#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:39:43 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181270 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/48/2234863.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2234863_Fobs loop_ _publ_author_name 'Gao, Shan' 'Ng, Seik Weng' _publ_section_title ; Poly[di-\m~3~-acetato-\m~8~-(naphthalene-1,5-disulfonato)-dilead(II)] ; _journal_coeditor_code XU5522 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m707 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 96.897 _cell_angle_gamma 90.000 _cell_length_a 10.4422 _cell_length_b 12.6663 _cell_length_c 6.8028 _exptl_crystal_F_000 744.00 _reflns_d_resolution_high 0.7702 _cod_data_source_file xu5522Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 325.14 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 10822.80 10779.95 325.77 o 4 0 0 8567.27 8092.70 233.32 o 5 0 0 11098.55 10778.75 304.37 o 6 0 0 4336.79 4211.73 97.08 o 7 0 0 4.83 27.81 9.49 o 8 0 0 1059.84 1011.25 35.04 o 9 0 0 1804.05 1944.08 161.82 o 10 0 0 3593.51 3609.15 153.21 o 11 0 0 5419.24 5769.76 167.70 o 12 0 0 9940.87 10711.59 408.46 o 13 0 0 12878.74 14670.33 1206.20 o 2 1 0 6522.79 6711.43 193.70 o 3 1 0 11094.18 10928.41 217.84 o 4 1 0 11419.44 11185.24 232.05 o 5 1 0 18989.74 19198.46 545.15 o 6 1 0 37222.34 36894.85 1408.12 o 7 1 0 27903.76 27456.61 931.38 o 8 1 0 12328.90 12313.84 348.65 o 9 1 0 10347.96 10237.63 249.30 o 10 1 0 7008.03 6779.10 202.13 o 11 1 0 6281.68 6478.06 145.75 o 12 1 0 2215.11 2269.12 47.60 o 13 1 0 169.42 195.27 24.64 o 0 2 0 266.68 439.76 18.01 o 1 2 0 5867.10 5838.75 75.43 o 2 2 0 2182.61 2147.53 41.19 o 3 2 0 4912.58 5122.91 140.96 o 4 2 0 2009.35 2026.01 36.72 o 5 2 0 248.85 267.96 14.24 o 6 2 0 74.29 95.69 11.57 o 7 2 0 164.91 208.51 8.76 o 8 2 0 105.28 107.91 9.83 o 9 2 0 295.14 330.71 13.84 o 10 2 0 64.24 92.69 10.73 o 11 2 0 227.70 245.29 28.46 o 12 2 0 144.42 181.06 20.73 o 13 2 0 17.10 28.59 18.05 o 1 3 0 8150.33 7863.13 124.71 o 2 3 0 5799.25 5417.41 123.86 o 3 3 0 2944.69 3154.61 113.76 o 4 3 0 4554.41 4777.31 93.34 o 5 3 0 8557.00 8406.02 198.30 o 6 3 0 22417.88 21752.54 702.81 o 7 3 0 15113.67 14621.48 332.96 o 8 3 0 2426.28 2438.75 42.06 o 9 3 0 1928.27 1945.34 41.37 o 10 3 0 1209.67 1143.53 34.65 o 11 3 0 3146.39 3052.63 105.69 o 12 3 0 2155.18 2302.37 98.74 o 13 3 0 217.37 201.40 33.89 o 0 4 0 105718.70 111237.29 8894.06 o 1 4 