#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:39:22 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181269 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/47/2234751.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2234751_Fobs loop_ _publ_author_name 'Oliveira, F. L.' 'Freire, K. R. L.' 'Aparicio, R.' 'Coelho, F.' _publ_section_title ; (1S,2E,6R,7aR)-2-Benzylidene-1,6-dihydroxy-2,3,5,6,7,7a-hexahydro-1H-pyrrolizin-3-one ; _journal_coeditor_code PV2526 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1572 _journal_volume 68 _journal_year 2012 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 6.5007 _cell_length_b 13.6783 _cell_length_c 13.8382 _exptl_crystal_F_000 520.00 _reflns_d_resolution_high 0.8307 _cod_data_source_file pv2526Isup3.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' cu_Kristerson_R142_1_0ma in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 107.48 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' '-x+1/2, -y, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 6 0 0 147.31 137.42 2.67 o 1 1 0 750.57 634.14 17.06 o 2 1 0 475.20 416.28 8.74 o 3 1 0 89.94 66.26 3.14 o 5 1 0 3.16 3.57 0.13 o 6 1 0 260.97 250.05 3.77 o 7 1 0 21.22 23.30 0.56 o 0 2 0 4411.44 3606.28 99.42 o 1 2 0 33.88 29.66 0.55 o 2 2 0 1246.64 1275.73 23.35 o 3 2 0 95.49 74.13 2.76 o 4 2 0 910.00 969.77 18.92 o 5 2 0 1.36 0.44 0.11 o 6 2 0 188.78 176.09 2.44 o 7 2 0 0.66 0.27 0.15 o 1 3 0 1.35 3.16 0.14 o 2 3 0 39.73 50.75 0.95 o 3 3 0 271.41 337.18 6.26 o 4 3 0 15.31 23.45 0.60 o 5 3 0 116.72 124.72 1.08 o 6 3 0 147.44 148.02 2.06 o 7 3 0 9.93 7.37 0.30 o 0 4 0 7.06 4.96 0.65 o 1 4 0 16.89 20.53 0.46 o 2 4 0 1.14 0.11 0.06 o 3 4 0 481.94 512.00 7.91 o 4 4 0 354.77 350.25 3.15 o 5 4 0 0.80 3.15 0.09 o 6 4 0 98.28 97.10 0.81 o 7 4 0 0.14 0.19 0.09 o 1 5 0 1.43 0.63 0.09 o 2 5 0 1177.62 1207.69 20.32 o 3 5 0 14.63 24.37 1.02 o 4 5 0 17.37 14.63 0.13 o 5 5 0 278.19 290.02 2.17 o 6 5 0 7.55 6.69 0.12 o 7 5 0 0.78 0.48 0.07 o 0 6 0 0.02 0.31 0.11 o 1 6 0 593.30 606.85 10.41 o 2 6 0 461.96 557.55 12.41 o 3 6 0 0.90 2.45 0.17 o 4 6 0 18.30 15.41 0.17 o 5 6 0 30.59 31.88 0.29 o 6 6 0 55.24 61.74 0.64 o 7 6 0 56.56 52.05 2.19 o 1 7 0 11.26 4.80 0.19 o 2 7 0 71.96 84.88 1.66 o 3 7 0 3.62 6.53 0.18 o 4 7 0 122.70 110.08 1.09 o 5 7 0 297.61 310.62 2.85 o 6 7 0 1.75 