#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:40:23 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181272 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/50/2235077.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2235077_Fobs loop_ _publ_author_name 'Ma, Xiaoli' 'Sun, Shuai' 'Hao, Pengfei' 'Yang, Ying' 'Yang, Zhi' _publ_section_title ; N-(2,6-Diisopropylphenyl)-N-{3-[(2,6-diisopropylphenyl)imino]butan-2-yl}azanide trichloridostannate(II) ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m719 _journal_page_last m720 _journal_volume 68 _journal_year 2012 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 89.310 _cell_angle_beta 88.730 _cell_angle_gamma 73.670 _cell_length_a 13.3730 _cell_length_b 13.3830 _cell_length_c 18.3030 _exptl_crystal_F_000 1304.00 _reflns_d_resolution_high 0.8300 _cod_data_source_file hp2032Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' I P-1 R = 0.06' _shelx_refln_list_code 4 _shelx_f_calc_maximum 279.45 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1115.75 1079.44 45.25 o 3 0 0 41677.05 45756.98 859.49 o 4 0 0 7649.89 7764.85 126.76 o 5 0 0 2015.19 2021.82 48.98 o 6 0 0 8572.57 9296.26 152.42 o 7 0 0 9324.64 8939.44 125.13 o 8 0 0 14276.45 14281.81 248.43 o 9 0 0 4338.15 4364.68 120.36 o 10 0 0 60.48 18.47 12.25 o 11 0 0 2878.36 2076.05 593.66 o 12 0 0 218.03 165.56 86.08 o 13 0 0 1997.98 2348.72 143.63 o 14 0 0 45.25 64.06 69.24 o 15 0 0 572.95 905.90 137.84 o -15 1 0 124.59 103.73 73.64 o -14 1 0 73.20 233.80 82.15 o -13 1 0 588.67 832.83 120.05 o -12 1 0 1810.53 1831.36 110.90 o -11 1 0 557.30 306.99 89.30 o -10 1 0 213.75 217.18 33.23 o -9 1 0 287.77 215.58 39.73 o -8 1 0 679.44 86.39 71.49 o -7 1 0 16.13 59.73 33.47 o -6 1 0 4377.91 4236.87 240.46 o -5 1 0 14510.45 15123.58 181.54 o -4 1 0 349.82 237.80 87.56 o -3 1 0 638.99 615.80 64.42 o -2 1 0 1955.34 1472.81 224.65 o -1 1 0 108.81 37.42 26.62 o 2 1 0 12771.89 13105.19 183.95 o 3 1 0 1149.05 1126.18 40.17 o 4 1 0 14191.30 14561.12 193.40 o 5 1 0 1272.79 1282.71 33.39 o 6 1 0 2940.39 3163.58 62.26 o 7 1 0 2828.35 2738.59 75.23 o 8 1 0 939.98 924.34 57.06 o 9 1 0 481.49 516.39 36.67 o 10 1 0 1092.15 1001.61 86.86 o 11 1 0 7865.79 8336.65 210.37 o 12 1 0 2261.18 2411.92 148.61 o 13 1 0 451.78 472.08 102.76 o 14 1 0 84.49 137.71 73.33 o 15 1 0 192.82 184.32 73.72 o -14 2 0 404.16 480.59 101.17 o -13 2 0 225.19 139.11 72.44 o -12 2 0 24.82 -9.81 65.21 o -11 2 0 9697.01 10303.77 237.82 o -10 2 0 4797.65 4870.72 188.59 o -9 2 0 247.70 238.74 51.54 o -8 2 0 1400.60 1299.32 113.37 o -7 2 0 5391.10 5266.86 188.11 o -6 2 0 892.70 928.22 114.03 o -5 2 0 3839.01 4162.86 107.95 o -4 2 0 3223.04 3174.17 83.78 o -3 2 0 7623.44 8120.02 231.34 o -2 2 0 18496.66 19043.49 275.40 o -1 2 0 3421.46 3116.58 81.51 o 0 2 0 824.58 812.07 75.68 o 1 2 0 6221.07 6322.28 107.45 o 2 2 0 26376.63 29813.54 365.28 o 3 2 0 4471.20 4553.74 76.00 o 5 2 0 21868.61 22549.84 144.50 o 6 2 0 23136.32 23140.22 197.68 o 7 2 0 459.42 419.83 26.38 o 8 2 0 4346.38 4264.59 93.58 o 9 2 0 1080.35 1027.42 55.29 o 10 2 0 62.24 52.65 28.91 o 11 2 0 274.57 219.54 130.36 o 12 2 0 190.69 92.80 138.29 o 13 2 0 1107.00 1262.57 95.11 o 14 2 0 750.77 804.48 94.38 o 15 2 0 16.09 72.16 75.00 o -14 3 0 196.82 194.30 107.16 o -13 3 0 58.88 64.57 53.12 o -12 3 0 16.79 94.72 75.83 o -11 3 0 686.04 733.95 62.70 o -10 3 0 3045.06 2852.00 127.61 o -9 3 0 116.50 123.43 26.58 o -8 3 0 990.25 950.66 95.14 o -7 3 0 8246.25 8352.70 179.20 o -6 3 0 11266.27 11248.64 191.67 o -5 3 0 415.26 544.36 52.84 o -4 3 0 201.10 197.99 22.70 o -3 3 0 568.01 484.25 43.54 o -2 3 0 10846.76 11212.94 258.97 o -1 3 0 157.94 186.25 32.83 o 0 3 0 34423.46 36656.77 556.04 o 1 3 0 1585.98 1556.22 56.78 o 2 3 0 8720.16 8635.07 106.97 o 3 3 0 46.84 51.86 12.83 o 4 3 0 865.25 798.70 40.15 o 5 3 0 5359.54 5340.48 87.32 o 6 3 0 168.78 102.37 27.91 o 7 3 0 3369.21 3257.15 87.03 o 8 3 0 10911.79 11038.71 156.63 o 9 3 0 8797.93 8412.01 275.03 o 10 3 0 2208.96 2032.89 38.82 o 11 3 0 737.97 894.82 92.28 o 12 3 0 3165.80 3123.66 162.35 o 13 3 0 353.95 316.22 68.69 o 14 3 0 82.96 106.65 127.44 o 15 3 0 801.16 808.03 86.43 o 16 3 0 281.72 334.61 84.14 o -13 4 0 5.45 161.08 115.68 o -12 4 0 359.41 487.18 105.38 o -11 4 0 1966.70 2641.13 236.62 o -10 4 0 171.10 95.70 40.82 o -9 4 0 147.81 82.27 55.21 o -8 4 0 468.90 405.99 65.78 o -7 4 0 764.19 644.16 171.81 o -6 4 0 831.98 684.14 46.38 o -5 4 0 7151.28 6921.53 141.54 o -4 4 0 5427.79 4992.48 134.92 o -3 4 0 391.63 331.96 27.22 o -2 4 0 2717.27 2627.09 87.23 o -1 4 0 3582.47 3460.17 66.39 o 0 4 0 1722.14 1741.16 66.88 o 1 4 0 13977.79 14348.53 150.17 o 2 4 0 7225.88 7414.28 129.11 o 3 4 0 62.87 75.06 17.60 o 4 4 0 8886.07 8761.39 116.25 o 5 4 0 2362.04 2311.45 59.62 o 6 4 0 236.84 250.01 35.76 o 7 4 0 2027.53 2332.76 155.68 o 8 4 0 1439.04 1513.83 75.79 o 9 4 0 76.12 45.42 19.89 