#------------------------------------------------------------------------------ #$Date: 2012-09-11 12:26:43 +0300 (Tue, 11 Sep 2012) $ #$Revision: 66590 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/49/2234917.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2234917_Fobs loop_ _publ_author_name 'W\"ohlert, Susanne' 'Jess, Inke' 'N\"ather, Christian' _publ_section_title ; A triclinic polymorph of poly[[bis[\m-1,2-bis(pyridin-4-yl)ethene-\k^2^N:N']bis(thiocyanato-\kN)cobalt(II)] 1,2-bis(pyridin-4-yl)ethene monosolvate] ; _journal_coeditor_code BT5886 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m733 _journal_page_last m734 _journal_volume 68 _journal_year 2012 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 99.892 _cell_angle_beta 90.547 _cell_angle_gamma 91.269 _cell_length_a 13.7954 _cell_length_b 13.8916 _cell_length_c 27.8480 _exptl_crystal_F_000 2238.00 _reflns_d_resolution_high 0.8720 _[local]_cod_data_source_file bt5886Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Co(tvp)2(NCS)2 tvp-Solvate at 170K in P-1 (sch64a)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 351.26 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 5 0 0 123384.61 163950.34 553.50 o 6 0 0 60342.73 71272.56 313.87 o 7 0 0 1675.62 1608.55 89.38 o 8 0 0 7944.17 8021.43 111.91 o 9 0 0 31153.09 32171.66 182.08 o 10 0 0 17629.23 17818.75 151.06 o 11 0 0 16051.24 17657.28 150.01 o 12 0 0 2427.29 2487.94 96.67 o 13 0 0 1297.22 1288.31 102.62 o 14 0 0 16495.62 16820.71 142.69 o 15 0 0 1497.45 1751.75 122.22 o -15 1 0 129.15 191.19 117.52 o -14 1 0 101.09 120.34 103.25 o -13 1 0 609.37 686.89 106.87 o -12 1 0 240.93 255.37 71.21 o -11 1 0 50.35 60.82 90.99 o -10 1 0 12.44 233.23 89.80 o -9 1 0 127.15 250.74 75.80 o -8 1 0 422.27 425.28 75.03 o -7 1 0 190.97 131.94 80.65 o -6 1 0 189.92 206.01 79.95 o -5 1 0 652.46 594.11 87.89 o -4 1 0 1133.14 944.40 87.31 o -3 1 0 206.59 214.99 88.38 o -2 1 0 620.38 447.93 92.17 o -1 1 0 7.47 -6.84 75.79 o 1 1 0 17.50 -0.35 75.21 o 2 1 0 517.99 294.83 72.79 o 3 1 0 6.40 6.72 84.62 o 4 1 0 166.84 139.76 63.81 o 5 1 0 62.80 117.05 72.38 o 6 1 0 23.62 72.01 54.10 o 7 1 0 195.70 219.91 56.83 o 8 1 0 87.58 60.71 73.44 o 9 1 0 103.80 63.54 73.08 o 10 1 0 99.02 29.70 80.15 o 11 1 0 254.53 294.64 90.31 o 12 1 0 11.91 52.09 70.12 o 13 1 0 637.49 659.90 102.63 o 14 1 0 2.76 -22.04 81.55 o 15 1 0 71.73 -30.76 95.47 o -15 2 0 137.60 195.20 115.40 o -14 2 0 23.86 38.54 97.94 o -13 2 0 256.35 200.54 101.16 o -12 2 0 181.92 199.82 70.02 o -11 2 0 37.04 -1.89 89.45 o -10 2 0 743.92 802.88 91.70 o -9 2 0 49.11 104.78 71.31 o -8 2 0 8.99 -19.68 73.30 o -7 2 0 72.18 111.39 64.59 o -6 2 0 1605.27 1526.12 75.55 o -5 2 0 166.05 187.73 57.55 o -4 2 0 109.23 49.28 