#------------------------------------------------------------------------------ #$Date: 2012-09-11 12:26:43 +0300 (Tue, 11 Sep 2012) $ #$Revision: 66590 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/47/2234757.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2234757_Fobs loop_ _publ_author_name 'Hou, Ze-Feng' 'Feng, Juan' 'Liu, Jing-Tian' 'Zhen, Xiao-Li' 'han, Jian-Rong han' _publ_section_title ; 3-(3,4-Dihydroxyphenyl)-1-methoxy-1-oxopropan-2-aminium chloride ; _journal_coeditor_code PV2536 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1516 _journal_volume 68 _journal_year 2012 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 4.9969 _cell_length_b 14.4983 _cell_length_c 16.1094 _exptl_crystal_F_000 520.00 _reflns_d_resolution_high 0.7600 _[local]_cod_data_source_file pv2536Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' shelx in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 153.96 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1520.71 1432.59 24.12 o 4 0 0 1067.16 1038.65 47.38 o 6 0 0 8.84 6.58 8.22 o 1 1 0 47.16 44.50 2.05 o 2 1 0 503.13 472.55 10.76 o 3 1 0 5.15 2.73 2.20 o 4 1 0 2325.44 2395.29 43.08 o 5 1 0 86.52 93.56 12.06 o 6 1 0 587.55 614.34 30.47 o 0 2 0 1406.60 1322.60 10.75 o 1 2 0 34.23 63.85 2.40 o 2 2 0 29.27 31.67 3.11 o 3 2 0 3397.49 3591.41 64.67 o 4 2 0 2.30 3.66 4.05 o 5 2 0 249.58 264.11 18.75 o 6 2 0 2.75 3.60 7.81 o 1 3 0 12190.62 10933.18 210.83 o 2 3 0 2109.46 2164.01 61.94 o 3 3 0 14.87 33.27 11.13 o 4 3 0 3.29 4.19 3.48 o 5 3 0 221.01 240.62 17.63 o 6 3 0 154.72 156.09 23.07 o 0 4 0 23702.79 22580.59 793.74 o 1 4 0 203.47 224.75 4.47 o 2 4 0 1318.41 1371.86 20.78 o 3 4 0 184.95 179.47 8.47 o 4 4 0 428.19 409.28 15.87 o 5 4 0 6.33 5.85 5.39 o 6 4 0 4.49 4.09 6.77 o 1 5 0 3607.35 3742.19 49.68 o 2 5 0 218.40 205.76 7.12 o 3 5 0 68.52 54.81 8.52 o 4 5 0 1151.05 1248.87 35.82 o 5 5 0 131.20 126.06 11.26 o 6 5 0 229.47 219.72 27.33 o 0 6 0 65.21 59.27 5.46 o 1 6 0 98.87 79.44 3.92 o 2 6 0 2258.07 2413.08 34.32 o 3 6 0 2.68 2.30 1.61 o 4 6 0 23.61 21.99 10.29 o 5 6 0 26.80 25.57 13.59 o 6 6 0 56.39 52.25 43.45 o 1 7 0 115.57 114.33 7.67 o 2 7 0 2527.00 2825.00 41.84 o 3 7 0 38.06 44.96 6.32 o 4 7 0 29.06 24.00 9.51 o 5 7 0 217.91 208.52 16.63 o 6 7 0 256.54 288.64 30.33 o 0 8 0 1628.65 1700.05 41.29 o 1 8 0 71.17 58.85 4.20 o 2 8 0 1457.71 1644.05 53.25 o 3 8 0 246.94 245.54 11.14 o 4 8 0 314.08 274.06 17.05 o 5 8 0 48.70 