#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:37:37 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181264 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/42/2234298.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2234298_Fobs loop_ _publ_author_name 'Al-Youbi, Abdulrahman O.' 'Asiri, Abdullah M.' 'Faidallah, Hassan M.' 'Ng, Seik Weng' 'Tiekink, Edward R. T.' _publ_section_title ; 4-{2-[(E)-Cyclopentylidene]hydrazin-1-yl}benzenesulfonamide ; _journal_coeditor_code JJ2126 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1196 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 94.019 _cell_angle_gamma 90.000 _cell_length_a 14.1173 _cell_length_b 5.2038 _cell_length_c 16.4239 _exptl_crystal_F_000 536.00 _reflns_d_resolution_high 0.7684 _cod_data_source_file jj2126Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 222.67 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1249.27 1389.73 30.59 o 3 0 0 986.18 925.03 31.13 o 4 0 0 15376.59 15377.33 143.51 o 5 0 0 375.29 324.96 24.35 o 6 0 0 10093.21 10682.42 146.51 o 7 0 0 9675.88 10622.79 114.76 o 8 0 0 999.33 1058.10 39.17 o 9 0 0 0.34 6.87 6.51 o 12 0 0 1.11 55.30 20.38 o 13 0 0 523.44 518.12 50.05 o 14 0 0 152.72 340.47 42.56 o 15 0 0 27.82 127.52 29.24 o 16 0 0 148.20 184.08 34.38 o 17 0 0 247.34 284.74 43.49 o 18 0 0 182.51 252.47 41.99 o 1 1 0 31.05 32.83 7.66 o 2 1 0 2107.02 2159.87 50.47 o 3 1 0 1060.61 1105.99 15.26 o 4 1 0 1190.40 1156.31 24.68 o 5 1 0 118.48 126.84 8.30 o 6 1 0 2161.03 2226.79 36.93 o 7 1 0 182.26 176.24 12.70 o 8 1 0 758.14 749.73 25.74 o 9 1 0 108.07 101.45 11.40 o 10 1 0 923.62 923.87 38.68 o 11 1 0 1079.14 1072.49 43.91 o 12 1 0 266.57 324.37 25.98 o 13 1 0 2.07 2.54 7.30 o 14 1 0 345.52 374.89 39.89 o 15 1 0 10.71 4.53 10.11 o 16 1 0 34.33 27.03 11.31 o 17 1 0 69.60 77.72 16.42 o 18 1 0 25.03 20.94 17.82 o 0 2 0 802.08 814.11 35.85 o 1 2 0 189.08 208.21 19.39 o 2 2 0 4450.95 4387.60 65.31 o 3 2 0 1980.59 2044.56 28.06 o 4 2 0 76.76 126.70 12.67 o 5 2 0 75.77 34.87 12.67 o 6 2 0 64.20 55.73 13.49 o 7 2 0 926.63 909.70 22.63 o 8 2 0 535.75 503.99 20.29 o 9 2 0 863.46 856.96 26.62 o 10 2 0 1469.87 1313.75 41.02 o 11 2 0 143.21 179.38 33.31 o 12 2 0 10.27 0.69 5.89 o 13 2 0 125.15 132.18 26.37 o 14 2 0 13.06 23.78 7.79 o 15 2 0 23.49 19.99 11.45 o 16 2 0 128.78 