74.16 o -3 2 0 11.25 -3.18 70.95 o -2 2 0 19.14 36.07 82.86 o -1 2 0 206.12 103.54 86.06 o 0 2 0 143.32 83.20 70.45 o 1 2 0 214.37 169.18 85.95 o 2 2 0 20.38 23.69 65.65 o 3 2 0 176.90 150.63 69.83 o 4 2 0 21.80 49.27 57.52 o 5 2 0 7.50 -16.15 53.51 o 6 2 0 802.08 786.41 73.12 o 7 2 0 129.90 159.51 77.69 o 8 2 0 505.76 496.03 62.89 o 9 2 0 46.92 86.04 58.58 o 10 2 0 647.26 629.98 69.03 o 11 2 0 32.70 93.23 71.78 o 12 2 0 214.18 260.78 84.53 o 13 2 0 24.35 23.45 100.06 o 14 2 0 2.47 -39.60 79.67 o 15 2 0 51.57 26.99 115.27 o -15 3 0 1144.63 1128.62 99.26 o -14 3 0 2195.10 2162.66 88.19 o -13 3 0 306.80 354.07 99.51 o -12 3 0 23.36 3.42 83.44 o -11 3 0 2672.49 2824.45 101.47 o -10 3 0 700.46 752.29 92.52 o -9 3 0 654.34 720.80 74.46 o -8 3 0 519.57 588.18 62.89 o -7 3 0 2235.15 2369.51 88.41 o -6 3 0 4876.48 5205.82 96.55 o -5 3 0 1782.62 1577.17 87.96 o -4 3 0 35660.06 37320.62 249.29 o -3 3 0 10676.67 9048.29 144.10 o -2 3 0 79.95 31.60 89.01 o -1 3 0 4464.94 4029.39 129.54 o 1 3 0 2460.01 3035.08 116.55 o 2 3 0 218.71 234.08 92.38 o 3 3 0 9871.38 8879.98 144.72 o 4 3 0 31018.56 32432.13 227.33 o 5 3 0 388.69 349.98 54.28 o 6 3 0 4746.86 4880.00 92.07 o 7 3 0 817.95 946.38 78.65 o 8 3 0 51.81 131.89 69.89 o 9 3 0 36.34 22.16 69.89 o 10 3 0 1363.03 1298.10 73.02 o 11 3 0 4201.84 4427.86 93.53 o 12 3 0 149.23 99.02 83.46 o 13 3 0 419.30 448.35 99.17 o 14 3 0 2456.27 2446.15 90.59 o 15 3 0 1132.06 1201.18 97.73 o -15 4 0 8.06 -47.61 115.02 o -14 4 0 617.58 697.57 100.97 o -13 4 0 2688.51 2870.09 94.66 o -12 4 0 1787.18 1901.93 91.24 o -11 4 0 0.25 37.36 88.03 o -10 4 0 24.64 37.60 88.27 o -9 4 0 2952.51 2783.09 90.56 o -8 4 0 2447.65 2373.69 86.13 o -7 4 0 42.65 -23.69 74.61 o -6 4 0 1107.84 1243.22 89.95 o -5 4 0 123.44 122.26 77.34 o -4 4 0 3008.56 3103.03 101.43 o -3 4 0 2256.14 2147.94 83.80 o -2 4 0 21771.48 19745.23 206.53 o -1 4 0 12637.55 12330.07 169.42 o 0 4 0 20.21 -20.74 68.24 o 1 4 0 10870.43 10190.23 154.02 o 2 4 0 19215.82 19419.40 200.30 o 3 4 0 2188.75 2413.72 120.35 o 4 4 0 383.47 384.68 59.59 o 5 4 0 15.06 128.46 68.71 o 6 4 0 71.22 171.39 81.92 o 7 4 0 247.60 292.20 61.44 o 8 4 0 1048.12 995.59 66.26 o 9 4 0 1633.55 1549.24 86.31 o 10 4 0 51.20 25.34 86.16 o 11 4 0 0.16 45.14 84.26 o 12 4 0 161.14 117.29 89.94 o 13 4 0 468.38 574.33 99.42 o 14 4 0 83.15 100.42 81.80 o 15 4 0 71.55 109.49 112.91 o -15 5 0 17.42 -33.47 113.85 o -14 5 0 197.88 250.27 111.40 o -13 5 0 7.37 92.28 96.87 o -12 5 0 40.33 119.63 99.94 o -11 5 0 701.34 615.89 89.20 o -10 5 0 280.75 256.10 90.08 o -9 5 0 52.17 42.55 73.78 o -8 5 0 631.32 665.90 76.94 o -7 5 0 578.11 480.52 77.29 o -6 5 0 2460.04 2268.54 79.20 o -5 5 0 165.31 58.24 83.36 o -4 5 0 0.15 295.33 65.64 o -3 5 0 1549.35 1751.72 93.69 o -2 5 0 6659.81 5428.92 136.75 o -1 5 0 1656.22 1511.80 83.95 o 0 5 0 1.04 -6.36 82.97 o 1 5 0 1968.24 1850.30 96.50 o 2 5 0 7644.31 7667.39 130.86 o 3 5 0 2217.31 2678.04 87.23 o 4 5 0 3.30 22.27 66.35 o 5 5 0 179.11 255.39 67.80 o 6 5 0 2293.39 2236.76 77.38 o 7 5 0 3203.34 3395.27 91.86 o 8 5 0 3058.71 2902.48 77.55 o 9 5 0 1014.21 1100.10 91.98 o 10 5 0 2294.18 2472.06 96.90 o 11 5 0 2920.94 2873.40 96.03 o 12 5 0 1540.00 1649.52 89.42 o 13 5 0 272.70 196.89 80.52 o 14 5 0 173.33 231.04 93.71 o -14 6 0 858.22 831.81 118.81 o -13 6 0 494.63 477.51 82.44 o -12 6 0 11.72 149.44 99.94 o -11 6 0 2465.35 2291.27 82.58 o -10 6 0 264.73 249.84 72.63 o -9 6 0 3842.44 3711.41 102.30 o -8 6 0 2754.93 2821.98 102.25 o -7 6 0 267.10 270.03 75.23 o -6 6 0 7772.94 6731.81 119.45 o -5 6 0 14073.86 12880.92 142.85 o -4 6 0 17019.71 15637.00 163.70 o -3 6 0 10015.73 10973.74 135.83 o -2 6 0 795.52 751.92 62.37 o -1 6 0 57198.59 68196.31 315.56 o 0 6 0 45559.79 61111.88 280.46 o 1 6 0 57561.82 75700.92 315.37 o 2 6 0 1110.67 1358.45 85.25 o 3 6 0 6827.13 8322.98 129.45 o 4 6 0 17364.74 18461.86 165.79 o 5 6 0 12928.26 12846.09 129.62 o 6 6 0 11252.24 11709.44 130.44 o 7 6 0 460.14 436.70 56.15 o 8 6 0 959.96 983.62 70.01 o 9 6 0 2094.40 2003.85 83.75 o 10 6 0 2460.30 2514.25 93.84 o 11 6 0 7962.99 7874.10 117.64 o 12 6 0 294.71 194.30 83.00 o 13 6 0 1488.88 1289.97 102.63 o 14 6 0 2434.66 2305.53 122.72 o -14 7 0 526.49 476.57 83.50 o -13 7 0 2723.99 2953.24 113.33 o -12 7 0 4945.96 5066.65 102.79 o -11 7 0 202.32 150.19 103.27 o -10 7 0 103.44 250.83 84.75 o -9 7 0 2870.64 2691.73 100.32 o -8 7 0 1748.05 1600.51 97.19 o -7 7 0 10.15 -44.78 68.94 o -6 7 0 323.35 362.99 75.12 o -5 7 0 1441.11 1603.24 73.07 o -4 7 0 6560.18 6227.19 102.69 o -3 7 0 1833.58 2010.34 90.69 o -2 7 0 14817.14 14417.85 137.15 o -1 7 0 12327.90 13600.54 142.02 o 0 7 0 10.44 25.10 79.79 o 1 7 0 12616.80 12739.13 138.81 o 2 7 0 14185.41 14338.18 148.36 o 3 7 0 2190.26 2202.95 89.93 o 4 7 0 2938.03 3849.23 97.54 o 5 7 0 1349.14 1541.70 83.21 o 6 7 0 637.29 619.53 75.41 o 7 7 0 76.55 74.37 78.26 o 8 7 0 409.91 413.61 76.07 o 9 7 0 1237.52 1252.67 92.47 o 10 7 0 181.72 360.49 82.99 o 11 7 0 8.33 29.23 98.76 o 12 7 0 1388.73 1316.06 103.21 o 13 7 0 237.28 373.83 116.71 o -13 8 0 15.23 0.59 80.97 o -12 8 0 0.47 25.10 98.17 o -11 8 0 333.82 174.51 102.23 o -10 8 0 19.68 54.45 82.03 o -9 8 0 7.19 -16.15 87.09 o -8 8 0 178.92 299.55 73.92 o -7 8 0 889.12 831.51 79.56 o -6 8 0 293.00 295.15 93.27 o -5 8 0 59.08 102.54 72.25 o -4 8 0 642.71 622.06 76.95 o -3 8 0 452.07 618.05 77.15 o -2 8 0 312.32 540.03 81.02 o -1 8 0 144.52 74.15 74.86 o 0 8 0 187.73 236.04 61.78 o 1 8 0 78.78 37.48 74.61 o 2 8 0 333.11 298.27 75.84 o 3 8 0 1252.07 