55.37 23.95 o 1 9 0 1029.77 1104.11 18.47 o 2 9 0 669.69 652.60 21.94 o 3 9 0 926.67 884.14 19.36 o 4 9 0 923.33 978.31 37.40 o 5 9 0 0.58 1.52 4.71 o 0 10 0 64.87 89.44 8.63 o 1 10 0 136.51 123.29 7.39 o 2 10 0 311.29 293.36 10.95 o 3 10 0 0.46 1.42 4.12 o 4 10 0 38.89 31.79 17.14 o 5 10 0 0.38 0.51 6.91 o 1 11 0 282.88 255.84 8.52 o 2 11 0 3.22 3.12 2.76 o 3 11 0 29.87 51.88 6.60 o 4 11 0 61.63 40.65 11.37 o 5 11 0 33.43 24.39 28.74 o 0 12 0 103.13 106.80 20.30 o 1 12 0 928.58 1026.47 31.37 o 2 12 0 323.26 287.50 17.04 o 3 12 0 9.71 14.40 7.60 o 4 12 0 99.58 86.46 49.68 o 5 12 0 10.64 7.00 5.60 o 1 13 0 1.05 3.30 4.89 o 2 13 0 75.75 64.57 15.71 o 3 13 0 9.49 3.15 5.00 o 4 13 0 310.04 327.54 27.25 o 0 14 0 356.45 342.85 42.10 o 1 14 0 96.24 78.79 17.00 o 2 14 0 88.38 94.95 11.68 o 3 14 0 7.23 7.85 5.75 o 4 14 0 5.74 8.34 9.28 o 1 15 0 0.70 1.54 5.35 o 2 15 0 20.18 15.25 9.01 o 3 15 0 5.18 9.58 6.80 o 4 15 0 44.40 58.88 19.13 o 0 16 0 33.99 32.46 35.17 o 1 16 0 2.00 4.01 6.55 o 2 16 0 25.74 10.18 11.21 o 3 16 0 118.73 102.58 22.59 o 1 17 0 98.87 93.03 17.60 o 2 17 0 45.77 22.14 18.76 o 0 18 0 82.60 96.00 25.93 o 1 18 0 16.11 16.76 14.82 o 2 18 0 233.93 229.92 18.85 o 1 0 1 7706.51 6874.20 84.04 o 2 0 1 411.32 434.15 8.11 o 3 0 1 245.54 226.37 9.89 o 4 0 1 543.06 504.30 13.95 o 5 0 1 186.20 176.10 15.93 o 6 0 1 95.83 91.47 21.69 o -6 1 1 20.39 14.35 16.05 o -5 1 1 12.49 13.62 9.19 o -4 1 1 0.23 1.28 2.86 o -3 1 1 1.15 2.67 2.80 o -2 1 1 527.50 464.23 35.79 o -1 1 1 4309.12 3862.50 48.66 o 0 1 1 0.86 1.70 0.56 o 1 1 1 4221.01 3887.62 48.90 o 2 1 1 504.02 523.33 9.17 o 3 1 1 1.19 3.35 2.07 o 4 1 1 0.58 2.70 3.53 o 5 1 1 13.29 15.94 8.57 o 6 1 1 20.06 20.22 17.44 o -6 2 1 96.40 89.95 14.54 o -5 2 1 29.15 35.01 19.50 o -4 2 1 26.26 29.97 6.80 o -3 2 1 482.46 452.13 12.88 o -2 2 1 207.32 210.10 14.99 o -1 2 1 3345.60 3118.71 22.60 o 0 2 1 194.63 172.00 4.66 o 1 2 1 3310.00 3105.55 31.74 o 2 2 1 211.59 222.86 6.06 o 3 2 1 482.29 446.57 13.03 o 4 2 1 24.58 26.65 11.28 o 5 2 1 28.24 33.38 17.41 o 6 2 1 98.14 91.60 20.63 o -6 3 1 17.71 14.04 12.38 o -5 3 1 198.56 211.63 16.61 o -4 3 1 47.41 44.17 8.73 o -3 3 1 490.98 488.23 18.64 o -2 3 1 132.75 138.26 4.31 o -1 3 1 488.15 491.43 5.96 o 0 3 1 508.52 536.69 9.73 o 1 3 1 521.44 530.21 7.10 o 2 3 1 142.78 145.46 4.33 o 3 3 1 503.12 493.02 14.62 o 4 3 1 47.01 43.18 7.35 o 5 3 1 200.20 210.31 16.32 o 6 3 1 17.98 12.94 16.51 o -6 4 1 383.37 403.89 