#------------------------------------------------------------------------------ #$Date: 2012-09-11 12:26:43 +0300 (Tue, 11 Sep 2012) $ #$Revision: 66590 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/47/2234744.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2234744_Fobs loop_ _publ_author_name 'Li, Shu-Qiang' 'Hu, Ning-Hai' _publ_section_title ; Poly[[tris(\m-4,4'-bipyridine-\k^2^N:N')bis(\m-L-lysinato-\k^3^N^1^,O^1^:O^1'^)dizinc(II)] tetranitrate 0.6-hydrate dimethylformamide disolvate] ; _journal_coeditor_code NK2149 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m633 _journal_page_last m634 _journal_volume 68 _journal_year 2012 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 93.197 _cell_angle_gamma 90.000 _cell_length_a 10.3039 _cell_length_b 24.9425 _cell_length_c 11.5740 _exptl_crystal_F_000 1352.00 _reflns_d_resolution_high 0.8094 _[local]_cod_data_source_file nk2149Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' HU05L in P2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 298.84 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 5 -27 0 0.23 -5.01 21.60 o 6 -27 0 187.66 163.75 40.05 o 4 -26 0 28.55 -12.66 18.36 o 5 -26 0 13.62 31.51 23.17 o 6 -26 0 646.60 692.80 66.56 o 4 -25 0 1836.37 1771.11 101.02 o 5 -25 0 201.01 258.39 42.51 o 6 -25 0 293.62 266.34 46.24 o 7 -25 0 202.56 255.44 47.32 o 4 -24 0 61.21 67.35 26.31 o 5 -24 0 99.22 95.82 30.53 o 7 -24 0 416.95 549.96 59.69 o 3 -23 0 3457.21 3487.35 147.16 o 4 -23 0 2230.41 2173.62 109.17 o 5 -23 0 943.29 1059.27 75.20 o 6 -23 0 319.43 450.61 53.41 o 7 -23 0 89.99 82.17 32.59 o 8 -23 0 10.65 19.05 23.76 o 3 -22 0 298.97 302.66 39.27 o 4 -22 0 320.28 286.37 40.05 o 5 -22 0 383.80 449.92 49.67 o 6 -22 0 1462.58 1527.35 94.05 o 7 -22 0 1455.73 1453.63 95.82 o 8 -22 0 589.13 545.93 64.20 o 3 -21 0 2394.08 2476.49 81.20 o 4 -21 0 1191.12 1246.39 77.75 o 5 -21 0 3026.06 2779.83 130.37 o 6 -21 0 26.02 -4.32 20.71 o 7 -21 0 55.32 122.71 35.24 o 8 -21 0 4.52 46.53 27.39 o 9 -21 0 550.36 619.17 66.85 o 2 -20 0 612.65 524.02 34.38 o 3 -20 0 834.96 782.56 76.92 o 4 -20 0 26.32 39.03 15.63 o 5 -20 0 192.76 152.17 33.57 o 6 -20 0 26.48 26.80 23.86 o 7 -20 0 3619.70 3675.15 165.71 o 8 -20 0 27.79 25.03 22.97 o 9 -20 0 569.72 559.97 61.75 o 2 -19 0 78.74 113.75 19.00 o 3 -19 0 8724.72 9000.69 216.83 o 4 -19 0 153.76 