#------------------------------------------------------------------------------ #$Date: 2012-09-11 12:26:43 +0300 (Tue, 11 Sep 2012) $ #$Revision: 66590 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/45/2234530.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2234530_Fobs loop_ _publ_author_name 'Devi, T. Uma' 'Priya, S.' 'Kalpana, G.' 'Selvanayagam, S.' 'Sridhar, B.' _publ_section_title ; Resorcinol ninhydrin complex: 1,5,9-trihydroxy-8-oxatetracyclo[7.7.0.0^2,7^.0^10,15^]hexadeca-2,4,6,10(15),11,13-hexaen-16-one ; _journal_coeditor_code BT5867 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1323 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 91.837 _cell_angle_gamma 90.000 _cell_length_a 9.1117 _cell_length_b 12.2995 _cell_length_c 10.1177 _exptl_crystal_F_000 560.00 _reflns_d_resolution_high 0.7571 _[local]_cod_data_source_file bt5867Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' AL28m in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 148.32 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 0.24 0.47 0.10 o 2 0 0 288.65 268.06 3.20 o 3 0 0 486.83 465.06 5.49 o 4 0 0 206.61 236.21 2.94 o 5 0 0 630.24 644.02 7.68 o 6 0 0 2975.23 3054.35 40.37 o 7 0 0 21.81 14.56 0.66 o 8 0 0 3.90 5.29 0.51 o 9 0 0 354.01 338.09 5.37 o 10 0 0 1.87 1.48 0.88 o 11 0 0 15.86 16.38 1.32 o 12 0 0 38.36 32.13 2.46 o 1 1 0 50.68 52.49 1.40 o 2 1 0 1042.73 990.29 8.64 o 3 1 0 76.28 82.57 0.89 o 4 1 0 11.53 18.73 0.56 o 5 1 0 17.31 21.68 0.75 o 6 1 0 172.17 158.01 1.70 o 7 1 0 43.55 42.53 0.81 o 8 1 0 0.51 0.02 0.23 o 9 1 0 13.17 14.29 0.62 o 10 1 0 49.52 47.99 1.13 o 11 1 0 10.72 12.96 0.79 o 1 2 0 1776.11 1722.09 13.93 o 2 2 0 1670.77 1776.87 16.27 o 3 2 0 752.40 789.76 6.97 o 4 2 0 431.80 505.89 4.60 o 5 2 0 19.13 16.63 0.42 o 6 2 0 898.94 980.48 8.77 o 7 2 0 491.76 466.01 4.83 o 8 2 0 551.36 516.95 5.37 o 9 2 0 14.19 13.24 0.55 o 10 2 0 0.62 0.19 0.33 o 11 2 0 2.00 2.72 0.48 o 1 3 0 2472.17 2551.31 28.82 o 2 3 0 385.98 374.40 3.15 o 3 3 0 331.40 335.37 2.87 o 4 3 0 33.87 22.48 0.41 o 5 3 0 99.02 102.67 1.19 o 6 3 0 194.28 193.72 2.20 o 7 3 0 182.00 170.94 2.09 o 8 3 0 8.42 7.38 0.42 o 9 3 0 16.04 15.45 0.58 o 10 3 0 6.21 5.95 0.48 o 11 3 0 0.67 0.07 0.47 o 0 4 0 739.72 827.39 11.12 o 1 4 0 5645.02 5663.35 45.57 o 2 4 0 716.66 790.52 6.51 o 3 4 0 28.25 23.91 