112.90 29.54 o 17 2 0 224.04 219.16 43.25 o 1 3 0 625.45 619.75 27.30 o 2 3 0 791.08 903.38 48.72 o 3 3 0 28.78 16.02 6.89 o 4 3 0 1807.04 1818.16 35.50 o 5 3 0 29.75 45.50 53.46 o 6 3 0 613.98 577.20 33.81 o 7 3 0 64.43 70.62 17.58 o 8 3 0 956.43 1009.23 64.89 o 9 3 0 1451.01 1477.16 52.90 o 10 3 0 539.19 660.92 56.90 o 11 3 0 444.20 394.59 46.22 o 12 3 0 125.52 124.23 28.88 o 13 3 0 328.64 310.45 44.16 o 14 3 0 41.00 63.42 23.82 o 15 3 0 157.98 151.96 33.60 o 16 3 0 22.50 41.97 20.29 o 0 4 0 416.01 388.43 35.31 o 1 4 0 10.76 -0.69 6.60 o 2 4 0 652.00 659.37 32.73 o 3 4 0 258.15 274.08 15.39 o 4 4 0 5.63 1.14 4.79 o 5 4 0 0.00 1.37 4.96 o 6 4 0 32.13 47.44 14.65 o 7 4 0 46.01 69.84 20.39 o 8 4 0 42.42 49.00 16.77 o 9 4 0 0.13 14.29 13.02 o 10 4 0 317.64 281.75 40.39 o 11 4 0 222.22 183.85 33.49 o 12 4 0 39.66 64.57 25.14 o 13 4 0 0.67 -17.54 17.54 o 14 4 0 55.09 116.26 31.26 o 1 5 0 1579.95 1574.47 55.41 o 2 5 0 347.52 385.27 27.76 o 3 5 0 180.43 190.17 20.06 o 4 5 0 14.80 26.30 9.24 o 5 5 0 357.40 329.63 26.14 o 6 5 0 403.64 410.65 46.26 o 7 5 0 50.75 49.63 19.00 o 8 5 0 461.71 418.10 49.07 o 9 5 0 22.12 1.85 10.33 o 10 5 0 2.07 -1.77 10.97 o 11 5 0 133.84 117.80 29.54 o 12 5 0 16.67 33.13 18.42 o 0 6 0 5.32 2.28 8.18 o 1 6 0 75.87 75.12 23.97 o 2 6 0 224.07 215.98 32.43 o 3 6 0 119.78 97.13 22.93 o 4 6 0 20.06 15.25 13.54 o 5 6 0 258.03 280.27 39.73 o 6 6 0 91.55 105.66 26.21 o 7 6 0 23.24 19.65 14.61 o 8 6 0 16.10 59.12 21.95 o -18 1 1 0.12 11.53 13.32 o -17 1 1 274.24 216.48 41.18 o -16 1 1 152.05 144.30 27.64 o -15 1 1 309.26 350.86 48.23 o -14 1 1 326.48 318.85 27.35 o -13 1 1 329.16 295.20 25.82 o -12 1 1 353.98 384.30 27.68 o -11 1 1 0.15 3.71 6.38 o -10 1 1 836.89 794.44 29.76 o -9 1 1 153.88 173.53 13.61 o -8 1 1 193.81 175.79 12.67 o -7 1 1 1628.71 1713.19 35.06 o -6 1 1 307.00 345.39 14.65 o -5 1 1 2134.69 2009.00 30.50 o -4 1 1 261.89 263.94 15.48 o -3 1 1 3587.04 3446.74 73.92 o -2 1 1 53.60 42.12 11.02 o -1 1 1 2075.08 1990.34 49.14 o 0 1 1 20142.40 19257.04 71.23 o 1 1 1 75.61 68.57 4.53 o 2 1 1 4802.22 4393.64 35.47 o 3 1 1 1307.75 1316.77 20.13 o 4 1 1 1239.97 1144.02 21.56 o 5 1 1 1942.62 2063.45 40.43 o 6 1 1 869.25 785.49 22.87 o 7 1 1 869.48 907.44 26.65 o 8 1 1 611.44 576.05 23.03 o 9 1 1 12.91 4.50 5.33 o 10 1 1 25.95 37.37 16.17 o 11 1 1 32.54 