136.40 21.00 o 5 -19 0 2664.28 2586.43 122.13 o 6 -19 0 260.14 210.09 37.70 o 7 -19 0 367.59 348.31 48.50 o 8 -19 0 21.80 8.84 23.27 o 9 -19 0 964.64 843.10 76.87 o 10 -19 0 114.60 98.66 33.87 o 1 -18 0 3268.35 3453.09 147.94 o 2 -18 0 310.35 320.86 26.46 o 3 -18 0 55.49 60.02 16.55 o 4 -18 0 246.81 256.60 24.85 o 5 -18 0 1450.63 1469.83 83.84 o 6 -18 0 90.76 80.21 28.57 o 7 -18 0 6046.94 6151.73 236.59 o 8 -18 0 698.56 769.67 68.23 o 9 -18 0 915.86 832.10 71.86 o 10 -18 0 66.93 39.76 24.35 o 1 -17 0 1619.76 1670.68 88.94 o 2 -17 0 2630.42 2451.75 75.69 o 3 -17 0 7482.36 7613.50 207.49 o 4 -17 0 1285.22 1412.38 54.17 o 5 -17 0 529.40 542.50 49.09 o 6 -17 0 510.67 516.48 52.03 o 7 -17 0 59.53 37.11 24.64 o 8 -17 0 165.63 171.11 38.78 o 9 -17 0 1315.36 1407.58 95.52 o 10 -17 0 305.75 426.75 57.82 o 1 -16 0 864.98 893.95 58.80 o 2 -16 0 1722.73 1849.89 62.22 o 3 -16 0 523.18 472.27 31.46 o 4 -16 0 257.88 270.81 35.49 o 5 -16 0 1168.31 1165.98 72.45 o 6 -16 0 1889.96 1774.06 96.99 o 7 -16 0 2772.79 2971.95 135.87 o 8 -16 0 2496.58 2560.91 128.21 o 9 -16 0 546.98 610.33 63.12 o 10 -16 0 30.58 27.39 27.78 o 1 -15 0 77.99 53.60 13.16 o 2 -15 0 5763.55 5985.27 149.28 o 3 -15 0 770.56 760.66 35.82 o 4 -15 0 12512.40 13192.46 293.48 o 5 -15 0 145.08 154.03 28.96 o 6 -15 0 2064.14 1952.44 98.47 o 7 -15 0 110.55 124.58 33.77 o 8 -15 0 41.74 18.85 24.44 o 9 -15 0 374.87 358.92 49.87 o 10 -15 0 746.02 885.21 76.28 o 11 -15 0 235.43 289.80 52.13 o 0 -14 0 10127.88 10382.83 346.94 o 1 -14 0 2277.02 2520.79 72.13 o 2 -14 0 3651.54 3977.31 102.61 o 3 -14 0 1212.87 1192.44 45.91 o 4 -14 0 118.92 120.11 21.06 o 5 -14 0 20.22 37.68 12.71 o 6 -14 0 2630.38 2561.79 117.41 o 7 -14 0 43.11 25.23 22.09 o 8 -14 0 6608.89 6976.57 255.25 o 9 -14 0 0.45 23.46 23.17 o 10 -14 0 139.56 87.08 31.32 o 11 -14 0 94.33 93.85 36.13 o 1 -13 0 2438.10 2429.92 69.11 o 2 -13 0 12229.87 13673.92 296.95 o 3 -13 0 146.66 134.80 16.12 o 4 -13 0 9096.84 9237.56 211.15 o 5 -13 0 276.94 285.98 23.25 o 6 -13 0 3545.17 3670.74 144.70 o 7 -13 0 217.52 244.55 37.50 o 8 -13 0 89.94 159.43 36.62 o 9 -13 0 24.74 40.25 23.76 o 10 -13 0 1438.59 1511.65 99.55 o 11 -13 0 59.01 58.61 34.36 o 0 -12 0 18877.54 21080.98 669.53 o 1 -12 0 33.20 41.31 10.64 o 2 -12 0 4650.99 4490.48 114.38 o 3 -12 0 328.81 366.15 23.17 o 4 -12 0 219.64 205.32 18.91 o 5 -12 0 577.89 