#------------------------------------------------------------------------------ #$Date: 2012-09-11 12:26:43 +0300 (Tue, 11 Sep 2012) $ #$Revision: 66590 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/45/2234506.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2234506_Fobs loop_ _publ_author_name 'Wei, Bin' _publ_section_title ; Bis(1H-imidazol-3-ium) naphthalene-1,5-disulfonate ; _journal_coeditor_code BH2419 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1529 _journal_volume 68 _journal_year 2012 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 93.663 _cell_angle_beta 103.296 _cell_angle_gamma 96.772 _cell_length_a 6.6764 _cell_length_b 6.7958 _cell_length_c 10.2510 _exptl_crystal_F_000 220.00 _reflns_d_resolution_high 0.7701 _[local]_cod_data_source_file bh2419Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' a in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 73.50 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 817.86 790.62 6.73 o 2 0 0 205.99 223.95 6.91 o 3 0 0 874.03 919.91 11.54 o 4 0 0 12.20 12.11 0.31 o 5 0 0 50.85 43.87 0.90 o 6 0 0 9.04 10.60 1.94 o 7 0 0 9.58 11.43 1.14 o 8 0 0 3.74 4.87 0.71 o -8 1 0 135.78 135.83 5.24 o -7 1 0 40.27 40.23 1.78 o -6 1 0 222.78 213.23 4.09 o -5 1 0 0.06 0.38 0.14 o -4 1 0 653.06 676.50 10.02 o -3 1 0 329.37 319.70 4.31 o -2 1 0 119.02 97.38 1.05 o -1 1 0 377.26 405.43 4.97 o 0 1 0 180.08 180.46 3.67 o 2 1 0 158.11 129.94 1.81 o 3 1 0 528.21 495.51 9.08 o 4 1 0 338.20 358.75 5.54 o 5 1 0 1.94 2.81 0.61 o 6 1 0 45.67 41.01 1.03 o 7 1 0 1.19 1.43 0.57 o 8 1 0 32.25 39.57 3.42 o -8 2 0 0.81 1.12 0.52 o -7 2 0 2.40 3.54 0.71 o -6 2 0 74.57 80.48 2.59 o -5 2 0 165.37 158.90 2.89 o -4 2 0 310.01 301.60 4.73 o -3 2 0 181.56 210.27 2.83 o -2 2 0 1.53 17.63 1.59 o -1 2 0 1025.55 1078.50 31.42 o 0 2 0 4139.10 4227.16 90.68 o 1 2 0 161.84 186.93 3.15 o 2 2 0 81.75 81.38 1.42 o 3 2 0 157.41 177.53 3.38 o 4 2 0 253.74 235.98 6.84 o 5 2 0 100.41 106.38 2.20 o 6 2 0 0.55 1.38 0.23 o 7 2 0 9.18 8.68 1.28 o -8 3 0 40.90 42.03 2.22 o -7 3 0 0.01 0.07 0.28 o -6 3 0 2.29 3.93 0.62 o -5 3 0 12.55 11.68 0.43 o -4 3 0 117.04 119.38 2.09 o -3 3 0 106.40 97.60 8.96 o -2 3 0 256.03 248.38 6.35 o -1 3 0 