#------------------------------------------------------------------------------ #$Date: 2012-09-11 12:26:43 +0300 (Tue, 11 Sep 2012) $ #$Revision: 66590 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/52/2235269.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2235269_Fobs loop_ _publ_author_name 'Jiang, Nan' 'Zuo, Jian' 'Zhu, Wenmin' 'Zhao, Xinjie' 'Zhai, Xin' _publ_section_title ; (E)-2-[2-(4-Chlorobenzylidene)hydrazinyl]-4-[3-(morpholin-4-ium-4-yl)propylamino]quinazolin-1-ium bis(perchlorate) ; _journal_coeditor_code VM2162 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1819 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 112.127 _cell_angle_gamma 90.000 _cell_length_a 16.1835 _cell_length_b 11.6719 _cell_length_c 16.7332 _exptl_crystal_F_000 1296.00 _reflns_d_resolution_high 0.8409 _[local]_cod_data_source_file vm2162Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 1 in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 260.30 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 92.80 213.40 36.45 o 6 0 0 1929.87 1811.67 102.52 o 8 0 0 0.37 22.41 22.24 o 10 0 0 796.68 672.70 57.69 o 12 0 0 1397.36 1217.51 83.47 o 14 0 0 3490.06 3882.31 160.00 o 16 0 0 19.17 0.00 42.45 o 1 1 0 925.43 1328.91 35.23 o 2 1 0 538.77 617.13 40.46 o 3 1 0 12.00 0.00 25.25 o 4 1 0 27399.39 25438.01 566.93 o 5 1 0 5013.52 5656.82 151.60 o 6 1 0 682.68 814.83 36.16 o 7 1 0 0.96 5.70 16.02 o 8 1 0 3945.73 3428.94 82.49 o 9 1 0 210.45 200.56 31.43 o 10 1 0 769.21 691.08 42.05 o 11 1 0 208.79 203.33 30.00 o 12 1 0 1357.60 1409.87 62.42 o 13 1 0 147.71 142.80 31.01 o 14 1 0 870.93 1000.47 71.30 o 15 1 0 530.15 565.42 88.44 o 16 1 0 0.45 0.00 34.31 o 17 1 0 88.03 55.54 76.61 o 1 2 0 2992.74 3216.36 81.20 o 2 2 0 67754.98 63062.59 959.38 o 3 2 0 8851.28 8111.48 156.98 o 4 2 0 95.37 28.07 18.92 o 5 2 0 10379.14 11835.14 231.27 o 6 2 0 58.27 116.52 15.98 o 7 2 0 2481.88 2445.44 64.77 o 8 2 0 376.39 356.54 29.45 o 9 2 0 28.68 10.43 17.61 o 10 2 0 81.11 84.12 23.69 o 11 2 0 131.12 98.20 25.57 o 12 2 0 782.79 880.36 59.27 o 13 2 0 854.91 961.36 57.57 o 14 2 0 1163.39 1195.05 65.15 o 15 2 0 120.51 120.61 43.95 o 16 2 0 22.75 0.00 58.87 o 17 2 0 7.42 10.79 43.38 o 2 3 0 319.05 172.42 18.88 o 3 3 0 0.61 0.00 8.35 o 4 3 0 206.36 359.62 19.22 o 5 3 0 198.59 282.80 27.86 o 6 3 0 308.56 216.13 19.73 o 7 3 0 1067.74 979.13 36.26 o 8 3 0 37.52 46.99 16.30 o 9 3 0 1952.23 2040.47 76.11 o 10 