#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:39:43 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181270 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/48/2234847.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2234847_Fobs loop_ _publ_author_name 'Wu, Xiang-Wen' 'Wang, Xiao-Yan' 'Ma, Jian-Ping' 'Dong, Yu-Bin' _publ_section_title ; Bis(\m-4,4;6,6-bis(biphenyl-2,2'-diyldioxy)-2,2-bis{2-[5-(pyridin-4-yl)-1,3,4-oxadiazol-2-yl]phenoxy}cyclotriphosphazene)di-\m-chlorido-bis[chloridocopper(II)] ; _journal_coeditor_code XU5503 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m648 _journal_page_last m649 _journal_volume 68 _journal_year 2012 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 85.401 _cell_angle_beta 81.984 _cell_angle_gamma 89.844 _cell_length_a 10.5537 _cell_length_b 14.4860 _cell_length_c 15.5510 _exptl_crystal_F_000 1134.00 _reflns_d_resolution_high 0.8255 _cod_data_source_file xu5503Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 100910bm in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 306.38 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 3487.16 3714.67 103.73 o 2 0 0 9603.86 10304.36 279.92 o 3 0 0 13.19 21.09 7.99 o 4 0 0 424.92 468.64 19.39 o 5 0 0 22.49 53.35 8.26 o 6 0 0 1.33 1.39 5.52 o 7 0 0 9.10 16.55 7.72 o 8 0 0 91.47 86.95 13.04 o 9 0 0 38.84 58.23 26.28 o 10 0 0 733.89 770.90 71.05 o 11 0 0 152.90 192.67 43.47 o 12 0 0 9.11 9.89 27.08 o -12 1 0 10.55 4.90 24.18 o -11 1 0 52.48 56.16 30.88 o -10 1 0 340.81 396.77 35.96 o -9 1 0 4028.93 3886.56 109.08 o -8 1 0 386.25 444.19 32.45 o -7 1 0 2.17 2.15 6.63 o -6 1 0 4011.00 4090.10 81.16 o -5 1 0 49.32 45.31 10.38 o -4 1 0 350.66 328.82 29.58 o -3 1 0 1.58 11.98 5.45 o -2 1 0 161.67 150.31 9.32 o -1 1 0 3573.00 3730.66 61.93 o 1 1 0 6511.11 7087.64 182.78 o 2 1 0 6063.97 7012.30 152.05 o 3 1 0 1235.70 1184.36 32.20 o 4 1 0 3406.65 3250.50 75.37 o 5 1 0 827.04 848.61 30.23 o 6 1 0 1771.05 1719.42 51.08 o 7 1 0 1106.83 1031.73 33.52 o 8 1 0 2.87 0.89 7.83 o 9 1 0 534.90 465.30 54.96 o 10 1 0 141.05 171.79 39.67 o 11 1 0 55.13 60.96 32.18 o 12 1 0 105.72 140.01 44.17 o -12 2 0 18.43 32.48 28.08 o -11 2 0 194.68 227.65 45.27 o -10 2 0 2652.91 2573.66 182.73 o -9 2 0 328.82 378.32 33.35 o -8 2 0 618.12 590.09 34.48 