0.44 o 4 4 0 481.80 498.23 4.25 o 5 4 0 1722.25 1854.54 16.20 o 6 4 0 86.12 68.93 1.43 o 7 4 0 24.63 27.32 0.71 o 8 4 0 30.89 25.99 0.68 o 9 4 0 10.89 9.55 0.53 o 10 4 0 37.57 34.47 0.97 o 11 4 0 0.47 1.17 0.51 o 1 5 0 107.82 144.55 1.33 o 2 5 0 37.90 36.68 0.47 o 3 5 0 796.79 795.38 6.62 o 4 5 0 32.06 33.71 0.49 o 5 5 0 356.27 350.84 3.39 o 6 5 0 235.75 234.04 4.08 o 7 5 0 49.69 43.27 0.79 o 8 5 0 3.28 2.81 0.32 o 9 5 0 26.53 24.67 0.79 o 10 5 0 0.68 1.41 0.41 o 11 5 0 0.19 0.03 0.39 o 0 6 0 35.52 25.32 0.67 o 1 6 0 894.67 936.52 8.27 o 2 6 0 301.47 332.51 2.89 o 3 6 0 72.88 82.72 0.93 o 4 6 0 876.33 918.50 7.66 o 5 6 0 50.17 48.91 1.11 o 6 6 0 170.25 152.47 2.82 o 7 6 0 135.90 129.90 1.61 o 8 6 0 14.18 14.10 0.55 o 9 6 0 5.83 4.87 0.45 o 10 6 0 0.15 0.18 0.35 o 11 6 0 3.88 4.35 0.71 o 1 7 0 159.79 157.29 1.96 o 2 7 0 2.43 3.46 0.16 o 3 7 0 1055.28 1120.96 9.28 o 4 7 0 29.40 22.22 0.48 o 5 7 0 23.62 23.40 0.52 o 6 7 0 206.81 194.30 2.14 o 7 7 0 0.28 0.72 0.27 o 8 7 0 6.79 7.46 0.55 o 9 7 0 11.78 9.89 0.65 o 10 7 0 0.00 0.35 0.50 o 0 8 0 98.82 84.49 1.62 o 1 8 0 44.10 39.53 1.02 o 2 8 0 42.72 50.98 1.82 o 3 8 0 28.58 29.32 0.69 o 4 8 0 6.48 4.18 0.39 o 5 8 0 203.94 209.51 2.73 o 6 8 0 14.24 9.71 0.47 o 7 8 0 28.40 25.88 0.77 o 8 8 0 8.40 10.57 0.74 o 9 8 0 26.17 31.78 1.49 o 10 8 0 25.11 31.03 1.76 o 1 9 0 101.97 101.08 1.49 o 2 9 0 1013.93 1024.63 9.95 o 3 9 0 2.32 2.35 0.24 o 4 9 0 110.48 106.78 1.65 o 5 9 0 33.82 30.29 0.94 o 6 9 0 0.55 0.43 0.27 o 7 9 0 18.66 16.63 0.74 o 8 9 0 14.45 15.23 0.87 o 9 9 0 8.31 8.97 0.99 o 10 9 0 34.47 44.07 2.63 o 0 10 0 0.23 0.28 0.31 o 1 10 0 0.43 0.26 0.18 o 2 10 0 114.85 106.68 1.47 o 3 10 0 462.59 462.22 4.84 o 4 10 0 80.22 73.34 1.33 o 5 10 0 22.44 20.75 0.71 o 6 10 0 73.46 71.12 1.92 o 7 10 0 54.88 53.61 1.55 o 8 10 0 5.35 5.16 0.80 o 9 10 0 43.81 51.31 2.05 o 1 11 0 5.98 4.83 0.35 o 2 11 0 96.72 94.90 1.42 o 3 11 0 305.52 296.14 3.69 o 4 11 0 1.77 1.74 0.31 o 5 11 0 105.43 107.56 1.88 o 6 11 0 18.09 17.92 0.79 o 7 11 0 43.72 48.24 1.55 o 8 11 0 3.60 2.63 0.57 o 0 12 0 277.43 282.58 4.59 o 1 12 0 72.14 72.32 1.21 o 2 12 0 1.05 1.26 0.26 o 3 12 0 7.83 7.48 0.47 o 4 12 0 102.20 102.22 1.76 o 5 12 0 6.94 4.59 0.50 o 6 12 0 19.53 21.58 0.90 o 7 12 0 2.07 2.27 0.53 o 8 12 0 8.02 9.48 1.40 o 1 13 0 56.85 62.03 1.14 o 2 13 0 3.98 2.91 0.36 o 3 13 