5.60 6.72 0.24 o 0 3 0 148.14 151.22 3.25 o 1 3 0 5.19 3.73 0.37 o 2 3 0 22.29 20.35 0.52 o 3 3 0 2.34 2.31 0.23 o 4 3 0 80.69 75.27 2.13 o 5 3 0 21.90 21.45 0.93 o 6 3 0 78.40 79.41 3.40 o 7 3 0 94.10 90.38 5.03 o -7 4 0 1.37 1.40 0.52 o -6 4 0 69.15 70.48 1.73 o -5 4 0 8.06 8.10 0.66 o -4 4 0 97.95 94.99 1.85 o -3 4 0 0.00 0.23 0.21 o -2 4 0 673.50 671.85 15.80 o -1 4 0 17.48 14.77 0.30 o 0 4 0 342.67 357.93 5.00 o 1 4 0 62.43 64.29 1.43 o 2 4 0 106.26 104.14 1.85 o 3 4 0 159.89 160.52 4.02 o 4 4 0 454.80 467.16 12.76 o 5 4 0 128.55 128.94 4.65 o 6 4 0 20.52 20.18 1.19 o -7 5 0 2.85 4.69 0.88 o -6 5 0 8.04 8.76 0.64 o -5 5 0 18.73 16.40 1.13 o -4 5 0 171.94 171.49 3.42 o -3 5 0 438.67 448.99 7.97 o -2 5 0 169.56 156.41 2.72 o -1 5 0 67.23 63.63 1.61 o 0 5 0 72.58 64.22 1.13 o 1 5 0 0.08 1.34 0.23 o 2 5 0 97.14 94.13 2.11 o 3 5 0 38.37 38.93 1.09 o 4 5 0 52.79 49.85 1.39 o 5 5 0 1.91 1.78 0.44 o 6 5 0 31.37 32.59 2.37 o -6 6 0 64.67 66.87 4.25 o -5 6 0 2.90 3.08 0.47 o -4 6 0 36.59 32.14 1.41 o -3 6 0 67.28 63.73 2.28 o -2 6 0 245.09 235.71 6.45 o -1 6 0 44.92 42.88 1.58 o 0 6 0 52.34 47.87 2.00 o 1 6 0 81.97 74.52 1.64 o 2 6 0 25.25 26.70 1.22 o 3 6 0 36.89 36.73 1.17 o 4 6 0 33.61 33.47 2.20 o 5 6 0 14.11 15.62 1.13 o -5 7 0 1.12 1.36 0.48 o -4 7 0 24.15 24.20 1.32 o -3 7 0 45.70 48.61 2.19 o -2 7 0 0.67 0.28 0.27 o -1 7 0 27.88 27.44 1.63 o 0 7 0 23.37 26.46 1.26 o 1 7 0 25.37 25.21 2.92 o 2 7 0 75.76 76.29 2.75 o 3 7 0 13.53 15.17 1.86 o 4 7 0 34.85 34.53 2.94 o -4 8 0 14.66 14.90 1.09 o -3 8 0 10.12 7.19 0.81 o -2 8 0 40.84 39.97 1.89 o -1 8 0 1.13 2.65 0.56 o 0 8 0 13.46 12.75 1.42 o 1 8 0 0.00 0.24 0.54 o 2 8 0 28.69 28.84 2.64 o -2 -8 1 12.48 10.96 1.71 o -1 -8 1 84.98 84.41 5.27 o 0 -8 1 9.16 9.40 0.77 o 1 -8 1 11.41 12.09 0.88 o 2 -8 1 1.20 1.97 0.43 o 3 -8 1 100.84 107.10 4.37 o 4 -8 1 10.07 14.72 1.69 o -4 -7 1 46.21 46.87 3.69 o -3 -7 1 209.39 210.81 15.19 o -2 -7 1 1.13 1.29 0.40 o -1 -7 1 0.58 1.64 0.49 o 0 -7 1 0.00 1.52 0.91 o 1 -7 1 24.32 24.08 1.14 o 2 -7 1 26.17 26.89 1.29 o 3 -7 1 7.98 8.34 0.73 o 4 -7 1 1.40 1.61 0.43 o 5 -7 1 1.38 2.33 0.79 o -5 -6 1 7.33 7.67 0.81 o -4 -6 1 10.49 11.78 1.24 o -3 -6 1 26.96 25.02 1.59 o -2 -6 1 59.00 57.83 1.44 