#------------------------------------------------------------------------------ #$Date: 2012-09-11 12:26:43 +0300 (Tue, 11 Sep 2012) $ #$Revision: 66590 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/49/2234923.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2234923_Fobs loop_ _publ_author_name 'Gao, Shan' 'Ng, Seik Weng' _publ_section_title ; catena-Poly[[(tetraaquacadmium)-\m-4,4'-bipyridine-\k^2^N:N'] 4-hydroxy-3-sulfonatobenzoate monohydrate] ; _journal_coeditor_code BT5895 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m715 _journal_volume 68 _journal_year 2012 _space_group_IT_number 60 _symmetry_space_group_name_Hall '-P 2n 2ab' _symmetry_space_group_name_H-M 'P b c n' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 16.3246 _cell_length_b 15.3063 _cell_length_c 16.5084 _exptl_crystal_F_000 2320.00 _reflns_d_resolution_high 0.7709 _[local]_cod_data_source_file bt5895Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Pbcn' _shelx_refln_list_code 4 _shelx_f_calc_maximum 710.99 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y+1/2, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y, -z+1/2' '-x, -y, -z' 'x-1/2, y-1/2, -z-1/2' '-x-1/2, y-1/2, z' 'x, -y, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 161044.28 149257.27 1734.11 o 6 0 0 171.48 257.21 76.35 o 8 0 0 74825.51 70728.72 853.64 o 10 0 0 24948.80 23628.21 345.54 o 12 0 0 40656.52 39103.30 557.82 o 14 0 0 55599.84 53824.55 849.24 o 16 0 0 2918.01 3376.23 275.46 o 18 0 0 12389.06 13028.50 367.68 o 20 0 0 344.94 146.93 187.54 o 3 1 0 122.14 121.61 20.60 o 5 1 0 1.39 19.04 26.93 o 7 1 0 2732.79 2686.73 57.98 o 9 1 0 803.25 886.75 55.99 o 11 1 0 848.85 915.42 74.83 o 13 1 0 0.50 58.93 55.64 o 15 1 0 267.21 255.86 74.19 o 17 1 0 244.09 285.92 88.65 o 19 1 0 114.31 135.96 110.98 o 21 1 0 35.10 0.84 91.39 o 2 2 0 126100.70 119821.58 851.12 o 4 2 0 5230.49 4791.98 70.20 o 6 2 0 12985.75 10885.27 112.43 o 8 2 0 16618.98 15241.45 159.34 o 10 2 0 67408.44 67192.65 622.73 o 12 2 0 67508.64 64585.24 641.35 o 14 2 0 15344.68 15122.54 237.33 o 16 2 0 19970.53 20582.70 310.56 o 18 2 0 6590.40 6573.76 230.74 o 20 2 0 10363.10 11079.68 289.70 o 1 3 0 835.47 785.27 26.75 o 3 3 0 1042.78 925.34 33.09 o 5 3 0 763.53 745.53 48.11 o 7 3 0 1330.93 1501.87 51.34 o 9 3 0 7098.97 7219.55 112.16 o 11 3 0 785.47 815.48 61.57 o 13 3 0 4715.21 4654.10 119.87 o 15 3 0 2511.55 2608.86 121.69 o 17 3 0 1788.88 1791.88 140.08 o 19 3 0 1257.95 962.22 277.62 o 0 4 0 505506.84 488550.81 7832.57 o 2 4 0 26240.98 25456.70 191.04 o 4 4 0 26899.34 24858.75 220.96 o 6 4 0 33607.52 31735.76 260.82 o 8 4 0 54457.80 52458.73 447.75 o 10 4 0 13842.49 13914.29 170.58 o 12 4 0 589.32 780.25 74.96 o 14 4 0 9551.93 8922.23 182.38 o 16 4 0 60.21 117.55 83.29 o 18 4 0 3465.63 3606.47 195.61 o 20 4 0 34.86 88.54 93.14 o 1 5 0 69050.64 66900.61 492.62 o 3 5 0 76942.34 