o -7 2 0 593.46 667.16 33.09 o -6 2 0 704.69 685.04 32.14 o -5 2 0 4333.47 4202.10 137.01 o -4 2 0 141.13 129.11 17.94 o -3 2 0 7918.69 8651.84 172.39 o -2 2 0 37970.86 41371.44 636.32 o -1 2 0 1524.61 1616.44 29.46 o 0 2 0 15117.67 16211.97 314.42 o 1 2 0 22766.74 25303.12 492.29 o 2 2 0 518.10 557.32 16.30 o 3 2 0 4069.97 4259.33 91.53 o 4 2 0 6898.56 7356.62 153.75 o 5 2 0 900.15 706.05 27.22 o 6 2 0 2532.36 2496.63 66.91 o 7 2 0 7.14 9.34 8.62 o 8 2 0 491.08 470.69 41.27 o 9 2 0 1056.91 958.77 71.45 o 10 2 0 106.00 69.05 27.48 o 11 2 0 13.29 35.58 27.08 o 12 2 0 66.14 41.47 28.68 o -12 3 0 21.26 -9.59 25.78 o -11 3 0 8.20 6.42 16.22 o -10 3 0 1.06 13.82 20.74 o -9 3 0 1863.01 1883.39 73.35 o -8 3 0 489.07 469.97 34.41 o -7 3 0 3.06 -12.12 9.63 o -6 3 0 209.81 228.43 22.05 o -5 3 0 1715.11 1646.77 50.64 o -4 3 0 114.46 52.88 16.24 o -3 3 0 2224.46 2350.50 45.39 o -2 3 0 2972.90 3168.91 56.42 o -1 3 0 910.25 1061.88 28.81 o 0 3 0 46174.68 50341.41 963.04 o 1 3 0 9348.76 11185.44 221.26 o 2 3 0 16335.34 17495.04 343.12 o 3 3 0 716.69 749.46 22.21 o 4 3 0 360.44 368.07 32.78 o 5 3 0 6067.01 5854.92 127.73 o 6 3 0 2375.76 2329.60 63.11 o 7 3 0 107.43 135.39 15.85 o 8 3 0 100.10 161.79 30.08 o 9 3 0 414.71 454.20 47.97 o 10 3 0 155.59 208.66 43.67 o 11 3 0 16.01 1.30 21.49 o 12 3 0 0.28 -1.60 27.88 o -12 4 0 295.55 289.21 55.26 o -11 4 0 344.67 353.31 38.04 o -10 4 0 97.05 109.61 22.45 o -9 4 0 140.88 161.77 24.86 o -8 4 0 268.65 276.94 30.43 o -7 4 0 2527.07 2501.76 75.05 o -6 4 0 2584.07 2517.78 75.05 o -5 4 0 1691.46 1557.48 48.79 o -4 4 0 519.74 397.24 15.14 o -3 4 0 3747.86 3576.06 65.66 o -2 4 0 1284.44 1194.91 26.94 o -1 4 0 1826.10 1961.08 48.83 o 0 4 0 16621.18 19142.76 374.07 o 1 4 0 159.13 161.18 10.65 o 2 4 0 4.02 5.33 4.85 o 3 4 0 253.76 173.29 11.36 o 4 4 0 172.50 144.18 10.83 o 5 4 0 6448.51 6844.51 178.83 o 6 4 0 2219.65 2035.87 93.64 o 7 4 0 2570.39 2491.87 111.23 o 8 4 0 383.73 363.16 42.87 o 9 4 0 148.06 177.58 36.68 o 10 4 0 7.36 -5.00 22.09 o 11 4 0 64.85 89.84 32.88 o 12 4 0 539.56 309.40 55.76 o -12 5 0 155.21 158.70 42.17 o -11 5 0 442.11 389.25 59.56 o -10 5 0 126.43 164.40 42.47 o -9 5 0 1380.43 1207.25 53.11 o -8 5 0 149.48 177.79 23.76 o -7 5 0 21.63 32.20 12.03 o -6 5 0 840.37 777.52 34.66 o -5 5 0 1008.35 