#------------------------------------------------------------------------------
#$Date: 2016-04-03 06:38:17 +0300 (Sun, 03 Apr 2016) $
#$Revision: 181266 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/44/2234485.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2234485_Fobs
loop_
_publ_author_name
'Burgoyne, Andrew R.'
'Meijboom, Reinout'
'Ogutu, Hezron'
_publ_section_title
;
trans-Dichloridobis[dicyclohexyl(phenyl)phosphane-\kP]palladium(II)
;
_journal_coeditor_code ZL2455
_journal_issue 4
_journal_name_full 'Acta Crystallographica Section E'
_journal_page_first m404
_journal_volume 68
_journal_year 2012
_space_group_IT_number 2
_symmetry_space_group_name_Hall '-P 1'
_symmetry_space_group_name_H-M 'P -1'
_cell_angle_alpha 113.115
_cell_angle_beta 107.321
_cell_angle_gamma 91.625
_cell_length_a 9.4390
_cell_length_b 10.0950
_cell_length_c 10.6230
_exptl_crystal_F_000 380.00
_reflns_d_resolution_high 0.8455
_cod_data_source_file zl2455Isup2.hkl
_cod_data_source_block I
#BEGIN Tags that were not found in dictionaries:
_shelx_title ' '
_shelx_refln_list_code 4
_shelx_f_calc_maximum 125.19
_shelx_f_squared_multiplier 1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
1 0 0 2215.81 2008.92 73.00 o
2 0 0 1519.62 1589.44 67.11 o
3 0 0 13.60 18.17 2.35 o
4 0 0 461.37 405.85 15.31 o
5 0 0 1750.55 1724.68 45.94 o
6 0 0 2632.09 2558.30 37.20 o
7 0 0 12.48 17.14 1.64 o
8 0 0 392.34 415.00 7.21 o
9 0 0 41.32 46.71 2.10 o
10 0 0 103.88 98.43 2.78 o
-10 1 0 110.92 109.66 3.87 o
-9 1 0 36.67 40.82 2.19 o
-8 1 0 243.42 263.01 5.07 o
-7 1 0 571.40 575.81 8.86 o
-6 1 0 2095.61 2036.21 47.85 o
-5 1 0 2163.36 2118.01 59.93 o
-4 1 0 358.63 340.59 15.31 o
-3 1 0 152.95 152.22 7.40 o
-2 1 0 2206.99 2222.36 93.85 o
-1 1 0 5028.29 4755.17 130.62 o
0 1 0 9074.76 9065.85 232.93 o
1 1 0 3160.01 3019.26 77.60 o
2 1 0 1267.95 1264.52 37.93 o
3 1 0 238.89 285.09 10.60 o
4 1 0 1678.12 1529.73 56.35 o
5 1 0 2136.91 2096.37 42.02 o
6 1 0 728.49 711.12 12.55 o
7 1 0 684.27 729.43 10.13 o
8 1 0 23.32 32.17 1.73 o
9 1 0 163.18 170.17 3.51 o
10 1 0 347.23 344.59 8.24 o
-10 2 0 291.62 292.15 8.58 o
-9 2 0 218.46 224.28 4.95 o
-8 2 0 189.17 200.38 4.46 o
-7 2 0 657.72 686.24 11.98 o
-6 2 0 2266.40 2247.27 41.24 o
-5 2 0 1039.91 962.40 59.63 o
-4 2 0 639.85 688.93 29.94 o
-3 2 0 355.43 399.13 17.49 o
-2 2 0 988.41 946.10 40.37 o
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0 2 0 774.25 730.04 18.97 o
1 2 0 163.73 187.96 5.11 o
2 2 0 0.95 4.23 0.55 o
3 2 0 0.43 13.91 1.01 o