75043.93 568.04 o 5 5 0 13561.26 13097.53 118.81 o 7 5 0 74943.10 72143.84 614.35 o 9 5 0 4672.75 4694.14 98.54 o 11 5 0 17427.20 17259.85 210.82 o 13 5 0 459.91 480.33 82.31 o 15 5 0 4472.90 4577.79 156.44 o 17 5 0 298.85 345.37 105.99 o 19 5 0 1723.13 1328.61 252.06 o 0 6 0 224.23 258.10 42.06 o 2 6 0 3275.02 3275.18 66.81 o 4 6 0 1597.86 1801.25 63.24 o 6 6 0 191.17 237.31 36.60 o 8 6 0 423.78 430.52 66.43 o 10 6 0 399.78 366.77 57.57 o 12 6 0 191.17 233.03 58.95 o 14 6 0 400.36 382.72 85.19 o 16 6 0 13.06 22.38 74.12 o 18 6 0 135.29 90.68 115.13 o 20 6 0 56.54 48.66 97.30 o 1 7 0 19035.73 18526.37 152.02 o 3 7 0 10867.15 10209.56 112.48 o 5 7 0 21729.32 20521.98 187.52 o 7 7 0 2157.02 2076.79 62.90 o 9 7 0 43047.20 41218.29 401.46 o 11 7 0 6694.15 6493.43 131.23 o 13 7 0 29048.99 28462.12 465.59 o 15 7 0 12475.27 12188.40 249.28 o 17 7 0 6409.61 6725.74 219.47 o 19 7 0 6430.27 7001.34 257.36 o 0 8 0 558.49 681.75 59.19 o 2 8 0 34243.33 35131.80 288.62 o 4 8 0 1013.03 945.33 46.35 o 6 8 0 8655.84 8989.47 116.55 o 8 8 0 350.41 348.74 53.25 o 10 8 0 2764.08 2692.85 92.37 o 12 8 0 4751.63 4615.03 122.00 o 14 8 0 84.23 115.58 95.48 o 16 8 0 29.08 4.11 80.68 o 18 8 0 244.55 246.65 107.02 o 1 9 0 92098.73 90993.03 797.27 o 3 9 0 53252.68 52137.36 447.99 o 5 9 0 108.84 63.83 39.79 o 7 9 0 14758.54 15073.84 180.55 o 9 9 0 2205.47 2289.49 85.29 o 11 9 0 19578.98 19651.82 259.02 o 13 9 0 3712.59 3869.44 139.48 o 15 9 0 10331.21 10580.45 232.75 o 17 9 0 1177.20 1221.86 125.43 o 0 10 0 6037.61 5716.54 178.66 o 2 10 0 7144.52 6762.12 105.87 o 4 10 0 703.62 797.23 61.59 o 6 10 0 262.94 301.87 50.98 o 8 10 0 16.63 32.16 44.49 o 10 10 0 1475.14 1621.37 84.78 o 12 10 0 4047.71 4183.23 136.30 o 14 10 0 97.26 123.29 83.93 o 16 10 0 8391.91 8365.69 251.91 o 18 10 0 341.54 333.90 120.86 o 1 11 0 9206.51 9309.52 126.90 o 3 11 0 938.14 978.86 58.87 o 5 11 0 387.41 505.74 53.71 o 7 11 0 75.70 69.59 49.77 o 9 11 0 3786.55 3970.13 110.21 o 11 11 0 2127.55 1948.42 102.08 o 13 11 0 6163.96 6144.62 165.98 o 15 11 0 2892.71 3028.22 149.75 o 17 11 0 183.65 217.06 110.28 o 0 12 0 11790.10 11477.88 234.57 o 2 12 0 52.62 86.31 48.97 o 4 12 0 4941.70 5006.62 104.07 o 6 12 0 127.24 91.75 48.94 o 8 12 0 1811.16 1663.50 94.37 o 10 12 0 77.52 40.40 54.33 o 12 12 0 579.89 490.25 80.07 o 14 12 0 2.39 70.98 73.81 o 16 12 0 555.31 542.47 129.84 o 1 13 0 673.50 726.34 66.58 o 3 13 0 623.50 588.74 63.44 o 5 13 0 4062.27 4469.92 141.00 o 7 13 0 10.57 84.69 56.37 o 9 13 0 125.88 111.81 65.81 o 11 13 0 88.59 66.51 64.60 o 13 13 0 1173.26 1287.82 106.71 o 15 13 0 13.02 28.77 87.78 o 0 14 0 9359.03 9710.27 227.53 o 2 14 0 66.03 92.78 60.44 o 4 14 0 9605.48 9368.45 171.90 o 6 14 0 750.73 651.98 75.05 o 8 14 0 101.43 152.88 71.01 o 10 14 0 1.08 115.46 85.75 o 12 14 0 160.21 319.91 96.37 o 14 14 0 1419.84 1336.44 153.51 o 1 15 0 2239.37 2479.40 104.46 o 3 15 