913.63 35.42 o -4 5 0 5107.08 5083.32 91.92 o -3 5 0 4915.60 4836.80 86.53 o -2 5 0 9595.38 10312.48 212.26 o -1 5 0 5.91 18.09 6.27 o 0 5 0 2263.84 2216.00 59.41 o 1 5 0 540.76 446.83 18.68 o 2 5 0 600.05 725.03 23.39 o 3 5 0 2720.13 3048.30 75.50 o 4 5 0 227.05 256.84 21.24 o 5 5 0 115.81 123.77 11.91 o 6 5 0 2695.17 2806.56 120.02 o 7 5 0 2130.53 1765.74 92.54 o 8 5 0 13.26 5.90 19.69 o 9 5 0 269.22 307.40 46.17 o 10 5 0 8.55 24.98 22.89 o 11 5 0 461.52 392.24 63.66 o 12 5 0 65.12 73.35 34.58 o -11 6 0 346.13 351.77 57.76 o -10 6 0 9.58 15.19 23.08 o -9 6 0 425.73 377.89 33.72 o -8 6 0 1104.11 1067.35 46.63 o -7 6 0 1175.21 998.88 42.75 o -6 6 0 201.10 195.51 19.98 o -5 6 0 109.38 121.87 10.83 o -4 6 0 71.89 45.07 7.69 o -3 6 0 12335.17 12476.22 258.06 o -2 6 0 3.86 3.30 9.69 o -1 6 0 879.89 1014.71 34.20 o 0 6 0 244.45 232.34 16.68 o 1 6 0 767.62 740.77 47.02 o 2 6 0 9410.03 10364.15 212.30 o 3 6 0 106.13 128.24 16.09 o 4 6 0 2734.56 2871.32 117.12 o 5 6 0 446.39 482.28 42.27 o 6 6 0 8.40 -12.99 12.09 o 7 6 0 645.46 668.66 56.26 o 8 6 0 442.94 461.50 52.17 o 9 6 0 147.87 163.69 37.88 o 10 6 0 369.93 366.06 53.47 o -11 7 0 1.96 22.89 28.38 o -10 7 0 3.21 27.78 25.88 o -9 7 0 22.79 10.59 22.69 o -8 7 0 1084.99 1086.94 47.16 o -7 7 0 250.80 261.72 24.91 o -6 7 0 309.98 369.24 26.85 o -5 7 0 83.92 93.42 12.72 o -4 7 0 23.99 18.49 7.86 o -3 7 0 5243.65 5198.65 121.89 o -2 7 0 3972.29 3747.61 92.37 o -1 7 0 234.06 212.44 17.87 o 0 7 0 442.08 399.93 28.93 o 1 7 0 1075.14 970.88 33.93 o 2 7 0 982.60 944.83 31.88 o 3 7 0 343.83 268.91 24.63 o 4 7 0 86.60 72.55 20.89 o 5 7 0 15.20 19.09 16.39 o 6 7 0 226.73 269.32 40.47 o 7 7 0 489.89 506.97 54.26 o 8 7 0 1228.94 1185.42 79.75 o 9 7 0 4.73 -12.19 23.18 o 10 7 0 78.83 76.25 35.18 o -11 8 0 48.63 68.95 34.08 o -10 8 0 22.98 -3.80 23.38 o -9 8 0 0.29 -26.38 18.59 o -8 8 0 853.31 878.63 70.85 o -7 8 0 103.70 82.75 27.68 o -6 8 0 3565.86 3253.87 88.37 o -5 8 0 224.36 223.15 37.68 o -4 8 0 143.05 167.85 18.15 o -3 8 0 200.55 187.78 25.88 o -2 8 0 2372.91 2353.05 67.11 o -1 8 0 2064.75 2174.40 62.99 o 0 8 0 286.56 301.64 21.84 o 1 8 0 5953.25 6079.66 137.13 o 2 8 0 5481.58 5324.59 121.31 o 3 8 0 4.24 6.59 6.93 o 4 8 0 508.10 526.16 47.37 o 5 8 0 1863.71 1901.86 98.24 o 6 8 0 364.16 372.16 48.97 