#------------------------------------------------------------------------------
#$Date: 2012-09-11 12:26:43 +0300 (Tue, 11 Sep 2012) $
#$Revision: 66590 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/49/2234932.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2234932_Fobs
loop_
_publ_author_name
'Najafi, Ezzatollah'
'Amini, Mostafa M.'
'Ng, Seik Weng'
_publ_section_title
;
4-(Dimethylamino)pyridinium
tetrachlorido(pyridine-2-carboxylato-\k^2^N,O)stannate(IV)
;
_journal_coeditor_code BT5909
_journal_issue 6
_journal_name_full 'Acta Crystallographica Section E'
_journal_page_first m744
_journal_volume 68
_journal_year 2012
_space_group_IT_number 2
_symmetry_space_group_name_Hall '-P 1'
_symmetry_space_group_name_H-M 'P -1'
_cell_angle_alpha 69.485
_cell_angle_beta 83.159
_cell_angle_gamma 67.900
_cell_length_a 7.6658
_cell_length_b 9.8948
_cell_length_c 13.5722
_exptl_crystal_F_000 496.00
_reflns_d_resolution_high 0.7680
_[local]_cod_data_source_file bt5909Isup2.hkl
_[local]_cod_data_source_block I
#BEGIN Tags that were not found in dictionaries:
_shelx_title ' P-1'
_shelx_refln_list_code 4
_shelx_f_calc_maximum 302.84
_shelx_f_squared_multiplier 1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
1 0 0 18577.14 18234.60 82.84 o
2 0 0 135.30 114.25 3.76 o
3 0 0 4964.35 4991.75 37.04 o
4 0 0 264.79 236.79 6.90 o
5 0 0 27.61 26.66 3.72 o
6 0 0 269.52 252.78 10.75 o
7 0 0 237.62 239.86 20.40 o
8 0 0 328.70 367.55 26.90 o
9 0 0 22.74 19.55 20.37 o
-8 1 0 332.86 366.65 38.93 o
-7 1 0 739.63 758.78 35.31 o
-6 1 0 3652.45 3774.71 72.18 o
-5 1 0 420.77 439.79 17.38 o
-4 1 0 558.28 570.55 9.28 o
-3 1 0 8698.18 8406.51 122.15 o
-2 1 0 1733.20 1716.49 19.44 o
-1 1 0 10898.17 10574.50 75.60 o
0 1 0 6738.27 7095.65 41.74 o
1 1 0 3949.03 4142.49 59.03 o
2 1 0 7652.46 7623.26 61.42 o
3 1 0 1927.02 1878.86 17.50 o
4 1 0 1570.39 1575.11 17.78 o
5 1 0 613.76 620.75 11.46 o
6 1 0 23.85 20.67 3.77 o
7 1 0 484.70 490.70 22.44 o
8 1 0 95.08 81.31 12.96 o
9 1 0 57.39 44.60 17.07 o
-8 2 0 1091.47 1167.24 71.05 o
-7 2 0 2318.26 2482.24 94.69 o
-6 2 0 3779.82 3819.88 71.48 o
-5 2 0 350.17 330.92 10.75 o
-4 2 0 31.06 27.10 3.43 o
-3 2 0 825.72 802.55 15.05 o
-2 2 0 4174.64 4119.19 30.67 o
-1 2 0 303.28 285.15 7.35 o
0 2 0 3444.28 3548.59 22.01 o
1 2 0 9956.59 10668.63 99.11 o
2 2 0 1060.62 1068.33 18.05 o
3 2 0 363.20 371.03 10.27 o