25.67 8.91 o 12 1 1 11.63 24.18 9.48 o 13 1 1 3.79 15.77 32.47 o 14 1 1 3.89 -8.29 8.39 o 15 1 1 46.89 47.50 12.98 o 16 1 1 104.69 92.48 27.80 o 17 1 1 85.68 83.30 19.75 o 18 1 1 198.34 284.27 48.85 o -17 2 1 9.04 23.21 16.04 o -16 2 1 70.31 82.01 23.02 o -15 2 1 44.95 86.51 26.70 o -14 2 1 9.16 11.44 10.01 o -13 2 1 109.86 117.11 15.74 o -12 2 1 7.79 -1.41 5.02 o -11 2 1 978.19 1040.61 37.90 o -10 2 1 591.25 634.77 23.71 o -9 2 1 1380.03 1311.18 31.15 o -8 2 1 193.10 210.16 11.37 o -7 2 1 781.86 751.42 18.19 o -6 2 1 425.69 438.36 22.69 o -5 2 1 486.58 184.39 251.88 o -4 2 1 1433.61 1434.40 70.80 o -3 2 1 119.02 119.31 12.85 o -2 2 1 1520.53 1490.50 40.42 o -1 2 1 338.74 403.58 17.63 o 0 2 1 110.24 74.21 8.22 o 1 2 1 271.22 316.70 15.74 o 2 2 1 8.66 9.69 3.46 o 3 2 1 226.28 283.40 11.73 o 4 2 1 835.12 877.38 21.67 o 5 2 1 104.82 144.25 10.28 o 6 2 1 480.53 438.77 18.41 o 7 2 1 14.87 16.02 5.48 o 8 2 1 88.56 81.90 8.62 o 9 2 1 22.46 38.36 7.52 o 10 2 1 547.65 568.58 28.59 o 11 2 1 750.57 728.31 33.91 o 12 2 1 26.35 40.27 18.77 o 13 2 1 3.64 10.98 7.29 o 14 2 1 471.97 417.28 29.48 o 15 2 1 63.80 79.99 27.42 o 16 2 1 79.73 145.60 34.65 o 17 2 1 112.57 66.00 26.11 o -16 3 1 60.79 45.82 22.51 o -15 3 1 26.53 23.17 16.36 o -14 3 1 144.65 138.11 31.81 o -13 3 1 75.40 151.44 32.25 o -12 3 1 2.75 0.66 9.33 o -11 3 1 394.50 383.23 45.35 o -10 3 1 1110.88 1080.25 47.39 o -9 3 1 862.43 807.46 38.81 o -8 3 1 149.72 141.13 15.98 o -7 3 1 590.77 543.99 47.57 o -6 3 1 2.00 -1.24 9.73 o -5 3 1 538.75 490.73 42.49 o -4 3 1 43.93 45.96 5.46 o -3 3 1 3669.67 1208.85 1846.05 o -2 3 1 2.99 4.60 4.93 o -1 3 1 62.74 65.39 9.84 o 0 3 1 109.37 119.02 17.33 o 1 3 1 1189.08 1197.26 46.96 o 2 3 1 438.25 440.26 23.60 o 3 3 1 70.09 108.29 10.16 o 4 3 1 0.70 0.57 3.10 o 5 3 1 131.27 122.51 10.76 o 6 3 1 158.58 159.45 11.09 o 7 3 1 26.19 29.95 13.67 o 8 3 1 1273.32 1151.55 69.01 o 9 3 1 190.31 161.93 29.20 o 10 3 1 286.02 277.65 37.45 o 11 3 1 15.70 22.23 11.19 o 12 3 1 196.42 189.76 33.70 o 13 3 1 76.96 62.86 22.45 o 14 3 1 40.78 49.03 20.11 o 15 3 1 322.31 442.45 55.55 o 16 3 1 1.65 -7.17 42.17 o -14 4 1 99.70 149.75 36.03 o -13 4 1 169.27 252.53 41.74 o -12 4 1 104.73 114.24 28.63 o -11 4 1 612.51 690.99 65.11 o -10 4 1 121.71 120.33 27.97 o -9 4 1 400.31 404.44 47.21 o -8 4 1 1142.90 1105.56 75.15 