#------------------------------------------------------------------------------ #$Date: 2012-09-11 12:26:43 +0300 (Tue, 11 Sep 2012) $ #$Revision: 66590 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/43/2234328.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2234328_Fobs loop_ _publ_author_name 'Asiri, Abdullah M.' 'Faidallah, Hassan M.' 'Al-Thabaiti, Shaeel A.' 'Ng, Seik Weng' 'Tiekink, Edward R. T.' _publ_section_title ; N-Acetyl-N-[2,4-dicyano-1-(4-methoxyphenyl)-9,10-dihydrophenanthren-3-yl]acetamide ; _journal_coeditor_code LH5437 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1177 _journal_page_last o1178 _journal_volume 68 _journal_year 2012 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 8.3321 _cell_length_b 19.4037 _cell_length_c 27.5887 _exptl_crystal_F_000 1824.00 _reflns_d_resolution_high 0.7680 _[local]_cod_data_source_file lh5437Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 577.05 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 332982.44 330733.75 838.15 o 4 0 0 26841.86 29403.51 351.91 o 6 0 0 16684.67 18585.47 340.05 o 8 0 0 7958.51 7995.96 254.69 o 2 1 0 14348.23 15305.75 132.37 o 4 1 0 1725.06 2465.17 386.60 o 6 1 0 779.23 779.43 50.23 o 8 1 0 4770.94 5024.93 142.87 o 2 2 0 33932.08 34046.30 519.75 o 4 2 0 1003.59 1376.31 57.24 o 6 2 0 45.94 50.63 30.54 o 8 2 0 903.30 925.34 62.76 o 2 3 0 33195.73 31057.57 214.33 o 4 3 0 2989.75 2947.05 85.43 o 6 3 0 464.67 574.99 61.90 o 8 3 0 24.16 28.80 11.84 o 0 4 0 22980.80 20668.04 224.02 o 2 4 0 8403.10 8125.62 123.66 o 4 4 0 540.00 591.99 63.48 o 6 4 0 1273.19 1312.67 94.10 o 8 4 0 0.69 22.24 16.18 o 2 5 0 15968.58 16321.94 142.39 o 4 5 0 3269.82 3958.22 136.82 o 6 5 0 9.11 17.76 12.11 o 8 5 0 15.59 -7.07 12.17 o 0 6 0 294.76 505.46 44.43 o 2 6 0 3488.81 3372.75 69.23 o 4 6 0 1703.49 1865.15 75.05 o 6 6 0 473.94 590.71 67.01 o 8 6 0 13.90 -11.87 11.87 o 2 7 0 8205.79 9255.83 122.98 o 4 7 0 2142.09 2264.19 101.64 o 6 7 0 375.09 490.47 62.94 o 8 7 0 416.02 447.00 65.81 o 0 8 0 16606.57 17177.90 289.14 o 2 8 0 2.25 28.35 9.01 o 4 8 0 2145.15 2305.02 85.07 o 6 8 0 235.99 307.80 29.56 o 8 8 0 504.00 731.67 84.97 o 2 9 0 230.66 227.51 74.06 o 4 9 0 161.30 156.47 23.97 o 6 9 0 8.99 133.92 25.08 o 8 9 0 678.08 703.44 85.14 o 0 10 0 21505.63 20834.99 357.51 o 2 10 0 85.46 103.14 19.60 o 4 10 0 4392.67 4308.50 155.49 o 6 10 0 3576.45 3456.07 176.00 o 8 10 0 1117.05 846.46 94.39 o 