#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:41:17 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181275 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/53/2235301.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2235301_Fobs loop_ _publ_author_name 'Al Mamari, Khalil' 'Ennajih, Hamid' 'Bouhfid, Rachid' 'Essassi, El Mokhtar' 'Ng, Seik Weng' _publ_section_title ; 1,1''-Bis(prop-2-en-1-yl)-1,1'',2,2''-tetrahydrodispiro[indole-3,7'-[6,9]diazatricyclo[7.3.0.0^2,6^]dodecane-8',3''-indole]-2,2''-dione ; _journal_coeditor_code XU5527 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1637 _journal_volume 68 _journal_year 2012 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 111.119 _cell_angle_gamma 90.000 _cell_length_a 14.9484 _cell_length_b 9.9173 _cell_length_c 17.5713 _exptl_crystal_F_000 1024.00 _reflns_d_resolution_high 0.7696 _cod_data_source_file xu5527Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 206.08 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 1397.71 1330.09 16.74 o 6 0 0 1275.76 1353.36 16.97 o 8 0 0 135.62 99.73 2.62 o 10 0 0 336.49 373.12 7.61 o 12 0 0 1333.65 1392.28 31.30 o 14 0 0 1896.80 1871.23 41.94 o 16 0 0 90.12 90.86 6.93 o 18 0 0 1.61 -5.30 3.53 o 3 1 0 4428.39 4217.72 42.51 o 5 1 0 1316.13 1292.30 17.71 o 7 1 0 57.96 40.50 0.86 o 9 1 0 9.19 5.77 0.53 o 11 1 0 370.28 407.83 5.48 o 13 1 0 74.35 64.73 2.46 o 15 1 0 17.30 10.55 1.81 o 17 1 0 15.88 15.35 3.38 o 0 2 0 24357.69 23567.64 347.12 o 2 2 0 7234.21 7514.21 72.03 o 4 2 0 1917.64 1869.37 21.57 o 6 2 0 1948.97 1966.36 22.72 o 8 2 0 1482.07 1571.08 20.81 o 10 2 0 152.35 133.62 2.14 o 12 2 0 27.73 31.99 2.06 o 14 2 0 1221.94 1245.25 20.30 o 16 2 0 1.20 2.97 1.68 o 1 3 0 481.39 477.96 4.15 o 3 3 0 41.47 34.12 1.47 o 5 3 0 75.28 49.18 0.96 o 7 3 0 1965.83 2035.46 19.83 o 9 3 0 579.16 572.67 7.18 o 11 3 0 1102.20 1124.40 16.18 o 13 3 0 456.65 476.76 7.73 o 15 3 0 62.10 64.38 3.15 o 17 3 0 121.32 116.78 5.62 o 0 4 0 1666.43 1662.08 23.75 o 2 4 0 1974.63 1958.25 17.45 o 4 4 0 8688.54 9699.27 92.69 o 6 4 0 146.67 179.40 2.54 o 8 4 0 7.01 9.44 0.67 o 10 4 0 126.49 125.81 2.12 o 12 4 0 71.00 62.53 2.03 o 14 4 0 47.89 53.64 2.72 o 16 4 0 177.64 186.07 5.44 o 1 5 0 3914.52 3965.94 