4 2 0 4734.95 4409.06 161.30 o
5 2 0 4630.47 4508.44 82.07 o
6 2 0 400.17 406.28 4.69 o
7 2 0 155.06 167.72 2.49 o
8 2 0 21.02 20.57 1.27 o
9 2 0 226.86 218.28 4.70 o
-10 3 0 300.96 302.58 8.91 o
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-7 3 0 477.89 475.93 10.56 o
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-5 3 0 604.50 551.60 12.73 o
-4 3 0 7.89 22.87 2.69 o
-3 3 0 0.95 7.91 1.35 o
-2 3 0 4074.37 3952.14 86.76 o
-1 3 0 5993.71 6132.19 134.31 o
0 3 0 2582.01 2578.61 66.48 o
1 3 0 465.50 492.92 13.02 o
2 3 0 185.85 176.96 5.11 o
3 3 0 834.01 821.04 21.59 o
4 3 0 1383.42 1273.01 61.64 o
5 3 0 2817.90 2747.12 32.77 o
6 3 0 1378.16 1415.12 15.14 o
7 3 0 2.84 6.05 0.86 o
8 3 0 54.77 53.22 1.78 o
9 3 0 256.64 249.06 5.12 o
-10 4 0 235.07 238.33 7.23 o
-9 4 0 586.22 574.25 14.38 o
-8 4 0 140.60 161.37 4.77 o
-7 4 0 1071.47 1075.84 17.92 o
-6 4 0 567.46 554.71 8.81 o
-5 4 0 210.12 205.24 6.23 o
-4 4 0 28.48 25.04 3.53 o
-3 4 0 166.43 168.19 8.41 o
-2 4 0 2699.65 2913.38 80.41 o
-1 4 0 15671.43 16676.73 365.54 o
0 4 0 606.12 562.44 14.93 o
1 4 0 75.71 72.35 2.50 o
2 4 0 2.42 4.83 0.95 o
3 4 0 780.58 720.08 26.96 o
4 4 0 1359.56 1244.18 22.53 o
5 4 0 1577.16 1505.98 22.10 o
6 4 0 63.59 73.80 1.55 o
7 4 0 30.37 27.23 1.01 o
8 4 0 0.60 0.86 0.94 o
-9 5 0 592.46 590.53 16.82 o
-8 5 0 90.87 94.44 3.06 o
-7 5 0 323.48 343.42 6.16 o
-6 5 0 765.90 762.60 11.97 o
-5 5 0 289.64 275.42 4.35 o
-4 5 0 373.55 377.58 7.40 o
-3 5 0 1235.03 1225.79 28.51 o
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-1 5 0 1818.28 1863.31 41.32 o
0 5 0 836.87 878.19 23.13 o
1 5 0 0.31 3.00 0.65 o
2 5 0 23.64 26.10 1.17 o
3 5 0 906.04 842.52 11.08 o
4 5 0 1893.76 1782.54 21.89 o
5 5 0 920.60 938.97 15.63 o
6 5 0 132.43 134.92 2.97 o
7 5 0 7.23 5.05 0.90 o
8 5 0 143.49 128.68 4.83 o
-9 6 0 272.57 281.22 8.41 o
-8 6 0 236.38 255.58 6.89 o
-7 6 0 23.33 32.38 3.52 o
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-5 6 0 1697.50 1622.88 22.37 o
-4 6 0 169.35 150.95 2.05 o
-3 6 0 610.43 586.89 7.03 o
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0 6 0 355.68 337.80 6.07 o
1 6 0 199.93 193.94 3.63 o
2 6 0 7.73 12.89 0.63 o
3 6 0 1945.07 1841.82 19.89 o
4 6 0 2222.95 2200.69 28.22 o
5 6 0 280.76 286.91 5.49 o
6 6 0 41.19 33.31 1.53 o
7 6 0 0.76 0.53 0.79 o
-9 7 0 83.14 96.88 3.53 o
-8 7 0 121.88 135.50 4.82 o
-7 7 0 348.33 350.76 7.72 o
-6 7 0 236.37 238.24 6.17 o
-5 7 0 433.97 410.62 6.21 o
-4 7 0 279.94 261.51 3.79 o
-3 7 0 416.29 412.24 5.20 o