2 11 0 144.23 106.28 18.91 o 4 11 0 144.44 118.58 24.26 o 6 11 0 32.76 22.43 16.84 o 8 11 0 284.55 244.57 55.82 o 0 12 0 4630.40 5091.78 195.54 o 2 12 0 977.70 1194.37 57.32 o 4 12 0 3281.77 3406.69 174.67 o 6 12 0 39.14 63.08 29.97 o 8 12 0 8.76 80.34 30.84 o 2 13 0 505.01 561.04 70.08 o 4 13 0 761.65 680.43 81.13 o 6 13 0 298.26 374.54 64.51 o 8 13 0 327.80 281.92 59.37 o 0 14 0 68.15 258.79 50.48 o 2 14 0 0.05 16.96 20.44 o 4 14 0 1081.01 1033.10 103.80 o 6 14 0 211.16 208.99 51.12 o 8 14 0 134.50 124.38 37.14 o 2 15 0 1235.10 1096.54 104.65 o 4 15 0 843.33 860.22 97.54 o 6 15 0 0.01 58.97 28.46 o 8 15 0 417.86 349.31 68.23 o 0 16 0 2913.06 2916.49 174.88 o 2 16 0 460.96 485.79 73.21 o 4 16 0 406.52 371.11 64.63 o 6 16 0 604.48 655.92 93.27 o 8 16 0 24.53 52.32 32.32 o 2 17 0 59.07 21.55 21.06 o 4 17 0 154.68 98.59 35.13 o 6 17 0 87.23 79.25 34.81 o 8 17 0 178.95 202.42 58.54 o 0 18 0 74.17 111.13 40.41 o 2 18 0 7.86 83.40 34.05 o 4 18 0 1398.65 1367.83 134.15 o 6 18 0 0.83 24.65 24.89 o 2 19 0 703.57 776.68 99.76 o 4 19 0 1.99 -16.57 16.57 o 6 19 0 353.11 455.12 84.29 o 0 20 0 5093.86 5403.43 271.46 o 2 20 0 11.28 36.78 27.66 o 4 20 0 191.40 182.90 51.77 o 6 20 0 4.11 26.39 32.11 o 2 21 0 20.01 17.30 26.52 o 4 21 0 99.22 91.93 41.03 o 6 21 0 0.00 10.65 19.13 o 0 22 0 1407.17 1863.43 169.63 o 2 22 0 477.21 637.03 101.19 o 4 22 0 469.33 588.50 99.59 o 2 23 0 346.31 350.70 79.06 o 4 23 0 69.45 99.12 46.11 o 2 24 0 157.88 203.41 63.93 o 1 1 1 5255.38 4998.09 66.28 o 2 1 1 146.78 258.57 12.35 o 3 1 1 3524.61 4003.45 79.77 o 4 1 1 919.59 1053.79 105.10 o 5 1 1 2333.57 2401.97 56.28 o 6 1 1 1904.94 1899.42 54.44 o 7 1 1 3904.50 3846.91 83.53 o 8 1 1 466.69 392.48 28.77 o 9 1 1 50.62 75.32 13.53 o 1 2 1 1343.64 1129.21 23.70 o 2 2 1 66577.33 65915.49 438.24 o 3 2 1 2834.44 2783.29 49.43 o 4 2 1 28765.97 29769.66 207.60 o 5 2 1 609.28 549.25 40.72 o 6 2 1 1197.17 1271.60 49.85 o 7 2 1 1762.24 1894.80 58.75 o 8 2 1 317.58 295.17 24.72 o 9 2 1 66.37 125.98 23.01 o 1 3 1 15065.63 14237.66 83.79 o 2 3 1 7240.04 7041.25 71.89 o 3 3 1 212.64 244.83 15.91 o 4 3 1 2004.06 1914.39 48.25 o 5 3 1 1139.72 1272.54 48.96 o 6 3 1 207.79 218.34 19.17 o 7 3 1 636.98 565.43 32.72 o 8 3 1 69.09 62.83 22.54 o 9 3 1 96.33 87.99 17.77 o 0 4 1 573.79 733.22 30.20 o 1 4 1 1.24 3.43 3.74 o 2 4 1 1137.88 1208.19 28.11 o 3 4 1 39.86 70.35 9.59 o 4 4 1 687.09 790.80 32.19 o 5 4 1 1248.01 1238.53 43.79 