35.00 o 3 5 0 8561.46 9327.61 99.07 o 5 5 0 0.83 9.57 0.75 o 7 5 0 160.15 152.93 2.61 o 9 5 0 10.29 9.35 0.80 o 11 5 0 79.44 69.45 2.19 o 13 5 0 22.07 26.94 2.01 o 15 5 0 41.55 29.35 2.31 o 0 6 0 2311.45 2475.59 44.45 o 2 6 0 31.74 27.55 0.93 o 4 6 0 129.74 151.87 2.42 o 6 6 0 215.35 226.93 3.23 o 8 6 0 217.47 209.61 3.31 o 10 6 0 402.95 430.18 6.07 o 12 6 0 176.64 167.88 4.14 o 14 6 0 180.37 175.90 5.47 o 16 6 0 5.04 3.98 2.75 o 1 7 0 7.94 5.35 0.71 o 3 7 0 962.87 935.72 9.29 o 5 7 0 4.95 10.52 0.90 o 7 7 0 219.31 182.98 3.17 o 9 7 0 989.70 1003.62 13.76 o 11 7 0 45.61 42.93 2.24 o 13 7 0 91.41 99.26 3.95 o 15 7 0 6.45 9.05 3.36 o 0 8 0 1020.60 885.79 13.36 o 2 8 0 6.39 3.22 0.77 o 4 8 0 120.93 121.69 3.27 o 6 8 0 706.00 638.49 10.19 o 8 8 0 23.06 16.99 1.62 o 10 8 0 18.31 16.75 1.93 o 12 8 0 12.56 18.09 2.97 o 14 8 0 82.52 99.99 11.78 o 1 9 0 958.34 980.76 10.05 o 3 9 0 22.17 26.58 1.68 o 5 9 0 1217.75 1152.26 20.32 o 7 9 0 28.03 15.46 2.04 o 9 9 0 20.07 23.69 2.23 o 11 9 0 0.01 0.38 2.63 o 0 10 0 472.21 455.57 20.37 o 2 10 0 0.64 1.42 1.66 o 4 10 0 361.11 317.64 7.26 o 6 10 0 93.74 95.31 3.92 o 8 10 0 165.89 153.26 4.94 o 10 10 0 23.63 31.18 4.82 o 1 11 0 453.61 428.19 13.18 o 3 11 0 9.58 5.91 2.48 o 5 11 0 9.15 3.32 2.39 o 7 11 0 355.67 389.21 10.35 o 9 11 0 19.91 20.60 4.13 o 0 12 0 2.28 -2.97 4.00 o 2 12 0 6.24 7.20 3.39 o 4 12 0 15.35 10.26 5.51 o 6 12 0 5.43 8.36 3.82 o -17 1 1 154.35 154.58 7.00 o -15 1 1 21.66 23.00 1.75 o -13 1 1 409.02 401.06 7.31 o -11 1 1 0.01 2.88 0.63 o -9 1 1 1805.50 1964.41 29.64 o -7 1 1 605.72 609.68 7.87 o -5 1 1 562.30 596.65 7.67 o -3 1 1 1648.91 1786.62 24.43 o -1 1 1 1549.34 982.99 42.86 o 1 1 1 226.06 117.40 5.44 o 3 1 1 656.86 591.31 5.63 o 5 1 1 46.45 41.69 0.64 o 7 1 1 686.93 673.23 7.69 o 9 1 1 282.84 230.78 2.96 o 11 1 1 8.27 8.96 1.08 o 13 1 1 34.99 34.96 2.07 o 15 1 1 48.60 44.45 2.72 o 17 1 1 314.09 311.96 9.96 o -18 2 1 14.58 20.76 4.44 o -16 2 1 220.29 227.50 5.99 o -14 2 1 1886.68 1918.44 27.10 o -12 2 1 98.47 81.20 2.04 o -10 2 1 1995.53 2137.75 36.98 o -8 2 1 96.22 136.97 5.52 o -6 2 1 6385.52 6585.36 70.14 o -4 2 1 9017.65 9125.01 104.32 o -2 2 1 5406.27 5583.72 49.30 o 0 2 1 0.91 0.28 0.17 o 2 2 1 11.52 6.96 0.63 o 4 2 1 11254.07 11693.21 