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-1 7 0 1316.27 1219.32 13.83 o
0 7 0 295.99 281.59 3.30 o
1 7 0 6.25 9.12 0.59 o
2 7 0 201.77 198.92 3.12 o
3 7 0 715.26 699.98 8.82 o
4 7 0 1291.24 1316.13 18.86 o
5 7 0 502.48 507.55 8.78 o
6 7 0 13.20 12.02 1.43 o
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-4 8 0 315.82 306.37 5.38 o
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-2 8 0 355.13 395.68 6.27 o
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0 8 0 688.33 680.78 10.18 o
1 8 0 26.44 26.92 1.82 o
2 8 0 492.31 493.96 7.39 o
3 8 0 492.83 489.16 8.65 o
4 8 0 621.58 629.69 10.73 o
5 8 0 137.18 137.73 4.02 o
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-6 9 0 337.11 343.41 5.16 o
-5 9 0 124.64 135.28 2.61 o
-4 9 0 148.91 157.69 2.70 o
-3 9 0 408.48 411.90 5.45 o
-2 9 0 461.62 475.85 8.00 o
-1 9 0 121.50 126.32 3.07 o
0 9 0 82.49 78.34 2.46 o
1 9 0 238.91 242.73 4.47 o
2 9 0 299.35 313.07 5.37 o
3 9 0 626.03 607.92 9.48 o
4 9 0 426.65 421.12 12.19 o
-5 10 0 214.77 223.21 5.08 o
-4 10 0 119.36 124.58 3.47 o
-3 10 0 162.71 169.50 3.49 o
-2 10 0 456.73 451.22 7.32 o
-1 10 0 322.84 321.57 6.35 o
0 10 0 103.93 106.04 2.35 o
1 10 0 26.94 21.52 1.01 o
2 10 0 313.73 311.87 6.06 o
0 -11 1 700.99 685.23 19.68 o
1 -11 1 202.40 212.77 6.90 o
2 -11 1 49.58 53.15 2.52 o
-3 -10 1 109.86 107.48 2.50 o
-2 -10 1 131.95 132.46 3.23 o
-1 -10 1 276.43 275.82 4.82 o
0 -10 1 464.33 480.70 9.47 o
1 -10 1 410.24 422.13 8.21 o
2 -10 1 24.98 22.05 1.02 o
3 -10 1 11.26 15.07 0.87 o
4 -10 1 247.72 255.15 4.99 o
5 -10 1 1018.47 985.87 14.27 o
6 -10 1 339.57 315.66 6.19 o
-5 -9 1 168.50 178.96 4.79 o
-4 -9 1 346.99 336.38 6.05 o
-3 -9 1 128.11 133.74 3.52 o
-2 -9 1 591.28 596.94 9.58 o
-1 -9 1 514.67 519.59 8.50 o
0 -9 1 370.67 369.45 6.77 o
1 -9 1 108.82 109.97 2.47 o
2 -9 1 62.37 61.81 2.59 o
3 -9 1 150.51 137.94 2.89 o
4 -9 1 652.10 647.46 12.61 o
5 -9 1 923.94 919.48 16.34 o
6 -9 1 394.20 388.16 6.21 o
7 -9 1 16.08 16.12 1.05 o
-6 -8 1 97.61 90.10 4.12 o
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-4 -8 1 268.52 278.63 5.43 o
-3 -8 1 718.39 722.49 11.01 o
-2 -8 1 540.48 536.13 7.18 o
-1 -8 1 617.34 601.44 9.12 o
0 -8 1 454.75 426.59 6.04 o
1 -8 1 51.04 59.66 1.81 o
2 -8 1 26.28 34.52 1.56 o
3 -8 1 379.06 351.86 5.08 o
4 -8 1 761.20 718.04 9.14 o
5 -8 1 1397.68 1399.03 19.29 o
6 -8 1 113.24 113.14 2.95 o
7 -8 1 1.97 2.57 0.95 o
8 -8 1 14.79 16.82 1.35 o
-7 -7 1 0.35 0.93 1.14 o
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-5 -7 1 646.64 668.18 11.46 o