o 6 4 1 1005.19 1055.41 59.73 o 7 4 1 175.93 140.11 19.09 o 8 4 1 2.05 -0.24 8.44 o 9 4 1 131.92 149.80 19.74 o 1 5 1 10882.06 11088.15 114.91 o 2 5 1 1418.53 1221.84 30.32 o 3 5 1 3974.19 4034.45 110.59 o 4 5 1 1631.32 1615.51 47.59 o 5 5 1 93.52 60.75 11.39 o 6 5 1 133.54 50.60 39.48 o 7 5 1 2.27 13.53 9.56 o 8 5 1 51.26 61.68 19.37 o 9 5 1 277.05 228.04 24.33 o 0 6 1 4116.29 4661.48 92.81 o 1 6 1 157.56 176.93 13.39 o 2 6 1 149.76 130.52 9.92 o 3 6 1 1192.85 1083.06 32.85 o 4 6 1 3518.79 3841.07 76.41 o 5 6 1 791.03 716.96 40.30 o 6 6 1 291.77 340.66 29.55 o 7 6 1 0.01 5.64 10.92 o 8 6 1 82.72 70.92 13.05 o 9 6 1 0.02 -1.75 7.92 o 1 7 1 2158.42 2365.01 45.67 o 2 7 1 1091.27 971.99 28.24 o 3 7 1 627.96 789.19 27.07 o 4 7 1 125.39 72.52 27.36 o 5 7 1 1461.63 1552.67 57.91 o 6 7 1 781.52 828.06 56.32 o 7 7 1 333.97 316.93 31.03 o 8 7 1 14.70 -1.06 11.71 o 9 7 1 16.52 -0.49 8.33 o 0 8 1 3150.73 2925.83 97.31 o 1 8 1 702.00 808.12 28.61 o 2 8 1 809.76 801.46 27.26 o 3 8 1 1592.03 1627.15 43.74 o 4 8 1 387.99 370.57 29.15 o 5 8 1 723.09 693.09 40.43 o 6 8 1 552.78 519.13 39.21 o 7 8 1 93.60 103.89 17.98 o 8 8 1 396.70 390.55 44.28 o 9 8 1 67.07 110.30 21.87 o 1 9 1 2992.49 3302.24 72.63 o 2 9 1 0.64 6.28 4.36 o 3 9 1 483.70 601.90 30.86 o 4 9 1 220.51 232.86 20.47 o 5 9 1 174.28 133.19 14.37 o 6 9 1 114.30 106.08 14.18 o 7 9 1 274.55 208.41 32.94 o 8 9 1 20.59 60.53 20.43 o 9 9 1 10.57 35.17 13.35 o 0 10 1 3652.74 4019.36 166.57 o 1 10 1 125.24 121.76 12.54 o 2 10 1 1078.16 1103.96 42.83 o 3 10 1 6.07 22.84 11.04 o 4 10 1 110.88 110.41 15.04 o 5 10 1 68.74 62.39 11.28 o 6 10 1 306.12 266.66 28.57 o 7 10 1 62.11 26.67 15.49 o 8 10 1 109.99 85.91 22.85 o 9 10 1 14.46 63.30 21.67 o 1 11 1 4844.95 5044.26 83.96 o 2 11 1 283.04 273.51 22.36 o 3 11 1 2029.97 2161.85 58.64 o 4 11 1 869.28 934.60 39.47 o 5 11 1 224.65 269.04 30.52 o 6 11 1 265.65 247.64 35.80 o 7 11 1 682.37 607.97 56.94 o 8 11 1 89.14 46.57 19.01 o 9 11 1 16.77 -18.16 18.16 o 0 12 1 1134.11 1081.94 82.09 o 1 12 1 685.70 745.19 35.82 o 2 12 1 3.07 4.31 6.24 o 3 12 1 657.12 635.92 64.82 o 4 12 1 1279.87 1214.19 73.71 o 5 12 1 103.40 94.54 22.15 o 6 12 1 1.53 1.30 15.61 o 7 12 1 50.67 22.88 16.79 o 8 12 1 100.72 78.88 34.41 o 9 12 1 44.96 46.99 15.09 o 1 13 1 36.19 23.92 9.87 o 2 13 1 125.48 159.49 28.21 o 3 13 1 464.97 487.39 47.47 o 4 13 1 56.56 28.60 15.19 o 5 13 1 87.75 76.79 20.70 o 6 13 1 308.63 306.61 