0 55311.54 54782.52 2038.52 o 2 4 0 27158.89 26824.77 777.06 o 3 4 0 26036.53 25868.55 850.29 o 4 4 0 27791.20 29941.09 1619.09 o 5 4 0 15812.10 17383.88 1341.83 o 6 4 0 5746.35 5711.40 134.97 o 7 4 0 730.32 712.14 31.16 o 8 4 0 692.28 691.84 20.08 o 9 4 0 4025.34 4044.45 155.43 o 10 4 0 2789.09 2555.00 143.49 o 11 4 0 5098.32 4998.22 169.81 o 12 4 0 7780.47 7503.37 463.32 o 13 4 0 8131.25 8216.56 467.54 o 1 5 0 6485.41 6910.07 163.26 o 2 5 0 16566.38 15938.61 419.48 o 3 5 0 38364.25 37286.90 1479.04 o 4 5 0 27122.99 27302.82 963.91 o 5 5 0 26729.65 28886.79 1267.55 o 6 5 0 22932.99 22302.66 810.47 o 7 5 0 16127.76 16071.66 579.04 o 8 5 0 15444.82 13587.14 621.09 o 9 5 0 13805.84 13972.36 492.97 o 10 5 0 11929.94 11877.70 409.72 o 11 5 0 6789.45 7010.98 294.16 o 12 5 0 1579.20 1595.00 97.23 o 0 6 0 10965.75 10513.96 290.52 o 1 6 0 10247.67 9765.35 175.19 o 2 6 0 13976.45 13491.13 335.78 o 3 6 0 7089.54 6662.63 132.69 o 4 6 0 3657.58 3626.81 68.10 o 5 6 0 263.95 297.29 11.12 o 6 6 0 101.87 152.81 23.09 o 7 6 0 1729.06 1710.48 75.60 o 8 6 0 389.97 417.10 22.87 o 9 6 0 720.28 755.85 49.03 o 10 6 0 3548.10 3498.41 169.73 o 11 6 0 3264.60 3380.19 147.89 o 12 6 0 2043.67 1955.28 139.08 o 1 7 0 2330.27 2236.46 47.47 o 2 7 0 742.40 698.61 20.65 o 3 7 0 79.24 87.21 9.85 o 4 7 0 99.96 122.72 11.23 o 5 7 0 537.14 561.24 25.03 o 6 7 0 2581.01 2647.63 46.42 o 7 7 0 2282.24 2295.71 90.78 o 8 7 0 651.79 654.72 35.38 o 9 7 0 189.44 281.51 35.10 o 10 7 0 166.87 151.82 27.45 o 11 7 0 367.60 373.94 42.55 o 12 7 0 206.01 191.24 44.19 o 0 8 0 30254.99 28079.43 1435.39 o 1 8 0 21204.64 19722.83 555.32 o 2 8 0 19926.15 18777.07 511.87 o 3 8 0 10936.89 10123.39 281.39 o 4 8 0 10695.76 10203.80 432.27 o 5 8 0 3611.41 3525.78 62.33 o 6 8 0 943.04 962.74 60.84 o 7 8 0 3.33 17.68 22.70 o 8 8 0 102.81 98.93 15.41 o 9 8 0 1379.01 1398.90 45.91 o 10 8 0 2592.92 2715.65 138.74 o 11 8 0 3212.29 2962.38 283.26 o 1 9 0 60.72 77.27 9.14 o 2 9 0 2306.23 2136.98 76.77 o 3 9 0 13740.13 13189.72 320.66 o 4 9 0 21279.72 21867.42 912.90 o 5 9 0 25339.53 26601.13 1025.04 o 6 9 0 19040.17 19899.13 832.09 o 7 9 0 13326.68 13674.16 679.58 o 8 9 0 12903.72 13137.11 476.13 o 9 9 0 12100.10 12565.48 549.30 o 10 9 0 7792.45 7400.92 413.88 o 11 9 0 4015.80 3919.82 217.20 o 0 10 0 18459.89 17546.43 715.82 o 1 10 0 16607.37 15697.02 469.17 o 2 10 0 14605.39 13570.68 407.59 o 3 10 0 11015.18 10552.06 245.45 o 4 10 0 3335.32 