#------------------------------------------------------------------------------ #$Date: 2012-09-11 12:26:43 +0300 (Tue, 11 Sep 2012) $ #$Revision: 66590 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/43/2234345.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2234345_Fobs loop_ _publ_author_name 'Isobe, Hiroyuki' 'Matsuno, Taisuke' 'Hitosugi, Shunpei' 'Nakanishi, Waka' _publ_section_title ; 2,11-Dibromo-5,8-dibutyl[4]helicene ; _journal_coeditor_code NK2148 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1239 _journal_volume 68 _journal_year 2012 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 75.012 _cell_angle_beta 84.682 _cell_angle_gamma 79.067 _cell_length_a 7.6112 _cell_length_b 13.3938 _cell_length_c 22.5517 _exptl_crystal_F_000 1008.00 _reflns_d_resolution_high 0.7563 _[local]_cod_data_source_file nk2148Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ' _shelx_refln_list_code 4 _shelx_f_calc_maximum 305.61 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 10115.90 10431.81 115.87 o 2 0 0 65269.14 69518.05 718.46 o 3 0 0 188.88 311.65 25.64 o 4 0 0 218.21 223.11 22.29 o 5 0 0 713.00 737.91 80.06 o 6 0 0 3409.60 3673.29 80.82 o 7 0 0 809.79 933.14 84.21 o 8 0 0 2274.43 2053.65 267.23 o 9 0 0 988.26 1042.07 65.05 o -9 1 0 11.19 -40.92 40.92 o -8 1 0 1146.79 1171.95 59.88 o -7 1 0 10.34 3.84 28.03 o -6 1 0 10590.09 10276.82 184.46 o -5 1 0 7947.84 7922.61 110.33 o -4 1 0 1.18 -15.96 15.96 o -3 1 0 425.61 460.26 23.58 o -2 1 0 2685.99 2483.25 37.54 o -1 1 0 12404.73 12423.30 132.70 o 0 1 0 2561.68 2704.85 42.78 o 1 1 0 1840.88 1845.52 27.65 o 2 1 0 12550.63 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