41.31 o 7 13 1 4.76 -14.47 14.47 o 8 13 1 7.93 -3.80 14.78 o 9 13 1 65.87 103.01 27.47 o 0 14 1 32.64 22.31 14.07 o 1 14 1 68.60 86.09 15.69 o 2 14 1 37.82 27.41 22.99 o 3 14 1 2.46 -9.04 13.77 o 4 14 1 487.75 465.24 49.63 o 5 14 1 262.47 224.04 34.59 o 6 14 1 4.41 0.27 16.07 o 7 14 1 221.01 157.96 32.99 o 8 14 1 51.32 87.66 24.67 o 9 14 1 3.44 23.25 31.64 o 1 15 1 203.15 191.03 21.98 o 2 15 1 4.62 -15.75 15.75 o 3 15 1 6167.63 5612.42 171.08 o 4 15 1 12.27 -10.49 19.34 o 5 15 1 489.48 389.56 47.69 o 6 15 1 256.88 322.01 44.71 o 7 15 1 39.23 39.57 33.24 o 8 15 1 58.75 75.53 22.99 o 0 16 1 1.90 -5.09 12.74 o 1 16 1 5.54 15.56 12.17 o 2 16 1 237.82 246.28 61.23 o 3 16 1 8.95 4.91 16.56 o 4 16 1 156.24 138.84 27.40 o 5 16 1 334.43 323.69 45.56 o 6 16 1 5.17 -10.25 13.26 o 7 16 1 52.48 39.18 20.04 o 8 16 1 36.41 43.66 21.11 o 1 17 1 23.37 35.68 13.20 o 2 17 1 22.83 1.36 14.81 o 3 17 1 117.15 97.95 24.97 o 4 17 1 7.03 27.62 19.05 o 5 17 1 333.80 317.23 58.35 o 6 17 1 83.65 59.97 39.18 o 7 17 1 93.35 165.71 77.38 o 8 17 1 107.03 95.41 32.06 o 0 18 1 1422.33 1327.66 88.79 o 1 18 1 4.99 7.22 11.05 o 2 18 1 409.71 403.56 56.33 o 3 18 1 53.86 41.15 32.93 o 4 18 1 208.68 191.60 43.28 o 5 18 1 120.52 143.73 34.20 o 6 18 1 307.42 389.31 53.45 o 7 18 1 337.95 357.04 92.12 o 1 19 1 1920.90 2116.14 95.44 o 2 19 1 219.16 162.15 37.79 o 3 19 1 5.42 36.32 43.43 o 4 19 1 4.87 15.41 16.37 o 5 19 1 24.11 2.52 15.22 o 6 19 1 17.97 42.89 20.59 o 7 19 1 3.18 30.65 41.17 o 0 20 1 125.84 134.32 38.21 o 1 20 1 4.93 -4.73 26.12 o 2 20 1 580.61 613.73 65.76 o 3 20 1 8.86 11.90 14.88 o 4 20 1 4.41 -16.61 48.53 o 5 20 1 9.98 27.19 16.15 o 6 20 1 10.82 7.63 23.23 o 1 21 1 728.03 676.49 70.19 o 2 21 1 27.98 0.43 14.88 o 3 21 1 24.99 26.14 35.25 o 4 21 1 12.51 10.46 21.09 o 5 21 1 0.27 -15.64 22.26 o 6 21 1 0.47 -0.46 28.46 o 0 22 1 1.90 -15.38 20.01 o 1 22 1 46.93 72.62 27.00 o 2 22 1 261.28 371.30 53.69 o 3 22 1 89.35 125.21 34.55 o 4 22 1 29.71 102.36 30.74 o 5 22 1 4.28 11.01 15.56 o 1 23 1 245.86 345.55 88.49 o 2 23 1 241.81 313.28 72.72 o 3 23 1 53.08 110.56 33.90 o 4 23 1 0.48 -20.87 20.87 o 1 24 1 7.50 20.93 19.80 o 2 24 1 319.24 528.18 69.80 o 3 24 1 116.54 144.79 39.31 o 1 25 1 62.78 150.17 53.96 o 2 0 2 10924.95 10337.08 177.39 o 3 0 2 244.18 190.38 20.79 o 4 0 2 3579.58 3673.69 85.85 o 5 0 2 4101.46 4444.20 105.78 o 6 0 2 377.34 376.56 41.60 o 7 0 2 4085.48 4248.94 145.84 o 8 0 2 1046.00 