1.29 0.05 o 7 7 0 14.87 14.86 0.64 o 0 8 0 223.89 245.84 4.90 o 1 8 0 246.18 263.88 4.65 o 2 8 0 173.50 158.19 1.90 o 3 8 0 32.01 28.89 0.27 o 4 8 0 84.21 89.22 0.70 o 5 8 0 39.22 33.26 0.48 o 6 8 0 21.70 25.58 0.33 o 1 9 0 216.76 199.00 2.79 o 2 9 0 228.80 222.02 1.48 o 3 9 0 320.84 312.67 2.35 o 4 9 0 11.34 12.21 0.14 o 5 9 0 0.38 -0.04 0.04 o 6 9 0 0.68 0.92 0.08 o 0 10 0 515.37 470.49 4.27 o 1 10 0 3.20 3.02 0.06 o 2 10 0 15.61 15.42 0.15 o 3 10 0 40.65 49.09 0.48 o 4 10 0 17.35 20.70 0.18 o 5 10 0 11.75 14.21 0.17 o 6 10 0 1.83 2.68 0.12 o 1 11 0 66.92 67.63 0.48 o 2 11 0 1.32 1.70 0.06 o 3 11 0 117.97 120.02 0.88 o 4 11 0 0.51 1.14 0.11 o 5 11 0 14.91 13.22 0.16 o 0 12 0 122.24 123.17 1.25 o 1 12 0 0.00 -0.04 0.04 o 2 12 0 14.03 13.79 0.16 o 3 12 0 25.92 31.27 0.30 o 4 12 0 2.19 1.66 0.05 o 5 12 0 24.56 17.72 0.24 o 1 13 0 36.88 39.86 0.32 o 2 13 0 75.68 77.72 0.64 o 3 13 0 9.79 10.17 0.12 o 4 13 0 41.55 39.45 0.34 o 0 14 0 0.97 1.18 0.11 o 1 14 0 0.86 0.63 0.06 o 2 14 0 102.16 92.34 0.71 o 3 14 0 7.78 7.57 0.09 o 4 14 0 70.54 70.65 1.54 o 1 15 0 33.61 30.39 0.30 o 2 15 0 28.47 29.02 0.26 o 3 15 0 0.71 0.63 0.06 o 0 16 0 0.02 0.40 0.13 o 1 16 0 8.09 7.91 0.18 o 1 0 1 1158.77 1010.90 28.03 o 2 0 1 710.31 724.65 16.77 o 3 0 1 285.77 308.17 11.07 o 5 0 1 55.23 54.06 0.80 o 6 0 1 4.90 4.86 0.18 o 7 0 1 0.05 0.49 0.11 o -7 1 1 4.91 7.47 0.23 o -6 1 1 72.78 78.10 1.13 o -5 1 1 10.39 9.86 0.22 o -4 1 1 85.91 79.69 2.27 o -3 1 1 2129.66 2320.28 41.03 o -2 1 1 706.69 675.82 12.01 o -1 1 1 4007.13 3353.31 79.56 o 0 1 1 86.53 56.41 0.99 o 1 1 1 4011.99 3276.10 119.05 o 2 1 1 703.26 657.74 15.14 o 3 1 1 2132.71 2348.94 48.38 o 5 1 1 10.56 9.81 0.20 o 6 1 1 73.02 78.39 1.12 o 7 1 1 4.81 7.38 0.30 o -7 2 1 7.24 7.97 0.34 o -6 2 1 140.63 123.34 1.73 o -5 2 1 118.66 120.32 1.37 o -4 2 1 4.77 4.35 0.13 o -3 2 1 343.09 369.05 6.42 o -2 2 1 456.86 502.88 8.22 o -1 2 1 5675.84 4849.89 92.23 o 0 2 1 200.90 190.09 3.21 o 1 2 1 5661.15 4844.25 88.34 o 2 2 1 455.85 515.81 8.79 o 3 2 1 348.01 374.08 6.46 o 4 2 1 4.53 6.14 0.48 o 5 2 1 117.37 115.81 1.40 o 6 2 1 140.79 125.16 1.95 o 7 2 1 7.28 8.02 0.30 o -7 3 1 1.56 1.29 0.11 o -6 3 1 133.84 119.75 1.22 o -5 3 1 102.58 109.55 0.90 o -4 3 1 483.27 496.15 7.39 o -3 3 1 15.03 21.00 0.41 o -2 3 1 117.17 128.12 1.95 o -1 3 1 2706.91 2499.09 41.49 o 0 3 