102.10 o 6 2 1 326.85 317.99 3.66 o 8 2 1 1131.26 1123.74 12.54 o 10 2 1 937.97 927.11 10.71 o 12 2 1 1977.00 1930.13 27.21 o 14 2 1 0.14 4.54 1.60 o 16 2 1 108.58 111.20 5.36 o -17 3 1 3.24 3.91 4.16 o -15 3 1 13.22 12.74 1.69 o -13 3 1 1315.76 1294.45 18.59 o -11 3 1 1.75 1.67 0.66 o -9 3 1 0.25 1.48 0.78 o -7 3 1 1046.95 1217.22 13.45 o -5 3 1 2712.95 3032.87 34.81 o -3 3 1 116.33 91.70 1.48 o -1 3 1 11.10 7.93 0.29 o 1 3 1 3644.20 3591.57 29.40 o 3 3 1 8866.66 9052.42 91.19 o 5 3 1 3933.29 4380.79 44.30 o 7 3 1 53.45 42.97 1.19 o 9 3 1 25.03 35.47 0.94 o 11 3 1 405.49 355.97 6.84 o 13 3 1 2.35 0.53 1.19 o 15 3 1 219.35 224.66 6.04 o 17 3 1 4.46 4.24 2.60 o -16 4 1 26.81 27.89 3.04 o -14 4 1 115.67 120.24 4.57 o -12 4 1 1084.46 1038.76 15.12 o -10 4 1 2845.34 2753.21 32.00 o -8 4 1 431.58 418.92 5.06 o -6 4 1 494.24 544.40 6.37 o -4 4 1 2690.74 2695.86 29.15 o -2 4 1 438.96 513.54 4.70 o 0 4 1 2010.12 2069.59 17.70 o 2 4 1 14.25 26.22 0.78 o 4 4 1 5122.54 5846.30 62.63 o 6 4 1 1263.03 1239.43 14.79 o 8 4 1 551.68 544.87 6.20 o 10 4 1 257.78 225.30 3.49 o 12 4 1 896.61 874.94 14.77 o 14 4 1 13.61 10.56 1.78 o 16 4 1 1.87 0.66 2.37 o -15 5 1 43.18 45.20 2.58 o -13 5 1 8.58 8.61 1.23 o -11 5 1 21.22 24.73 1.33 o -9 5 1 26.59 35.07 1.12 o -7 5 1 66.81 51.10 1.58 o -5 5 1 444.47 432.82 4.74 o -3 5 1 2171.04 2394.59 24.71 o -1 5 1 556.14 618.38 5.71 o 1 5 1 54.59 60.67 1.14 o 3 5 1 371.65 338.74 3.51 o 5 5 1 1206.23 1204.08 12.80 o 7 5 1 823.30 956.52 11.78 o 9 5 1 769.40 743.12 8.92 o 11 5 1 720.55 704.82 12.15 o 13 5 1 466.89 459.91 10.03 o 15 5 1 78.54 74.30 4.54 o -16 6 1 132.43 116.10 11.67 o -14 6 1 69.07 84.74 3.42 o -12 6 1 129.55 125.19 4.65 o -10 6 1 1.11 -0.18 0.83 o -8 6 1 144.82 137.91 2.63 o -6 6 1 253.76 236.36 3.29 o -4 6 1 34.96 32.24 1.01 o -2 6 1 1479.99 1669.41 14.58 o 0 6 1 463.05 568.66 5.88 o 2 6 1 195.31 137.13 1.92 o 4 6 1 133.35 115.78 2.14 o 6 6 1 59.86 56.04 1.37 o 8 6 1 21.81 18.94 1.20 o 10 6 1 591.53 607.69 8.18 o 12 6 1 149.38 160.12 4.18 o 14 6 1 0.17 1.01 2.37 o -15 7 1 83.94 97.20 5.49 o -13 7 1 4.55 4.36 3.07 o -11 7 1 20.79 10.87 1.47 o -9 7 1 132.03 99.55 2.44 o -7 7 1 1039.73 1096.87 12.91 o -5 7 1 1464.49 1565.41 15.82 o -3 7 1 760.72 797.73 9.01 o -1 