31.88 o -5 4 1 498.29 495.49 26.83 o -4 4 1 506.46 486.16 17.75 o -3 4 1 8.97 13.14 4.69 o -2 4 1 2510.88 2659.33 41.68 o -1 4 1 11956.70 10727.41 137.07 o 0 4 1 2530.74 2483.17 48.37 o 1 4 1 11916.05 11050.10 94.98 o 2 4 1 2459.76 2632.74 33.35 o 3 4 1 10.10 20.59 5.62 o 4 4 1 500.71 493.84 16.94 o 5 4 1 487.44 484.60 28.31 o 6 4 1 389.84 400.15 38.13 o -6 5 1 38.30 30.70 31.87 o -5 5 1 509.35 503.47 23.02 o -4 5 1 57.21 49.96 10.50 o -3 5 1 561.53 563.09 14.77 o -2 5 1 3129.76 3234.73 60.39 o -1 5 1 295.03 327.01 9.96 o 0 5 1 7319.72 7007.90 105.12 o 1 5 1 284.47 301.23 7.26 o 2 5 1 3119.66 3197.37 41.87 o 3 5 1 561.19 567.23 23.08 o 4 5 1 59.50 52.25 8.61 o 5 5 1 507.98 502.82 25.43 o 6 5 1 40.37 34.86 31.99 o -6 6 1 84.70 89.93 24.27 o -5 6 1 32.56 45.97 9.24 o -4 6 1 613.16 623.19 30.54 o -3 6 1 159.46 157.11 6.60 o -2 6 1 902.16 928.29 16.22 o -1 6 1 532.78 598.82 17.43 o 0 6 1 2274.20 2407.51 45.39 o 1 6 1 518.50 552.88 11.71 o 2 6 1 895.17 928.90 18.23 o 3 6 1 167.77 169.35 8.46 o 4 6 1 612.66 651.93 30.11 o 5 6 1 27.68 41.96 18.96 o 6 6 1 88.12 92.28 20.30 o -6 7 1 138.29 136.16 18.11 o -5 7 1 15.27 13.06 6.68 o -4 7 1 167.77 152.60 12.46 o -3 7 1 424.11 433.83 10.49 o -2 7 1 2548.00 2745.83 38.65 o -1 7 1 1193.00 1209.23 19.59 o 0 7 1 8.89 11.56 3.64 o 1 7 1 1190.63 1145.41 19.84 o 2 7 1 2528.98 2685.67 41.69 o 3 7 1 433.10 454.32 12.87 o 4 7 1 168.02 163.66 14.44 o 5 7 1 15.33 12.83 9.67 o 6 7 1 137.72 137.10 18.61 o -5 8 1 100.89 101.72 11.94 o -4 8 1 229.01 230.16 15.99 o -3 8 1 317.41 305.10 12.71 o -2 8 1 5.94 7.03 2.72 o -1 8 1 235.77 232.83 8.05 o 0 8 1 264.52 243.14 8.54 o 1 8 1 231.65 229.35 7.34 o 2 8 1 6.48 6.47 3.41 o 3 8 1 324.41 318.79 11.45 o 4 8 1 235.50 247.56 16.00 o 5 8 1 95.92 104.43 13.53 o -5 9 1 221.29 220.06 18.33 o -4 9 1 132.63 112.86 12.45 o -3 9 1 146.11 148.41 9.33 o -2 9 1 1041.05 1029.17 21.52 o -1 9 1 1087.15 1086.58 19.16 o 0 9 1 3346.14 3255.96 135.87 o 1 9 1 1082.62 1055.28 23.20 o 2 9 1 1025.36 994.35 18.65 o 3 9 1 143.11 150.14 8.15 o 4 9 1 137.10 118.39 10.90 o 5 9 1 221.58 209.88 22.23 o -5 10 1 14.24 13.12 14.16 o -4 10 1 624.04 599.38 25.55 o -3 10 1 415.69 385.22 18.65 o -2 10 1 268.53 263.69 11.39 o -1 10 1 21.07 24.13 4.71 o 0 10 1 448.69 451.48 18.21 o 1 10 1 18.43 19.07 8.87 o 2 10 1 274.60 261.21 9.61 o 3 10 1 401.61 384.26 17.94 o 4 10 1 635.39 603.63 27.70 o 5 10 1 14.52 16.87 18.54 o -5 11 1 7.75 5.77 6.53 o -4 11 1 147.55 