1 6112.13 5358.14 86.70 o 1 3 1 2711.96 2453.08 43.14 o 2 3 1 115.71 127.90 2.64 o 3 3 1 14.85 21.07 0.46 o 4 3 1 481.25 488.68 6.24 o 5 3 1 103.46 108.51 1.02 o 6 3 1 133.15 121.40 1.47 o 7 3 1 1.62 1.50 0.21 o -7 4 1 7.72 7.63 0.25 o -6 4 1 165.97 162.89 1.38 o -5 4 1 558.18 540.38 3.70 o -4 4 1 22.15 22.69 0.29 o -3 4 1 324.35 331.52 5.15 o -2 4 1 219.48 219.43 3.15 o -1 4 1 543.83 508.80 8.62 o 0 4 1 11551.15 9690.74 191.30 o 1 4 1 550.57 514.54 8.64 o 2 4 1 219.03 220.58 3.47 o 3 4 1 322.81 340.10 5.01 o 4 4 1 22.43 22.35 0.26 o 5 4 1 557.99 532.29 3.81 o 6 4 1 166.09 164.70 1.26 o 7 4 1 7.52 8.34 0.43 o -7 5 1 4.52 5.13 0.13 o -6 5 1 56.01 51.07 0.42 o -5 5 1 37.02 38.58 0.32 o -4 5 1 155.35 156.39 1.08 o -3 5 1 14.03 12.05 0.28 o -2 5 1 32.08 35.74 0.70 o -1 5 1 611.53 579.24 9.98 o 0 5 1 697.64 684.94 13.00 o 1 5 1 618.37 587.61 10.27 o 2 5 1 31.50 35.80 0.71 o 3 5 1 14.29 13.22 0.32 o 4 5 1 154.15 155.45 1.22 o 5 5 1 37.02 38.70 0.32 o 6 5 1 55.55 51.35 0.41 o 7 5 1 4.58 5.00 0.43 o -7 6 1 2.78 4.50 0.14 o -6 6 1 34.13 32.60 0.35 o -5 6 1 91.84 93.61 0.76 o -4 6 1 74.33 75.68 0.60 o -3 6 1 150.76 160.51 2.08 o -2 6 1 1192.95 1225.14 24.88 o -1 6 1 271.04 258.32 4.08 o 0 6 1 27.74 37.70 0.68 o 1 6 1 268.93 257.85 4.48 o 2 6 1 1196.85 1229.94 27.43 o 3 6 1 151.53 159.16 1.85 o 4 6 1 75.05 75.81 0.59 o 5 6 1 91.14 93.48 0.84 o 6 6 1 33.79 32.37 0.33 o 7 6 1 2.87 4.38 0.32 o -7 7 1 4.60 4.49 0.32 o -6 7 1 49.31 50.03 0.56 o -5 7 1 80.37 81.02 0.77 o -4 7 1 187.23 185.97 1.39 o -3 7 1 127.67 126.78 1.46 o -2 7 1 30.38 26.47 0.49 o -1 7 1 13.81 15.32 0.42 o 0 7 1 44.52 51.97 0.83 o 1 7 1 13.84 15.48 0.78 o 2 7 1 29.25 25.35 0.52 o 3 7 1 128.90 126.98 1.15 o 4 7 1 188.11 183.96 1.36 o 5 7 1 80.58 81.62 0.80 o 6 7 1 49.54 50.39 0.56 o 7 7 1 4.49 4.38 0.32 o -6 8 1 4.26 5.49 0.11 o -5 8 1 3.44 4.22 0.09 o -4 8 1 172.99 157.68 1.21 o -3 8 1 77.90 76.69 0.79 o -2 8 1 9.90 8.26 0.15 o -1 8 1 354.08 372.29 6.75 o 0 8 1 392.72 387.11 5.34 o 1 8 1 353.34 371.10 7.25 o 2 8 1 9.76 8.07 0.22 o 3 8 1 77.27 76.46 0.65 o 4 8 1 171.71 154.78 1.23 o 5 8 1 3.43 4.07 0.11 o 6 8 1 4.14 5.02 0.10 o -6 9 1 13.66 13.05 0.20 o -5 9 1 42.13 43.78 0.45 o -4 9 1 35.07 35.54 0.30 o -3 9 1 54.37 54.69 0.46 o -2 9 1 24.46 23.83 0.22 o -1 9 1 94.74 105.55 1.20 o 0 9 1 162.44 180.43 2.79 o 1 9 1 94.27 105.98 