o -1 -6 1 267.15 263.85 5.12 o 0 -6 1 80.97 75.71 2.44 o 1 -6 1 7.63 9.05 0.43 o 2 -6 1 103.29 107.44 2.32 o 3 -6 1 53.30 50.67 1.23 o 4 -6 1 16.55 16.20 1.32 o 5 -6 1 27.04 26.29 1.65 o 6 -6 1 0.03 -0.06 0.48 o -6 -5 1 0.01 0.10 0.28 o -5 -5 1 63.45 60.90 2.51 o -4 -5 1 43.95 44.77 1.81 o -3 -5 1 208.65 200.38 3.89 o -2 -5 1 0.00 1.21 0.23 o -1 -5 1 17.65 18.42 0.48 o 0 -5 1 29.77 27.09 1.33 o 1 -5 1 499.07 487.65 8.16 o 2 -5 1 21.34 26.49 1.08 o 3 -5 1 4.95 7.06 1.33 o 4 -5 1 0.14 0.49 0.17 o 5 -5 1 2.19 3.24 0.29 o 6 -5 1 3.98 4.72 0.58 o 7 -5 1 11.99 14.63 1.52 o -7 -4 1 62.96 70.05 4.92 o -6 -4 1 58.66 53.88 2.22 o -5 -4 1 76.42 76.96 2.56 o -4 -4 1 18.88 16.77 0.55 o -3 -4 1 92.57 98.01 1.74 o -2 -4 1 76.16 82.92 1.41 o -1 -4 1 0.53 2.37 0.29 o 0 -4 1 30.72 23.96 2.51 o 1 -4 1 526.35 544.28 10.74 o 2 -4 1 4.53 3.91 0.29 o 3 -4 1 366.85 364.35 6.01 o 4 -4 1 495.29 491.40 8.82 o 5 -4 1 131.36 129.64 2.63 o 6 -4 1 3.20 5.27 1.05 o 7 -4 1 0.30 0.61 0.40 o -7 -3 1 34.47 36.24 2.99 o -6 -3 1 4.93 4.24 0.56 o -5 -3 1 258.74 248.53 5.37 o -4 -3 1 342.32 342.85 5.87 o -3 -3 1 352.37 341.26 5.12 o -2 -3 1 9.70 11.03 0.26 o -1 -3 1 76.00 83.40 1.08 o 0 -3 1 146.54 140.17 3.46 o 1 -3 1 921.31 936.16 30.13 o 2 -3 1 256.95 266.57 4.23 o 3 -3 1 83.30 88.73 1.46 o 4 -3 1 21.42 20.02 0.83 o 5 -3 1 107.99 106.67 1.99 o 6 -3 1 76.61 75.52 2.74 o 7 -3 1 0.97 1.23 0.45 o 8 -3 1 6.81 7.67 0.93 o -8 -2 1 64.47 63.34 4.44 o -7 -2 1 86.03 101.43 5.91 o -6 -2 1 32.25 32.01 1.59 o -5 -2 1 0.95 0.48 0.23 o -4 -2 1 46.27 43.29 1.56 o -3 -2 1 508.25 505.14 6.98 o -2 -2 1 46.97 58.62 0.87 o -1 -2 1 50.33 38.99 0.43 o 0 -2 1 1558.34 1425.57 69.33 o 1 -2 1 2884.87 2867.76 87.41 o 2 -2 1 20.38 33.07 0.56 o 3 -2 1 112.17 100.16 3.62 o 4 -2 1 416.37 405.85 5.93 o 5 -2 1 34.78 33.27 0.72 o 6 -2 1 34.48 34.52 1.47 o 7 -2 1 0.36 0.35 0.31 o 8 -2 1 17.40 18.06 1.94 o -7 -1 1 8.94 8.42 0.97 o -6 -1 1 45.47 42.50 1.13 o -5 -1 1 348.99 361.00 7.59 o -4 -1 1 86.42 82.24 1.81 o -3 -1 1 58.95 74.72 1.09 o -2 -1 1 256.19 250.72 2.53 o -1 -1 1 256.65 251.31 2.79 o 0 -1 1 820.61 849.71 14.75 o 1 -1 1 3843.43 3722.53 92.52 o 2 -1 1 41.96 34.65 0.63 o 3 -1 1 122.24 124.19 2.28 o 4 -1 1 57.55 55.11 0.89 o 5 -1 1 355.87 349.83 5.55 o 6 -1 1 103.87 100.86 3.21 o 7 -1 1 2.75 2.65 0.47 o 8 -1 1 1.53 2.44 0.59 o -8 0 1 48.77 51.27 3.79 o -7 0 1 61.05 60.71 2.09 o -6 0 1 44.84 43.46 1.15 o -5 0 1 7.63 9.76 0.44 o -4 0 1 24.29 21.54 0.80 o -3 0 1 924.70 875.79 11.16 o -2 0 1 1619.18 1401.61 18.54 o -1 0 1 126.58 100.93 1.52 o 1 0 1 3438.52 3176.00 36.66 o 2 0 1 3.43 9.15 0.25 o 3 0 1 147.71 135.01 1.61 o 4 0 1 606.35 633.56 8.89 o 5 0 1 44.67 44.64 1.87 o 6 0 1 41.20 34.47 1.64 o 7 0 1 25.37 24.36 1.24 o 8 0 1 78.87 81.61 4.26 o -8 1 1 0.57 0.83 0.42 o -7 1 1 82.19 80.28 2.83 o -6 1 1 31.16 27.03 0.99 o -5 1 1 361.87 359.97 6.27 o -4 1 1 7.27 10.49 0.32 o -3 1 1 58.72 76.69 1.08 o -2 1 1 32.40 37.67 0.95 o -1 1 1 1625.47 1629.77 20.52 o 0 1 1 2923.46 2851.50 32.42 o 1 1 1 5402.65 5153.87 66.23 o 2 1 1 1786.91 1959.33 23.50 o 3 1 1 0.00 0.36 0.09 o 4 1 1 0.84 1.46 0.14 o 5 1 1 5.94 8.45 0.31 o 6 1 1 5.02 8.75 0.70 o 7 1 1 1.41 1.72 0.45 o -8 2 1 30.59 27.36 1.59 o -7 2 1 178.97 174.55 5.47 o -6 2 1 191.49 184.27 3.84 o -5 2 1 9.46 12.21 0.50 o -4 2 1 12.34 13.13 0.40 o -3 2 1 82.72 76.70 4.99 o -2 2 1 1787.44 1764.24 20.31 o -1 2 1 1337.51 1366.88 13.68 o 0 2 1 26.49 29.12 0.61 o 1 2 1 7.97 4.41 0.17 o 2 2 1 8.80 17.48 0.36 o 3 2 1 273.89 268.63 4.06 o 4 2 1 28.04 33.46 1.03 o 5 2 1 12.45 11.47 0.44 o 6 2 1 16.91 15.05 0.82 o 7 2 1 6.48 9.10 0.82 o -8 3 1 2.56 2.05 0.44 o -7 3 1 25.05 28.61 1.52 o -6 3 1 15.29 14.62 0.60 o -5 3 1 73.90 73.76 2.13 o -4 3 1 0.89 2.10 0.32 o -3 3 1 35.35 42.72 0.73 o -2 3 1 119.15 132.67 4.75 o -1 3 1 358.42 328.05 8.63 o 0 3 1 70.14 77.81 0.95 o 1 3 1 154.11 168.13 3.42 o 2 3 1 12.24 15.08 0.37 o 3 3 1 379.57 381.84 6.47 o 4 3 1 258.34 253.50 4.87 o 5 3 1 18.47 18.82 1.23 o 6 3 1 57.97 62.56 2.18 o 7 3 1 0.18 -0.02 0.42 o -8 4 1 1.21 0.47 0.60 o -7 4 1 13.18 13.58 0.92 o -6 4 1 2.09 2.19 0.29 o -5 4 1 183.24 177.55 3.57 o -4 4 1 8.87 9.30 0.59 o -3 4 1 1.93 2.64 0.28 o -2 4 1 1093.94 1167.26 35.50 o -1 4 1 242.75 241.93 5.25 o 0 4 1 182.92 184.26 5.50 o 1 4 1 57.95 54.80 2.62 o 2 4 1 196.95 193.49 3.37 o 3 4 1 56.62 57.69 1.32 o 4 4 1 103.65 99.95 2.39 o 5 4 1 80.85 78.49 2.05 o 6 4 1 48.06 46.17 3.15 o -7 5 1 4.79 4.86 1.08 o -6 5 1 12.61 