1046.47 78.23 o 4 8 0 221.86 165.19 73.57 o 5 8 0 88.55 94.53 70.96 o 6 8 0 1380.52 1316.09 84.84 o 7 8 0 4067.77 4114.69 106.37 o 8 8 0 2206.59 2334.20 83.28 o 9 8 0 1090.57 1050.84 89.02 o 10 8 0 1100.33 1027.98 87.83 o 11 8 0 1589.53 1555.10 103.95 o 12 8 0 1604.43 1677.21 103.23 o 13 8 0 406.77 513.52 116.85 o -13 9 0 293.18 497.17 113.77 o -12 9 0 42.60 203.07 116.21 o -11 9 0 865.13 605.68 103.84 o -10 9 0 6.33 42.07 99.94 o -9 9 0 1526.13 1394.92 90.14 o -8 9 0 597.59 553.15 88.83 o -7 9 0 2.74 60.81 89.57 o -6 9 0 1114.85 1064.46 97.31 o -5 9 0 4763.73 4134.26 105.36 o -4 9 0 283.57 299.63 88.79 o -3 9 0 1713.31 1525.00 82.78 o -2 9 0 640.11 599.84 75.76 o -1 9 0 10596.48 10518.59 118.31 o 0 9 0 128.43 316.63 76.86 o 1 9 0 8923.44 10255.88 111.17 o 2 9 0 312.36 341.40 73.11 o 3 9 0 874.25 896.65 82.05 o 4 9 0 14.91 -12.49 91.45 o 5 9 0 2890.46 2711.64 108.53 o 6 9 0 2360.06 2519.34 99.17 o 7 9 0 1349.89 1367.84 93.08 o 8 9 0 13.59 81.67 67.29 o 9 9 0 300.83 316.69 95.03 o 10 9 0 457.61 610.88 83.85 o 11 9 0 2610.00 2697.65 94.03 o 12 9 0 952.10 1129.98 117.88 o -12 10 0 1322.40 1415.39 120.06 o -11 10 0 12.25 23.45 107.95 o -10 10 0 293.66 414.07 99.27 o -9 10 0 192.17 217.85 99.97 o -8 10 0 62.91 -44.79 78.03 o -7 10 0 707.48 813.05 64.89 o -6 10 0 745.13 697.62 78.12 o -5 10 0 2343.16 2458.67 100.47 o -4 10 0 1035.94 917.90 91.51 o -3 10 0 2488.15 3372.55 105.61 o -2 10 0 10552.98 10649.04 131.01 o -1 10 0 8192.62 9268.44 123.17 o 0 10 0 157.74 275.62 90.07 o 1 10 0 6657.77 7188.58 116.60 o 2 10 0 10147.31 10464.96 130.42 o 3 10 0 4375.69 3928.32 109.06 o 4 10 0 0.72 -74.36 89.21 o 5 10 0 1215.06 1026.75 85.03 o 6 10 0 1175.53 1031.32 77.46 o 7 10 0 1042.49 1228.16 87.95 o 8 10 0 160.55 59.18 83.81 o 9 10 0 518.27 389.68 99.66 o 10 10 0 9.58 92.16 80.14 o 11 10 0 2.79 7.78 116.32 o -11 11 0 54.39 4.48 115.38 o -10 11 0 0.27 98.05 108.54 o -9 11 0 79.02 179.74 98.30 o -8 11 0 12.97 16.74 99.82 o -7 11 0 578.52 696.53 103.68 o -6 11 0 812.43 718.99 74.34 o -5 11 0 54.00 38.66 84.62 o -4 11 0 705.77 675.62 91.92 o -3 11 0 1260.03 1062.96 92.24 o -2 11 0 243.66 319.98 91.85 o -1 11 0 193.26 99.38 77.81 o 0 11 0 755.93 772.13 93.58 o 1 11 0 123.22 -34.42 77.68 o 2 11 0 92.21 0.35 89.11 o 3 11 0 409.65 511.12 92.11 o 4 11 0 386.43 482.08 90.10 o 5 11 0 27.01 114.79 84.15 o 6 11 0 1292.72 1247.37 77.58 o 7 11 0 3365.49 3574.75 111.46 o 8 11 0 201.33 140.64 81.11 o 9 11 0 12.25 4.12 96.64 o 10 11 0 1031.88 1086.92 118.25 o -10 12 0 119.33 164.31 113.98 o -9 12 0 321.00 318.93 117.08 o -8 12 0 312.59 281.08 101.04 o -7 12 0 494.34 447.21 100.72 o -6 12 0 177.44 81.69 100.44 o -5 12 0 1213.55 1376.47 87.96 o -4 12 0 30.62 -83.68 83.68 o -3 12 0 329.20 468.35 83.60 o -2 12 0 1053.33 883.15 