o 7 8 0 9.03 15.79 22.98 o 8 8 0 473.03 454.90 58.06 o 9 8 0 66.60 48.97 30.18 o 10 8 0 3.94 -35.23 23.48 o 11 8 0 18.58 36.88 32.48 o -10 9 0 39.54 21.49 25.48 o -9 9 0 141.85 123.72 37.58 o -8 9 0 261.60 324.79 54.46 o -7 9 0 445.60 478.09 58.76 o -6 9 0 8.01 13.49 22.19 o -5 9 0 543.94 413.23 49.77 o -4 9 0 16.70 21.27 9.78 o -3 9 0 50.26 70.45 13.88 o -2 9 0 589.39 520.19 44.62 o -1 9 0 16.51 11.96 8.91 o 0 9 0 31.26 25.30 10.88 o 1 9 0 8.53 2.65 8.66 o 2 9 0 4279.68 4223.39 102.65 o 3 9 0 909.52 808.97 58.36 o 4 9 0 923.25 903.51 65.36 o 5 9 0 722.80 671.76 58.96 o 6 9 0 25.28 17.29 24.38 o 7 9 0 35.11 6.30 20.89 o 8 9 0 145.88 143.01 38.77 o 9 9 0 98.01 100.23 36.08 o 10 9 0 49.68 42.27 33.68 o -10 10 0 56.95 88.14 33.58 o -9 10 0 277.64 366.96 59.66 o -8 10 0 3.60 -8.39 22.79 o -7 10 0 67.39 79.55 34.78 o -6 10 0 812.39 832.66 68.36 o -5 10 0 0.29 -17.39 16.99 o -4 10 0 19.10 25.83 11.98 o -3 10 0 426.47 430.55 29.09 o -2 10 0 767.54 819.30 38.43 o -1 10 0 894.61 879.36 38.87 o 0 10 0 154.28 150.93 19.02 o 1 10 0 91.58 96.62 29.48 o 2 10 0 2592.09 2304.89 108.93 o 3 10 0 144.56 236.94 40.07 o 4 10 0 1125.90 851.54 65.06 o 5 10 0 38.76 49.57 24.58 o 6 10 0 867.76 832.96 69.55 o 7 10 0 24.92 31.58 27.48 o 8 10 0 139.99 116.02 37.58 o 9 10 0 9.05 27.48 30.18 o 10 10 0 345.89 393.94 64.46 o -9 11 0 44.52 74.75 33.08 o -8 11 0 732.31 795.08 84.74 o -7 11 0 98.14 190.38 48.37 o -6 11 0 185.47 147.10 39.57 o -5 11 0 11.84 10.49 25.78 o -4 11 0 17.56 20.09 22.79 o -3 11 0 173.31 211.03 27.63 o -2 11 0 170.32 186.91 22.71 o -1 11 0 1281.93 1124.94 46.79 o 0 11 0 563.26 514.53 30.22 o 1 11 0 255.62 243.11 23.69 o 2 11 0 65.47 67.56 25.28 o 3 11 0 2038.32 2017.68 106.13 o 4 11 0 74.74 47.07 24.88 o 5 11 0 168.72 160.99 38.37 o 6 11 0 75.57 90.34 32.98 o 7 11 0 14.29 40.47 31.58 o 8 11 0 238.73 213.06 49.57 o 9 11 0 167.96 118.52 41.97 o -9 12 0 39.63 -3.60 24.78 o -8 12 0 8.79 21.09 31.18 o -7 12 0 840.28 811.17 84.14 o -6 12 0 629.23 672.46 73.25 o -5 12 0 174.69 233.55 44.77 o -4 12 0 1273.99 1168.14 78.05 o -3 12 0 75.61 97.63 19.30 o -2 12 0 97.52 111.25 20.59 o -1 12 0 920.92 862.06 53.22 o 0 12 0 574.97 529.13 53.32 o 1 12 0 393.71 403.24 48.47 o 2 12 0 1761.27 1734.97 97.54 o 3 12 0 155.52 148.70 35.08 o 4 12 0 67.58 60.36 26.28 