3429.96 131.58 o 5 10 0 753.85 897.72 77.53 o 6 10 0 115.59 115.48 12.49 o 7 10 0 217.72 336.04 41.90 o 8 10 0 109.19 159.64 34.41 o 9 10 0 1014.11 1143.07 81.00 o 10 10 0 2069.81 2056.95 137.62 o 1 11 0 38.62 38.78 13.78 o 2 11 0 228.28 244.29 18.50 o 3 11 0 227.99 232.73 21.01 o 4 11 0 369.22 455.73 32.45 o 5 11 0 14.05 33.82 14.88 o 6 11 0 436.00 476.16 21.95 o 7 11 0 437.48 402.66 26.42 o 8 11 0 227.74 237.48 45.03 o 9 11 0 265.62 288.59 43.06 o 0 12 0 2845.33 2768.87 103.65 o 1 12 0 3948.08 3860.71 136.88 o 2 12 0 6391.83 6268.84 172.05 o 3 12 0 4991.69 4932.70 166.74 o 4 12 0 2739.83 2902.70 110.73 o 5 12 0 418.08 394.23 28.32 o 6 12 0 45.06 41.73 9.06 o 7 12 0 2.91 13.06 27.60 o 8 12 0 39.50 86.69 42.51 o 9 12 0 494.97 460.12 56.32 o 1 13 0 125.37 112.28 15.83 o 2 13 0 1412.44 1418.75 73.63 o 3 13 0 4717.57 4815.56 135.21 o 4 13 0 9635.98 9828.99 431.12 o 5 13 0 8616.92 9299.24 926.00 o 6 13 0 9316.36 8811.09 754.76 o 7 13 0 7447.97 7659.09 545.49 o 8 13 0 7158.13 7645.04 628.33 o 0 14 0 17320.07 17592.83 1032.45 o 1 14 0 10705.50 10694.09 397.40 o 2 14 0 8754.45 9085.97 299.98 o 3 14 0 6334.12 6311.85 192.62 o 4 14 0 3076.79 3301.96 178.54 o 5 14 0 1931.81 2299.26 283.30 o 6 14 0 511.27 636.02 72.85 o 7 14 0 4.92 21.51 65.43 o 1 15 0 457.69 519.46 29.89 o 2 15 0 364.02 361.09 28.99 o 3 15 0 914.43 865.47 75.24 o 4 15 0 551.56 816.56 169.95 o 5 15 0 1235.58 1080.39 166.39 o 0 16 0 214.51 228.63 34.73 o 1 16 0 73.93 137.23 20.55 o 2 16 0 999.11 1082.23 91.87 o 3 16 0 528.69 748.97 88.31 o -13 1 1 1743.89 1690.18 76.30 o -12 1 1 2270.61 2245.16 80.10 o -11 1 1 6739.02 6873.91 219.51 o -10 1 1 5562.13 5624.80 157.57 o -9 1 1 15503.95 14768.22 393.90 o -8 1 1 7689.05 6835.53 273.96 o -7 1 1 5802.23 5091.73 165.83 o -6 1 1 6445.97 6388.62 391.22 o -5 1 1 8440.17 8091.06 192.72 o -4 1 1 6854.23 6462.90 128.42 o -3 1 1 7.83 30.05 5.48 o -2 1 1 6356.85 5982.92 257.92 o -1 1 1 20852.72 21442.32 669.44 o 0 1 1 3361.09 3489.38 91.94 o 1 1 1 15454.96 15762.10 430.75 o 2 1 1 21304.58 21745.44 499.80 o 3 1 1 30244.65 30240.96 806.10 o 4 1 1 54438.45 56304.25 2244.86 o 5 1 1 15435.66 14848.13 377.21 o 6 1 1 7541.73 7283.39 157.17 o 7 1 1 5665.57 5397.21 113.65 o 8 1 1 7211.88 7099.85 214.28 o 9 1 1 4619.60 4785.83 145.97 o 10 1 1 425.96 421.08 17.97 o 11 1 1 72.52 105.55 16.76 o 12 1 1 223.14 262.85 21.47 o 13 1 1 20.42 25.85 18.19 o -13 2 1 1831.31 1879.41 75.35 o -12 2 