o -7 4 1 130.04 123.05 25.23 o -6 4 1 950.51 933.18 64.46 o -5 4 1 40.48 20.96 12.51 o -4 4 1 2159.39 2112.14 80.17 o -3 4 1 73.73 57.66 18.20 o -2 4 1 1757.23 1811.73 53.15 o -1 4 1 1075.51 994.30 39.60 o 0 4 1 1520.84 1467.29 47.80 o 1 4 1 1080.64 1019.13 40.42 o 2 4 1 13.88 31.36 9.35 o 3 4 1 739.11 758.04 30.39 o 4 4 1 298.59 310.27 17.08 o 5 4 1 679.36 671.39 26.59 o 6 4 1 20.31 24.76 13.61 o 7 4 1 1121.10 1086.45 69.07 o 8 4 1 425.39 388.18 43.43 o 9 4 1 5.74 -3.13 11.89 o 10 4 1 3.74 19.63 15.64 o 11 4 1 138.76 155.91 30.88 o 12 4 1 265.89 343.97 47.12 o 13 4 1 91.90 120.81 28.85 o 14 4 1 205.12 218.81 40.96 o -12 5 1 33.65 81.37 25.63 o -11 5 1 87.35 54.38 22.19 o -10 5 1 19.75 21.31 16.13 o -9 5 1 45.88 65.69 23.43 o -8 5 1 7.63 -15.11 15.11 o -7 5 1 23.69 25.50 15.54 o -6 5 1 26.52 26.68 8.88 o -5 5 1 77.68 68.55 27.08 o -4 5 1 2.15 4.77 5.65 o -3 5 1 142.58 164.66 17.92 o -2 5 1 546.96 595.75 33.76 o -1 5 1 154.78 129.94 16.27 o 0 5 1 42.49 63.64 16.02 o 1 5 1 315.27 315.87 24.96 o 2 5 1 766.78 800.22 40.23 o 3 5 1 25.74 16.13 7.61 o 4 5 1 424.64 461.21 31.45 o 5 5 1 61.51 44.34 15.62 o 6 5 1 88.46 62.65 19.53 o 7 5 1 0.57 -12.03 12.03 o 8 5 1 142.49 168.01 31.65 o 9 5 1 244.07 201.58 35.08 o 10 5 1 34.06 16.85 11.87 o 11 5 1 104.46 88.94 25.51 o 12 5 1 199.27 224.03 39.65 o -8 6 1 25.72 27.60 17.20 o -7 6 1 0.07 11.37 14.45 o -6 6 1 61.94 92.38 25.70 o -5 6 1 4.28 15.25 12.36 o -4 6 1 86.64 101.41 23.59 o -3 6 1 60.35 19.03 12.35 o -2 6 1 172.37 155.95 28.81 o -1 6 1 284.62 273.67 37.23 o 0 6 1 7.94 12.86 14.46 o 1 6 1 264.11 250.70 31.12 o 2 6 1 45.59 42.70 12.13 o 3 6 1 44.66 57.82 27.37 o 4 6 1 80.68 104.24 23.93 o 5 6 1 66.17 95.03 23.71 o 6 6 1 40.12 65.32 20.44 o 7 6 1 20.71 22.15 13.39 o 8 6 1 1.13 -11.71 11.71 o -18 0 2 237.69 316.37 45.45 o -17 0 2 86.09 102.00 26.25 o -16 0 2 17.76 8.72 12.74 o -12 0 2 279.10 333.47 38.11 o -11 0 2 659.83 640.12 49.44 o -10 0 2 386.36 428.03 38.74 o -9 0 2 377.89 393.89 31.97 o -8 0 2 1971.10 1851.98 51.60 o -7 0 2 836.94 856.10 32.99 o -6 0 2 140.93 134.14 12.51 o -5 0 2 3785.32 3788.85 57.71 o -4 0 2 877.62 811.70 34.30 o -3 0 2 6263.00 6256.24 58.83 o -2 0 2 3026.12 2905.24 48.69 o -1 0 2 459.03 458.73 17.07 o 0 0 2 860.30 865.52 22.66 o 1 0 2 1775.80 1704.92 36.86 o 2 0 2 2315.02 2157.75 47.90 o 3 0 2 11331.34 