1.35 o 2 9 1 23.96 23.16 0.21 o 3 9 1 53.97 54.61 0.43 o 4 9 1 35.31 35.88 0.30 o 5 9 1 41.24 44.02 0.47 o 6 9 1 13.66 13.25 0.21 o -6 10 1 19.34 18.86 0.34 o -5 10 1 17.18 17.52 0.19 o -4 10 1 167.51 175.45 1.36 o -3 10 1 38.16 37.05 0.33 o -2 10 1 21.44 21.73 0.20 o -1 10 1 124.56 118.24 0.84 o 0 10 1 28.87 26.88 0.20 o 1 10 1 124.34 118.47 0.82 o 2 10 1 21.26 21.40 0.19 o 3 10 1 38.66 37.75 0.30 o 4 10 1 167.21 173.86 1.36 o 5 10 1 17.24 17.61 0.21 o 6 10 1 19.37 18.97 0.53 o -5 11 1 20.33 16.33 0.18 o -4 11 1 175.13 182.88 1.27 o -3 11 1 69.59 66.91 0.52 o -2 11 1 90.80 102.31 0.80 o -1 11 1 17.79 19.43 0.18 o 0 11 1 87.96 90.59 0.62 o 1 11 1 17.84 19.36 0.18 o 2 11 1 90.77 103.66 0.76 o 3 11 1 69.74 66.85 0.51 o 4 11 1 174.51 182.60 1.27 o 5 11 1 20.31 16.62 0.19 o -5 12 1 15.91 15.05 0.20 o -4 12 1 14.90 12.68 0.12 o -3 12 1 52.73 49.53 0.40 o -2 12 1 20.66 22.08 0.21 o -1 12 1 104.34 104.63 0.75 o 0 12 1 29.18 31.56 0.26 o 1 12 1 104.00 104.50 0.73 o 2 12 1 20.66 22.39 0.22 o 3 12 1 52.81 49.38 0.43 o 4 12 1 14.96 12.57 0.13 o 5 12 1 15.71 14.70 0.18 o -4 13 1 29.01 25.32 0.25 o -3 13 1 11.86 14.73 0.14 o -2 13 1 28.56 27.60 0.26 o -1 13 1 8.60 7.59 0.11 o 0 13 1 92.94 89.74 0.66 o 1 13 1 8.54 7.36 0.11 o 2 13 1 28.65 28.05 0.25 o 3 13 1 11.74 14.78 0.16 o 4 13 1 29.00 25.45 0.24 o -4 14 1 9.48 8.01 0.20 o -3 14 1 24.86 21.75 0.19 o -2 14 1 17.98 16.97 0.17 o -1 14 1 4.52 4.59 0.09 o 0 14 1 0.14 -0.04 0.04 o 1 14 1 4.49 4.43 0.09 o 2 14 1 17.87 17.00 0.17 o 3 14 1 24.91 21.65 0.18 o 4 14 1 9.35 8.11 0.26 o -3 15 1 22.49 22.47 0.32 o -2 15 1 0.34 0.32 0.04 o -1 15 1 18.29 21.68 0.22 o 0 15 1 4.11 2.50 0.09 o 1 15 1 18.22 21.55 0.23 o 2 15 1 0.35 0.50 0.04 o 3 15 1 22.55 22.17 0.31 o -1 16 1 7.60 8.45 0.13 o 0 16 1 19.41 23.91 0.51 o 1 16 1 7.65 8.16 0.17 o 0 0 2 1994.58 1755.46 39.83 o 1 0 2 5313.12 4119.68 173.45 o 2 0 2 144.83 181.28 3.96 o 3 0 2 364.87 395.15 6.79 o 4 0 2 32.06 44.29 1.11 o 5 0 2 194.95 190.34 2.44 o 6 0 2 220.83 227.71 3.12 o 7 0 2 69.66 72.47 1.12 o -7 1 2 24.61 24.54 0.46 o -6 1 2 101.26 100.42 1.42 o -5 1 2 14.04 18.13 0.23 o -4 1 2 44.15 52.98 0.86 o -3 1 2 22.01 13.51 0.45 o -2 1 2 1413.94 1462.82 22.48 o -1 1 2 1785.65 1596.24 27.69 o 0 1 2 1178.22 1061.13 16.43 o 1 1 2 1801.84 1589.19 27.52 o 2 1 2 1415.71 1455.26 23.90 o 3 1 2 21.65 13.19 0.44 o 4 1 