0 4033.55 4433.18 149.17 o 5 15 0 2422.91 2575.34 115.82 o 7 15 0 2778.82 2844.61 114.51 o 9 15 0 5329.26 5540.11 229.75 o 11 15 0 2977.87 2660.43 153.32 o 13 15 0 1323.22 1165.40 139.42 o 0 16 0 213.63 271.15 98.43 o 2 16 0 1102.87 1281.66 110.51 o 4 16 0 2.55 4.22 58.98 o 6 16 0 784.45 683.83 125.01 o 8 16 0 33.46 26.60 62.66 o 10 16 0 399.53 334.96 94.63 o 12 16 0 812.20 782.21 135.84 o 1 17 0 6939.72 7475.63 215.41 o 3 17 0 8517.19 8991.02 215.24 o 5 17 0 4191.71 4334.98 156.00 o 7 17 0 4097.06 4359.00 158.68 o 9 17 0 3510.57 3456.79 182.06 o 0 18 0 1436.16 1269.81 208.16 o 2 18 0 308.62 218.73 97.35 o 4 18 0 1846.62 1357.37 190.33 o 6 18 0 316.94 135.15 83.69 o 8 18 0 0.56 63.22 82.72 o 1 19 0 4797.33 5446.54 264.42 o 3 19 0 1709.53 1286.63 250.53 o 5 19 0 654.97 408.08 130.43 o 2 1 1 4549.53 4269.49 32.47 o 3 1 1 8902.01 8956.25 49.39 o 4 1 1 1801.71 1821.61 29.87 o 5 1 1 889.04 984.61 29.72 o 6 1 1 1070.30 1223.86 30.55 o 7 1 1 2075.61 1819.61 36.62 o 8 1 1 564.98 657.69 33.63 o 9 1 1 226.93 177.96 27.99 o 10 1 1 447.60 437.69 36.89 o 11 1 1 8972.56 8565.60 99.59 o 12 1 1 3396.41 3284.08 77.62 o 13 1 1 54.43 80.58 42.29 o 14 1 1 812.03 791.49 58.34 o 15 1 1 284.88 255.88 54.38 o 16 1 1 3.67 -49.79 49.79 o 17 1 1 93.67 128.40 60.93 o 18 1 1 58.33 81.75 64.85 o 19 1 1 248.62 164.75 65.12 o 20 1 1 57.18 100.77 79.10 o 21 1 1 6.46 -29.12 85.34 o 1 2 1 2936.70 2870.38 26.42 o 2 2 1 41702.98 40340.01 172.82 o 3 2 1 70.14 80.91 14.24 o 4 2 1 7760.25 6965.09 50.26 o 5 2 1 1139.30 1151.15 27.48 o 6 2 1 24293.56 22115.49 131.10 o 7 2 1 487.35 550.22 27.68 o 8 2 1 4079.29 3769.20 53.40 o 9 2 1 231.13 235.72 30.04 o 10 2 1 20536.16 20078.07 152.43 o 11 2 1 86.78 89.77 37.93 o 12 2 1 9207.10 9073.67 112.22 o 13 2 1 49.22 130.32 42.45 o 14 2 1 4145.80 4286.57 94.29 o 15 2 1 734.81 755.39 60.84 o 16 2 1 6147.56 6587.12 132.41 o 17 2 1 4.89 -24.23 53.77 o 18 2 1 2891.25 3116.36 125.93 o 19 2 1 2.22 -44.48 65.18 o 21 2 1 0.01 33.88 75.37 o 1 3 1 7416.20 7216.33 40.06 o 2 3 1 529.43 561.86 17.74 o 3 3 1 233.38 319.27 17.40 o 4 3 1 88.51 101.79 16.23 o 5 3 1 1693.67 1498.39 32.66 o 6 3 1 3.09 26.54 19.13 o 7 3 1 3665.09 3645.66 47.67 o 8 3 1 1490.12 1583.20 40.30 o 9 3 1 20445.60 20149.11 143.74 o 10 3 1 581.89 612.69 39.19 o 11 3 1 489.44 609.52 47.70 o 12 3 1 939.76 997.42 53.67 o 13 3 1 7713.70 7901.02 126.02 o 14 3 1 3576.00 3587.95 86.51 o 15 3 1 283.06 306.16 53.23 o 16 3 1 27.62 -2.50 45.97 o 17 3 1 444.81 446.89 69.28 o 18 3 1 39.60 -12.46 66.92 o 19 3 1 260.13 111.27 67.63 o 20 3 1 108.78 86.83 69.00 o 0 4 1 155400.88 148701.28 1203.53 o 1 4 1 585.60 629.20 19.86 o 2 4 1 8940.66 8932.84 54.12 o 3 4 1 31726.38 31126.77 152.86 o 4 4 1 61819.82 58049.57 303.16 o 5 4 1 310.78 249.65 22.87 o 6 4 1 69705.84 67628.75 384.86 o 7 4 1 214.35 161.50 25.62 o 8 4 1 57346.55 53798.27 331.58 o 9 4 1 412.73 409.87 33.66 o 10 4 