0 261.25 246.18 3.31 o 4 13 0 15.82 15.16 0.77 o 5 13 0 13.53 12.63 0.74 o 6 13 0 7.18 8.18 0.77 o 7 13 0 7.97 7.55 1.23 o 0 14 0 183.19 176.63 3.38 o 1 14 0 63.07 59.66 1.19 o 2 14 0 1.87 2.12 0.38 o 3 14 0 0.09 0.37 0.33 o 4 14 0 3.83 4.59 0.55 o 5 14 0 0.76 0.19 0.37 o 1 15 0 25.25 26.95 0.83 o 2 15 0 4.77 5.14 0.57 o 3 15 0 4.65 3.84 0.55 o 4 15 0 1.61 2.03 0.88 o 0 16 0 41.58 37.45 1.48 o 1 16 0 94.61 104.39 2.17 o 2 16 0 24.65 26.66 1.76 o -11 1 1 0.38 0.31 0.79 o -10 1 1 7.72 7.63 0.46 o -9 1 1 378.62 367.71 4.07 o -8 1 1 273.57 267.15 3.06 o -7 1 1 17.66 21.37 0.63 o -6 1 1 230.62 189.07 1.96 o -5 1 1 95.83 106.34 1.36 o -4 1 1 800.54 801.66 7.10 o -3 1 1 125.76 119.17 1.20 o -2 1 1 544.71 541.07 4.74 o -1 1 1 2546.50 2619.51 26.33 o 0 1 1 247.41 253.82 2.11 o 1 1 1 11790.49 8515.90 193.83 o 2 1 1 1644.53 1641.11 13.27 o 3 1 1 963.23 904.01 7.42 o 4 1 1 1.44 0.65 0.11 o 5 1 1 323.86 353.45 3.09 o 6 1 1 570.37 630.29 5.76 o 7 1 1 191.45 205.93 2.40 o 8 1 1 233.33 219.52 2.60 o 9 1 1 8.05 7.66 0.47 o 10 1 1 56.07 50.66 1.32 o 11 1 1 38.36 44.07 1.29 o -11 2 1 7.44 7.31 0.63 o -10 2 1 0.01 0.12 0.28 o -9 2 1 1.74 2.15 0.30 o -8 2 1 995.34 1004.38 9.88 o -7 2 1 6.18 6.99 0.37 o -6 2 1 6.63 4.91 0.30 o -5 2 1 291.03 283.12 2.76 o -4 2 1 27.86 26.84 0.72 o -3 2 1 3908.64 3997.13 34.35 o -2 2 1 21998.82 16955.60 478.25 o -1 2 1 435.84 458.84 4.89 o 0 2 1 0.57 4.31 0.23 o 1 2 1 43.16 39.90 0.78 o 2 2 1 3.80 1.63 0.12 o 3 2 1 2757.55 2811.54 22.69 o 4 2 1 148.52 157.40 1.48 o 5 2 1 2.73 1.00 0.22 o 6 2 1 0.67 0.83 0.31 o 7 2 1 467.89 463.20 4.80 o 8 2 1 18.36 18.23 0.58 o 9 2 1 29.47 26.16 0.80 o 10 2 1 148.17 142.68 2.52 o 11 2 1 157.03 168.84 2.94 o -11 3 1 12.83 12.61 0.79 o -10 3 1 1.40 1.81 0.37 o -9 3 1 26.76 24.90 0.75 o -8 3 1 148.31 152.09 1.99 o -7 3 1 81.57 62.90 1.05 o -6 3 1 25.43 22.18 0.49 o -5 3 1 420.33 472.77 4.39 o -4 3 1 2113.33 2315.39 20.06 o -3 3 1 2643.81 2694.83 21.78 o -2 3 1 388.37 419.25 3.51 o -1 3 1 9908.52 9526.89 81.74 o 0 3 1 1398.24 1432.62 11.64 o 1 3 1 497.09 507.35 4.19 o 2 3 1 511.55 525.63 4.37 o 3 3 1 983.32 968.10 7.95 o 4 3 1 142.89 126.02 1.39 o 5 3 1 24.13 24.72 0.50 o 6 3 1 48.81 48.63 0.89 o 7 3 1 6.87 8.31 0.40 o 8 3 1 153.02 146.49 2.13 o 9 3 1 35.61 33.15 0.89 o 10 3 1 0.08 0.63 0.39 o 11 3 1 24.14 28.97 1.07 o -11 4 1 0.00 0.03 