120.03 20.69 o -3 11 1 231.45 244.67 12.88 o -2 11 1 224.29 218.35 9.89 o -1 11 1 461.19 465.46 22.32 o 0 11 1 28.41 27.41 6.12 o 1 11 1 492.05 510.25 16.37 o 2 11 1 224.49 212.22 8.03 o 3 11 1 241.86 248.11 16.11 o 4 11 1 147.40 132.05 25.08 o 5 11 1 7.46 5.31 6.38 o -5 12 1 123.50 121.56 20.02 o -4 12 1 52.57 51.41 30.69 o -3 12 1 336.99 315.72 17.00 o -2 12 1 236.42 247.86 13.53 o -1 12 1 172.60 165.07 10.23 o 0 12 1 25.28 20.72 8.94 o 1 12 1 176.73 169.57 12.18 o 2 12 1 230.70 243.99 15.94 o 3 12 1 323.97 301.65 16.19 o 4 12 1 53.26 53.28 34.71 o 5 12 1 126.94 130.02 21.12 o -4 13 1 341.02 318.92 25.50 o -3 13 1 96.26 97.92 12.01 o -2 13 1 615.79 650.29 30.99 o -1 13 1 163.38 154.72 11.77 o 0 13 1 1332.14 1420.26 62.83 o 1 13 1 155.51 141.00 19.00 o 2 13 1 605.99 606.11 28.29 o 3 13 1 99.06 94.33 10.03 o 4 13 1 346.92 314.07 26.13 o -4 14 1 827.56 832.83 50.73 o -3 14 1 9.95 12.34 8.08 o -2 14 1 231.83 221.96 15.10 o -1 14 1 43.18 44.53 17.16 o 0 14 1 283.25 267.51 21.39 o 1 14 1 40.16 34.91 17.19 o 2 14 1 235.94 220.50 14.17 o 3 14 1 10.66 12.19 7.24 o 4 14 1 839.11 829.71 49.84 o -4 15 1 3.29 5.62 6.15 o -3 15 1 7.71 10.50 8.48 o -2 15 1 55.57 60.57 22.98 o -1 15 1 242.86 247.14 16.02 o 0 15 1 143.88 141.99 17.85 o 1 15 1 244.86 243.59 22.63 o 2 15 1 51.92 47.95 12.66 o 3 15 1 6.61 11.27 9.14 o 4 15 1 2.57 3.20 5.92 o -3 16 1 186.12 162.49 19.27 o -2 16 1 113.03 113.83 13.04 o -1 16 1 169.78 167.87 17.91 o 0 16 1 95.56 100.88 16.31 o 1 16 1 173.03 176.27 15.86 o 2 16 1 111.52 98.61 21.73 o 3 16 1 175.63 142.86 30.69 o -2 17 1 115.83 123.72 12.18 o -1 17 1 207.55 213.45 24.51 o 0 17 1 300.77 307.55 20.88 o 1 17 1 202.08 207.57 17.29 o 2 17 1 117.63 129.19 21.76 o -2 18 1 172.93 157.27 19.01 o -1 18 1 2.97 2.70 5.95 o 0 18 1 12.50 8.20 9.36 o 1 18 1 2.36 4.31 8.01 o 2 18 1 177.19 165.48 17.11 o 0 19 1 149.75 142.92 15.54 o 0 0 2 2557.05 2224.68 85.56 o 1 0 2 489.62 448.52 7.02 o 2 0 2 2800.09 2825.35 47.08 o 3 0 2 1197.15 1191.80 28.57 o 4 0 2 22.14 20.97 3.73 o 5 0 2 659.47 617.38 30.03 o 6 0 2 346.98 391.91 28.16 o -6 1 2 82.21 83.48 16.91 o -5 1 2 82.25 81.41 14.93 o -4 1 2 85.16 81.44 8.17 o -3 1 2 429.02 421.14 8.29 o -2 1 2 1506.71 1513.69 21.27 o -1 1 2 2378.20 2311.06 25.92 o 0 1 2 4731.55 4179.96 125.40 o 1 1 2 2388.26 2277.75 37.15 o 2 1 2 1508.56 1535.25 22.66 o 3 1 2 422.35 419.19 9.55 o 4 1 2 92.28 86.28 5.71 o 5 1 2 84.59 95.08 14.43 o 6 1 2 77.62 80.40 40.93 o -6 2 2 3.28 