o 5 12 0 98.20 98.64 34.68 o 6 12 0 68.22 75.25 34.68 o 7 12 0 450.27 372.56 60.26 o 8 12 0 63.50 81.65 36.58 o 9 12 0 361.26 480.99 72.15 o -8 13 0 1.25 30.98 32.48 o -7 13 0 0.49 -4.00 26.28 o -6 13 0 66.07 110.53 36.98 o -5 13 0 41.83 71.75 34.48 o -4 13 0 10.73 -3.00 23.58 o -3 13 0 922.81 813.47 64.46 o -2 13 0 561.51 620.69 57.71 o -1 13 0 3399.26 3360.82 99.91 o 0 13 0 154.90 165.79 36.88 o 1 13 0 1579.66 1466.74 88.44 o 2 13 0 39.32 33.28 23.68 o 3 13 0 5.44 -3.30 18.99 o 4 13 0 52.72 54.36 24.68 o 5 13 0 185.59 176.28 40.57 o 6 13 0 11.62 28.48 29.48 o 7 13 0 18.24 5.60 28.98 o 8 13 0 587.78 597.41 77.65 o -7 14 0 47.46 55.36 35.28 o -6 14 0 422.92 471.69 69.45 o -5 14 0 14.88 17.39 30.78 o -4 14 0 1.75 -0.20 23.88 o -3 14 0 8.13 -5.40 23.88 o -2 14 0 123.47 174.62 27.13 o -1 14 0 4441.28 4218.96 120.50 o 0 14 0 107.07 92.94 32.18 o 1 14 0 132.73 165.69 39.67 o 2 14 0 184.44 220.66 44.17 o 3 14 0 161.96 181.58 39.77 o 4 14 0 81.63 53.56 29.98 o 5 14 0 35.63 89.54 35.08 o 6 14 0 117.24 136.51 41.07 o 7 14 0 14.70 30.68 34.28 o -6 15 0 30.07 59.36 35.78 o -5 15 0 176.30 233.75 52.57 o -4 15 0 37.39 38.67 32.48 o -3 15 0 1.79 16.79 29.58 o -2 15 0 876.13 956.82 64.91 o -1 15 0 151.87 210.36 42.87 o 0 15 0 594.80 613.60 65.16 o 1 15 0 1.73 1.30 23.68 o 2 15 0 19.79 18.99 25.18 o 3 15 0 40.77 7.99 24.28 o 4 15 0 0.92 5.50 26.28 o 5 15 0 494.33 380.35 61.16 o 6 15 0 39.35 69.35 35.98 o -5 16 0 1.05 16.79 32.88 o -4 16 0 40.33 43.17 35.98 o -3 16 0 2.45 -12.29 26.28 o -1 16 0 715.50 771.30 75.95 o 0 16 0 14.45 -14.59 24.08 o 1 16 0 771.76 809.87 80.65 o 2 16 0 251.09 280.92 51.77 o 3 16 0 982.79 882.02 78.95 o 4 16 0 267.91 311.00 57.16 o 5 16 0 8.70 -9.59 30.78 o -1 17 0 90.74 169.69 44.67 o 0 17 0 77.36 125.02 40.67 o 1 17 0 33.62 95.24 37.58 o 2 17 0 11.85 -10.49 27.98 o -2 -17 1 58.91 85.04 35.58 o -1 -17 1 3.50 27.58 26.98 o 0 -17 1 200.22 165.59 42.67 o -4 -16 1 563.26 505.17 69.75 o -3 -16 1 3.81 0.50 27.28 o -2 -16 1 541.44 413.53 58.96 o -1 -16 1 136.86 119.62 37.78 o 0 -16 1 87.79 161.29 41.77 o 1 -16 1 354.32 382.95 57.16 o 3 -16 1 39.08 27.48 30.38 o 4 -16 1 32.74 24.38 29.38 o 5 -16 1 43.12 16.59 31.38 o -6 -15 1 138.26 197.17 51.07 o -5 -15 1 26.51 39.17 32.08 o -4 -15 1 166.19 178.68 45.97 o -3 -15 1 3.16 23.08 26.68 