1 19140.32 18921.29 151.35 o 11 4 1 19.74 87.95 33.89 o 12 4 1 18124.53 18085.67 167.25 o 13 4 1 241.48 248.59 48.20 o 14 4 1 8214.11 8224.20 123.63 o 15 4 1 198.75 246.10 57.81 o 16 4 1 3268.66 3362.14 97.51 o 17 4 1 510.68 471.95 72.76 o 18 4 1 9697.14 10142.56 174.12 o 19 4 1 39.62 51.64 66.22 o 20 4 1 3698.81 3733.12 224.26 o 1 5 1 2587.11 2384.54 38.53 o 2 5 1 59589.58 60054.96 305.61 o 3 5 1 15638.38 15160.38 83.94 o 4 5 1 4623.09 4489.45 41.20 o 5 5 1 377.48 406.22 21.88 o 6 5 1 1003.55 1042.42 33.92 o 7 5 1 2720.22 2640.06 43.61 o 8 5 1 1057.57 1289.97 44.45 o 9 5 1 11.30 71.55 31.94 o 10 5 1 405.91 375.14 42.99 o 11 5 1 7043.15 7314.01 95.58 o 12 5 1 8.74 98.63 38.78 o 13 5 1 272.33 298.38 44.84 o 14 5 1 77.55 46.11 42.41 o 15 5 1 743.58 696.27 62.88 o 16 5 1 0.16 33.34 50.50 o 17 5 1 5.02 32.48 51.64 o 18 5 1 151.18 190.62 78.58 o 19 5 1 845.82 673.92 108.04 o 20 5 1 32.72 83.13 69.94 o 0 6 1 39907.64 39537.25 291.03 o 1 6 1 8667.75 8502.49 58.34 o 2 6 1 24555.30 22806.79 123.92 o 3 6 1 681.87 661.84 24.65 o 4 6 1 34839.20 34282.75 189.47 o 5 6 1 141.22 191.59 21.32 o 6 6 1 26346.28 24226.74 153.09 o 7 6 1 277.49 338.48 28.46 o 8 6 1 27174.55 26414.53 181.39 o 9 6 1 73.15 111.43 29.83 o 10 6 1 32079.25 30679.18 227.80 o 11 6 1 645.54 692.17 45.18 o 12 6 1 21440.89 21160.96 194.14 o 13 6 1 816.62 995.92 62.02 o 14 6 1 1542.94 1485.40 70.99 o 15 6 1 2045.35 2023.52 82.71 o 16 6 1 11328.85 11379.02 159.41 o 17 6 1 1.14 -58.57 58.57 o 18 6 1 4619.35 4822.25 127.13 o 19 6 1 6.93 33.14 66.51 o 20 6 1 6814.55 7156.34 174.57 o 1 7 1 69.28 33.57 18.43 o 2 7 1 92.49 142.58 21.64 o 3 7 1 4619.64 4589.03 50.25 o 4 7 1 17.02 -4.92 17.91 o 5 7 1 968.77 1059.01 32.97 o 6 7 1 399.82 522.69 29.98 o 7 7 1 416.89 453.42 30.07 o 8 7 1 2953.22 3192.72 54.31 o 9 7 1 753.33 814.30 42.93 o 10 7 1 89.56 94.02 35.16 o 11 7 1 2219.45 2188.34 65.01 o 12 7 1 333.15 364.10 45.12 o 13 7 1 28.53 -7.84 37.92 o 14 7 1 1422.71 1539.31 76.39 o 15 7 1 20.33 14.67 47.43 o 16 7 1 378.13 334.02 65.04 o 17 7 1 524.67 519.17 78.29 o 18 7 1 2.84 13.78 62.29 o 19 7 1 76.84 169.30 78.84 o 0 8 1 103306.94 101466.25 866.95 o 1 8 1 649.85 688.99 28.83 o 2 8 1 6325.69 6186.28 57.98 o 3 8 1 6185.02 6567.68 61.69 o 4 8 1 9185.72 9151.85 82.71 o 5 8 1 3555.69 3712.26 51.80 o 6 8 1 4328.90 4256.44 55.03 o 7 8 1 85.34 102.58 27.73 o 8 8 1 11234.37 10281.58 101.72 o 9 8 1 34.50 60.01 32.47 o 10 8 1 7273.74 7624.15 94.84 o 11 8 1 429.42 491.83 45.80 o 12 8 1 10102.33 9692.95 123.87 o 13 8 1 7.02 -39.50 39.50 o 14 8 1 5456.60 5766.31 125.31 o 15 8 1 116.40 184.80 58.20 o 16 8 1 223.21 210.39 65.81 o 17 8 1 553.90 604.31 79.23 o 18 8 1 3504.00 3348.29 130.49 o 19 8 1 106.13 94.58 73.16 o 1 9 1 34248.71 34061.07 210.70 o 2 9 1 3477.88 3741.93 50.57 o 3 9 1 15218.97 14714.81 110.82 o 4 9 1 4869.90 4761.85 58.75 o 5 9 1 5157.44 5103.89 64.24 o 6 9 1 838.25 