-4 -7 1 368.27 373.50 6.94 o
-3 -7 1 803.73 798.34 10.80 o
-2 -7 1 12.84 17.95 0.82 o
-1 -7 1 708.92 654.06 7.05 o
0 -7 1 294.19 293.13 3.77 o
1 -7 1 381.52 382.20 4.85 o
2 -7 1 478.35 453.08 5.35 o
3 -7 1 741.44 720.13 8.58 o
4 -7 1 654.57 615.52 7.62 o
5 -7 1 1258.34 1282.37 18.16 o
6 -7 1 4.05 7.27 1.09 o
7 -7 1 83.99 77.74 2.88 o
8 -7 1 141.25 145.89 6.98 o
-8 -6 1 104.86 89.43 2.11 o
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-3 -6 1 435.61 433.29 5.12 o
-2 -6 1 56.50 60.30 1.55 o
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2 -6 1 1246.62 1249.36 24.97 o
3 -6 1 694.87 633.86 14.04 o
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8 -6 1 263.99 263.78 7.15 o
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-5 -5 1 1531.68 1503.80 24.57 o
-4 -5 1 1755.77 1672.18 19.52 o
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-2 -5 1 626.78 620.25 15.15 o
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0 -5 1 1298.47 1321.84 34.43 o
1 -5 1 1257.67 1379.03 38.36 o
2 -5 1 50.83 102.09 5.89 o
3 -5 1 1365.85 1261.91 22.71 o
4 -5 1 2532.09 2455.30 57.76 o
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6 -5 1 89.57 87.92 2.39 o
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8 -5 1 138.99 147.42 4.63 o
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-8 -4 1 2.47 -0.20 0.91 o
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-6 -4 1 375.57 395.84 5.45 o
-5 -4 1 2103.72 2021.94 36.05 o
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-3 -4 1 816.42 825.25 21.82 o
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0 -4 1 3179.72 3322.52 85.63 o
1 -4 1 1201.55 1261.59 27.91 o
2 -4 1 13.58 17.83 2.52 o
3 -4 1 320.50 278.70 12.78 o
4 -4 1 2071.48 2096.38 46.15 o
5 -4 1 609.10 577.75 12.51 o
6 -4 1 139.89 134.72 3.05 o
7 -4 1 100.29 110.17 2.71 o
8 -4 1 879.40 871.05 21.32 o
9 -4 1 624.49 623.24 15.57 o
10 -4 1 339.53 323.10 9.25 o
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-8 -3 1 23.50 16.84 0.90 o
-7 -3 1 185.00 195.65 2.87 o
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-5 -3 1 1901.14 1734.42 52.22 o
-4 -3 1 1077.67 1064.32 27.83 o
-3 -3 1 497.88 599.86 15.88 o
-2 -3 1 208.16 199.84 5.59 o
-1 -3 1 320.68 288.56 8.91 o
0 -3 1 2788.85 2919.50 61.31 o
1 -3 1 920.72 873.40 16.54 o
2 -3 1 4801.00 4618.96 194.60 o
3 -3 1 1240.26 1200.57 51.13 o
4 -3 1 1766.55 1868.98 79.39 o
5 -3 1 277.50 251.87 7.52 o
6 -3 1 278.91 286.22 6.02 o
7 -3 1 179.41 197.07 4.33 o