564.46 29.66 o 6 -12 0 4664.30 4837.21 176.61 o 7 -12 0 67.91 73.63 28.08 o 8 -12 0 4707.89 4579.51 187.61 o 9 -12 0 1532.56 1495.74 93.85 o 10 -12 0 265.65 300.99 50.95 o 11 -12 0 65.20 69.70 36.52 o 1 -11 0 10378.41 10480.56 232.01 o 2 -11 0 9141.39 10364.34 229.80 o 3 -11 0 4173.35 4342.95 109.35 o 4 -11 0 4846.66 4757.53 116.65 o 5 -11 0 954.51 958.98 37.50 o 6 -11 0 3644.96 3828.30 151.97 o 7 -11 0 83.05 73.73 28.08 o 8 -11 0 1390.49 1378.92 86.59 o 9 -11 0 191.70 153.93 39.46 o 10 -11 0 1373.53 1296.85 93.85 o 11 -11 0 514.52 494.00 62.93 o 0 -10 0 11433.54 11231.42 376.39 o 1 -10 0 3440.13 3623.03 90.26 o 2 -10 0 4760.31 5491.99 128.77 o 3 -10 0 1412.30 1279.68 42.22 o 4 -10 0 266.76 271.82 19.29 o 5 -10 0 1404.00 1278.17 43.53 o 6 -10 0 4690.01 4858.22 176.12 o 7 -10 0 3156.25 3275.20 137.24 o 8 -10 0 4484.24 4316.90 176.12 o 9 -10 0 1995.56 2002.31 109.17 o 10 -10 0 138.74 136.65 37.99 o 11 -10 0 90.29 95.91 36.52 o 12 -10 0 5.58 10.90 28.86 o 1 -9 0 4023.74 4141.44 113.09 o 2 -9 0 11.24 1.33 6.79 o 3 -9 0 22822.53 24444.51 510.09 o 4 -9 0 11018.70 12541.76 272.81 o 5 -9 0 2597.88 2586.86 97.88 o 6 -9 0 699.57 696.23 52.52 o 7 -9 0 208.43 194.77 32.20 o 8 -9 0 467.11 526.40 50.56 o 9 -9 0 343.80 316.41 46.14 o 10 -9 0 2305.53 2187.26 120.95 o 11 -9 0 1982.21 1968.83 116.73 o 12 -9 0 295.55 363.53 58.51 o 0 -8 0 23753.60 25011.78 768.00 o 1 -8 0 17938.25 20034.46 424.01 o 2 -8 0 35116.41 37379.59 764.24 o 3 -8 0 1061.94 1234.37 38.18 o 4 -8 0 779.90 782.60 30.53 o 5 -8 0 1923.11 2105.81 67.59 o 6 -8 0 604.72 633.80 50.07 o 7 -8 0 5282.79 5722.33 205.96 o 8 -8 0 970.14 911.27 39.25 o 9 -8 0 2654.02 2686.47 132.34 o 10 -8 0 27.99 38.48 28.08 o 11 -8 0 188.19 173.08 42.80 o 12 -8 0 150.05 149.71 43.49 o 1 -7 0 23886.28 26114.48 549.29 o 2 -7 0 4498.55 4327.31 144.80 o 3 -7 0 4810.84 5663.96 191.29 o 4 -7 0 35.17 21.23 8.49 o 5 -7 0 2727.03 2706.86 108.68 o 6 -7 0 59.92 52.63 9.97 o 7 -7 0 445.68 482.86 27.93 o 8 -7 0 212.82 190.41 20.08 o 9 -7 0 4771.20 5166.38 201.94 o 10 -7 0 191.71 172.98 39.66 o 11 -7 0 2218.34 2120.61 120.75 o 12 -7 0 166.70 138.32 43.10 o 0 -6 0 4067.51 3647.95 85.23 o 1 -6 0 89229.24 97601.73 2009.13 o 2 -6 0 6628.73 8403.60 180.87 o 3 -6 0 228.27 190.28 15.41 o 4 -6 0 96.19 90.66 8.27 o 5 -6 0 99.03 120.19 13.06 o 6 -6 0 2778.32 3049.85 63.80 o 7 -6 0 7156.49 7373.81 