849.00 37.09 o 10 18 0 856.30 860.45 49.29 o 11 18 0 1669.78 1758.70 70.52 o 12 18 0 134.38 174.78 41.49 o 13 18 0 98.18 174.34 60.73 o 1 19 0 107.03 118.19 14.01 o 2 19 0 34.93 51.26 13.06 o 3 19 0 1509.81 1606.31 44.67 o 4 19 0 1936.56 1966.84 49.59 o 5 19 0 16.28 3.44 13.72 o 6 19 0 286.55 315.40 28.71 o 7 19 0 21.59 62.86 18.07 o 8 19 0 144.50 159.68 24.13 o 9 19 0 0.73 25.25 24.34 o 10 19 0 629.78 595.22 45.24 o 11 19 0 3.15 -7.10 37.12 o 12 19 0 57.44 66.01 38.48 o 0 20 0 1742.39 1842.39 52.29 o 1 20 0 7640.38 7761.35 95.20 o 2 20 0 8830.06 8665.30 105.25 o 3 20 0 153.12 181.84 15.77 o 4 20 0 233.10 211.87 17.24 o 5 20 0 5431.88 5538.98 94.76 o 6 20 0 554.95 619.19 25.09 o 7 20 0 191.98 224.50 21.48 o 8 20 0 1902.36 1857.57 68.79 o 9 20 0 17.67 51.04 29.74 o 10 20 0 2020.49 1895.16 67.55 o 11 20 0 17.61 -11.07 34.94 o 12 20 0 43.89 40.23 40.14 o 1 21 0 1733.91 1787.98 31.71 o 2 21 0 459.20 474.27 17.51 o 3 21 0 4.55 28.22 14.15 o 4 21 0 45.68 43.01 15.94 o 5 21 0 476.15 477.76 22.85 o 6 21 0 129.53 124.02 19.29 o 7 21 0 196.72 252.33 22.66 o 8 21 0 85.39 97.01 22.18 o 9 21 0 7.85 39.06 26.86 o 10 21 0 148.59 138.44 40.52 o 11 21 0 3.43 41.37 38.47 o 12 21 0 171.00 190.71 43.85 o 0 22 0 4265.71 4285.08 93.25 o 1 22 0 3339.28 3278.65 54.94 o 2 22 0 1364.84 1421.21 29.51 o 3 22 0 79.84 58.10 15.67 o 4 22 0 0.44 -5.31 16.25 o 5 22 0 9368.92 9351.42 130.14 o 6 22 0 7.61 -11.69 21.46 o 7 22 0 2246.07 2268.41 48.57 o 8 22 0 567.34 584.83 63.74 o 9 22 0 172.43 173.39 49.97 o 10 22 0 1157.91 1137.70 82.09 o 11 22 0 1.12 14.93 39.22 o 12 22 0 261.59 315.70 49.35 o 1 23 0 299.36 337.48 20.30 o 2 23 0 857.06 909.61 40.60 o 3 23 0 1394.78 1389.36 36.57 o 4 23 0 188.54 207.65 19.24 o 5 23 0 454.23 363.53 22.70 o 6 23 0 17.52 27.99 30.56 o 7 23 0 20.64 61.77 24.27 o 8 23 0 433.67 382.97 27.76 o 9 23 0 8.50 33.26 27.91 o 10 23 0 20.09 -25.06 37.08 o 11 23 0 51.77 104.14 39.55 o 0 24 0 14667.18 15402.22 289.17 o 1 24 0 105.34 110.67 17.34 o 2 24 0 3016.89 3090.29 54.01 o 3 24 0 6623.96 6665.89 113.54 o 4 24 0 28.56 29.73 17.39 o 5 24 0 4770.07 4619.08 75.23 o 6 24 0 24.87 27.86 19.89 o 7 24 0 3812.58 3655.18 87.10 o 8 24 0 517.46 558.15 34.76 o 9 24 0 35.73 71.70 29.20 o 10 24 0 1728.74 1837.46 84.77 o 11 24 0 91.80 119.95 42.32 o 1 25 0 332.53 335.20 22.05 o 2 25 0 7.80 25.56 17.81 o 3 25 0 2031.43 2048.90 80.16 o 4 25 0 1002.19 1066.55 43.33 o 5 25 0 37.76 89.18 20.78 o 6 25 0 1341.04 1277.12 38.73 o 7 25 0 773.91 819.17 32.78 o 8 25 0 511.15 530.26 30.82 o 9 25 0 77.66 76.35 30.62 o 10 25 0 689.66 615.20 61.49 o 11 25 0 337.66 368.21 57.56 o 0 26 0 3187.96 3110.49 78.93 o 1 26 0 477.66 450.24 31.88 o 2 26 0 8345.42 8339.19 119.39 o 3 26 0 714.95 649.29 32.66 o 4 26 0 762.41 720.33 34.98 o 5 26 0 10135.71 9887.20 161.55 o 6 26 0 585.74 607.70 29.63 o 7 26 0 1156.12 1236.32 50.38 o 8 26 0 4768.90 4719.42 