8 -3 1 1222.80 1229.02 23.29 o
9 -3 1 515.34 521.47 13.23 o
10 -3 1 169.11 169.37 5.21 o
-10 -2 1 580.11 557.23 11.90 o
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-8 -2 1 36.78 35.81 1.39 o
-7 -2 1 13.08 17.20 1.28 o
-6 -2 1 1743.10 1802.16 18.46 o
-5 -2 1 4442.40 4152.53 131.86 o
-4 -2 1 187.96 171.39 6.73 o
-3 -2 1 914.94 989.67 25.75 o
-2 -2 1 570.02 598.20 15.64 o
-1 -2 1 6176.22 6120.77 157.58 o
0 -2 1 8219.57 8253.97 212.11 o
1 -2 1 4760.72 4531.84 190.73 o
2 -2 1 2018.82 1987.89 84.27 o
3 -2 1 2224.62 2227.07 94.19 o
4 -2 1 482.16 431.27 19.93 o
5 -2 1 726.84 742.92 18.48 o
6 -2 1 197.70 191.68 4.95 o
7 -2 1 132.46 129.40 3.05 o
8 -2 1 485.31 510.93 10.20 o
9 -2 1 823.55 826.68 23.04 o
10 -2 1 108.56 98.06 3.53 o
-10 -1 1 319.99 313.25 7.04 o
-9 -1 1 11.03 13.43 1.18 o
-8 -1 1 81.38 96.70 2.59 o
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-6 -1 1 3306.34 3266.71 61.80 o
-5 -1 1 2583.04 2381.04 66.39 o
-4 -1 1 461.35 421.50 15.47 o
-3 -1 1 1224.05 1209.04 31.34 o
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0 -1 1 2176.75 2301.91 83.59 o
1 -1 1 1226.03 1185.10 61.22 o
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3 -1 1 2606.24 2740.23 115.72 o
4 -1 1 8.93 5.89 2.35 o
5 -1 1 352.15 349.00 10.02 o
6 -1 1 579.18 566.68 9.49 o
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-5 0 1 2529.44 2389.15 63.29 o
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1 0 1 4.52 19.68 3.03 o
2 0 1 3.02 14.80 2.19 o
4 0 1 1100.01 995.04 48.78 o
5 0 1 1061.07 994.29 35.58 o
6 0 1 275.80 267.88 3.79 o
7 0 1 1241.86 1306.23 22.96 o
8 0 1 492.89 510.91 8.63 o
9 0 1 493.62 512.30 10.94 o
10 0 1 120.48 118.41 4.04 o
-10 1 1 120.23 127.83 3.42 o
-9 1 1 7.59 6.64 0.91 o
-8 1 1 14.72 16.53 1.59 o
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-2 1 1 7.99 33.13 1.68 o
-1 1 1 5373.25 5307.79 116.43 o
0 1 1 1176.79 1175.07 30.45 o
1 1 1 14521.52 14624.03 531.50 o
2 1 1 1034.08 1017.44 30.40 o
3 1 1 63.55 55.84 5.21 o
4 1 1 1388.97 1314.71 42.60 o
5 1 1 1370.37 1423.54 35.46 o
6 1 1 136.77 143.12 2.56 o
7 1 1 1464.69 1540.02 26.15 o
8 1 1 256.02 266.92 5.03 o
9 1 1 158.87 175.58 4.31 o
-10 2 1 53.52 54.18 2.14 o
-9 2 1 6.76 7.93 1.71 o
-8 2 1 142.40 150.80 3.40 o
-7 2 1 1460.00 1442.33 22.20 o
-6 2 1 2373.96 2239.50 46.93 o
-5 2 1 547.58 480.49 15.86 o
-4 2 1 7.34 14.32 1.43 o
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0 2 1 5284.62 5237.51 134.63 o
1 2 1 1630.58 1642.00 42.46 o
2 2 1 152.66 161.43 4.19 o