3 0 386.26 431.76 35.52 o 11 3 0 1070.60 1223.84 56.47 o 12 3 0 40.69 32.08 26.51 o 13 3 0 263.32 229.39 36.59 o 14 3 0 71.97 46.29 34.64 o 15 3 0 161.29 206.50 47.46 o 16 3 0 306.51 329.82 55.35 o 17 3 0 58.30 93.40 48.50 o 0 4 0 3272.03 3331.76 142.51 o 1 4 0 3199.60 2880.28 128.27 o 2 4 0 271.02 279.16 25.58 o 3 4 0 2137.22 2104.59 57.00 o 4 4 0 9544.10 9563.78 166.14 o 5 4 0 1624.80 1709.85 41.82 o 6 4 0 5378.11 5522.96 88.37 o 7 4 0 168.47 120.01 19.30 o 8 4 0 393.83 397.27 24.39 o 9 4 0 32.22 95.12 26.26 o 10 4 0 441.58 380.43 35.35 o 11 4 0 1014.07 1037.93 53.99 o 12 4 0 24.44 25.47 25.80 o 13 4 0 28.04 40.94 31.94 o 14 4 0 1.73 24.51 30.10 o 15 4 0 43.42 91.30 40.68 o 16 4 0 68.39 113.34 50.33 o 17 4 0 0.68 0.00 64.51 o 1 5 0 0.05 26.06 36.45 o 2 5 0 398.01 261.45 24.77 o 3 5 0 1761.99 1978.87 57.14 o 4 5 0 17.38 0.00 9.68 o 5 5 0 974.30 1145.73 43.52 o 6 5 0 194.38 269.66 20.01 o 7 5 0 131.46 184.32 35.73 o 8 5 0 1725.71 1840.13 48.49 o 9 5 0 31.91 69.68 19.89 o 10 5 0 1354.13 1449.74 63.32 o 11 5 0 50.78 103.32 28.20 o 12 5 0 5.91 31.75 29.73 o 13 5 0 45.93 48.77 34.71 o 14 5 0 166.07 124.89 74.82 o 15 5 0 56.48 84.32 40.35 o 16 5 0 5.47 17.99 39.80 o 0 6 0 340.59 633.18 66.94 o 1 6 0 510.58 737.23 50.88 o 2 6 0 52.40 10.35 14.85 o 3 6 0 305.99 454.49 30.33 o 4 6 0 10700.70 11016.94 171.92 o 5 6 0 612.82 643.42 23.97 o 6 6 0 1026.92 1075.59 47.15 o 7 6 0 73.51 69.68 21.61 o 8 6 0 144.35 166.77 38.82 o 9 6 0 518.78 622.15 43.24 o 10 6 0 647.40 702.93 41.98 o 11 6 0 60.54 53.57 24.37 o 12 6 0 21.46 0.00 31.90 o 13 6 0 7.93 3.41 44.05 o 14 6 0 20.24 0.00 47.72 o 15 6 0 12.97 42.87 41.22 o 16 6 0 38.11 72.47 46.13 o 1 7 0 110.23 139.76 30.85 o 2 7 0 204.18 177.89 30.82 o 3 7 0 524.82 573.78 30.81 o 4 7 0 50.54 20.37 14.81 o 5 7 0 339.78 359.25 24.32 o 6 7 0 0.62 0.00 17.88 o 7 7 0 510.46 487.80 39.75 o 8 7 0 1463.89 1662.33 64.81 o 9 7 0 1.16 26.24 24.45 o 10 7 0 502.08 586.35 45.72 o 11 7 0 98.03 118.08 45.16 o 12 7 0 85.88 111.34 41.27 o 13 7 0 0.05 0.00 65.50 o 14 7 0 0.92 16.93 45.65 o 15 7 0 25.08 0.00 101.15 o 0 8 0 556.91 628.37 81.19 o 1 8 0 966.00 1090.79 89.87 o 2 8 0 1182.14 1111.33 53.83 o 3 8 0 361.69 458.64 37.25 o 4 8 0 41.36 22.55 20.61 o 5 8 0 704.34 881.69 56.59 o 6 8 0 2707.28 3131.84 78.31 o 7 8 0 323.68 466.97 40.90 o 8 8 0 783.43 930.26 52.21 o 9 8 0 593.83 442.12 55.44 o 10 8 0 17.19 33.05 33.73 o 11 8 0 3.30 52.88 48.84 o 12 8 0 0.07 0.00 33.27 o 13 