1 2454.17 2379.10 87.53 o -11 2 1 1716.93 1716.50 46.37 o -10 2 1 34.11 37.17 11.79 o -9 2 1 1086.52 1032.80 31.75 o -8 2 1 11048.64 10398.71 255.96 o -7 2 1 15299.04 13503.17 468.03 o -6 2 1 26905.57 24588.61 1839.57 o -5 2 1 46889.73 44881.27 1910.12 o -4 2 1 51489.50 50477.38 2553.11 o -3 2 1 70803.86 72878.15 4226.45 o -2 2 1 102697.33 117834.52 7383.19 o -1 2 1 13451.71 14110.15 310.82 o 0 2 1 28396.64 30813.63 1273.08 o 1 2 1 31472.78 32274.81 1449.61 o 2 2 1 60666.94 63062.31 3044.17 o 3 2 1 22146.92 22906.90 609.87 o 4 2 1 30.00 71.70 6.96 o 5 2 1 9057.68 9389.51 174.45 o 6 2 1 6605.63 6512.46 119.43 o 7 2 1 8743.43 8678.95 195.70 o 8 2 1 10429.42 10196.11 259.35 o 9 2 1 16833.80 17013.57 574.21 o 10 2 1 18065.22 18482.47 566.49 o 11 2 1 13796.33 14474.16 425.48 o 12 2 1 5307.23 5850.16 183.32 o 13 2 1 4795.60 5589.09 203.14 o -13 3 1 3100.47 3208.15 162.86 o -12 3 1 5437.05 5065.90 203.34 o -11 3 1 8051.26 7516.71 349.48 o -10 3 1 13551.24 12591.41 433.89 o -9 3 1 19715.73 18890.99 915.67 o -8 3 1 25134.34 22783.76 1137.47 o -7 3 1 13154.77 11800.89 518.06 o -6 3 1 6812.02 6308.54 261.68 o -5 3 1 4300.63 4354.66 127.82 o -4 3 1 1084.28 951.52 43.34 o -3 3 1 2123.37 2231.75 74.15 o -2 3 1 4915.07 4922.24 168.93 o -1 3 1 1834.42 1854.66 29.23 o 0 3 1 26209.03 27104.16 955.64 o 1 3 1 41274.58 41987.05 1617.41 o 2 3 1 36323.20 36219.62 1420.65 o 3 3 1 45665.79 49216.25 2053.10 o 4 3 1 46285.62 47453.48 1927.02 o 5 3 1 34733.69 34899.79 1247.35 o 6 3 1 19137.36 19575.09 568.16 o 7 3 1 15559.95 15225.97 405.20 o 8 3 1 8961.95 8908.41 222.00 o 9 3 1 5349.13 5452.50 117.44 o 10 3 1 343.14 412.39 29.96 o 11 3 1 14.20 41.65 23.30 o 12 3 1 68.79 75.74 18.83 o -13 4 1 532.65 549.62 98.85 o -12 4 1 54.35 51.79 25.78 o -11 4 1 47.22 53.62 25.81 o -10 4 1 96.99 79.72 22.45 o -9 4 1 5.09 7.91 18.00 o -8 4 1 20.77 37.44 28.03 o -7 4 1 1040.13 962.20 82.53 o -6 4 1 8260.81 8074.12 500.90 o -5 4 1 5769.31 5558.14 176.99 o -4 4 1 4785.40 4948.82 121.11 o -3 4 1 2837.61 2852.29 57.72 o -2 4 1 3329.12 3365.31 45.29 o -1 4 1 11951.89 12008.89 243.07 o 0 4 1 4534.12 4049.24 156.42 o 1 4 1 2166.81 2222.24 52.65 o 2 4 1 1123.42 1237.70 38.87 o 3 4 1 531.16 600.52 25.14 o 4 4 1 421.40 442.35 10.34 o 5 4 1 87.06 94.66 4.87 o 6 4 1 671.70 689.41 23.09 o 7 4 1 5104.27 5323.04 160.28 o 8 4 1 1641.16 1746.34 46.03 o 9 4 1 848.23 903.74 23.31 o 10 4 1 401.11 431.94 23.69 o 11 4 1 623.51 666.16 