2 43.81 54.26 0.99 o 5 1 2 13.99 17.46 0.27 o 6 1 2 102.06 100.96 1.43 o 7 1 2 24.69 24.80 0.76 o -7 2 2 29.02 26.14 0.49 o -6 2 2 242.03 232.13 2.78 o -5 2 2 83.69 89.75 0.87 o -4 2 2 54.66 64.42 1.74 o -3 2 2 837.22 941.14 15.42 o -2 2 2 902.59 875.88 13.49 o -1 2 2 826.91 837.98 14.35 o 0 2 2 6144.52 5241.02 81.00 o 1 2 2 824.70 836.69 13.85 o 2 2 2 901.43 879.11 17.16 o 3 2 2 840.69 962.43 16.46 o 4 2 2 54.77 65.22 1.45 o 5 2 2 83.14 88.27 0.78 o 6 2 2 241.20 230.14 3.14 o 7 2 2 29.22 25.49 0.76 o -7 3 2 15.75 17.72 0.34 o -6 3 2 47.24 44.82 0.45 o -5 3 2 55.65 51.86 0.39 o -4 3 2 89.03 86.99 1.35 o -3 3 2 586.75 640.88 9.91 o -2 3 2 700.82 691.14 9.41 o -1 3 2 2606.63 2466.73 40.59 o 0 3 2 3892.51 3400.80 52.65 o 1 3 2 2600.52 2422.18 38.73 o 2 3 2 703.37 696.24 10.97 o 3 3 2 589.95 646.15 11.46 o 4 3 2 87.61 84.74 1.43 o 5 3 2 54.81 51.31 0.36 o 6 3 2 47.65 45.42 0.36 o 7 3 2 15.62 17.64 0.75 o -7 4 2 23.53 20.06 0.40 o -6 4 2 8.78 8.54 0.11 o -5 4 2 66.23 68.08 0.49 o -4 4 2 646.97 616.07 5.11 o -3 4 2 318.98 399.80 5.60 o -2 4 2 511.53 537.79 7.69 o -1 4 2 3869.64 3804.66 62.67 o 0 4 2 2938.87 2763.16 48.09 o 1 4 2 3871.11 3640.88 60.62 o 2 4 2 513.50 537.78 7.79 o 3 4 2 321.43 403.05 5.75 o 4 4 2 647.64 616.50 5.28 o 5 4 2 65.49 66.80 0.47 o 6 4 2 9.01 8.91 0.10 o 7 4 2 23.38 19.45 0.86 o -7 5 2 17.57 19.83 0.32 o -6 5 2 4.97 7.50 0.09 o -5 5 2 1.80 1.73 0.04 o -4 5 2 85.48 86.04 0.66 o -3 5 2 333.03 331.87 4.67 o -2 5 2 799.26 816.60 14.32 o -1 5 2 622.73 603.13 9.93 o 0 5 2 614.94 604.69 11.55 o 1 5 2 623.97 604.42 9.96 o 2 5 2 794.93 831.84 15.61 o 3 5 2 335.88 331.64 4.52 o 4 5 2 86.06 85.02 0.61 o 5 5 2 1.97 1.90 0.08 o 6 5 2 4.87 7.18 0.12 o 7 5 2 17.79 19.45 0.86 o -7 6 2 19.82 17.90 0.45 o -6 6 2 5.40 6.04 0.11 o -5 6 2 27.24 26.87 0.27 o -4 6 2 287.83 286.75 2.16 o -3 6 2 23.54 28.51 0.40 o -2 6 2 379.42 395.12 8.15 o -1 6 2 250.53 239.95 4.01 o 0 6 2 38.45 43.17 0.76 o 1 6 2 247.17 237.95 4.18 o 2 6 2 379.65 390.96 8.92 o 3 6 2 23.84 28.99 0.35 o 4 6 2 287.87 282.41 1.95 o 5 6 2 27.03 26.84 0.27 o 6 6 2 5.31 6.17 0.10 o 7 6 2 19.70 18.92 0.75 o -7 7 2 0.13 0.21 0.11 o -6 7 2 7.06 6.98 0.12 o -5 7 2 176.57 181.97 1.66 o -4 7 2 52.14 54.81 0.42 o -3 7 2 7.98 10.35 0.18 o -2 7 2 136.29 142.63 2.41 o -1 7 2 686.22 693.02 10.80 o 0 7 2 616.58 654.36 9.55 o 1 7 2 686.66 