12.01 0.75 o -5 5 1 3.51 3.78 0.48 o -4 5 1 58.82 53.88 3.07 o -3 5 1 345.16 341.31 13.92 o -2 5 1 267.76 261.65 11.65 o -1 5 1 415.29 389.75 10.24 o 0 5 1 151.94 147.59 2.56 o 1 5 1 68.33 66.95 2.40 o 2 5 1 89.65 94.26 2.41 o 3 5 1 95.15 91.63 4.07 o 4 5 1 169.51 169.86 3.96 o 5 5 1 33.24 32.44 1.59 o 6 5 1 47.50 47.23 3.38 o -6 6 1 6.59 8.47 0.92 o -5 6 1 20.48 21.69 1.10 o -4 6 1 51.23 46.69 3.23 o -3 6 1 57.47 54.59 2.74 o -2 6 1 482.49 465.39 12.92 o -1 6 1 12.60 14.28 1.57 o 0 6 1 53.51 53.41 1.73 o 1 6 1 15.37 15.04 0.80 o 2 6 1 52.17 51.29 1.83 o 3 6 1 18.72 19.02 0.77 o 4 6 1 6.12 5.49 0.71 o -6 7 1 31.07 36.14 3.38 o -5 7 1 13.14 14.89 1.09 o -4 7 1 0.21 2.07 0.41 o -3 7 1 31.04 28.85 1.99 o -2 7 1 1.52 2.42 0.57 o -1 7 1 2.54 2.22 0.40 o 0 7 1 42.59 40.58 1.65 o 1 7 1 1.37 2.41 0.48 o 2 7 1 2.23 3.51 0.61 o 3 7 1 9.54 11.25 1.28 o -4 8 1 24.36 25.33 2.15 o -3 8 1 0.01 1.92 0.49 o -2 8 1 11.12 10.24 0.92 o -1 8 1 5.13 6.16 0.64 o 0 8 1 8.10 8.84 0.82 o 1 8 1 6.45 7.94 1.31 o 2 8 1 6.14 6.01 1.05 o -1 -8 2 0.03 1.14 0.72 o 0 -8 2 28.23 28.85 2.42 o 1 -8 2 11.87 11.27 0.86 o 2 -8 2 3.37 5.00 0.68 o 3 -8 2 3.73 4.49 1.21 o 4 -8 2 12.16 14.17 1.66 o -4 -7 2 62.21 57.28 4.09 o -3 -7 2 14.47 12.37 1.02 o -2 -7 2 148.10 146.33 6.83 o -1 -7 2 40.79 36.50 1.07 o 0 -7 2 166.52 162.24 6.79 o 1 -7 2 92.79 88.44 5.24 o 2 -7 2 3.42 4.43 0.56 o 3 -7 2 4.78 6.37 0.59 o 4 -7 2 23.25 26.01 1.32 o 5 -7 2 58.37 64.50 4.41 o -5 -6 2 4.65 5.49 0.66 o -4 -6 2 211.09 210.72 11.91 o -3 -6 2 259.25 268.93 8.19 o -2 -6 2 13.45 13.88 0.62 o -1 -6 2 21.89 21.39 0.69 o 0 -6 2 8.46 8.46 0.61 o 1 -6 2 105.52 107.24 3.02 o 2 -6 2 15.65 20.48 0.99 o 3 -6 2 34.54 34.27 0.97 o 4 -6 2 0.13 0.31 0.18 o 5 -6 2 4.36 4.86 0.57 o 6 -6 2 12.81 14.92 1.54 o -6 -5 2 31.53 34.70 1.88 o -5 -5 2 164.77 163.06 5.55 o -4 -5 2 6.68 7.19 0.62 o -3 -5 2 0.77 1.43 0.29 o -2 -5 2 78.74 77.24 2.25 o -1 -5 2 51.21 47.69 1.55 o 0 -5 2 201.90 196.30 3.99 o 1 -5 2 46.37 42.93 0.98 o 2 -5 2 45.50 50.32 1.14 o 3 -5 2 28.86 25.59 1.16 o 4 -5 2 3.69 3.79 0.42 o 5 -5 2 101.19 99.67 3.16 o 6 -5 2 0.22 0.37 0.29 o 7 -5 2 41.02 48.23 3.62 o -7 -4 2 0.16 0.81 0.66 o -6 -4 2 0.27 0.41 0.45 o -5 -4 2 0.02 0.10 0.21 o -4 -4 2 