4 2 0 33.21 31.51 3.29 o
5 2 0 1420.13 1429.46 19.63 o
6 2 0 75.92 88.87 5.80 o
7 2 0 202.88 207.87 14.18 o
8 2 0 1000.14 1008.89 54.55 o
9 2 0 92.22 94.22 18.82 o
-8 3 0 1279.34 1248.62 76.35 o
-7 3 0 568.97 598.92 37.95 o
-6 3 0 3035.20 3159.78 59.49 o
-5 3 0 5455.53 5434.35 72.40 o
-4 3 0 479.20 490.17 16.30 o
-3 3 0 592.81 538.91 17.31 o
-2 3 0 1087.57 1029.99 15.33 o
-1 3 0 819.90 830.38 14.02 o
0 3 0 564.52 595.59 11.94 o
1 3 0 0.16 6.05 2.53 o
2 3 0 224.44 227.28 8.66 o
3 3 0 27.77 34.22 3.87 o
4 3 0 1132.18 1111.30 21.11 o
5 3 0 2212.83 2172.31 42.96 o
6 3 0 55.56 55.09 5.92 o
7 3 0 357.81 359.42 14.55 o
8 3 0 1424.55 1415.79 65.85 o
9 3 0 215.00 249.28 30.21 o
-7 4 0 351.46 370.96 37.65 o
-6 4 0 1867.71 1845.54 77.66 o
-5 4 0 3630.03 3676.12 54.53 o
-4 4 0 812.62 762.75 21.01 o
-3 4 0 56.26 58.04 4.37 o
-2 4 0 1000.87 1026.41 17.48 o
-1 4 0 3.52 2.53 2.40 o
0 4 0 385.95 470.48 13.38 o
1 4 0 126.79 99.87 6.97 o
2 4 0 2563.82 2415.30 55.69 o
3 4 0 781.52 761.25 19.27 o
4 4 0 4106.33 3978.95 88.50 o
5 4 0 9047.20 8908.20 136.16 o
6 4 0 1839.68 1755.88 31.85 o
7 4 0 2.52 6.34 3.15 o
8 4 0 722.59 746.69 28.37 o
9 4 0 622.51 638.76 68.74 o
-6 5 0 28.22 28.99 11.07 o
-5 5 0 197.62 193.67 13.77 o
-4 5 0 4.40 8.16 4.69 o
-3 5 0 27.16 30.67 4.26 o
-2 5 0 128.56 124.37 7.23 o
-1 5 0 2196.66 2235.72 39.88 o
0 5 0 84.15 94.98 7.13 o
1 5 0 245.47 229.39 7.81 o
2 5 0 12015.50 12749.80 113.06 o
3 5 0 6095.34 6428.99 97.40 o
4 5 0 4334.21 4276.85 56.39 o
5 5 0 12567.49 12316.69 286.52 o
6 5 0 4189.53 4170.55 61.44 o
7 5 0 423.77 420.62 20.99 o
8 5 0 705.80 736.64 30.59 o
9 5 0 335.75 396.20 40.09 o
-6 6 0 76.69 106.00 20.75 o
-5 6 0 24.50 8.46 17.70 o
-4 6 0 1160.57 1165.03 53.07 o
-3 6 0 484.88 451.73 21.06 o
-2 6 0 861.54 864.73 27.32 o
-1 6 0 3261.19 3187.99 90.78 o
0 6 0 316.14 321.54 17.09 o
1 6 0 23.88 13.85 6.30 o
2 6 0 2614.52 2668.72 49.45 o
3 6 0 7317.87 7566.61 84.24 o
4 6 0 5583.89 5734.42 87.91 o
5 6 0 3529.09 3443.06 69.36 o
6 6 0 4220.93 4039.22 81.90 o
7 6 0 2040.27 2196.58 60.14 o
8 6 0 356.58 377.89 25.77 o
9 6 0 4.57 -5.73 10.60 o
-5 7 0 402.36 439.50 42.76 o
-4 7 0 2019.12 2079.68 85.20 o
-3 7 0 2028.18 2075.17 75.61 o
-2 7 0 651.55 607.49 28.75 o
-1 7 0 1706.54 1650.50 47.57 o
0 7 0 2391.71 2380.34 40.08 o
1 7 0 126.46 149.40 12.65 o
2 7 0 445.01 492.24 32.88 o
3 7 0 4102.01 4271.04 78.84 o