1032.37 64.02 o 9 0 2 994.93 758.74 56.56 o 1 1 2 13680.60 13306.89 163.43 o 2 1 2 6192.71 5493.28 52.40 o 3 1 2 12452.80 12814.20 137.54 o 4 1 2 2308.17 2480.28 50.20 o 5 1 2 3508.47 3712.58 68.31 o 6 1 2 41.71 45.85 9.39 o 7 1 2 3309.15 3540.53 79.08 o 8 1 2 66.11 84.42 15.24 o 9 1 2 2001.73 2058.10 66.49 o 0 2 2 2442.35 2175.15 56.31 o 1 2 2 445.00 462.65 11.21 o 2 2 2 4475.13 4793.56 53.92 o 3 2 2 10.91 46.02 8.20 o 4 2 2 361.63 507.38 27.12 o 5 2 2 351.49 373.55 22.48 o 6 2 2 27.52 21.53 7.49 o 7 2 2 320.31 302.62 23.92 o 8 2 2 95.27 106.92 15.15 o 9 2 2 826.39 938.59 45.57 o 1 3 2 3422.55 2936.28 37.80 o 2 3 2 10.88 31.08 5.05 o 3 3 2 25003.76 24318.17 150.33 o 4 3 2 1787.33 2036.74 49.24 o 5 3 2 410.65 422.91 31.26 o 6 3 2 155.87 142.06 16.08 o 7 3 2 213.23 222.16 20.57 o 8 3 2 104.73 97.34 15.43 o 9 3 2 87.62 97.99 16.06 o 0 4 2 39242.86 38331.12 257.15 o 1 4 2 33.80 70.93 7.40 o 2 4 2 11285.67 10947.19 112.70 o 3 4 2 596.10 603.76 25.44 o 4 4 2 1822.69 1765.44 47.63 o 5 4 2 229.68 201.76 23.10 o 6 4 2 91.72 119.16 19.88 o 7 4 2 16.16 22.99 9.76 o 8 4 2 77.24 64.38 12.80 o 9 4 2 904.43 1123.25 60.00 o 1 5 2 11.11 17.64 5.33 o 2 5 2 2573.33 2228.56 44.57 o 3 5 2 4566.89 4266.98 61.14 o 4 5 2 5420.61 5452.57 99.75 o 5 5 2 56.77 26.34 15.98 o 6 5 2 1627.32 1653.04 132.37 o 7 5 2 0.01 -9.95 10.88 o 8 5 2 0.04 7.82 11.82 o 9 5 2 110.64 134.82 22.73 o 0 6 2 21385.39 20785.57 196.69 o 1 6 2 506.08 607.86 24.25 o 2 6 2 5130.21 5066.89 72.51 o 3 6 2 1158.06 1142.06 33.41 o 4 6 2 2210.82 2223.92 49.80 o 5 6 2 1404.40 1421.86 55.63 o 6 6 2 1049.09 1105.23 63.54 o 7 6 2 145.78 134.22 24.77 o 8 6 2 60.46 38.71 17.83 o 9 6 2 9.77 6.85 10.22 o 1 7 2 10.42 27.91 6.50 o 2 7 2 348.49 397.84 19.74 o 3 7 2 37.68 81.36 9.97 o 4 7 2 12.46 9.00 7.57 o 5 7 2 967.18 933.24 44.35 o 6 7 2 154.84 183.97 19.22 o 7 7 2 175.03 126.66 18.55 o 8 7 2 280.24 281.21 35.14 o 9 7 2 3.40 -0.67 11.60 o 0 8 2 13.49 -9.72 9.72 o 1 8 2 1032.67 1217.08 39.29 o 2 8 2 979.87 1185.54 36.09 o 3 8 2 494.42 396.82 21.73 o 4 8 2 2935.86 3124.40 80.26 o 5 8 2 207.86 255.62 24.59 o 6 8 2 4498.48 4610.95 107.13 o 7 8 2 61.43 97.91 14.62 o 8 8 2 1204.16 1112.57 73.56 o 9 8 2 22.94 34.78 13.72 o 1 9 2 7273.98 7975.11 122.37 o 2 9 2 595.85 472.45 21.70 o 3 9 2 650.36 804.22 36.09 o 4 9 2 349.35 341.66 24.57 o 5 9 2 282.08 310.03 22.32 o 6 9 2 425.78 406.10 29.27 o 7 9 2 31.57 88.34 16.53 o 8 9 2 804.95 745.00 61.09 o 9 