874.62 38.38 o 7 9 1 9188.33 9066.46 98.65 o 8 9 1 1.24 36.99 29.32 o 9 9 1 7413.95 7395.27 93.56 o 10 9 1 499.43 551.93 47.35 o 11 9 1 6118.96 6087.80 93.27 o 12 9 1 121.14 141.93 46.89 o 13 9 1 5730.21 5711.82 105.46 o 14 9 1 6.51 30.07 47.14 o 15 9 1 4855.86 5027.92 112.83 o 16 9 1 0.32 71.39 62.92 o 17 9 1 1226.84 1180.47 97.16 o 18 9 1 0.62 26.92 63.71 o 0 10 1 72.25 54.34 45.28 o 1 10 1 2814.26 2847.83 54.83 o 2 10 1 11185.91 10983.87 98.35 o 3 10 1 1238.08 1476.09 42.15 o 4 10 1 721.51 779.63 41.84 o 5 10 1 100.42 150.96 29.86 o 6 10 1 1024.67 1143.67 44.81 o 7 10 1 201.94 283.27 36.15 o 8 10 1 105.69 72.75 32.80 o 9 10 1 16.60 10.32 31.86 o 10 10 1 3319.46 3217.53 78.34 o 11 10 1 402.58 407.17 53.35 o 12 10 1 2132.14 2118.10 75.23 o 13 10 1 615.17 512.23 59.91 o 14 10 1 0.87 -45.68 45.68 o 15 10 1 666.78 621.18 69.06 o 16 10 1 1039.09 1133.08 89.84 o 17 10 1 13.55 25.25 64.43 o 18 10 1 45.75 4.32 60.78 o 1 11 1 23694.58 23290.20 172.52 o 2 11 1 685.78 793.94 40.63 o 3 11 1 26003.89 25100.45 181.22 o 4 11 1 50.91 12.81 27.58 o 5 11 1 13695.36 14106.31 123.76 o 6 11 1 1257.00 1413.21 52.01 o 7 11 1 10262.36 10235.13 107.18 o 8 11 1 458.94 475.63 46.48 o 9 11 1 22966.64 23004.22 200.66 o 10 11 1 184.77 243.05 43.76 o 11 11 1 15009.65 15097.74 159.25 o 12 11 1 46.07 26.36 40.54 o 13 11 1 13115.18 13413.29 172.32 o 14 11 1 107.08 123.11 54.47 o 15 11 1 5121.69 5382.35 134.12 o 16 11 1 475.21 380.88 74.98 o 17 11 1 5725.38 5500.52 193.79 o 0 12 1 5061.66 5431.22 109.06 o 1 12 1 17.18 -20.71 29.72 o 2 12 1 1485.06 1711.02 53.91 o 3 12 1 1610.96 1755.75 53.47 o 4 12 1 1262.10 1481.85 52.37 o 5 12 1 1540.63 1737.31 59.09 o 6 12 1 469.08 492.62 42.46 o 7 12 1 822.06 863.99 48.64 o 8 12 1 120.40 156.25 41.92 o 9 12 1 643.26 639.84 54.13 o 10 12 1 146.12 218.65 47.28 o 11 12 1 17.50 -44.95 44.95 o 12 12 1 84.35 176.92 49.96 o 13 12 1 8.03 34.86 49.46 o 14 12 1 68.94 29.04 53.04 o 15 12 1 214.75 174.99 63.03 o 16 12 1 254.31 243.35 69.84 o 1 13 1 15145.88 15075.96 142.00 o 2 13 1 289.89 337.11 42.11 o 3 13 1 20264.34 20983.66 180.41 o 4 13 1 810.05 766.31 50.70 o 5 13 1 13254.72 13049.78 156.34 o 6 13 1 3.31 58.68 37.21 o 7 13 1 24292.91 24706.44 217.54 o 8 13 1 31.18 10.18 35.45 o 9 13 1 17452.34 17492.00 183.47 o 10 13 1 133.86 123.76 46.86 o 11 13 1 12387.02 12579.25 182.34 o 12 13 1 29.58 -46.04 51.73 o 13 13 1 4382.88 4499.72 125.35 o 14 13 1 61.77 53.15 57.78 o 15 13 1 6036.54 5991.14 145.01 o 0 14 1 343.41 357.62 60.56 o 1 14 1 33.50 -12.55 34.46 o 2 14 1 130.76 186.63 42.88 o 3 14 1 3816.79 3883.12 82.49 o 4 14 1 16.33 0.23 37.96 o 5 14 1 0.17 0.27 37.96 o 6 14 1 78.16 70.01 43.26 o 7 14 1 3.68 33.47 38.55 o 8 14 1 93.41 150.07 47.81 o 9 14 1 217.58 193.46 53.62 o 10 14 1 58.71 67.76 46.65 o 11 14 1 1.60 20.82 49.35 o 12 14 1 44.96 45.01 49.69 o 13 14 1 89.34 120.12 61.49 o 14 14 1 28.64 145.59 68.58 o 1 15 