38.80 o 12 4 1 2701.05 2823.07 195.95 o -12 5 1 540.48 613.47 49.33 o -11 5 1 1901.35 1739.97 89.90 o -10 5 1 3896.34 3770.52 135.72 o -9 5 1 4859.34 4635.94 162.85 o -8 5 1 1981.54 1719.87 286.02 o -7 5 1 93.46 74.11 29.36 o -6 5 1 421.55 498.16 60.11 o -5 5 1 1739.64 1625.28 47.16 o -4 5 1 1578.60 1497.87 39.77 o -3 5 1 1852.88 2131.27 41.81 o -2 5 1 2962.38 2989.87 101.35 o -1 5 1 3139.51 3131.47 53.81 o 0 5 1 2571.99 2557.74 44.89 o 1 5 1 1445.12 1482.10 25.63 o 2 5 1 5471.97 5517.44 199.09 o 3 5 1 8489.71 8982.03 388.19 o 4 5 1 8367.75 8519.36 173.59 o 5 5 1 2348.42 2558.01 89.92 o 6 5 1 348.98 423.48 13.00 o 7 5 1 3365.77 3560.47 78.37 o 8 5 1 3614.13 3639.61 80.71 o 9 5 1 3670.14 3777.05 100.03 o 10 5 1 88.93 95.92 13.29 o 11 5 1 412.10 478.55 30.87 o 12 5 1 465.30 441.39 51.35 o -12 6 1 807.33 911.06 131.08 o -11 6 1 111.88 113.56 22.30 o -10 6 1 78.09 99.93 21.12 o -9 6 1 381.76 467.39 47.11 o -8 6 1 3201.07 3014.16 250.00 o -7 6 1 5129.85 4974.44 338.14 o -6 6 1 14589.44 13870.53 553.05 o -5 6 1 19050.92 18746.14 709.28 o -4 6 1 31492.23 32682.39 1180.37 o -3 6 1 44035.91 45671.99 1892.17 o -2 6 1 55853.16 55507.71 2838.76 o -1 6 1 33572.96 32752.51 1262.55 o 0 6 1 20942.56 20360.53 564.37 o 1 6 1 12872.00 12433.27 295.21 o 2 6 1 13520.31 13433.84 358.82 o 3 6 1 3546.57 3522.67 74.85 o 4 6 1 10.53 39.77 9.74 o 5 6 1 3824.62 3977.06 75.14 o 6 6 1 2739.75 2913.06 57.46 o 7 6 1 7087.01 7886.92 161.06 o 8 6 1 4320.28 4966.14 210.79 o 9 6 1 8651.80 8984.45 231.18 o 10 6 1 8858.60 9340.24 307.96 o 11 6 1 6961.09 7010.11 399.37 o 12 6 1 5925.32 6542.24 339.81 o -12 7 1 7088.53 6707.37 408.21 o -11 7 1 9159.82 8274.13 446.09 o -10 7 1 8983.76 8728.99 442.40 o -9 7 1 16274.47 16229.58 987.22 o -8 7 1 22877.76 21715.49 1504.44 o -7 7 1 21297.92 20838.57 1273.30 o -6 7 1 8153.82 8078.38 292.05 o -5 7 1 1835.30 1805.57 66.14 o -4 7 1 56.96 96.31 12.55 o -3 7 1 164.37 199.53 17.00 o -2 7 1 934.41 894.47 25.90 o -1 7 1 3559.22 3351.83 53.69 o 0 7 1 13193.50 12894.49 304.38 o 1 7 1 25980.24 24797.32 839.16 o 2 7 1 18171.04 17052.62 636.82 o 3 7 1 30352.70 29817.91 1160.18 o 4 7 1 34934.10 36122.42 1420.76 o 5 7 1 38624.66 38302.79 1625.62 o 6 7 1 35598.27 41874.33 2019.33 o 7 7 1 13377.64 15463.57 661.69 o 8 7 1 7129.06 8635.68 593.28 o 9 7 1 2042.88 2341.10 110.98 o 10 7 1 396.72 527.34 41.88 o 11 7 1 118.69 156.97 34.64 o -11 8 1 15.05 -0.84 26.97 o -10 8 1 49.56 93.21 