686.22 11.43 o 2 7 2 137.75 143.91 2.95 o 3 7 2 7.89 10.21 0.17 o 4 7 2 52.21 54.71 0.45 o 5 7 2 178.87 186.57 1.82 o 6 7 2 7.25 7.31 0.14 o -6 8 2 28.24 27.66 0.39 o -5 8 2 1.86 1.86 0.09 o -4 8 2 103.85 100.77 0.78 o -3 8 2 176.22 167.87 1.40 o -2 8 2 415.50 421.65 4.16 o -1 8 2 131.60 131.00 2.33 o 0 8 2 19.88 23.44 0.46 o 1 8 2 133.06 133.21 2.70 o 2 8 2 415.43 420.61 3.79 o 3 8 2 175.63 167.85 1.25 o 4 8 2 103.50 99.75 0.73 o 5 8 2 1.89 1.83 0.08 o 6 8 2 28.64 28.25 0.36 o -6 9 2 13.53 13.14 0.20 o -5 9 2 221.56 221.45 2.08 o -4 9 2 11.68 9.90 0.25 o -3 9 2 85.28 80.36 0.69 o -2 9 2 64.97 60.08 0.45 o -1 9 2 187.23 183.03 1.50 o 0 9 2 175.82 145.12 2.59 o 1 9 2 185.91 182.46 1.51 o 2 9 2 65.48 60.40 0.43 o 3 9 2 85.95 81.69 0.61 o 4 9 2 11.78 10.06 0.20 o 5 9 2 221.50 222.51 2.08 o 6 9 2 13.71 13.14 0.25 o -6 10 2 2.43 2.32 0.12 o -5 10 2 25.31 25.32 0.26 o -4 10 2 12.86 12.37 0.13 o -3 10 2 69.31 62.02 0.49 o -2 10 2 44.87 46.78 0.40 o -1 10 2 136.49 130.58 0.96 o 0 10 2 0.04 0.20 0.05 o 1 10 2 137.07 130.68 0.88 o 2 10 2 45.13 47.43 0.36 o 3 10 2 70.04 63.19 0.47 o 4 10 2 13.25 12.48 0.14 o 5 10 2 25.25 25.92 0.27 o -5 11 2 63.92 61.02 0.55 o -4 11 2 59.42 56.91 0.42 o -3 11 2 32.25 35.62 0.30 o -2 11 2 3.31 2.55 0.07 o -1 11 2 183.86 191.73 1.38 o 0 11 2 1.68 0.91 0.05 o 1 11 2 183.80 193.76 1.40 o 2 11 2 3.51 2.94 0.09 o 3 11 2 32.26 35.95 0.32 o 4 11 2 59.38 55.95 0.44 o 5 11 2 63.68 60.54 0.59 o -5 12 2 11.39 11.76 0.18 o -4 12 2 2.81 2.53 0.05 o -3 12 2 1.99 2.26 0.06 o -2 12 2 72.38 76.43 0.62 o -1 12 2 50.27 54.67 0.43 o 0 12 2 16.18 19.52 0.18 o 1 12 2 50.53 54.51 0.43 o 2 12 2 72.57 76.37 0.60 o 3 12 2 1.99 2.40 0.07 o 4 12 2 2.67 2.38 0.06 o 5 12 2 11.27 11.60 0.17 o -4 13 2 7.36 9.71 0.13 o -3 13 2 10.29 11.40 0.11 o -2 13 2 55.37 55.65 0.44 o -1 13 2 6.71 8.29 0.11 o 0 13 2 40.61 42.25 0.34 o 1 13 2 6.76 8.24 0.12 o 2 13 2 55.44 55.94 0.44 o 3 13 2 10.36 11.61 0.13 o 4 13 2 7.39 9.82 0.17 o -4 14 2 3.08 4.17 0.32 o -3 14 2 11.79 10.28 0.11 o -2 14 2 11.45 12.78 0.13 o -1 14 2 37.79 34.36 0.29 o 0 14 2 39.72 37.73 0.37 o 1 14 2 37.87 34.38 0.31 o 2 14 2 11.32 12.70 0.14 o 3 14 2 12.04 10.46 0.12 o 4 14 2 3.13 3.85 0.21 o -3 15 2 9.41 8.02 0.43 o -2 15 2 44.29 45.71 0.38 o -1 15 2 21.40 23.07 0.31 o 0 15 2 4.52 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