11002.80 123.36 o 4 0 2 118.98 87.30 14.42 o 5 0 2 6278.35 6285.75 113.83 o 6 0 2 316.47 281.40 27.43 o 7 0 2 1550.40 1593.24 67.00 o 8 0 2 427.35 409.83 36.89 o 9 0 2 238.41 237.72 26.74 o 10 0 2 794.44 862.81 59.34 o 11 0 2 0.54 0.35 11.78 o 12 0 2 939.37 1056.20 69.28 o 13 0 2 0.13 -11.95 13.38 o 14 0 2 189.87 154.11 29.23 o 15 0 2 269.50 355.53 45.83 o 16 0 2 0.12 16.56 16.28 o 17 0 2 134.99 161.75 33.51 o 18 0 2 21.13 -20.46 20.46 o -18 1 2 17.57 47.85 26.17 o -16 1 2 5.78 11.22 7.64 o -15 1 2 55.21 49.45 12.60 o -14 1 2 85.75 91.11 15.33 o -13 1 2 6.17 9.19 7.66 o -12 1 2 315.81 332.01 25.80 o -11 1 2 598.06 585.35 32.38 o -10 1 2 1.67 8.04 8.23 o -9 1 2 256.18 272.79 21.88 o -8 1 2 432.85 450.44 26.09 o -7 1 2 1451.29 1455.06 52.75 o -6 1 2 95.03 82.86 10.19 o -5 1 2 704.95 650.52 25.98 o -4 1 2 486.81 503.64 18.97 o -3 1 2 523.11 509.51 16.14 o -2 1 2 290.64 297.56 22.70 o -1 1 2 8.08 6.92 10.26 o 0 1 2 5405.63 5850.89 73.55 o 1 1 2 4175.23 4017.76 32.05 o 2 1 2 142.95 126.49 6.02 o 3 1 2 564.17 573.79 13.35 o 4 1 2 1337.72 1381.99 28.51 o 5 1 2 3.25 2.98 4.15 o 6 1 2 1.77 0.32 5.11 o 7 1 2 231.03 215.25 13.70 o 8 1 2 100.52 115.25 11.03 o 9 1 2 592.56 575.54 24.97 o 10 1 2 16.20 16.20 8.34 o 11 1 2 155.32 128.42 26.05 o 12 1 2 89.64 75.20 22.13 o 13 1 2 17.09 7.61 8.21 o 14 1 2 442.59 498.29 36.12 o 15 1 2 147.68 188.79 23.58 o 16 1 2 32.14 35.11 12.51 o 17 1 2 0.48 14.10 9.64 o -17 2 2 6.44 -6.48 15.15 o -16 2 2 0.74 7.54 12.14 o -15 2 2 356.79 385.80 50.04 o -14 2 2 52.11 48.09 10.88 o -13 2 2 322.49 316.53 22.89 o -12 2 2 350.21 343.36 23.61 o -11 2 2 11.10 13.61 17.98 o -10 2 2 70.16 61.26 9.62 o -9 2 2 555.86 538.88 19.18 o -8 2 2 1094.84 1038.71 36.46 o -7 2 2 65.08 79.79 11.04 o -6 2 2 920.37 884.93 38.89 o -5 2 2 33.63 30.05 6.39 o -4 2 2 710.31 688.51 31.41 o -3 2 2 323.93 418.85 29.79 o -2 2 2 726.27 775.88 21.23 o -1 2 2 311.40 291.53 13.67 o 0 2 2 3140.49 3290.44 57.29 o 1 2 2 916.54 976.36 26.90 o 2 2 2 12.64 17.83 3.58 o 3 2 2 206.22 209.23 10.72 o 4 2 2 109.29 141.28 9.49 o 5 2 2 321.92 358.43 21.95 o 6 2 2 107.91 122.34 8.90 o 7 2 2 2.35 -0.16 5.20 o 8 2 2 2.53 2.92 5.43 o 9 2 2 160.75 135.87 14.29 o 10 2 2 347.87 326.05 22.52 o 11 2 2 118.47 131.80 28.19 o 12 2 2 6.10 10.56 8.16 o 13 2 2 209.04 198.76 17.99 o 14 2 2 71.45 75.23 15.41 o 15 2 