4 7 0 1025.75 1061.05 39.46 o
5 7 0 1078.15 1135.10 53.00 o
6 7 0 946.92 948.47 34.06 o
7 7 0 36.19 27.96 10.18 o
8 7 0 369.28 336.77 30.91 o
9 7 0 2.83 -2.20 11.18 o
-4 8 0 1786.03 1899.45 126.93 o
-3 8 0 4357.75 4505.98 135.96 o
-2 8 0 1685.38 1767.31 73.07 o
-1 8 0 2184.65 2052.59 90.01 o
0 8 0 3930.87 3852.38 108.56 o
1 8 0 145.18 153.52 20.88 o
2 8 0 74.95 94.47 20.54 o
3 8 0 166.79 145.95 19.65 o
4 8 0 23.96 20.38 12.37 o
5 8 0 841.40 845.74 38.10 o
6 8 0 725.89 782.77 53.11 o
7 8 0 209.69 196.68 25.33 o
8 8 0 19.38 8.79 7.18 o
9 8 0 194.18 184.21 40.19 o
-3 9 0 3012.08 2950.40 103.20 o
-2 9 0 1899.63 1871.51 80.83 o
-1 9 0 1433.97 1503.84 71.46 o
0 9 0 1733.67 1787.96 76.17 o
1 9 0 1234.16 1159.64 60.24 o
2 9 0 669.96 665.48 44.71 o
3 9 0 136.20 89.70 33.29 o
4 9 0 2.13 4.10 10.69 o
5 9 0 59.66 39.51 11.18 o
6 9 0 4.96 7.39 6.88 o
7 9 0 1796.41 1750.73 69.14 o
8 9 0 823.48 818.00 72.20 o
-2 10 0 1213.33 1166.41 86.76 o
-1 10 0 1153.23 1107.96 65.78 o
0 10 0 435.95 380.70 38.29 o
1 10 0 43.95 14.16 12.03 o
2 10 0 1.11 3.15 6.63 o
3 10 0 0.05 10.36 10.16 o
4 10 0 630.53 631.98 56.29 o
5 10 0 147.30 152.57 22.73 o
6 10 0 10.69 2.49 17.82 o
7 10 0 1203.72 1172.62 125.23 o
8 10 0 2225.33 1987.78 119.64 o
0 11 0 22.77 25.13 12.18 o
1 11 0 306.08 307.12 36.08 o
2 11 0 271.24 317.46 52.08 o
3 11 0 7.25 13.43 10.72 o
4 11 0 326.38 313.90 35.00 o
5 11 0 928.46 849.98 56.25 o
6 11 0 34.22 26.23 12.15 o
7 11 0 686.76 740.49 76.90 o
3 12 0 184.41 210.42 41.75 o
4 12 0 200.65 170.15 27.76 o
-6 -11 1 14.36 19.66 10.03 o
-5 -11 1 565.76 536.67 46.00 o
-4 -11 1 989.64 995.66 62.63 o
-3 -11 1 688.53 574.60 63.91 o
-2 -11 1 1168.12 1197.37 96.14 o
-1 -11 1 483.97 487.33 46.30 o
0 -11 1 10.75 2.06 9.02 o
-7 -10 1 73.65 75.75 16.50 o
-6 -10 1 470.84 428.09 52.09 o
-5 -10 1 582.67 609.81 45.85 o
-4 -10 1 1709.74 1706.67 76.77 o
-3 -10 1 2622.32 2728.97 98.42 o
-2 -10 1 3275.19 3319.91 111.57 o
-1 -10 1 3348.89 3388.26 113.34 o
0 -10 1 286.64 322.28 35.96 o
1 -10 1 264.69 268.08 33.51 o
-8 -9 1 50.22 14.36 13.23 o
-7 -9 1 363.16 313.50 33.49 o
-6 -9 1 199.34 177.08 20.04 o
-5 -9 1 1212.60 1164.47 49.63 o
-4 -9 1 4356.26 4410.52 95.25 o
-3 -9 1 2562.54 2640.98 90.13 o
-2 -9 1 2718.76 2775.00 93.79 o
-1 -9 1 4708.17 4790.05 125.16 o
0 -9 1 2159.67 2029.31 83.24 o
1 -9 1 21.56 21.75 16.45 o
2 -9 1 63.50 70.86 16.68 o