o -2 -15 1 46.33 72.45 32.28 o -1 -15 1 48.21 28.28 24.48 o 0 -15 1 42.80 77.45 31.18 o 1 -15 1 871.52 786.49 68.06 o 2 -15 1 21.39 21.79 26.88 o 3 -15 1 131.84 219.96 46.77 o 4 -15 1 254.00 258.73 50.87 o 5 -15 1 0.48 -9.09 27.98 o 6 -15 1 34.51 108.83 41.67 o -7 -14 1 0.24 -29.28 26.98 o -6 -14 1 73.64 107.03 40.17 o -5 -14 1 124.42 125.92 38.57 o -4 -14 1 1047.61 977.96 80.65 o -3 -14 1 38.46 29.08 26.68 o -2 -14 1 135.23 130.21 36.18 o -1 -14 1 1.26 -2.30 21.09 o 0 -14 1 1344.37 1269.87 84.05 o 1 -14 1 33.74 64.87 20.14 o 2 -14 1 536.53 512.98 40.51 o 3 -14 1 11.97 14.39 24.68 o 4 -14 1 167.32 180.68 42.37 o 5 -14 1 421.95 420.23 62.76 o 6 -14 1 89.52 67.06 33.88 o 7 -14 1 23.31 45.47 33.98 o -8 -13 1 93.24 94.84 44.27 o -7 -13 1 17.25 24.68 31.88 o -6 -13 1 0.66 -19.69 25.18 o -5 -13 1 3.29 3.70 24.18 o -4 -13 1 131.44 119.42 34.18 o -3 -13 1 59.74 40.67 27.28 o -2 -13 1 809.80 854.94 68.26 o -1 -13 1 319.86 294.01 45.57 o 0 -13 1 10.11 27.88 19.69 o 1 -13 1 2565.77 2565.62 84.01 o 2 -13 1 536.10 666.62 62.86 o 3 -13 1 546.14 500.97 59.06 o 4 -13 1 410.12 541.35 65.56 o 5 -13 1 111.39 111.53 37.08 o 6 -13 1 89.43 130.61 39.67 o 7 -13 1 0.55 20.09 28.18 o 8 -13 1 33.56 2.00 29.68 o -8 -12 1 618.17 556.64 75.05 o -7 -12 1 23.43 29.88 31.68 o -6 -12 1 68.69 20.39 27.48 o -5 -12 1 2089.26 1587.86 101.53 o -4 -12 1 3.65 -25.18 17.39 o -3 -12 1 75.14 83.15 29.68 o -2 -12 1 263.92 321.39 47.17 o -1 -12 1 770.38 698.84 58.56 o 0 -12 1 78.06 102.70 19.72 o 1 -12 1 1183.87 1119.40 73.90 o 2 -12 1 198.27 218.00 45.12 o 3 -12 1 840.47 799.76 41.90 o 4 -12 1 122.21 128.72 35.78 o 5 -12 1 1086.50 1233.89 85.24 o 6 -12 1 81.27 107.43 35.78 o 7 -12 1 50.05 34.88 30.38 o 8 -12 1 4.45 7.69 26.48 o 9 -12 1 7.45 60.46 30.78 o -9 -11 1 597.43 643.18 80.05 o -8 -11 1 143.64 182.48 49.77 o -7 -11 1 219.63 225.05 47.87 o -6 -11 1 0.78 23.58 26.08 o -5 -11 1 44.76 34.68 26.58 o -4 -11 1 2196.54 2004.39 109.33 o -3 -11 1 20.05 5.30 19.69 o -2 -11 1 184.18 169.09 35.18 o -1 -11 1 1015.80 984.95 91.09 o 0 -11 1 579.82 526.12 31.22 o 1 -11 1 92.47 87.85 17.12 o 2 -11 1 398.05 390.06 30.22 o 3 -11 1 778.53 752.64 38.29 o 4 -11 1 290.98 238.24 43.67 o 5 -11 1 1601.94 1853.89 104.63 o 6 -11 1 935.45 956.67 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