3.17 6.81 o -5 2 2 107.48 108.24 12.08 o -4 2 2 83.46 78.68 9.31 o -3 2 2 561.61 548.85 15.43 o -2 2 2 611.55 610.24 11.27 o -1 2 2 4512.77 4542.00 99.59 o 0 2 2 84.03 82.83 2.87 o 1 2 2 4570.94 4376.40 53.28 o 2 2 2 604.58 632.18 10.97 o 3 2 2 542.51 582.62 35.65 o 4 2 2 81.38 78.58 6.57 o 5 2 2 108.89 99.73 12.77 o 6 2 2 4.50 7.15 10.02 o -6 3 2 22.53 18.80 16.73 o -5 3 2 225.96 228.93 17.43 o -4 3 2 374.27 346.54 14.61 o -3 3 2 584.24 579.63 15.00 o -2 3 2 843.34 851.33 16.50 o -1 3 2 3131.92 2981.27 32.01 o 0 3 2 4.98 7.15 1.61 o 1 3 2 3133.70 3018.60 35.33 o 2 3 2 861.87 852.95 14.81 o 3 3 2 606.11 619.64 16.16 o 4 3 2 369.31 357.55 12.55 o 5 3 2 224.58 239.13 18.79 o 6 3 2 22.81 19.17 15.39 o -6 4 2 143.16 141.83 24.55 o -5 4 2 29.50 28.85 19.41 o -4 4 2 4.12 5.62 5.33 o -3 4 2 234.27 226.87 8.33 o -2 4 2 1188.36 1210.37 24.30 o -1 4 2 394.70 406.90 6.43 o 0 4 2 99.35 88.51 3.23 o 1 4 2 380.62 404.07 6.34 o 2 4 2 1190.55 1238.07 28.52 o 3 4 2 240.72 251.54 12.34 o 4 4 2 5.13 6.74 3.91 o 5 4 2 28.00 30.70 13.88 o 6 4 2 140.60 145.38 22.06 o -6 5 2 123.15 130.15 32.07 o -5 5 2 2.98 3.00 3.35 o -4 5 2 174.85 169.68 11.26 o -3 5 2 137.03 135.87 5.75 o -2 5 2 1323.98 1424.51 21.58 o -1 5 2 3165.55 3280.92 46.68 o 0 5 2 12.85 14.47 2.14 o 1 5 2 3119.50 3127.22 42.25 o 2 5 2 1351.80 1417.28 22.30 o 3 5 2 130.98 135.23 6.65 o 4 5 2 180.21 176.40 10.85 o 5 5 2 3.45 4.72 4.08 o 6 5 2 119.18 129.98 18.29 o -6 6 2 3.02 3.07 5.96 o -5 6 2 6.97 8.94 5.55 o -4 6 2 21.99 19.82 8.52 o -3 6 2 344.74 348.11 11.21 o -2 6 2 675.86 702.06 13.63 o -1 6 2 766.06 800.97 15.60 o 0 6 2 953.15 987.96 18.44 o 1 6 2 781.74 781.55 16.29 o 2 6 2 653.47 699.07 16.54 o 3 6 2 342.43 354.30 13.19 o 4 6 2 18.31 13.60 6.76 o 5 6 2 8.21 11.08 8.08 o 6 6 2 2.90 3.93 8.63 o -6 7 2 9.77 7.41 11.25 o -5 7 2 139.84 151.64 13.22 o -4 7 2 87.87 74.91 12.32 o -3 7 2 266.48 235.83 8.28 o -2 7 2 847.69 884.13 15.79 o -1 7 2 62.92 66.39 4.80 o 0 7 2 345.34 350.36 8.17 o 1 7 2 59.64 67.73 4.88 o 2 7 2 866.79 902.83 19.27 o 3 7 2 269.15 262.02 9.91 o 4 7 2 84.10 72.07 9.54 o 5 7 2 138.23 147.10 15.73 o 6 7 2 9.35 13.08 12.43 o -5 8 2 109.57 112.45 11.22 o -4 8 2 29.99 29.17 14.23 o -3 8 2 281.78 275.35 9.83 o -2 8 2 62.28 60.53 5.52 o -1 8 2 663.91 714.04 16.53 o 0 8 2 629.25 600.64 14.17 o 1 8 2 688.50 779.09 44.56 o 2 8 2 62.79 58.65 5.79 o 3 8 2 273.44 275.64 10.82 o 4 8 2 26.87 22.03 11.64 o 5 8 2 110.23 114.33 13.86 o -5 9 