1 5736.39 6325.18 112.34 o 2 15 1 649.40 648.15 55.45 o 3 15 1 6889.36 6823.94 110.37 o 4 15 1 57.30 63.11 46.11 o 5 15 1 7820.87 8433.57 129.67 o 6 15 1 379.91 305.81 52.28 o 7 15 1 4329.08 4384.13 100.58 o 8 15 1 61.37 32.20 46.13 o 9 15 1 9203.89 9502.55 153.34 o 10 15 1 299.44 264.78 55.53 o 11 15 1 1986.11 1751.38 94.12 o 12 15 1 32.71 74.70 54.70 o 13 15 1 3838.98 4032.95 147.58 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47.64 o 8 6 10 243.35 263.42 59.74 o 9 6 10 847.94 915.74 75.71 o 10 6 10 1028.59 1177.87 78.99 o 11 6 10 110.94 103.49 67.70 o 12 6 10 1.84 36.78 66.17 o 13 6 10 12.81 37.11 22.09 o 14 6 10 27.33 71.33 71.84 o 15 6 10 660.48 257.48 102.52 o 16 6 10 37.41 97.69 88.13 o 17 6 10 0.08 22.44 75.36 o 1 7 10 33942.97 33864.20 199.65 o 2 7 10 4275.10 4540.22 49.85 o 3 7 10 16623.41 16615.98 175.29 o 4 7 10 959.49 928.69 62.17 o 5 7 10 7766.67 7724.95 124.93 o 6 7 10 10158.09 10226.54 153.01 o 7 7 10 15723.70 15857.42 197.68 o 8 7 10 1848.90 1916.95 88.57 o 9 7 10 11298.70 11180.46 168.15 o 10 7 10 8207.50 8237.27 177.55 o 11 7 10 8972.92 9430.23 173.83 o 12 7 10 3081.52 3498.93 132.93 o 13 7 10 7017.20 7291.91 180.34 o 14 7 10 1809.85 1114.96 299.20 o 15 7 10 4006.71 4115.91 205.87 o 16 7 10 216.84 162.09 93.18 o 17 7 10 1802.21 842.17 268.26 o 0 8 10 569.25 543.98 40.22 o 1 8 10 90.53 46.97 24.56 o 2 8 10 1687.72 1901.19 65.07 o 3 8 10 107.36 126.67 41.28 o 4 8 10 454.25 383.90 49.75 o 5 8 10 0.15 58.51 45.74 o 6 8 10 1069.20 1270.84 70.56 o 7 8 10 762.02 781.76 66.91 o 8 8 10 2554.71 2781.87 96.88 o 9 8 10 3.86 -31.72 63.21 o 10 8 10 1591.81 1541.51 104.29 o 11 8 10 71.86 78.69 69.75 o 12 8 10 111.26 109.58 70.38 o 13 8 10 66.23 -9.53 68.21 o 14 8 10 435.58 326.28 103.27 o 15 8 10 101.79 88.71 82.21 o 16 8 10 887.40 624.64 139.87 o 1 9 10 6448.83 6520.00 65.32 o 2 9 10 711.02 675.13 48.38 o 3 9 10 10463.80 10652.40 139.51 o 4 9 10 259.36 228.44 50.86 o 5 9 10 10206.67 10605.10 154.98 o 6 9 10 2292.54 2621.67 96.55 o 7 9 10 1825.78 1757.41 85.19 o 8 9 10 295.97 283.17 82.25 o 9 9 10 12248.48 12816.64 210.39 o 10 9 10 832.86 889.18 88.84 o 11 9 10 5775.22 6056.24 185.59 o 12 9 10 694.71 710.07 122.49 o 13 9 10 6380.41 6892.55 191.23 o 14 9 10 346.37 240.11 103.46 o 15 9 10 1057.40 726.89 162.34 o 16 9 10 108.03 57.24 92.67 o 0 10 10 3865.59 4047.42 77.46 o 1 10 10 276.05 296.98 34.34 o 2 10 10 2468.25 2622.94 75.61 o 3 10 10 57.14 111.60 47.49 o 4 10 10 821.33 902.36 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2694.82 2620.80 69.01 o 12 3 11 517.46 507.55 45.57 o 13 3 11 54.53 55.92 41.21 o 14 3 11 1253.49 1127.47 81.81 o 15 3 11 1590.16 1494.97 76.36 o 16 3 11 135.53 222.52 72.02 o 17 3 11 87.77 168.08 89.90 o 0 4 11 25003.86 24423.01 277.40 o 1 4 11 814.06 877.80 33.00 o 2 4 11 32043.04 31155.91 196.69 o 3 4 11 10.33 9.55 20.82 o 4 4 11 3628.48 3502.56 58.49 o 5 4 11 2173.93 