75.55 o -1 12 0 185.62 151.01 72.03 o 0 12 0 486.51 591.02 87.87 o 1 12 0 381.79 620.99 87.62 o 2 12 0 562.48 633.90 72.66 o 3 12 0 159.88 87.23 83.81 o 4 12 0 574.87 604.64 101.68 o 5 12 0 381.99 409.89 104.12 o 6 12 0 15.62 -23.69 98.64 o 7 12 0 229.71 294.96 97.38 o 8 12 0 0.48 3.65 80.26 o 9 12 0 35.03 26.05 114.20 o -9 13 0 949.62 922.62 97.70 o -8 13 0 715.13 768.89 116.90 o -7 13 0 3826.07 3696.21 101.41 o -6 13 0 443.45 507.43 84.55 o -5 13 0 546.05 382.73 102.02 o -4 13 0 725.85 807.32 102.76 o -3 13 0 3297.92 3306.25 113.58 o -2 13 0 6652.11 6260.81 124.27 o -1 13 0 4903.04 5038.55 116.12 o 0 13 0 217.22 202.06 100.32 o 1 13 0 5615.03 5663.60 117.90 o 2 13 0 6435.52 5934.67 122.44 o 3 13 0 3065.26 3156.99 112.70 o 4 13 0 152.43 86.76 82.04 o 5 13 0 1244.33 1051.33 104.48 o 6 13 0 1510.79 1289.29 86.33 o 7 13 0 1759.92 1757.22 123.45 o 8 13 0 280.40 142.89 115.77 o -7 14 0 145.76 122.23 115.87 o -6 14 0 43.24 88.28 93.93 o -5 14 0 97.43 210.16 116.33 o -4 14 0 1141.39 1074.15 102.10 o -3 14 0 1344.15 976.47 102.72 o -2 14 0 133.07 138.97 98.54 o -1 14 0 553.16 440.64 104.62 o 0 14 0 1474.03 1518.04 102.98 o 1 14 0 1181.71 1224.05 104.71 o 2 14 0 102.23 165.96 97.12 o 3 14 0 23.48 130.35 82.85 o 4 14 0 42.43 58.69 115.03 o 5 14 0 205.53 241.66 115.76 o 6 14 0 618.52 625.71 96.72 o -4 15 0 60.09 -38.78 94.52 o -3 15 0 244.26 198.29 115.41 o -2 15 0 81.23 62.47 115.51 o -1 15 0 1248.54 980.16 97.74 o 0 15 0 946.14 830.38 118.12 o 1 15 0 567.51 513.16 96.48 o 2 15 0 134.72 108.44 115.04 o 3 15 0 41.66 62.70 114.91 o -4 -15 1 140.29 150.76 114.10 o -3 -15 1 132.91 246.94 114.81 o -2 -15 1 706.37 726.06 117.61 o -1 -15 1 377.52 361.99 118.74 o 0 -15 1 144.61 150.41 117.64 o 1 -15 1 886.29 901.23 98.76 o 2 -15 1 722.19 784.24 117.97 o 3 -15 1 39.58 -14.26 114.68 o 4 -15 1 44.45 8.72 92.87 o 5 -15 1 944.30 975.59 84.72 o -6 -14 1 235.90 127.91 117.65 o -5 -14 1 1443.78 1054.71 107.57 o -4 -14 1 1978.48 1523.96 106.24 o -3 -14 1 971.41 969.58 101.61 o -2 -14 1 35.35 -98.41 98.41 o -1 -14 1 5143.92 5602.30 120.73 o 0 -14 1 5369.21 5964.30 118.76 o 1 -14 1 6642.00 6667.27 109.81 o 2 -14 1 3.23 62.58 98.41 o 3 -14 1 762.97 605.58 101.11 o 4 -14 1 1197.01 1173.04 102.47 o 5 -14 1 2434.13 2230.92 120.85 o 6 -14 1 1184.58 1144.03 118.63 o 7 -14 1 209.76 164.68 116.00 o -8 -13 1 127.39 129.66 115.28 o -7 -13 1 5304.43 4423.13 115.97 o -6 -13 1 4336.33 3903.13 113.23 o -5 -13 1 362.61 195.97 103.64 o -4 -13 1 4648.90 4480.60 118.65 o -3 -13 1 52.50 497.61 85.57 o -2 -13 1 154.42 796.03 104.32 o -1 -13 1 338.93 742.96 104.12 o 0 -13 1 317.57 292.41 101.28 o 1 -13 1 943.89 1039.65 105.16 o 2 -13 1 65.01 116.21 102.89 o 3 -13 1 0.00 -72.95 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