163.71 o 8 -6 0 607.24 575.50 47.07 o 9 -6 0 1522.55 1487.01 90.02 o 10 -6 0 197.71 131.35 36.72 o 11 -6 0 273.77 329.56 50.95 o 12 -6 0 75.31 106.71 37.89 o 1 -5 0 3622.48 3794.70 82.46 o 2 -5 0 8584.67 9357.62 285.19 o 3 -5 0 13779.50 13198.83 308.95 o 4 -5 0 20202.18 22316.53 365.03 o 5 -5 0 5051.57 5588.08 122.93 o 6 -5 0 105.88 71.15 11.99 o 7 -5 0 187.92 176.58 17.27 o 8 -5 0 125.38 132.47 17.27 o 9 -5 0 5963.24 6007.51 224.22 o 10 -5 0 462.31 419.29 51.64 o 11 -5 0 3436.36 3494.12 163.85 o 12 -5 0 68.67 45.65 30.04 o 0 -4 0 3494.53 3656.71 82.07 o 1 -4 0 37830.40 38790.13 813.15 o 3 -4 0 12.68 11.18 4.35 o 4 -4 0 642.02 621.35 23.35 o 5 -4 0 5730.06 5798.91 128.23 o 6 -4 0 3876.69 3941.19 93.87 o 7 -4 0 8087.10 8358.87 180.89 o 8 -4 0 1996.28 1921.67 59.88 o 9 -4 0 1492.37 1564.76 88.26 o 10 -4 0 534.91 542.99 55.27 o 11 -4 0 44.81 70.68 32.79 o 12 -4 0 95.45 38.78 31.12 o 1 -3 0 1015.39 922.09 24.30 o 2 -3 0 2837.37 3591.91 63.25 o 3 -3 0 5336.99 6104.44 127.17 o 4 -3 0 783.87 996.78 39.12 o 5 -3 0 3163.95 3171.17 77.68 o 6 -3 0 672.33 669.12 27.50 o 7 -3 0 76.88 75.75 13.51 o 8 -3 0 51.86 28.57 17.23 o 9 -3 0 2460.36 2400.69 118.00 o 10 -3 0 2720.08 2583.88 126.35 o 11 -3 0 2637.96 2617.94 135.08 o 12 -3 0 408.17 379.92 56.84 o 0 -2 0 31127.51 32064.23 1005.38 o 1 -2 0 3063.50 3503.80 75.75 o 2 -2 0 20983.88 23823.70 614.85 o 3 -2 0 2116.52 2201.50 102.54 o 4 -2 0 608.97 549.83 21.10 o 5 -2 0 2699.63 3189.08 75.82 o 6 -2 0 2567.42 2490.50 139.26 o 7 -2 0 692.48 572.46 28.03 o 8 -2 0 2347.24 2469.61 69.65 o 9 -2 0 108.21 44.08 26.51 o 10 -2 0 1064.86 1052.01 77.75 o 11 -2 0 26.60 -7.26 23.07 o 12 -2 0 338.50 333.29 53.01 o 1 -1 0 560.07 475.92 18.26 o 2 -1 0 63859.36 66803.49 1309.01 o 3 -1 0 485.27 413.99 16.39 o 4 -1 0 7017.37 7874.77 159.55 o 5 -1 0 400.35 365.02 18.48 o 6 -1 0 1870.69 1999.59 55.35 o 7 -1 0 1063.38 1102.12 39.08 o 8 -1 0 46.13 35.04 13.12 o 9 -1 0 204.27 215.34 25.52 o 10 -1 0 7138.66 7496.29 271.74 o 11 -1 0 220.89 272.03 45.75 o 12 -1 0 1451.60 1479.64 98.86 o 1 0 0 210.62 249.14 7.85 o 2 0 0 10180.47 11890.07 228.96 o 3 0 0 35.18 8.26 5.64 o 4 0 0 2396.73 2379.68 56.66 o 5 0 0 359.09 279.89 28.76 o 6 0 0 4881.54 5462.13 120.93 o 7 0 0 712.97 620.21 28.12 o 8 0 0 4647.07 4659.37 111.95 o 9 0 0 329.76 337.54 50.71 o 10 0 0 1016.11 1017.84 76.08 o 11 0 0 33.27 43.98 