0.37 o -10 4 1 0.28 0.18 0.31 o -9 4 1 39.40 38.27 0.99 o -8 4 1 216.59 217.56 2.63 o -7 4 1 334.49 332.26 3.33 o -6 4 1 50.87 46.41 0.81 o -5 4 1 182.68 174.57 1.86 o -4 4 1 0.32 2.06 0.27 o -3 4 1 485.13 543.24 4.56 o -2 4 1 1420.63 1454.30 11.82 o -1 4 1 2265.82 2335.53 27.02 o 0 4 1 2458.49 2577.33 25.14 o 1 4 1 350.15 336.74 2.85 o 2 4 1 1.61 1.95 0.15 o 3 4 1 235.44 242.75 2.16 o 4 4 1 56.13 67.90 0.78 o 5 4 1 6.19 4.07 0.39 o 6 4 1 322.02 317.10 3.14 o 7 4 1 32.34 27.12 0.65 o 8 4 1 3.01 1.05 0.31 o 9 4 1 64.20 61.21 1.27 o 10 4 1 19.89 19.59 0.88 o 11 4 1 13.28 12.95 0.79 o -11 5 1 20.91 26.93 1.03 o -10 5 1 19.72 23.38 0.88 o -9 5 1 8.67 9.96 0.55 o -8 5 1 31.01 25.28 0.69 o -7 5 1 3.03 4.79 0.61 o -6 5 1 540.44 541.68 5.80 o -5 5 1 941.06 929.78 8.98 o -4 5 1 832.27 953.79 7.92 o -3 5 1 309.49 332.91 2.91 o -2 5 1 46.69 52.74 0.60 o -1 5 1 64.31 76.62 0.78 o 0 5 1 694.18 713.19 6.32 o 1 5 1 1248.19 1330.82 10.86 o 2 5 1 353.23 370.60 3.18 o 3 5 1 22.63 15.19 0.38 o 4 5 1 189.10 185.63 1.77 o 5 5 1 68.30 64.86 0.90 o 6 5 1 79.24 71.54 1.10 o 7 5 1 640.87 633.50 5.93 o 8 5 1 3.82 3.05 0.41 o 9 5 1 0.58 0.69 0.33 o 10 5 1 11.49 9.43 0.68 o 11 5 1 49.11 54.83 1.72 o -11 6 1 47.13 55.05 1.72 o -10 6 1 6.69 6.51 0.59 o -9 6 1 3.65 4.20 0.43 o -8 6 1 1.62 1.21 0.31 o -7 6 1 21.72 19.50 0.64 o -6 6 1 101.86 100.30 1.83 o -5 6 1 0.30 0.09 0.17 o -4 6 1 58.74 61.96 0.84 o -3 6 1 1773.09 1898.81 15.48 o -2 6 1 20.12 21.94 0.44 o -1 6 1 148.52 168.66 1.55 o 0 6 1 0.23 0.46 0.25 o 1 6 1 208.20 219.89 2.13 o 2 6 1 98.30 96.16 0.99 o 3 6 1 1140.95 1250.44 10.29 o 4 6 1 4.76 8.14 0.33 o 5 6 1 9.83 10.23 0.66 o 6 6 1 2.05 1.27 0.23 o 7 6 1 4.57 5.58 0.34 o 8 6 1 6.30 4.86 0.43 o 9 6 1 7.85 7.15 0.51 o 10 6 1 3.35 3.23 0.45 o 11 6 1 0.30 -0.26 0.62 o -10 7 1 2.05 2.98 0.61 o -9 7 1 16.98 19.43 0.74 o -8 7 1 21.89 18.83 0.70 o -7 7 1 14.32 12.19 0.50 o -6 7 1 181.64 184.81 2.31 o -5 7 1 146.03 146.97 1.68 o -4 7 1 191.42 190.86 2.45 o -3 7 1 1082.20 1208.16 9.98 o -2 7 1 439.25 444.78 3.82 o -1 7 1 17.55 23.44 0.55 o 0 7 1 967.12 1055.87 9.34 o 1 7 1 301.07 307.63 2.94 o 2 7 1 3.09 3.88 0.18 o 3 7 1 0.04 0.45 0.15 o 4 7 1 287.04 312.72 2.85 o 5 7 1 56.44 56.70 0.86 o 6 7 1 18.92 15.88 0.49 o 7 7 1 51.45 46.77 0.94 o 8 7 1 16.00 15.67 0.59 o 9 7 1 23.34 20.14 0.88 o 10 7 1 25.06 28.95 1.22 