3 -9 1 70.24 76.45 18.05 o
-9 -8 1 815.73 831.79 83.31 o
-8 -8 1 752.83 762.45 49.96 o
-7 -8 1 359.47 391.62 35.69 o
-6 -8 1 497.85 510.05 39.55 o
-5 -8 1 397.61 368.90 33.18 o
-4 -8 1 1286.64 1323.06 49.16 o
-3 -8 1 2237.14 2360.95 64.91 o
-2 -8 1 396.40 411.88 33.66 o
-1 -8 1 2635.57 2749.02 96.84 o
0 -8 1 1668.25 1676.14 45.26 o
1 -8 1 30.76 38.51 12.30 o
2 -8 1 75.40 63.03 15.12 o
3 -8 1 92.26 72.27 17.62 o
4 -8 1 15.46 -5.55 14.17 o
-9 -7 1 1606.63 1614.74 66.51 o
-8 -7 1 599.14 599.76 41.84 o
-7 -7 1 3117.16 3098.51 133.17 o
-6 -7 1 1013.15 977.78 51.15 o
-5 -7 1 2002.82 2041.37 72.47 o
-4 -7 1 1006.92 987.03 71.24 o
-3 -7 1 4905.14 5178.87 89.53 o
-2 -7 1 568.74 619.89 31.10 o
-1 -7 1 465.76 436.46 30.93 o
0 -7 1 289.23 266.27 15.19 o
1 -7 1 20.38 28.72 5.53 o
2 -7 1 182.44 180.82 16.05 o
3 -7 1 249.59 251.81 27.29 o
4 -7 1 108.21 110.13 19.00 o
5 -7 1 26.22 32.85 13.33 o
-9 -6 1 2499.68 2492.06 79.40 o
-8 -6 1 706.32 670.49 34.81 o
-7 -6 1 1832.76 1884.23 67.36 o
-6 -6 1 1225.55 1232.39 39.85 o
-5 -6 1 799.63 800.82 42.55 o
-4 -6 1 825.32 847.25 42.79 o
-3 -6 1 556.82 574.20 34.86 o
-2 -6 1 1.51 -0.17 2.83 o
-1 -6 1 797.46 812.54 22.24 o
0 -6 1 1326.22 1422.16 35.99 o
1 -6 1 894.94 865.75 27.96 o
2 -6 1 238.97 235.08 12.94 o
3 -6 1 532.65 562.33 28.77 o
4 -6 1 820.40 861.11 35.92 o
5 -6 1 5.95 -1.52 7.55 o
6 -6 1 3.05 4.78 13.06 o
-9 -5 1 2118.94 2224.07 72.56 o
-8 -5 1 546.74 537.65 26.52 o
-7 -5 1 8.58 10.57 7.24 o
-6 -5 1 906.18 901.58 33.48 o
-5 -5 1 100.28 93.56 10.45 o
-4 -5 1 216.21 245.93 17.83 o
-3 -5 1 35.20 37.65 9.22 o
-2 -5 1 231.23 270.05 17.51 o
-1 -5 1 1273.47 1286.96 21.28 o
0 -5 1 1325.88 1187.84 24.44 o
1 -5 1 7050.80 6798.89 139.93 o
2 -5 1 6311.03 6269.73 56.37 o
3 -5 1 2281.86 2277.81 39.72 o
4 -5 1 4221.51 4424.66 75.79 o
5 -5 1 753.43 794.34 29.62 o
6 -5 1 43.72 40.59 13.25 o
-9 -4 1 459.02 445.81 31.80 o
-8 -4 1 131.04 121.99 16.25 o
-7 -4 1 87.10 85.18 9.09 o
-6 -4 1 122.59 130.70 12.44 o
-5 -4 1 403.77 421.18 16.88 o
-4 -4 1 710.00 730.33 21.96 o
-3 -4 1 449.37 505.05 22.00 o
-2 -4 1 3372.87 3514.95 69.50 o
-1 -4 1 2027.56 2117.66 37.44 o
0 -4 1 2487.89 2641.25 36.10 o
1 -4 1 16982.68 16993.16 176.15 o
2 -4 1 8213.31 8112.27 68.71 o
3 -4 1 2297.35 2166.84 46.40 o
4 -4 1 3208.69 3140.91 53.64 o
5 -4 1 2802.56 2829.33 52.38 o
6 -4 1 118.12 117.03 20.19 o
7 -4 1 1.27 -0.67 24.80 o