2146.37 47.99 o 6 4 11 17878.30 17695.21 146.98 o 7 4 11 202.14 172.66 30.95 o 8 4 11 10800.06 10517.16 108.40 o 9 4 11 0.15 23.21 28.52 o 10 4 11 14787.36 13841.83 226.49 o 11 4 11 14.08 6.40 34.09 o 12 4 11 18184.28 16887.56 277.11 o 13 4 11 205.79 251.69 40.55 o 14 4 11 4339.34 4452.54 121.11 o 15 4 11 39.29 78.17 69.07 o 16 4 11 5413.29 5703.92 172.87 o 17 4 11 53.59 71.87 81.25 o 1 5 11 263.10 247.72 26.62 o 2 5 11 1630.08 1695.00 43.17 o 3 5 11 439.43 448.33 29.64 o 4 5 11 1647.92 1790.43 52.28 o 5 5 11 2767.05 2942.85 75.72 o 6 5 11 392.64 420.00 54.57 o 7 5 11 1259.55 1254.41 69.95 o 8 5 11 1070.53 1090.28 69.76 o 9 5 11 4523.61 4620.54 111.02 o 10 5 11 168.80 196.04 62.50 o 11 5 11 432.60 560.99 77.92 o 12 5 11 76.84 51.31 23.64 o 13 5 11 1911.93 1861.36 85.06 o 14 5 11 309.09 322.28 83.03 o 15 5 11 2.69 -6.11 69.36 o 16 5 11 797.90 708.56 118.11 o 17 5 11 775.11 782.28 118.85 o 0 6 11 26122.12 25928.27 232.42 o 1 6 11 25.66 34.34 23.77 o 2 6 11 11477.15 11537.47 81.63 o 3 6 11 1006.02 1013.13 45.06 o 4 6 11 16960.01 16998.62 176.97 o 5 6 11 2078.25 2024.21 76.09 o 6 6 11 12634.80 12606.30 155.76 o 7 6 11 630.70 732.06 65.48 o 8 6 11 8817.38 9210.82 149.61 o 9 6 11 0.88 -37.35 54.60 o 10 6 11 16896.25 17040.47 227.29 o 11 6 11 691.54 743.21 81.34 o 12 6 11 7362.28 7916.77 164.59 o 13 6 11 3.16 23.10 62.89 o 14 6 11 3680.49 3987.59 158.95 o 15 6 11 0.30 15.15 74.18 o 16 6 11 1914.88 1429.58 271.10 o 17 6 11 292.72 716.37 337.21 o 1 7 11 32.33 44.78 22.16 o 2 7 11 270.13 251.43 34.90 o 3 7 11 2.21 20.13 40.05 o 4 7 11 91.57 100.22 41.75 o 5 7 11 2468.16 2552.59 83.81 o 6 7 11 1685.54 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63.20 o 7 9 11 9947.49 10034.13 177.91 o 8 9 11 696.80 772.08 78.21 o 9 9 11 5803.88 6055.90 152.28 o 10 9 11 985.30 920.48 95.93 o 11 9 11 1899.70 1821.94 253.17 o 12 9 11 339.12 315.67 92.93 o 13 9 11 2796.33 3178.60 158.42 o 14 9 11 2.64 54.90 89.12 o 15 9 11 2837.62 1682.88 498.35 o 0 10 11 2012.58 2016.94 57.66 o 1 10 11 645.06 636.86 27.18 o 2 10 11 985.29 1074.89 66.98 o 3 10 11 3254.61 3322.95 94.59 o 4 10 11 1122.65 1174.00 74.66 o 5 10 11 1486.36 1462.49 77.31 o 6 10 11 841.86 704.89 78.08 o 7 10 11 616.70 503.46 77.35 o 8 10 11 33.00 22.75 54.48 o 9 10 11 733.25 680.25 83.60 o 10 10 11 1220.00 990.88 115.24 o 11 10 11 253.53 172.12 87.59 o 12 10 11 19.75 63.09 76.40 o 13 10 11 0.95 46.07 105.06 o 14 10 11 191.82 125.08 96.86 o 1 11 11 16279.53 15767.77 211.22 o 2 11 11 717.44 718.19 60.53 o 3 11 11 13276.30 14137.57 187.62 o 4 11 11 30.00 74.27 54.99 o 5 11 11 6367.32 6764.63 139.42 o 6 11 11 27.11 35.16 57.09 o 7 11 11 9784.26 10062.82 208.05 o 8 11 11 362.44 353.92 79.79 o 9 11 11 6389.29 6382.08 166.55 o 10 11 11 422.76 219.62 109.99 o 11 11 11 7472.77 8008.77 202.60 o 12 11 11 633.10 411.60 96.06 o 13 11 11 4012.26 4415.44 206.14 o 0 12 11 721.23 625.84 