o -10 8 1 0.03 1.23 0.62 o -9 8 1 64.77 72.90 2.36 o -8 8 1 93.00 95.37 1.86 o -7 8 1 8.76 6.55 0.52 o -6 8 1 237.06 235.02 4.13 o -5 8 1 233.23 235.55 3.00 o -4 8 1 44.61 51.15 0.99 o -3 8 1 252.61 259.53 4.74 o -2 8 1 116.16 105.09 3.79 o -1 8 1 21.46 21.62 0.57 o 0 8 1 608.12 641.86 6.34 o 1 8 1 11.88 12.82 0.40 o 2 8 1 167.65 169.10 2.18 o 3 8 1 63.69 66.51 1.02 o 4 8 1 29.07 31.21 0.71 o 5 8 1 96.71 96.48 1.38 o 6 8 1 12.29 11.15 0.46 o 7 8 1 188.76 175.07 2.48 o 8 8 1 1.72 2.08 0.37 o 9 8 1 98.47 107.62 4.21 o 10 8 1 0.00 0.70 0.70 o -9 9 1 0.24 0.44 0.50 o -8 9 1 27.12 33.90 1.27 o -7 9 1 2.46 2.36 0.39 o -6 9 1 33.12 26.79 0.88 o -5 9 1 251.97 238.22 3.08 o -4 9 1 370.24 368.14 4.36 o -3 9 1 3.02 4.83 0.46 o -2 9 1 62.69 60.11 1.08 o -1 9 1 5.26 4.91 0.29 o 0 9 1 23.62 21.36 0.52 o 1 9 1 393.53 397.22 4.55 o 2 9 1 3.95 3.00 0.26 o 3 9 1 55.46 50.47 0.91 o 4 9 1 270.44 268.98 3.34 o 5 9 1 126.19 121.08 1.84 o 6 9 1 0.83 0.83 0.29 o 7 9 1 2.43 1.91 0.39 o 8 9 1 39.73 42.75 1.24 o 9 9 1 7.64 9.22 0.99 o -9 10 1 17.58 20.39 1.49 o -8 10 1 88.71 98.81 2.02 o -7 10 1 0.03 1.19 0.35 o -6 10 1 27.57 23.94 1.71 o -5 10 1 56.30 53.85 1.34 o -4 10 1 27.44 23.52 0.71 o -3 10 1 74.07 70.36 1.12 o -2 10 1 221.47 222.29 2.80 o -1 10 1 0.80 0.82 0.37 o 0 10 1 77.74 81.38 1.21 o 1 10 1 60.93 58.44 1.25 o 2 10 1 19.91 22.79 0.58 o 3 10 1 2.73 4.57 0.60 o 4 10 1 26.34 25.57 0.74 o 5 10 1 2.38 1.81 0.31 o 6 10 1 42.19 40.55 1.12 o 7 10 1 139.78 134.63 2.44 o 8 10 1 1.16 0.74 0.43 o 9 10 1 30.49 31.95 2.28 o -8 11 1 16.18 20.97 1.08 o -7 11 1 10.76 9.95 0.68 o -6 11 1 0.40 0.50 0.32 o -5 11 1 74.01 72.95 1.62 o -4 11 1 325.43 314.51 5.63 o -3 11 1 76.48 71.60 1.33 o -2 11 1 278.09 275.92 3.13 o -1 11 1 27.00 26.38 0.66 o 0 11 1 113.38 106.51 1.52 o 1 11 1 33.10 29.93 0.70 o 2 11 1 24.11 26.00 0.65 o 3 11 1 96.20 90.26 1.38 o 4 11 1 18.93 16.56 0.63 o 5 11 1 12.23 10.47 0.59 o 6 11 1 107.97 107.82 2.06 o 7 11 1 0.03 0.59 0.41 o 8 11 1 29.93 32.55 1.32 o -8 12 1 35.15 40.38 2.46 o -7 12 1 22.63 23.08 0.94 o -6 12 1 43.06 43.99 1.80 o -5 12 1 8.44 6.81 0.57 o -4 12 1 12.46 12.21 0.70 o -3 12 1 105.28 97.51 1.91 o -2 12 1 110.17 102.33 1.55 o -1 12 1 215.85 217.42 2.63 o 0 12 1 22.93 26.55 0.70 o 1 12 1 78.00 72.94 1.23 o 2 12 1 23.75 18.29 0.59 o 3 12 1 101.17 91.44 1.59 o 4 12 1 87.85 82.96 