o 10 4 0 413.99 295.16 57.78 o 11 4 0 3935.96 3785.43 111.87 o 12 4 0 1999.49 2104.82 130.71 o 13 4 0 1117.04 1166.06 72.64 o 14 4 0 125.86 75.31 48.14 o 15 4 0 505.09 565.52 89.85 o 16 4 0 59.87 55.98 43.90 o -13 5 0 13.25 -7.49 63.48 o -12 5 0 705.68 893.02 101.72 o -11 5 0 57.57 143.06 42.32 o -10 5 0 781.62 806.76 81.48 o -9 5 0 1078.11 1186.45 85.10 o -8 5 0 88.71 100.34 61.30 o -7 5 0 39.08 90.52 51.52 o -6 5 0 403.70 353.21 101.71 o -5 5 0 1849.80 1917.97 192.98 o -4 5 0 5404.37 5254.18 244.69 o -3 5 0 1300.89 1364.02 58.11 o -2 5 0 24496.88 25154.28 419.69 o -1 5 0 12374.99 12426.14 203.38 o 0 5 0 11050.75 11377.84 276.98 o 1 5 0 164.13 128.96 25.66 o 2 5 0 19398.61 20772.17 116.40 o 3 5 0 945.56 1071.73 30.64 o 4 5 0 274.78 262.89 26.40 o 5 5 0 1547.54 1484.69 40.52 o 6 5 0 7585.68 7751.61 129.04 o 7 5 0 10029.09 9919.50 230.15 o 8 5 0 35.14 41.12 24.20 o 9 5 0 3473.80 3383.75 95.32 o 10 5 0 1693.23 1648.98 39.42 o 11 5 0 136.72 44.34 82.37 o 12 5 0 11.85 -2.99 18.75 o 13 5 0 147.88 174.15 123.79 o 14 5 0 1163.30 1234.81 65.54 o 15 5 0 841.51 909.04 60.39 o 16 5 0 294.92 257.61 111.35 o -12 6 0 30.37 79.80 72.95 o -11 6 0 108.38 129.98 57.65 o -10 6 0 496.39 666.15 95.05 o -9 6 0 2740.77 2697.67 121.82 o -8 6 0 135.51 113.15 50.26 o -7 6 0 2759.55 2455.56 508.21 o -6 6 0 6730.88 6858.33 244.83 o -5 6 0 2781.82 2941.50 162.53 o -4 6 0 984.98 921.31 87.20 o -3 6 0 4720.95 4586.58 159.39 o -2 6 0 8505.29 8579.51 119.14 o -1 6 0 5624.07 5631.66 175.75 o 0 6 0 16889.37 17818.72 258.48 o 1 6 0 15134.22 14910.36 298.39 o 2 6 0 16541.86 16164.08 246.62 o 3 6 0 81.69 27.70 19.86 o 4 6 0 3662.00 3665.59 114.86 o 5 6 0 548.74 587.70 51.29 o 6 6 0 85.80 81.32 25.41 o 7 6 0 4597.94 4470.29 83.06 o 8 6 0 431.13 510.19 60.27 o 9 6 0 6851.11 6596.21 141.88 o 10 6 0 2565.91 2380.84 96.46 o 11 6 0 41.12 35.14 25.82 o 12 6 0 67.51 46.82 23.40 o 13 6 0 193.14 218.18 45.29 o 14 6 0 12.66 20.37 29.16 o 15 6 0 22.05 70.58 35.62 o 16 6 0 268.09 317.12 156.49 o -11 7 0 2873.69 2983.46 156.42 o -10 7 0 6.33 29.55 43.48 o -9 7 0 1022.00 1202.93 194.39 o -8 7 0 43.81 63.78 56.73 o -7 7 0 416.43 454.70 127.71 o -6 7 0 185.47 46.33 61.16 o -5 7 0 218.98 193.72 90.09 o -4 7 0 2903.31 2865.66 181.44 o -3 7 0 4775.52 5083.62 156.69 o -2 7 0 435.96 140.54 68.83 o -1 7 0 104.15 105.78 46.61 o 0 7 0 3839.03 3857.62 152.02 o 1 7 0 6290.33 6939.60 925.56 o 2 7 0 2310.51 2488.83 464.79 o 3 7 0 380.23 303.23 