9 2 7.48 6.50 11.88 o 0 10 2 352.72 437.77 38.04 o 1 10 2 0.55 10.51 6.03 o 2 10 2 348.52 305.06 27.41 o 3 10 2 1446.28 1433.95 56.35 o 4 10 2 191.83 220.93 18.89 o 5 10 2 126.44 139.83 18.82 o 6 10 2 186.04 188.47 24.04 o 7 10 2 4.57 -9.59 11.52 o 8 10 2 717.31 799.36 65.34 o 9 10 2 8.09 38.59 36.77 o 1 11 2 65.77 61.29 11.42 o 2 11 2 491.82 469.77 46.26 o 3 11 2 2810.98 2906.06 68.12 o 4 11 2 555.08 528.93 33.33 o 5 11 2 508.85 562.71 40.42 o 6 11 2 9.99 15.86 10.51 o 7 11 2 299.96 290.35 40.21 o 8 11 2 545.87 526.55 54.68 o 9 11 2 6.60 29.08 16.43 o 0 12 2 29.60 9.19 12.67 o 1 12 2 157.28 167.40 18.45 o 2 12 2 81.51 51.93 9.08 o 3 12 2 28.51 43.71 21.17 o 4 12 2 1.80 -2.13 9.85 o 5 12 2 52.65 28.92 15.08 o 6 12 2 247.80 210.21 32.82 o 7 12 2 32.91 29.56 13.46 o 8 12 2 22.81 1.88 10.36 o 9 12 2 55.54 87.79 26.70 o 1 13 2 1311.98 1306.83 60.25 o 2 13 2 234.99 273.48 28.05 o 3 13 2 2184.52 2042.47 96.22 o 4 13 2 30.93 48.10 22.32 o 5 13 2 99.94 158.81 49.51 o 6 13 2 388.13 489.15 52.26 o 7 13 2 4.73 5.47 14.81 o 8 13 2 7.39 -1.01 15.41 o 9 13 2 0.00 -25.74 25.74 o 0 14 2 922.94 1052.76 81.83 o 1 14 2 120.97 99.80 17.38 o 2 14 2 225.19 260.48 36.57 o 3 14 2 341.48 342.01 42.47 o 4 14 2 472.71 417.58 46.13 o 5 14 2 509.17 494.38 52.30 o 6 14 2 792.54 757.17 66.23 o 7 14 2 26.47 24.04 12.33 o 8 14 2 81.48 62.06 22.29 o 9 14 2 330.77 398.32 75.89 o 1 15 2 5.19 7.58 12.12 o 2 15 2 103.53 80.37 34.43 o 3 15 2 157.01 180.18 32.31 o 4 15 2 23.31 30.39 19.79 o 5 15 2 448.65 530.06 56.02 o 6 15 2 9.81 -6.77 11.75 o 7 15 2 2.53 -6.96 15.66 o 8 15 2 426.03 487.19 113.18 o 0 16 2 142.55 96.13 22.54 o 1 16 2 179.72 135.89 21.54 o 2 16 2 99.85 109.73 25.73 o 3 16 2 120.56 121.58 44.58 o 4 16 2 38.07 23.87 15.18 o 5 16 2 145.20 132.20 35.07 o 6 16 2 317.18 288.00 43.46 o 7 16 2 285.53 343.87 48.92 o 8 16 2 80.74 38.06 39.35 o 1 17 2 1410.39 1340.51 70.87 o 2 17 2 473.02 526.24 55.33 o 3 17 2 51.25 47.76 21.15 o 4 17 2 5.26 -9.12 16.45 o 5 17 2 126.86 92.54 42.21 o 6 17 2 1.14 -6.36 11.99 o 7 17 2 957.48 1115.53 89.12 o 8 17 2 146.09 221.27 41.28 o 0 18 2 61.35 50.33 20.26 o 1 18 2 9.45 27.16 16.26 o 2 18 2 262.45 214.33 36.71 o 3 18 2 15.68 0.76 21.86 o 4 18 2 13.35 4.93 28.21 o 5 18 2 0.69 -13.15 14.54 o 6 18 2 238.50 229.75 41.39 o 7 18 2 119.65 100.66 29.51 o 1 19 2 157.57 219.18 31.10 o 2 19 2 0.71 6.41 17.92 o 3 19 2 425.10 375.63 64.75 o 4 19 2 177.29 173.29 33.72 o 5 19 2 