8 0 32.04 56.12 46.88 o 14 8 0 120.00 148.33 60.48 o 1 9 0 248.70 330.26 36.71 o 2 9 0 37.90 0.00 46.24 o 3 9 0 774.45 685.53 65.63 o 4 9 0 33.00 12.40 36.51 o 5 9 0 100.18 102.62 51.44 o 6 9 0 1072.57 1008.58 65.70 o 7 9 0 229.83 296.58 57.33 o 8 9 0 238.65 252.25 35.64 o 9 9 0 370.41 302.45 46.27 o 10 9 0 6.12 17.36 42.28 o 11 9 0 239.41 283.85 50.51 o 12 9 0 83.46 121.03 44.52 o 13 9 0 3.58 0.00 44.58 o 0 10 0 1289.31 1433.95 128.47 o 1 10 0 6.30 0.00 25.32 o 2 10 0 2.39 60.88 49.52 o 3 10 0 101.65 176.30 44.26 o 4 10 0 282.37 284.25 88.21 o 5 10 0 94.29 76.39 35.67 o 6 10 0 347.80 439.64 51.83 o 7 10 0 49.90 52.01 35.77 o 8 10 0 423.82 473.86 72.09 o 9 10 0 7.14 0.00 37.95 o 10 10 0 4.90 43.09 43.34 o 11 10 0 40.47 11.28 49.29 o 12 10 0 2.61 4.70 52.04 o 1 11 0 383.22 495.97 66.45 o 2 11 0 279.92 392.55 96.27 o 3 11 0 0.96 0.00 33.90 o 4 11 0 269.49 232.59 43.17 o 5 11 0 74.38 123.68 45.64 o 6 11 0 5.81 69.85 36.45 o 7 11 0 29.54 33.89 67.54 o 8 11 0 32.15 0.00 42.16 o 9 11 0 7.52 29.12 48.19 o 10 11 0 98.41 24.97 49.73 o 1 12 0 103.17 28.48 61.69 o 2 12 0 13.78 23.81 42.97 o 3 12 0 1.43 0.00 57.78 o 4 12 0 37.64 31.83 34.64 o 5 12 0 117.87 132.35 42.13 o 6 12 0 35.26 50.29 39.39 o 7 12 0 0.50 59.08 55.64 o 8 12 0 12.53 77.24 54.09 o 1 13 0 14.58 0.00 65.24 o 2 13 0 151.81 162.18 101.15 o 3 13 0 27.68 20.95 38.25 o 4 13 0 34.41 27.83 39.51 o 5 13 0 69.65 54.37 44.87 o 6 13 0 9.01 50.34 51.40 o -17 0 1 589.98 687.62 127.20 o -15 0 1 1108.42 1119.71 100.75 o -13 0 1 916.27 1020.64 80.48 o -11 0 1 96.11 105.82 34.28 o -9 0 1 3036.59 3137.40 112.38 o -7 0 1 24.78 130.59 32.37 o -5 0 1 159.91 243.56 37.18 o 3 0 1 2792.10 3407.59 137.03 o 5 0 1 24153.15 23394.24 753.56 o 7 0 1 193.87 294.54 37.23 o 9 0 1 400.99 405.07 47.16 o 11 0 1 31.36 45.42 35.31 o 13 0 1 47.12 15.61 38.35 o 15 0 1 1.63 0.00 54.17 o 17 0 1 259.04 320.67 100.31 o -18 1 1 46.52 36.70 64.23 o -17 1 1 395.13 275.67 63.01 o -16 1 1 295.44 208.01 62.63 o -15 1 1 438.22 485.66 55.78 o -14 1 1 313.19 257.55 37.95 o -13 1 1 124.71 106.00 30.73 o -12 1 1 2.56 31.53 23.61 o -11 1 1 121.83 108.46 25.17 o -10 1 1 107.31 102.87 28.39 o -9 1 1 752.31 572.24 34.45 o -8 1 1 209.09 286.52 25.97 o -7 1 1 39.86 50.76 15.97 o -6 1 1 892.80 921.09 36.04 o -5 1 1 10075.42 8805.53 213.76 o -4 1 1 0.89 8.41 17.06 o -3 1 1 33456.10 33824.00 1044.27 o 0 1 1 167.12 40.15 8.33 o 1 1 1 2077.99 2123.24 56.56 o 2 1 1 17603.53 15975.08 359.79 