28.67 o 12 0 0 359.92 375.80 53.99 o 1 1 0 599.13 513.49 13.35 o 2 1 0 65071.43 68974.74 1300.73 o 3 1 0 524.97 433.74 16.58 o 4 1 0 7019.47 7821.97 159.33 o 5 1 0 332.62 304.64 17.56 o 6 1 0 1957.67 2070.83 55.63 o 7 1 0 1043.91 1054.18 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4337.55 74.63 o 3 7 0 5209.32 5955.57 80.96 o 4 7 0 32.55 24.70 5.56 o 5 7 0 2661.11 2708.01 68.21 o 6 7 0 55.99 55.97 12.02 o 7 7 0 447.91 510.03 28.61 o 8 7 0 203.28 159.44 18.89 o 9 7 0 4897.67 5218.87 127.61 o 10 7 0 188.10 159.61 21.13 o 11 7 0 2153.19 2162.23 113.00 o 0 8 0 23471.12 25050.55 654.51 o 1 8 0 17675.86 20490.19 377.60 o 2 8 0 35110.48 36597.24 677.62 o 3 8 0 1008.75 1115.78 30.93 o 4 8 0 807.68 789.88 18.69 o 5 8 0 1979.12 2053.57 36.31 o 6 8 0 608.16 631.51 18.14 o 7 8 0 5337.45 5718.16 131.45 o 8 8 0 962.46 962.17 40.00 o 9 8 0 2686.39 2980.29 83.44 o 10 8 0 20.72 26.60 14.58 o 1 9 0 4058.66 4328.05 91.07 o 2 9 0 11.67 3.04 7.27 o 3 9 0 22731.18 24225.21 378.35 o 4 9 0 11120.74 12487.27 202.08 o 5 9 0 2610.78 2633.04 43.80 o 6 9 0 708.25 713.49 19.73 o 7 9 0 190.73 190.00 11.94 o 8 9 0 455.81 491.36 30.10 o 9 9 0 386.66 422.40 54.73 o 10 9 0 2255.24 2363.48 87.86 o 0 10 0 11940.11 12281.76 323.77 o 1 10 0 3530.80 3713.34 82.35 o 2 10 0 4697.95 5503.50 164.93 o 3 10 0 1402.10 1261.38 31.00 o 4 10 0 266.36 230.54 13.57 o 5 10 0 1269.82 1167.10 25.84 o 6 10 0 4687.74 4689.90 72.26 o 7 10 0 3046.85 3235.68 55.11 o 8 10 0 4449.57 4499.24 150.74 o 9 10 0 1927.02 2046.69 69.90 o 10 10 0 176.49 214.70 32.10 o 1 11 0 10307.55 10670.89 208.56 o 2 11 0 9152.87 10420.79 205.43 o 3 11 0 4188.94 4513.98 81.41 o 4 11 0 4788.07 4659.53 85.94 o 5 11 0 782.56 809.52 26.69 o 6 11 0 3690.86 3953.62 63.11 o 7 11 0 74.61 63.69 9.27 o 8 11 0 1333.04 1358.03 50.70 o 9 11 0 241.73 245.43 32.49 o 10 11 0 1413.19 1506.15 77.75 o 0 12 0 19112.81 21700.54 571.95 o 1 12 0 84.75 90.89 13.05 o 2 12 0 4923.17 4880.23 104.74 o 3 12 0 317.48 365.59 21.52 o 4 12 0 201.81 213.79 21.03 o 5 12 0 627.78 613.93 22.97 o 6 12 0 4613.17 4562.42 88.43 o 7 12 0 47.45 30.85 10.14 o 8 12 0 4777.89 4805.70 162.77 o 9 12 0 1450.51 1402.58 75.00 o 10 12 0 277.70 274.59 36.72 o 1 13 0 2479.43 2442.40 64.26 o 2 13 0 12187.64 13392.20 265.03 o 3 13 0 135.78 134.07 11.70 o 4 13 0 9066.35 9153.07 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