2 5.20 3.19 7.08 o -4 9 2 114.18 123.91 13.62 o -3 9 2 570.75 585.32 17.69 o -2 9 2 368.37 366.87 11.78 o -1 9 2 2676.73 2705.21 57.29 o 0 9 2 4.80 4.25 2.06 o 1 9 2 2662.87 2713.30 97.49 o 2 9 2 363.35 346.43 9.79 o 3 9 2 569.08 581.34 14.64 o 4 9 2 112.68 114.25 12.56 o 5 9 2 5.02 5.47 7.24 o -5 10 2 110.28 124.30 26.69 o -4 10 2 12.60 14.28 9.26 o -3 10 2 1398.62 1378.00 47.56 o -2 10 2 313.45 318.24 12.81 o -1 10 2 114.34 108.65 6.95 o 0 10 2 1249.46 1249.64 33.75 o 1 10 2 120.99 117.74 9.85 o 2 10 2 305.55 305.94 8.97 o 3 10 2 1388.84 1298.63 45.66 o 4 10 2 11.82 14.37 15.05 o 5 10 2 112.71 122.32 16.22 o -5 11 2 77.53 80.22 20.48 o -4 11 2 154.68 153.11 12.78 o -3 11 2 165.68 147.16 11.46 o -2 11 2 28.69 39.56 8.34 o -1 11 2 63.63 60.18 5.68 o 0 11 2 782.78 794.22 25.56 o 1 11 2 66.90 71.35 8.28 o 2 11 2 29.19 42.32 16.06 o 3 11 2 171.17 139.67 11.84 o 4 11 2 154.73 152.27 24.09 o 5 11 2 77.79 92.57 17.61 o -5 12 2 67.12 64.07 15.37 o -4 12 2 209.01 193.87 16.29 o -3 12 2 75.66 70.63 9.44 o -2 12 2 254.17 241.73 14.02 o -1 12 2 39.59 38.57 5.96 o 0 12 2 113.83 118.83 12.62 o 1 12 2 43.95 48.60 8.67 o 2 12 2 249.58 256.13 15.58 o 3 12 2 73.79 72.77 9.17 o 4 12 2 206.89 191.09 19.21 o 5 12 2 66.61 45.68 37.02 o -4 13 2 11.09 11.03 10.03 o -3 13 2 129.00 122.83 11.35 o -2 13 2 688.87 695.69 25.18 o -1 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97.63 84.67 16.92 o -2 18 2 229.35 238.89 20.13 o -1 18 2 6.78 10.70 9.97 o 0 18 2 99.87 93.80 24.48 o 1 18 2 6.09 9.75 7.00 o 2 18 2 232.94 219.69 29.71 o 1 0 3 2405.55 2393.63 41.25 o 2 0 3 1553.69 1525.22 31.64 o 3 0 3 1214.12 1259.94 18.36 o 4 0 3 9.97 9.01 3.20 o 5 0 3 178.48 173.51 14.79 o 6 0 3 197.29 210.62 23.15 o -6 1 3 14.01 15.04 19.28 o -5 1 3 233.56 240.20 18.15 o -4 1 3 65.17 58.58 4.73 o -3 1 3 207.10 198.36 5.55 o -2 1 3 2828.14 2809.01 36.44 o -1 1 3 410.47 422.74 10.41 o 0 1 3 2984.99 2797.54 41.65 o 1 1 3 403.78 431.85 5.05 o 2 1 3 2805.34 2787.75 40.29 o 3 1 3 210.76 213.41 6.54 o 4 1 3 62.80 63.01 3.77 o 5 1 3 236.22 235.03 17.17 o 6 1 3 14.10 15.68 11.10 o -6 2 3 49.99 42.78 26.93 o -5 2 3 122.47 134.79 15.00 o -4 2 3 133.72 129.56 8.97 o -3 2 3 140.83 122.61 5.65 o -2 2 3 350.93 339.81 7.31 o -1 2 3 52.10 48.99 2.72 o 0 2 3 3475.51 3515.04 53.75 o 1 2 3 55.24 46.22 3.46 o 2 2 3 370.75 354.84 8.44 o 3 2 3 132.38 118.22 6.41 o 4 2 3 139.02 133.37 7.35 o 5 2 3 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