143.84 140.59 4.88 o -3 -4 2 113.29 111.91 1.88 o -2 -4 2 42.06 40.78 0.77 o -1 -4 2 101.17 104.79 1.63 o 0 -4 2 0.64 4.05 0.21 o 1 -4 2 613.47 606.07 10.06 o 2 -4 2 7.45 5.76 0.42 o 3 -4 2 8.93 11.18 0.68 o 4 -4 2 94.89 96.72 1.83 o 5 -4 2 75.10 75.93 2.70 o 6 -4 2 34.30 34.74 1.58 o 7 -4 2 0.02 0.37 0.35 o -7 -3 2 10.18 8.75 0.82 o -6 -3 2 3.51 4.75 0.54 o -5 -3 2 223.29 205.93 7.22 o -4 -3 2 202.32 212.39 3.38 o -3 -3 2 48.20 51.67 1.27 o -2 -3 2 13.77 12.10 0.22 o -1 -3 2 1.06 2.77 0.13 o 0 -3 2 355.50 425.06 13.44 o 1 -3 2 561.32 652.41 10.70 o 2 -3 2 663.87 693.73 9.76 o 3 -3 2 314.59 319.08 4.90 o 4 -3 2 342.98 318.59 12.24 o 5 -3 2 444.02 467.28 15.14 o 6 -3 2 9.98 8.05 0.81 o 7 -3 2 33.70 32.79 1.84 o -8 -2 2 11.85 14.00 1.80 o -7 -2 2 105.04 108.23 3.63 o -6 -2 2 154.84 156.74 3.31 o -5 -2 2 159.84 154.98 2.75 o -4 -2 2 253.98 241.06 3.66 o -3 -2 2 516.51 533.85 9.22 o -2 -2 2 25.03 29.18 1.26 o -1 -2 2 4.67 3.86 0.08 o 0 -2 2 185.58 177.16 1.93 o 1 -2 2 1351.11 1319.57 23.51 o 2 -2 2 1.42 0.99 0.07 o 3 -2 2 17.12 18.86 0.66 o 4 -2 2 208.10 199.75 6.24 o 5 -2 2 124.52 122.46 3.70 o 6 -2 2 114.50 111.65 3.70 o 7 -2 2 24.83 26.88 1.58 o 8 -2 2 19.16 17.64 1.30 o -8 -1 2 18.15 22.99 2.18 o -7 -1 2 158.12 141.67 7.21 o -6 -1 2 45.33 48.26 2.15 o -5 -1 2 35.09 32.34 0.83 o -4 -1 2 1104.74 1039.74 15.39 o -3 -1 2 333.72 311.80 3.76 o -2 -1 2 684.46 630.01 6.66 o -1 -1 2 3309.23 3486.16 111.39 o 0 -1 2 0.34 1.05 0.49 o 1 -1 2 10.36 9.49 0.13 o 2 -1 2 1.50 3.60 0.21 o 3 -1 2 407.72 402.38 3.10 o 4 -1 2 74.67 68.90 1.75 o 5 -1 2 6.53 8.03 0.66 o 6 -1 2 3.60 3.83 1.12 o 7 -1 2 19.23 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3.76 4.03 1.00 o -3 1 12 24.95 23.84 2.38 o -2 1 12 6.87 8.86 0.83 o -1 1 12 6.21 3.71 1.19 o 0 1 12 10.77 10.97 1.38 o 1 1 12 0.30 0.06 0.40 o -4 2 12 73.21 75.88 5.44 o -3 2 12 6.27 7.18 1.78 o -2 2 12 0.01 -0.18 0.47 o -1 2 12 1.62 1.93 0.61 o 0 2 12 22.03 22.66 2.22 o -3 3 12 31.45 27.59 1.67 o -2 3 12 11.32 13.43 1.15 o -1 3 12 4.35 3.53 1.04 o -2 -2 13 90.99 88.65 5.25 o -1 -2 13 88.97 96.28 6.44 o -3 -1 13 14.81 16.86 1.37 o -2 -1 13 0.35 1.01 0.66 o -1 -1 13 8.30 7.86 1.35 o -3 0 13 36.99 34.91 3.08 o -3 1 13 14.26 13.81 1.84 o