-9 -3 1 18.09 8.21 14.04 o
-8 -3 1 5.07 -1.72 5.29 o
-7 -3 1 1788.40 1898.86 36.10 o
-6 -3 1 1446.28 1428.58 28.24 o
-5 -3 1 1523.82 1466.94 32.56 o
-4 -3 1 1414.77 1370.29 25.73 o
-3 -3 1 324.33 329.87 12.81 o
-2 -3 1 3541.43 3474.81 43.17 o
-1 -3 1 358.76 319.03 16.07 o
0 -3 1 3.57 11.11 2.17 o
1 -3 1 5923.05 5807.41 63.83 o
2 -3 1 19077.45 18370.21 134.82 o
3 -3 1 3168.92 3175.63 35.34 o
4 -3 1 1264.06 1260.03 25.33 o
5 -3 1 1564.21 1571.82 28.91 o
6 -3 1 0.75 9.41 3.88 o
7 -3 1 3.10 -0.87 8.13 o
-9 -2 1 14.48 13.38 8.89 o
-8 -2 1 366.91 384.81 25.47 o
-7 -2 1 886.48 904.61 36.45 o
-6 -2 1 1128.15 1145.49 23.12 o
-5 -2 1 10166.38 10298.68 112.92 o
-4 -2 1 13285.04 13101.48 157.81 o
-3 -2 1 1369.39 1305.72 19.75 o
-2 -2 1 1208.93 1243.74 17.80 o
-1 -2 1 6716.08 7045.63 71.69 o
0 -2 1 941.25 1081.54 20.39 o
1 -2 1 290.92 269.61 7.27 o
2 -2 1 6399.42 6420.89 52.00 o
3 -2 1 1589.45 1563.60 27.11 o
4 -2 1 487.55 488.32 14.31 o
5 -2 1 363.72 356.68 11.67 o
6 -2 1 28.88 29.04 4.84 o
7 -2 1 2.31 3.39 6.13 o
8 -2 1 12.55 8.16 12.54 o
-9 -1 1 71.73 50.53 17.93 o
-8 -1 1 928.17 984.97 54.05 o
-7 -1 1 2643.85 2697.59 53.21 o
-6 -1 1 2301.79 2290.89 36.17 o
-5 -1 1 8068.29 7924.52 115.44 o
-4 -1 1 17995.21 17682.37 119.10 o
-3 -1 1 3466.85 3395.89 29.57 o
-2 -1 1 75.15 71.01 3.61 o
-1 -1 1 3501.29 3551.47 50.14 o
0 -1 1 11455.32 11619.59 66.86 o
1 -1 1 2768.54 2795.67 31.37 o
2 -1 1 784.53 802.09 17.65 o
3 -1 1 62.30 63.17 4.30 o
4 -1 1 78.63 72.73 5.19 o
5 -1 1 47.34 42.66 4.14 o
6 -1 1 1219.29 1188.64 32.65 o
7 -1 1 42.00 51.32 10.10 o
8 -1 1 20.81 16.72 11.04 o
-9 0 1 16.30 4.18 8.46 o
-8 0 1 133.49 112.31 21.61 o
-7 0 1 2163.79 2160.05 44.58 o
-6 0 1 1861.94 1931.03 33.78 o
-5 0 1 2322.88 2347.86 31.97 o
-4 0 1 10961.41 10826.94 122.63 o
-3 0 1 9965.97 9788.74 101.36 o
-2 0 1 438.98 441.53 10.88 o
-1 0 1 4082.81 4204.69 28.49 o
1 0 1 32.83 34.21 2.18 o
2 0 1 2.88 4.30 0.97 o
3 0 1 1973.14 2017.47 22.97 o
4 0 1 1183.68 1159.66 21.26 o
5 0 1 1322.53 1296.41 19.75 o
6 0 1 3988.84 3996.99 54.45 o
7 0 1 3277.75 3409.55 76.57 o
8 0 1 270.26 283.96 24.05 o
9 0 1 282.12 309.86 47.64 o
-8 1 1 47.03 50.72 15.50 o
-7 1 1 1603.06 1636.67 72.39 o
-6 1 1 1324.79 1324.93 30.03 o
-5 1 1 12.28 12.06 3.33 o
-4 1 1 1496.57 1500.58 22.27 o
-3 1 1 779.95 758.65 14.65 o
-2 1 1 34.38 45.37 2.64 o
-1 1 1 48.60 42.39 2.51 o