22.17 o -9 8 1 17.59 46.63 58.38 o -8 8 1 182.36 218.35 39.19 o -7 8 1 3235.56 3037.97 183.06 o -6 8 1 11368.85 10695.55 424.30 o -5 8 1 12440.08 14452.25 1123.89 o -4 8 1 8433.59 8811.82 277.33 o -3 8 1 8270.58 7766.21 186.65 o -2 8 1 14676.50 14073.51 398.39 o -1 8 1 18926.10 17995.53 532.74 o 0 8 1 16374.36 15142.44 415.13 o 1 8 1 4980.97 4700.08 97.04 o 2 8 1 1735.98 1618.73 45.19 o 3 8 1 583.56 539.53 25.43 o 4 8 1 12.28 48.56 8.03 o 5 8 1 20.03 38.10 5.51 o 6 8 1 2014.78 2067.27 48.50 o 7 8 1 6248.76 6539.44 159.81 o 8 8 1 4451.53 4683.44 121.67 o 9 8 1 2269.61 2472.38 105.38 o 10 8 1 1551.09 1626.24 92.97 o 11 8 1 2458.03 2494.04 181.10 o -11 9 1 0.53 6.66 46.54 o -10 9 1 8.41 50.51 20.98 o -9 9 1 0.40 90.38 39.65 o -8 9 1 23.63 38.96 41.89 o -7 9 1 60.97 52.50 27.04 o -6 9 1 8.73 53.16 23.49 o -5 9 1 186.53 208.79 10.12 o -4 9 1 125.55 135.65 16.67 o -3 9 1 38.33 59.52 12.41 o -2 9 1 217.08 218.21 15.68 o -1 9 1 397.36 420.85 20.95 o 0 9 1 0.34 5.26 8.49 o 1 9 1 32.50 66.60 8.84 o 2 9 1 146.36 206.84 24.55 o 3 9 1 608.38 608.22 18.47 o 4 9 1 135.63 143.28 9.74 o 5 9 1 2.54 38.70 6.94 o 6 9 1 4.05 14.81 10.22 o 7 9 1 81.96 90.68 12.38 o 8 9 1 69.70 123.64 20.34 o 9 9 1 2.68 -4.91 22.72 o 10 9 1 28.10 55.34 28.35 o -10 10 1 75.84 145.15 50.95 o -9 10 1 103.31 157.67 49.02 o -8 10 1 1017.18 1117.84 120.93 o -7 10 1 3436.57 3477.83 155.67 o -6 10 1 8601.44 8349.84 345.82 o -5 10 1 5763.32 5668.59 160.41 o -4 10 1 6678.95 7159.79 232.31 o -3 10 1 7381.62 7309.47 178.81 o -2 10 1 14035.82 13567.13 377.04 o -1 10 1 15702.82 14914.03 472.37 o 0 10 1 11149.85 10624.18 282.74 o 1 10 1 2485.40 2259.56 61.29 o 2 10 1 1212.11 1191.49 27.40 o 3 10 1 449.03 487.07 14.80 o 4 10 1 177.86 202.52 8.05 o 5 10 1 29.45 73.74 15.31 o 6 10 1 386.80 467.28 40.05 o 7 10 1 3000.91 3207.09 67.86 o 8 10 1 2236.41 2388.20 111.56 o 9 10 1 4221.10 4444.98 202.83 o 10 10 1 3287.37 3559.23 254.46 o -10 11 1 5149.73 5264.89 379.64 o -9 11 1 6941.78 7484.06 511.43 o -8 11 1 10819.48 11473.82 1153.43 o -7 11 1 9752.12 9928.28 468.37 o -6 11 1 5572.69 6091.97 269.26 o -5 11 1 1802.51 2057.02 68.84 o -4 11 1 910.04 945.69 51.62 o -3 11 1 798.04 807.12 28.14 o -2 11 1 35.84 83.54 27.25 o -1 11 1 2457.03 2336.72 67.10 o 0 11 1 17014.39 16273.46 567.65 o 1 11 1 23302.63 21648.25 775.96 o 2 11 1 19598.04 18455.58 616.17 o 3 11 1 13636.37 13598.47 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