80.74 o 9 26 0 276.58 316.98 42.83 o 10 26 0 1283.01 1308.24 104.00 o 1 27 0 1760.06 1804.77 51.49 o 2 27 0 2864.34 2959.62 65.30 o 3 27 0 190.16 262.69 27.43 o 4 27 0 1113.91 1123.24 73.29 o 5 27 0 508.43 455.64 33.02 o 6 27 0 3.26 17.77 27.83 o 7 27 0 256.32 298.71 27.92 o 8 27 0 61.80 50.50 55.29 o 9 27 0 213.86 215.65 35.23 o 10 27 0 630.47 681.78 100.00 o 0 28 0 20696.91 21444.60 398.60 o 1 28 0 180.57 250.00 24.23 o 2 28 0 234.17 221.47 27.63 o 3 28 0 4955.71 4830.84 91.52 o 4 28 0 277.24 289.01 31.58 o 5 28 0 2025.64 2170.47 59.75 o 6 28 0 406.89 426.89 35.01 o 7 28 0 1845.75 1923.21 57.66 o 8 28 0 23.79 65.73 39.95 o 9 28 0 34.01 53.46 33.39 o 1 29 0 183.11 180.78 24.74 o 2 29 0 398.52 364.66 31.12 o 3 29 0 757.86 822.70 39.37 o 4 29 0 842.11 829.51 40.44 o 5 29 0 810.55 854.61 41.16 o 6 29 0 1795.71 1923.41 87.50 o 7 29 0 1710.03 1858.27 58.60 o 8 29 0 314.14 325.43 46.44 o 9 29 0 188.34 300.30 70.90 o 0 30 0 1195.59 1344.09 55.75 o 1 30 0 550.02 573.34 30.22 o 2 30 0 1862.73 1775.31 54.98 o 3 30 0 3.74 5.24 26.61 o 4 30 0 68.58 60.68 50.80 o 5 30 0 1812.13 1823.59 58.06 o 6 30 0 354.00 352.52 36.18 o 7 30 0 175.48 168.63 33.31 o 8 30 0 757.30 700.01 55.09 o 1 31 0 1275.95 1359.11 51.39 o 2 31 0 675.38 696.23 39.82 o 3 31 0 7.79 6.91 37.20 o 4 31 0 0.52 32.35 31.60 o 5 31 0 22.64 45.26 31.56 o 6 31 0 97.05 122.65 42.63 o 7 31 0 28.14 64.84 34.29 o 8 31 0 7.65 -32.25 44.18 o 0 32 0 1468.05 1618.93 64.70 o 1 32 0 279.96 264.45 33.29 o 2 32 0 334.48 428.57 37.39 o 3 32 0 581.53 543.37 36.95 o 4 32 0 787.66 796.67 43.96 o 5 32 0 10.45 0.28 31.40 o 6 32 0 373.64 400.99 39.35 o 7 32 0 19.83 70.86 35.47 o 1 33 0 509.86 500.33 72.87 o 2 33 0 191.86 224.02 52.52 o 3 33 0 968.40 970.82 52.17 o 4 33 0 241.05 248.50 36.59 o 5 33 0 528.11 552.53 40.38 o 6 33 0 8.36 32.80 53.35 o 0 34 0 83.18 115.07 60.62 o 1 34 0 2505.41 2629.76 67.75 o 2 34 0 64.49 77.08 33.31 o 3 34 0 609.31 596.51 40.62 o 4 34 0 1815.68 1991.23 62.81 o 5 34 0 402.20 395.97 40.25 o 1 35 0 134.96 75.24 41.60 o 2 35 0 261.24 275.80 43.76 o 3 35 0 59.06 65.89 34.89 o 4 35 0 89.01 182.74 37.33 o 0 36 0 64.88 -19.49 61.95 o 1 36 0 2227.44 2222.48 100.68 o 2 36 0 83.41 103.65 42.73 o 3 36 0 237.96 210.43 48.21 o -15 1 1 70.22 76.32 71.67 o -14 1 1 5.90 70.12 34.04 o -13 1 1 103.91 225.92 33.79 o -12 1 1 641.22 643.39 28.42 o -11 1 1 1597.36 1780.17 51.78 o -10 1 1 631.96 656.27 25.30 o -9 1 1 109.76 129.73 15.79 o -8 1 1 11191.75 11404.94 150.77 o -7 1 1 5323.02 4915.57 69.26 o -6 1 1 5483.09 5146.56 136.93 o -5 1 1 268.42 220.81 9.22 o -4 1 1 1761.58 1632.08 24.89 o -3 1 1 54876.27 63352.74 1131.48 o -2 1 1 81.87 65.76 7.84 o 1 1 1 9058.97 9752.78 252.39 o 2 1 1 981.94 918.40 22.22 o 3 1 1 9295.43 9248.29 240.51 o 4 1 1 13289.23 13114.37 169.46 o 5 1 1 8395.83 9091.31 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96.20 157.85 35.76 o