0 1 1 139.72 161.97 7.56 o
1 1 1 4093.17 4147.68 54.26 o
2 1 1 4265.47 4191.06 38.80 o
3 1 1 1686.83 1666.22 17.52 o
4 1 1 2835.09 2769.66 37.02 o
5 1 1 633.89 623.37 13.09 o
6 1 1 5095.35 4878.93 102.59 o
7 1 1 7801.79 7716.16 111.15 o
8 1 1 1167.73 1228.21 50.49 o
9 1 1 467.88 454.00 45.09 o
-8 2 1 3.80 8.66 9.35 o
-7 2 1 89.76 85.48 19.20 o
-6 2 1 539.82 582.72 27.06 o
-5 2 1 30.21 34.59 3.91 o
-4 2 1 59.64 58.01 3.36 o
-3 2 1 281.41 277.22 7.03 o
-2 2 1 1329.56 1284.46 15.59 o
-1 2 1 773.10 746.66 9.61 o
0 2 1 5904.22 6111.72 51.72 o
1 2 1 5184.72 5359.81 56.25 o
2 2 1 3607.52 3870.69 54.28 o
3 2 1 235.74 227.54 8.10 o
4 2 1 6924.86 6937.12 80.06 o
5 2 1 2078.14 2060.60 40.91 o
6 2 1 3323.89 3324.22 56.23 o
7 2 1 6204.69 5985.94 113.00 o
8 2 1 1460.95 1371.86 79.37 o
9 2 1 331.49 384.05 36.40 o
-8 3 1 40.02 18.11 33.53 o
-7 3 1 3.36 2.97 9.44 o
-6 3 1 20.28 18.84 5.85 o
-5 3 1 12.41 12.10 2.65 o
-4 3 1 236.93 212.10 7.06 o
-3 3 1 1296.51 1286.50 16.75 o
-2 3 1 6213.34 6101.00 61.59 o
-1 3 1 3795.64 3739.41 40.66 o
0 3 1 11527.43 11644.55 73.41 o
1 3 1 18402.20 18779.57 229.67 o
2 3 1 634.14 572.14 18.85 o
3 3 1 695.78 762.36 19.80 o
4 3 1 3047.52 3005.82 36.29 o
5 3 1 2052.48 2100.82 29.11 o
6 3 1 522.49 504.46 16.38 o
7 3 1 983.67 987.39 30.22 o
8 3 1 1204.78 1203.35 61.00 o
9 3 1 930.96 881.72 59.79 o
-7 4 1 16.45 7.60 10.35 o
-6 4 1 92.73 82.12 16.91 o
-5 4 1 124.23 130.49 10.26 o
-4 4 1 186.15 179.43 6.93 o
-3 4 1 1455.29 1420.34 25.69 o
-2 4 1 10205.91 9996.79 87.06 o
-1 4 1 7773.36 7512.75 65.01 o
0 4 1 4255.94 4115.80 46.00 o
1 4 1 25191.52 24986.11 478.50 o
2 4 1 7986.91 8336.80 77.59 o
3 4 1 963.97 980.91 29.13 o
4 4 1 1368.33 1384.08 29.32 o
5 4 1 1076.62 1013.44 24.73 o
6 4 1 769.44 766.48 18.82 o
7 4 1 677.06 630.77 22.15 o
8 4 1 94.33 95.62 12.29 o
9 4 1 0.03 -7.41 8.10 o
-7 5 1 453.48 486.71 45.52 o
-6 5 1 1.54 -1.43 12.41 o
-5 5 1 1153.21 1165.43 39.34 o
-4 5 1 550.33 515.79 19.05 o
-3 5 1 104.36 105.04 9.60 o
-2 5 1 7405.15 7290.49 59.55 o
-1 5 1 11547.07 11326.45 106.99 o
0 5 1 9278.68 9617.84 74.86 o
1 5 1 5864.54 5782.45 73.63 o
2 5 1 4028.57 3853.83 174.61 o
3 5 1 1645.35 1679.14 47.00 o
4 5 1 328.93 334.55 14.89 o
5 5 1 216.59 209.29 11.99 o
6 5 1 6.06 4.82 4.21 o
7 5 1 22.10 20.09 6.74 o
8 5 1 133.40 133.59 15.57 o
9 5 1 258.96 285.37 38.09 o
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