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9 2 1 264.27 272.22 6.20 o
-10 3 1 47.43 49.28 2.69 o
-9 3 1 66.50 72.74 4.34 o
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-6 3 1 1379.36 1269.31 26.82 o
-5 3 1 889.48 937.05 24.00 o
-4 3 1 17.09 20.98 2.19 o
-3 3 1 1234.45 1240.26 34.50 o
-2 3 1 1659.76 1666.37 36.85 o
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0 3 1 1146.15 1137.17 29.61 o
1 3 1 481.05 481.69 12.84 o
2 3 1 2.85 10.81 1.01 o
3 3 1 873.19 898.83 33.30 o
4 3 1 744.33 682.53 15.76 o
5 3 1 948.92 952.10 10.62 o
6 3 1 397.08 423.32 5.12 o
7 3 1 141.06 150.11 2.58 o
8 3 1 310.92 317.46 6.02 o
9 3 1 362.18 338.24 11.27 o
-10 4 1 126.84 130.69 4.54 o
-9 4 1 20.45 22.56 3.36 o
-8 4 1 198.84 204.71 5.59 o
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-6 4 1 1151.51 1096.24 17.59 o
-5 4 1 224.89 215.65 5.64 o
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7 4 1 372.03 373.04 4.98 o
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1 -3 11 167.79 162.70 4.39 o
-7 -2 11 72.58 70.22 5.21 o
-6 -2 11 1095.41 1089.01 17.77 o
-5 -2 11 1047.76 1068.18 17.42 o
-4 -2 11 425.36 411.94 7.10 o
-3 -2 11 67.57 57.63 2.58 o
-2 -2 11 0.37 2.30 0.83 o
-1 -2 11 445.95 431.94 7.56 o
0 -2 11 346.12 335.27 22.20 o
1 -2 11 364.12 349.85 12.95 o
-7 -1 11 157.77 141.79 4.37 o
-6 -1 11 810.85 769.13 13.64 o
-5 -1 11 998.95 964.91 15.77 o
-4 -1 11 154.99 157.06 3.10 o
-3 -1 11 0.35 2.59 1.18 o
-2 -1 11 88.40 78.94 2.01 o
-1 -1 11 511.35 501.72 8.92 o
0 -1 11 387.60 389.20 14.13 o
-6 0 11 768.15 762.43 19.51 o
-5 0 11 522.91 509.48 14.80 o
-4 0 11 39.78 37.00 1.86 o
-3 0 11 17.45 16.98 1.85 o
-2 0 11 322.05 310.13 9.23 o
-1 0 11 724.72 692.99 22.03 o
-4 1 11 31.74 36.83 2.19 o
-3 1 11 4.27 4.88 1.18 o
-4 -7 12 21.15 18.33 1.35 o
-3 -7 12 147.48 89.82 5.72 o
-5 -6 12 70.65 66.61 3.03 o
-4 -6 12 55.32 51.47 2.52 o
-3 -6 12 337.15 290.00 35.91 o
-2 -6 12 832.17 775.04 24.39 o
-1 -6 12 443.48 405.85 13.12 o
-6 -5 12 142.94 134.72 4.71 o
-5 -5 12 149.55 144.98 5.05 o
-4 -5 12 103.68 99.23 3.87 o
-3 -5 12 658.26 553.27 74.34 o
-2 -5 12 519.26 484.95 9.61 o
-1 -5 12 307.93 286.77 9.59 o
-6 -4 12 231.79 222.02 7.06 o
-5 -4 12 176.11 174.25 5.72 o
-4 -4 12 141.03 124.97 4.37 o
-3 -4 12 751.18 686.54 12.69 o
-2 -4 12 531.75 481.17 10.80 o
-5 -3 12 68.72 66.78 2.14 o
-4 -3 12 186.17 172.13 9.33 o
-3 -3 12 345.11 324.61 8.72 o
-2 -3 12 528.91 485.31 12.11 o
-5 -2 12 72.63 62.23 2.86 o
-4 -2 12 205.40 186.36 5.89 o
-3 -2 12 402.28 376.79 7.35 o
-2 -2 12 483.48 438.32 11.10 o