1.52 o 5 12 1 129.31 124.89 2.24 o 6 12 1 87.50 81.39 2.62 o 7 12 1 2.10 2.22 0.53 o 8 12 1 0.09 1.58 0.88 o -7 13 1 44.72 48.46 2.81 o -6 13 1 3.26 2.16 0.46 o -5 13 1 13.03 13.10 0.74 o -4 13 1 8.05 8.28 0.63 o -3 13 1 55.44 53.55 1.36 o -2 13 1 61.73 57.66 1.24 o -1 13 1 129.30 120.68 1.77 o 0 13 1 105.04 111.46 1.81 o 1 13 1 21.26 21.48 0.90 o 2 13 1 41.73 41.08 0.93 o 3 13 1 32.17 33.19 0.94 o 4 13 1 0.09 0.44 0.29 o 5 13 1 1.16 1.65 0.41 o 6 13 1 4.39 4.77 0.67 o -6 14 1 9.97 7.72 1.58 o -5 14 1 1.89 1.47 0.46 o -4 14 1 9.64 9.31 0.70 o -3 14 1 0.43 1.08 0.37 o -2 14 1 4.21 5.24 0.53 o -1 14 1 234.77 236.57 2.96 o 0 14 1 30.04 29.26 0.81 o 1 14 1 78.72 77.10 1.36 o 2 14 1 19.88 21.19 0.69 o 3 14 1 7.98 7.65 0.55 o 4 14 1 19.94 21.25 0.79 o 5 14 1 2.07 2.01 0.68 o -4 15 1 10.83 10.18 1.58 o -3 15 1 28.03 31.39 1.12 o -2 15 1 13.73 12.74 0.79 o -1 15 1 45.30 50.44 1.24 o 0 15 1 71.75 73.67 1.54 o 1 15 1 82.69 82.18 1.47 o 2 15 1 33.94 36.07 1.05 o 3 15 1 29.91 31.16 1.00 o 4 15 1 37.86 40.03 2.46 o -1 16 1 25.45 27.83 1.49 o 0 16 1 0.03 -0.14 0.39 o 1 16 1 1.01 1.29 0.51 o -11 0 2 1.21 1.23 0.62 o -10 0 2 61.18 66.55 2.23 o -9 0 2 130.00 131.57 2.60 o -8 0 2 1326.43 1313.59 18.01 o -7 0 2 671.74 657.31 11.18 o -6 0 2 169.21 173.25 5.26 o -5 0 2 1088.24 1191.38 14.01 o -4 0 2 615.91 555.96 6.63 o -3 0 2 63.62 64.04 0.98 o -2 0 2 129.03 101.43 1.36 o -1 0 2 0.58 0.88 0.12 o 0 0 2 1116.84 1123.82 12.95 o 1 0 2 1534.85 1591.17 22.27 o 2 0 2 524.36 552.36 6.47 o 3 0 2 78.42 54.79 0.85 o 4 0 2 162.97 206.58 2.67 o 5 0 2 297.64 287.86 3.64 o 6 0 2 552.73 544.69 17.61 o 7 0 2 26.52 19.08 0.72 o 8 0 2 444.69 431.94 8.01 o 9 0 2 189.66 179.19 4.10 o 10 0 2 10.87 8.19 0.87 o 11 0 2 4.87 5.47 0.87 o -11 1 2 4.15 4.75 0.57 o -10 1 2 2.45 3.39 0.42 o -9 1 2 8.12 7.58 0.44 o -8 1 2 534.90 541.09 5.61 o -7 1 2 49.57 47.67 0.89 o -6 1 2 9.38 8.17 0.34 o -5 1 2 1171.42 1223.14 10.09 o -4 1 2 231.11 251.94 2.25 o -3 1 2 685.35 643.29 5.34 o -2 1 2 179.33 184.57 1.62 o -1 1 2 1115.53 1158.69 10.05 o 0 1 2 202.23 202.05 1.73 o 1 1 2 1086.54 1112.55 9.69 o 2 1 2 22.71 21.58 0.38 o 3 1 2 1556.08 1582.17 12.86 o 4 1 2 3489.08 3729.01 30.07 o 5 1 2 44.11 41.28 0.57 o 6 1 2 133.15 123.19 2.44 o 7 1 2 11.49 10.63 0.45 o 8 1 2 5.70 3.64 0.44 o 9 1 2 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