o 3 1 1 11126.73 12073.09 282.69 o 4 1 1 44.03 6.63 21.89 o 5 1 1 4646.75 4921.35 140.50 o 6 1 1 709.85 652.58 33.69 o 7 1 1 2942.31 2540.54 70.68 o 8 1 1 777.60 905.28 42.15 o 9 1 1 1834.61 1687.47 59.40 o 10 1 1 1.21 3.89 18.80 o 11 1 1 438.95 486.58 40.22 o 12 1 1 52.42 8.94 22.86 o 13 1 1 511.34 523.34 47.39 o 14 1 1 513.96 512.72 90.12 o 15 1 1 3.28 0.00 30.55 o 16 1 1 95.56 44.34 36.38 o 17 1 1 262.04 240.70 53.44 o -17 2 1 378.28 349.12 71.25 o -16 2 1 563.51 416.52 82.78 o -15 2 1 963.59 925.67 185.27 o -14 2 1 128.15 141.40 50.04 o -13 2 1 53.01 20.97 26.26 o -12 2 1 125.37 140.69 29.94 o -11 2 1 177.15 137.61 28.10 o -10 2 1 563.16 578.47 37.66 o -9 2 1 594.23 565.24 36.36 o -8 2 1 2403.97 2758.15 71.06 o -7 2 1 1095.25 961.78 38.56 o -6 2 1 2146.10 2348.63 58.08 o -5 2 1 620.73 628.82 40.36 o -4 2 1 29.03 110.03 21.60 o -3 2 1 10.03 20.40 22.87 o 0 2 1 1379.39 1221.28 43.31 o 1 2 1 19024.77 16346.49 257.51 o 2 2 1 3728.35 3619.35 67.98 o 3 2 1 36434.55 42629.64 837.26 o 4 2 1 3327.14 3841.32 113.69 o 5 2 1 33.89 47.61 20.22 o 6 2 1 1666.64 1844.34 46.80 o 7 2 1 41.97 27.00 14.76 o 8 2 1 650.10 809.05 70.03 o 9 2 1 1093.04 965.36 63.66 o 10 2 1 80.01 20.00 22.35 o 11 2 1 644.76 641.98 57.71 o 12 2 1 17.54 16.76 32.64 o 13 2 1 26.63 0.00 25.76 o 14 2 1 804.86 779.61 99.70 o 15 2 1 61.27 104.58 35.32 o 16 2 1 66.88 87.73 43.88 o 17 2 1 33.83 0.88 51.72 o -17 3 1 25.63 0.00 38.91 o -16 3 1 4.56 50.24 60.92 o -15 3 1 3.88 22.75 34.85 o -14 3 1 589.97 513.84 55.96 o -13 3 1 3136.17 3181.42 112.91 o -12 3 1 730.42 844.55 50.53 o -11 3 1 1838.01 2066.92 82.99 o -10 3 1 19.05 32.08 20.87 o -9 3 1 311.13 317.32 29.64 o -8 3 1 289.39 316.35 29.23 o -7 3 1 297.54 150.23 29.89 o -6 3 1 3198.50 2843.49 60.05 o -5 3 1 804.96 413.69 28.08 o -4 3 1 3.54 0.00 13.82 o -3 3 1 8381.32 6839.83 159.50 o 0 3 1 2541.85 2675.30 111.08 o 1 3 1 16762.07 16054.71 363.57 o 2 3 1 686.48 843.29 27.77 o 3 3 1 14501.64 15011.89 218.08 o 4 3 1 581.49 546.43 32.49 o 5 3 1 1637.14 1538.17 48.05 o 6 3 1 1036.36 1083.16 36.77 o 7 3 1 3756.24 3622.39 76.18 o 8 3 1 2289.43 2441.11 61.58 o 9 3 1 23.85 35.95 20.27 o 10 3 1 10.50 5.83 21.25 o 11 3 1 90.65 88.83 27.15 o 12 3 1 799.70 896.18 69.11 o 13 3 1 23.20 3.15 41.83 o 14 3 1 16.42 1.41 27.38 o 15 3 1 2.36 9.38 34.31 o 16 3 1 67.05 14.56 40.35 o 17 3 1 72.55 42.19 48.63 o -17 4 1 36.62 52.26 45.43 o -16 4 1 3.50 0.00 47.21 o -15 4 1 347.23 285.31 59.34 o -14 4 1 177.87 270.75 75.87 o -13 4 1 804.61 809.12 62.10 o -12 4 1 236.84 186.67 37.20 o -11 4 1 1600.08 1775.03 65.71 o -10 4 1 563.34 480.12 36.52 o -9 4 1 42.25 30.14 19.31 o -8 4 1 59.44 40.22 16.26 o -7 4 1 286.19 302.72 24.24 o -6 4 1 1149.45 1639.35 36.18 o -5 4 1 223.04 225.22 21.78 o -4 4 1 166.16 179.93 22.94 o -3 4 1 3848.94 4621.92 86.99 o -2 4 1 440.48 501.63 51.66 o -1 4 1 4648.66 3846.70 156.96 o 0 4 1 3643.97 3238.00 142.04 o 1 4 1 257.68 124.45 39.55 o 2 4 1 1206.46 1146.94 37.47 o 3 4 1 1012.91 1119.42 45.39 o 4 4 1 3073.10 3710.14 82.23 o 5 4 1 1076.01 1069.44 50.73 o 6 4 1 1598.38 1427.86 49.98 o 7 4 1 1.11 0.00 12.66 o 8 4 1 1670.41 1669.73 45.18 o 9 4 1 548.02 558.51 34.60 o 10 4 1 17.47 43.21 22.86 o 11 4 1 828.28 926.21 53.37 o 12 4 1 3.10 0.25 24.91 o 13 4 1 92.57 84.96 31.05 o 14 4 1 23.51 30.23 45.38 o 15 4 1 67.53 60.49 39.29 o 16 4 1 24.91 24.88 41.64 o -16 5 1 61.82 14.64 37.47 o -15 5 1 112.56 137.26 42.42 o -14 5 1 274.06 269.74 61.61 o -13 5 1 47.39 44.10 32.32 o -12 5 1 543.26 508.37 52.09 o -11 5 1 1601.02 1808.02 81.07 o -10 5 1 1804.73 1920.62 60.11 o -9 5 1 1870.13 2061.04 59.45 o -8 5 1 69.10 67.27 18.89 o -7 5 1 2339.38 2336.38 58.90 o -6 5 1 1267.08 1398.24 44.79 o -5 5 1 962.79 1080.94 56.33 o -4 5 1 295.17 397.97 21.02 o -3 5 1 101.98 30.98 16.52 o -2 5 1 8.67 5.00 25.11 o -1 5 1 222.54 202.46 43.90 o 0 5 1 713.47 575.17 41.52 o 1 5 1 3920.20 3479.09 87.86 o 2 5 1 1031.79 1005.32 36.43 o 3 5 1 2464.04 2316.10 59.55 o 4 5 1 240.69 265.80 20.23 o 5 5 1 1772.18 1735.36 55.49 o 6 5 1 169.15 191.80 20.18 o 7 5 1 588.74 577.54 31.60 o 8 5 1 364.55 346.26 47.42 o 9 5 1 4.41 0.00 18.14 o 10 5 1 84.24 123.07 24.96 o 11 5 1 2.66 0.00 23.49 o 12 5 1 190.59 240.08 35.60 o 13 5 1 72.49 65.76 35.36 o 14 5 1 251.87 91.64 58.32 o 15 5 1 90.15 31.82 38.84 o 16 5 1 124.57 192.64 53.03 o -16 6 1 0.78 0.00 35.92 o -15 6 1 51.53 24.72 36.52 o -14 6 1 31.11 22.76 36.02 o -13 6 1 1313.49 1652.59 87.69 o -12 6 1 23.00 17.22 29.87 o -11 6 1 517.63 619.50 47.59 o -10 6 1 161.82 141.19 26.28 o -9 6 1 73.89 74.51 21.61 o -8 6 1 1.22 0.00 19.83 o -7 6 1 53.90 34.81 19.72 o -6 6 1 0.19 0.00 13.56 o -5 6 1 264.59 261.01 17.02 o -4 6 1 484.25 409.39 26.87 o -3 6 1 1826.34 1936.72 60.79 o -2 6 1 74.12 62.10 24.42 o -1 6 1 43.08 14.45 21.36 o 0 6 1 117.22 136.10 24.17 o 1 6 1 11740.88 11403.42 231.65 o 2 6 1 156.49 161.84 31.35 o 3 6 1 6.70 8.33 11.35 o 4 6 1 374.66 