101.17 104.80 28.65 o 6 19 2 111.91 94.36 44.73 o 7 19 2 17.81 100.50 30.27 o 0 20 2 2391.11 2383.12 180.21 o 1 20 2 8.75 4.31 16.81 o 2 20 2 648.64 686.73 70.04 o 3 20 2 99.68 115.26 33.46 o 4 20 2 30.88 -7.01 17.33 o 5 20 2 121.19 206.98 40.03 o 6 20 2 275.83 314.49 50.72 o 1 21 2 582.82 615.32 55.51 o 2 21 2 17.03 8.85 16.22 o 3 21 2 12.32 11.41 24.42 o 4 21 2 67.29 97.88 27.30 o 5 21 2 13.99 22.61 27.31 o 6 21 2 364.50 458.21 61.95 o 0 22 2 701.90 840.45 113.61 o 1 22 2 46.07 110.37 29.22 o 2 22 2 107.00 130.50 31.06 o 3 22 2 49.74 44.51 55.58 o 4 22 2 1.33 22.68 16.82 o 5 22 2 25.38 -19.50 19.50 o 1 23 2 1495.84 1791.90 172.84 o 2 23 2 89.75 143.67 39.13 o 3 23 2 68.63 111.40 33.14 o 4 23 2 195.91 285.53 51.02 o 0 24 2 33.99 77.82 45.27 o 1 24 2 0.00 0.48 29.98 o 2 24 2 44.47 47.50 21.97 o 3 24 2 58.07 88.91 46.07 o 1 25 2 226.30 516.88 100.75 o 1 1 3 41551.80 37700.05 300.73 o 2 1 3 1001.73 616.66 20.27 o 3 1 3 2341.73 2901.63 40.96 o 4 1 3 2579.50 2406.30 47.68 o 5 1 3 363.57 500.24 27.99 o 6 1 3 13.18 18.44 8.35 o 7 1 3 6053.96 6339.37 103.58 o 8 1 3 26.18 40.74 12.46 o 9 1 3 258.51 238.17 36.03 o 0 2 3 4202.99 3640.26 79.49 o 1 2 3 1475.14 1791.40 28.31 o 2 2 3 5289.17 5043.25 46.40 o 3 2 3 9446.38 9532.57 108.13 o 4 2 3 5917.47 5864.12 85.96 o 5 2 3 4281.63 4259.13 80.70 o 6 2 3 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32 100.29 31.58 27.53 o 3 9 32 64.00 67.72 36.96 o 0 10 32 128.47 269.23 67.00 o 1 10 32 339.10 447.92 57.93 o 2 10 32 708.32 1004.48 139.51 o 1 11 32 149.48 203.09 42.25 o 1 1 33 132.76 195.68 33.16 o 2 1 33 49.84 32.27 56.64 o 3 1 33 812.31 693.20 82.42 o 4 1 33 0.48 -14.42 48.28 o 0 2 33 1180.47 1484.59 232.52 o 1 2 33 9.69 7.61 13.36 o 2 2 33 703.11 1054.65 98.62 o 3 2 33 31.91 24.39 16.76 o 4 2 33 496.79 538.22 77.38 o 1 3 33 4.99 -6.22 10.91 o 2 3 33 78.80 84.06 32.93 o 3 3 33 6.44 14.95 19.54 o 4 3 33 163.52 180.21 48.09 o 0 4 33 126.46 170.99 37.65 o 1 4 33 0.11 11.62 11.06 o 2 4 33 261.74 188.32 69.69 o 3 4 33 1.30 28.78 23.14 o 1 5 33 546.55 591.73 47.37 o 2 5 33 82.23 118.96 37.82 o 3 5 33 152.94 169.39 46.53 o 0 6 33 62.87 62.53 55.70 o 1 6 33 0.68 8.36 16.00 o 2 6 33 24.81 35.77 19.53 o 3 6 33 36.58 62.98 35.41 o 1 7 33 5.99 18.36 13.16 o 2 7 33 227.02 305.33 54.61 o 3 7 33 23.19 -20.93 20.93 o 0 8 33 33.95 53.52 37.05 o 1 8 33 188.95 142.87 23.90 o 2 8 33 44.37 105.98 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