114.91 o 4 7 0 28696.64 31565.74 763.17 o 5 7 0 5791.94 5735.13 154.03 o 6 7 0 413.32 503.00 57.48 o 7 7 0 886.71 843.07 83.54 o 8 7 0 120.64 117.32 22.73 o 9 7 0 2245.86 2076.13 82.47 o 10 7 0 2309.47 2157.13 77.73 o 11 7 0 821.16 763.91 57.54 o 12 7 0 1155.27 1106.83 70.70 o 13 7 0 92.69 102.05 43.35 o 14 7 0 16.78 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104.68 -13.42 96.49 o -6 12 0 209.49 270.14 68.36 o -5 12 0 178.68 215.81 77.41 o -4 12 0 75.08 25.25 60.18 o -3 12 0 229.88 204.15 70.09 o -2 12 0 161.72 160.27 113.61 o -1 12 0 491.53 421.73 71.71 o 0 12 0 437.70 563.26 88.83 o 1 12 0 590.05 544.97 87.86 o 2 12 0 2441.07 2294.84 129.61 o 3 12 0 1573.96 1770.73 196.09 o 4 12 0 1147.76 1173.18 197.93 o 5 12 0 80.71 75.14 117.66 o 6 12 0 102.44 136.85 162.08 o 7 12 0 977.36 969.09 129.25 o 8 12 0 707.35 749.95 116.54 o 9 12 0 104.29 74.17 32.63 o 10 12 0 1017.70 1143.95 105.51 o 11 12 0 3064.11 3063.86 129.46 o 12 12 0 497.55 563.99 85.67 o 13 12 0 7.53 209.37 138.02 o -5 13 0 217.04 186.20 163.92 o -4 13 0 27.77 26.02 51.89 o -3 13 0 515.37 654.91 94.01 o -2 13 0 1653.02 1756.28 242.75 o -1 13 0 268.83 170.63 82.25 o 0 13 0 119.19 97.47 79.33 o 1 13 0 564.51 585.71 86.86 o 2 13 0 1063.34 1080.12 236.94 o 3 13 0 129.06 48.02 110.09 o 4 13 0 893.81 826.08 149.26 o 5 13 0 2351.33 2728.83 145.18 o 6 13 0 3260.94 3267.89 157.44 o 7 13 0 208.02 157.52 86.78 o 8 13 0 1114.08 1205.30 252.09 o 9 13 0 155.07 294.68 86.15 o 10 13 0 72.87 129.31 94.51 o 11 13 0 99.86 43.49 54.76 o 12 13 0 2.71 33.85 62.68 o -3 14 0 456.97 632.75 123.72 o -2 14 0 129.12 164.45 96.53 o -1 14 0 4.41 75.23 60.54 o 0 14 0 667.48 742.09 260.01 o 1 14 0 850.33 752.27 155.50 o 2 14 0 374.12 425.15 132.35 o 3 14 0 228.15 349.18 87.40 o 4 14 0 248.18 213.44 89.51 o 5 14 0 74.09 48.72 65.25 o 6 14 0 176.40 223.35 79.57 o 7 14 0 280.48 281.04 92.25 o 8 14 0 1371.75 1522.69 126.70 o 9 14 0 560.07 464.78 137.53 o 10 14 0 298.09 261.79 67.38 o 11 14 0 6.25 55.94 48.40 o -1 15 0 10.25 -9.64 89.55 o 0 15 0 57.27 124.86 80.81 o 1 15 0 1066.55 1365.81 204.60 o 2 15 0 252.61 249.33 73.82 o 3 15 0 81.66 162.43 65.98 o 4 15 0 988.00 1180.66 161.67 o 5 15 0 1676.96 1682.38 146.86 o 6 15 0 58.10 55.84 57.32 o 7 15 0 47.31 47.06 76.17 o 8 15 0 176.42 241.99 119.01 o 9 15 0 19.66 51.37 42.24 o 3 16 0 285.09 340.19 73.22 o 4 16 0 98.01 151.80 71.46 o 5 16 0 73.26 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