358.40 29.67 o 5 6 1 88.07 38.75 19.02 o 6 6 1 17.86 26.62 16.46 o 7 6 1 129.60 178.58 27.85 o 8 6 1 25.30 11.62 22.10 o 9 6 1 5.86 0.00 22.68 o 10 6 1 163.59 160.78 32.28 o 11 6 1 14.07 0.00 24.99 o 12 6 1 0.72 9.14 41.33 o 13 6 1 3.58 42.41 50.45 o 14 6 1 6.39 10.61 47.93 o 15 6 1 106.33 16.72 49.68 o -15 7 1 7.40 0.00 36.98 o -14 7 1 8.32 0.00 78.08 o -13 7 1 3.82 48.90 42.72 o -12 7 1 411.74 510.81 70.25 o -11 7 1 70.51 78.80 34.64 o -10 7 1 8.54 0.00 29.12 o -9 7 1 1848.87 2096.72 78.46 o -8 7 1 111.79 71.22 39.16 o -7 7 1 294.27 287.00 27.27 o -6 7 1 211.97 199.65 22.97 o -5 7 1 0.38 0.00 16.30 o -4 7 1 171.28 188.23 22.81 o -3 7 1 287.49 266.28 27.42 o -2 7 1 2406.91 2641.01 104.62 o -1 7 1 862.20 712.28 55.37 o 0 7 1 777.41 887.46 50.39 o 1 7 1 975.90 866.72 37.99 o 2 7 1 2774.34 2974.11 85.74 o 3 7 1 987.71 1010.95 37.70 o 4 7 1 9.43 0.00 12.20 o 5 7 1 1360.24 1517.21 57.16 o 6 7 1 4.61 0.00 18.36 o 7 7 1 2.71 0.00 19.97 o 8 7 1 24.73 6.69 22.14 o 9 7 1 10.32 10.30 24.18 o 10 7 1 135.57 119.96 39.02 o 11 7 1 208.52 167.41 35.98 o 12 7 1 78.32 115.68 42.13 o 13 7 1 112.49 136.80 71.36 o 14 7 1 11.61 0.00 60.19 o 15 7 1 30.52 0.00 49.87 o -14 8 1 35.21 0.00 71.32 o -13 8 1 97.10 16.57 43.54 o -12 8 1 24.32 5.66 38.36 o -11 8 1 414.59 511.78 57.15 o -10 8 1 373.26 374.20 49.57 o -9 8 1 107.65 106.75 33.77 o -8 8 1 317.67 334.09 31.78 o -7 8 1 580.92 614.50 42.26 o -6 8 1 436.28 368.58 34.08 o -5 8 1 57.34 30.32 40.46 o -4 8 1 282.60 269.26 42.86 o -3 8 1 28.78 5.57 25.11 o -2 8 1 2.17 7.69 17.80 o -1 8 1 4299.93 4463.36 152.41 o 0 8 1 15.26 0.00 14.72 o 1 8 1 271.30 218.33 24.37 o 2 8 1 17.09 55.33 20.47 o 3 8 1 5.35 4.33 16.69 o 4 8 1 148.55 202.84 27.96 o 5 8 1 760.30 675.86 43.66 o 6 8 1 1285.51 1322.00 59.32 o 7 8 1 56.30 28.27 33.04 o 8 8 1 12.58 6.24 25.45 o 9 8 1 40.09 30.20 26.31 o 10 8 1 42.25 2.92 25.35 o 11 8 1 3.30 11.24 33.15 o 12 8 1 17.88 0.00 32.78 o 13 8 1 0.08 0.00 36.77 o 14 8 1 1.09 0.00 74.03 o -13 9 1 115.60 19.21 74.50 o -12 9 1 44.59 15.70 39.55 o -11 9 1 336.39 385.48 69.92 o -10 9 1 173.00 138.00 51.36 o -9 9 1 29.34 81.55 46.52 o -8 9 1 74.19 64.21 31.41 o -7 9 1 1.47 0.00 30.85 o -6 9 1 685.01 819.55 108.39 o -5 9 1 176.09 144.52 41.54 o -4 9 1 36.93 35.96 42.17 o -3 9 1 646.03 764.41 68.83 o -2 9 1 372.98 354.61 86.50 o -1 9 1 124.43 88.98 34.25 o 0 9 1 84.15 60.12 34.08 o 1 9 1 1169.88 1048.68 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