2 161.51 157.10 20.95 o 16 2 2 6.15 -12.07 15.05 o 17 2 2 49.31 105.46 32.82 o -16 3 2 77.14 32.05 20.99 o -15 3 2 17.67 8.86 14.11 o -14 3 2 211.58 272.44 43.64 o -13 3 2 27.58 36.52 16.55 o -12 3 2 230.81 221.29 37.02 o -11 3 2 35.90 45.85 16.35 o -10 3 2 87.01 56.22 11.98 o -9 3 2 373.54 311.24 23.95 o -8 3 2 79.00 86.15 12.21 o -7 3 2 1083.99 1031.91 38.09 o -6 3 2 2.40 11.29 11.00 o -5 3 2 454.27 462.68 31.46 o -4 3 2 196.25 196.12 26.93 o -3 3 2 167.25 178.14 25.36 o -2 3 2 524.34 512.37 23.31 o -1 3 2 951.51 939.28 31.66 o 0 3 2 422.50 400.45 21.32 o 1 3 2 73.56 72.38 13.07 o 2 3 2 1123.00 1084.62 32.29 o 3 3 2 662.35 716.80 22.82 o 4 3 2 236.22 219.63 15.68 o 5 3 2 4.75 2.25 4.37 o 6 3 2 113.03 112.41 10.07 o 7 3 2 313.98 285.24 18.81 o 8 3 2 32.01 29.59 13.93 o 9 3 2 51.76 52.52 18.23 o 10 3 2 47.04 52.41 9.47 o 11 3 2 94.29 90.99 11.41 o 12 3 2 114.88 109.56 17.61 o 13 3 2 15.28 23.82 17.33 o 14 3 2 179.86 219.17 37.80 o 15 3 2 18.16 15.73 10.27 o 16 3 2 314.64 350.52 57.10 o -14 4 2 65.32 95.16 25.71 o -13 4 2 20.06 3.05 15.12 o -12 4 2 3.85 18.04 15.46 o -11 4 2 102.30 94.71 25.95 o -10 4 2 0.15 25.07 15.48 o -9 4 2 202.57 144.13 29.95 o -8 4 2 583.44 573.14 31.48 o -7 4 2 41.27 43.00 16.76 o -6 4 2 47.66 43.10 18.17 o -5 4 2 4.65 0.19 9.79 o -4 4 2 0.81 -1.34 2.24 o -3 4 2 54.47 49.22 9.08 o -2 4 2 125.83 120.27 14.16 o -1 4 2 1.90 -6.19 11.61 o 0 4 2 352.21 386.78 24.32 o 1 4 2 18.12 12.75 7.23 o 2 4 2 45.86 52.94 10.93 o 3 4 2 0.20 2.22 5.05 o 4 4 2 367.11 397.77 32.70 o 5 4 2 12.07 5.01 5.56 o 6 4 2 53.03 47.32 8.42 o 7 4 2 12.10 14.00 5.07 o 8 4 2 18.07 33.52 15.64 o 9 4 2 0.36 -8.76 12.66 o 10 4 2 89.36 58.90 19.16 o 11 4 2 82.87 64.64 20.46 o 12 4 2 3.34 1.56 11.51 o 13 4 2 11.62 26.74 15.17 o 14 4 2 7.31 25.64 18.36 o -12 5 2 13.16 9.25 14.78 o -11 5 2 33.60 18.89 15.42 o -10 5 2 210.75 213.43 38.49 o -9 5 2 34.02 37.10 18.37 o -8 5 2 15.17 22.02 13.33 o -7 5 2 108.74 102.78 23.92 o -6 5 2 5.13 7.60 15.74 o -5 5 2 98.69 93.20 13.65 o -4 5 2 257.04 260.33 23.88 o -3 5 2 208.57 192.35 17.63 o -2 5 2 245.81 245.01 21.00 o -1 5 2 1.82 -6.28 6.28 o 0 5 2 317.51 318.06 24.71 o 1 5 2 274.62 268.28 23.27 o 2 5 2 291.24 303.55 19.49 o 3 5 2 201.40 203.86 21.24 o 4 5 2 890.06 822.13 42.05 o 5 5 2 0.14 -8.53 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