71.15 o 1 12 11 1508.70 1372.30 84.74 o 2 12 11 0.69 24.66 45.80 o 3 12 11 165.85 189.22 56.93 o 4 12 11 553.64 543.75 77.99 o 5 12 11 25.74 119.70 62.78 o 6 12 11 168.70 165.92 62.64 o 7 12 11 1465.18 1333.72 110.64 o 8 12 11 369.67 315.08 78.57 o 9 12 11 2.73 -38.38 77.27 o 10 12 11 116.60 73.07 79.29 o 11 12 11 1.65 6.78 67.73 o 12 12 11 228.45 61.52 108.46 o 1 13 11 13225.45 13161.49 171.21 o 2 13 11 34.56 28.76 49.49 o 3 13 11 7280.96 7673.46 148.30 o 4 13 11 58.43 86.02 60.99 o 5 13 11 6880.50 7556.71 160.33 o 6 13 11 51.30 98.89 64.79 o 7 13 11 4432.48 4604.13 147.49 o 8 13 11 20.62 -61.30 71.62 o 9 13 11 13355.51 14182.80 275.93 o 10 13 11 330.36 233.43 89.96 o 11 13 11 3312.43 3874.89 353.89 o 0 14 11 6.06 -19.93 82.72 o 1 14 11 46.45 44.70 56.36 o 2 14 11 107.45 126.69 59.14 o 3 14 11 63.62 37.72 61.71 o 4 14 11 17.34 75.15 58.69 o 5 14 11 153.97 115.05 66.88 o 6 14 11 141.04 28.44 70.97 o 7 14 11 2.12 31.27 69.00 o 8 14 11 22.18 8.87 70.93 o 9 14 11 5.47 -46.54 79.66 o 10 14 11 22.13 31.46 89.56 o 1 15 11 4736.59 5003.45 245.58 o 2 15 11 195.00 159.19 79.23 o 3 15 11 5477.49 5646.11 153.02 o 4 15 11 40.24 56.17 67.06 o 5 15 11 1345.51 1185.89 144.68 o 6 15 11 87.99 94.77 88.20 o 7 15 11 5109.65 5911.23 169.71 o 8 15 11 272.14 384.07 97.48 o 0 16 11 305.51 145.70 159.16 o 1 16 11 107.62 160.91 116.69 o 2 16 11 622.87 333.85 125.94 o 3 16 11 108.65 97.01 90.45 o 4 16 11 280.80 299.32 81.96 o 5 16 11 95.65 156.36 89.24 o 6 16 11 227.28 164.67 91.27 o 1 17 11 776.14 881.98 394.62 o 0 0 12 57832.86 56366.73 915.34 o 1 0 12 3496.58 3740.33 78.27 o 2 0 12 54313.77 54741.17 487.04 o 3 0 12 2680.68 2578.52 72.31 o 4 0 12 2068.52 2455.39 69.42 o 5 0 12 9903.93 9942.90 133.80 o 6 0 12 44953.22 45516.54 438.38 o 7 0 12 67.38 46.67 42.35 o 8 0 12 24608.49 24284.77 278.89 o 9 0 12 2569.94 2764.03 84.82 o 10 0 12 12797.82 12482.73 197.09 o 11 0 12 780.89 765.81 81.34 o 12 0 12 21872.13 22916.78 322.02 o 13 0 12 744.52 702.71 94.52 o 14 0 12 14881.85 15604.11 271.04 o 15 0 12 238.61 369.10 104.43 o 16 0 12 14990.95 15759.93 310.62 o 17 0 12 452.64 543.86 112.53 o 1 1 12 38.76 100.84 28.86 o 2 1 12 1590.91 1817.77 45.88 o 3 1 12 25.70 83.66 27.22 o 4 1 12 8197.38 8216.70 81.27 o 5 1 12 278.89 253.05 34.85 o 6 1 12 128.39 192.76 31.23 o 7 1 12 15.29 49.48 28.08 o 8 1 12 832.37 863.60 43.82 o 9 1 12 125.49 73.28 32.15 o 10 1 12 5006.76 4872.60 80.88 o 11 1 12 77.80 83.55 40.65 o 12 1 12 1001.66 943.11 56.82 o 13 1 12 70.70 142.17 47.60 o 14 1 12 6.86 39.10 46.31 o 15 1 12 2.90 9.64 47.94 o 16 1 12 1.34 -20.42 56.00 o 17 1 12 87.93 -16.87 56.26 o 0 2 12 31019.56 30108.29 290.24 o 1 2 12 1848.43 2116.15 46.70 o 2 2 12 25120.27 24953.34 184.07 o 3 2 12 1257.04 1363.15 48.26 o 4 2 12 30280.01 29809.16 208.01 o 5 2 12 10041.51 10083.47 100.05 o 6 2 12 17894.55 17352.26 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