7 1 3640.48 3840.73 34.24 o 1 7 1 102.48 124.00 1.89 o 3 7 1 94.30 92.28 1.67 o 5 7 1 775.50 784.01 8.93 o 7 7 1 48.16 33.54 1.50 o 9 7 1 31.10 15.88 1.60 o 11 7 1 217.57 224.86 6.11 o 13 7 1 85.97 90.39 5.16 o -14 8 1 719.99 820.78 21.14 o -12 8 1 21.82 15.55 2.85 o -10 8 1 168.48 179.81 4.60 o -8 8 1 389.83 457.43 7.88 o -6 8 1 123.67 130.69 3.40 o -4 8 1 1104.65 1105.01 13.10 o -2 8 1 754.99 754.25 7.85 o 0 8 1 1460.72 1523.16 15.50 o 2 8 1 479.29 484.15 5.65 o 4 8 1 417.19 399.32 5.57 o 6 8 1 86.10 41.22 2.31 o 8 8 1 3.00 -1.13 1.24 o 10 8 1 7.88 5.92 1.92 o 12 8 1 17.48 20.82 3.30 o -13 9 1 173.17 201.92 8.14 o -11 9 1 79.36 76.12 7.45 o -9 9 1 46.70 43.55 3.46 o -7 9 1 104.00 83.09 3.01 o -5 9 1 448.10 443.23 7.25 o -3 9 1 22.69 7.12 2.15 o -1 9 1 8.55 5.38 0.94 o 1 9 1 13.76 8.56 1.04 o 3 9 1 3.90 2.58 1.27 o 5 9 1 47.34 29.72 2.10 o 7 9 1 151.61 159.28 4.73 o 9 9 1 194.41 182.10 5.16 o 11 9 1 28.19 26.40 3.72 o -10 10 1 0.00 0.37 2.79 o -8 10 1 9.47 11.25 2.16 o -6 10 1 1.73 0.58 1.73 o -4 10 1 128.42 113.07 3.64 o -2 10 1 34.18 33.09 2.44 o 0 10 1 66.27 75.76 3.19 o 2 10 1 63.63 52.95 5.46 o 4 10 1 67.19 55.72 3.22 o 6 10 1 15.28 7.76 2.05 o 8 10 1 46.55 35.51 2.80 o 10 10 1 138.68 156.72 14.60 o -9 11 1 7.24 13.50 7.11 o -7 11 1 9.82 10.52 2.82 o -5 11 1 1.36 -1.02 2.31 o -3 11 1 385.42 441.56 17.08 o -1 11 1 79.00 76.37 5.32 o 1 11 1 0.07 -1.03 2.80 o 3 11 1 39.35 27.41 3.87 o 5 11 1 138.60 151.42 6.03 o 7 11 1 76.29 98.43 5.04 o 9 11 1 109.05 154.49 7.68 o -6 12 1 113.31 112.67 6.87 o -4 12 1 623.85 705.68 19.84 o -2 12 1 86.87 77.72 5.60 o 0 12 1 51.76 45.96 4.75 o 2 12 1 27.63 34.14 4.47 o 4 12 1 401.02 447.61 14.34 o 6 12 1 2.13 3.36 4.76 o -18 0 2 748.76 808.77 28.38 o -16 0 2 2035.70 2078.89 46.46 o -14 0 2 65.53 58.94 3.13 o -12 0 2 1890.75 1898.21 31.26 o -10 0 2 3617.38 3876.48 87.32 o -8 0 2 534.83 462.92 10.57 o -6 0 2 6005.20 6375.58 154.85 o 0 0 2 15001.03 9402.68 610.99 o 2 0 2 37699.53 35579.94 619.24 o 4 0 2 4557.49 4339.85 53.80 o 6 0 2 1743.93 1890.26 33.57 o 8 0 2 0.70 3.31 1.99 o 10 0 2 153.57 143.07 3.21 o 12 0 2 2326.18 2217.83 97.40 o 14 0 2 3170.02 3114.15 106.64 o 16 0 2 768.09 790.04 28.20 o -17 1 2 314.50 320.64 7.69 o -15 1 2 169.57 163.69 3.98 o -13 1 2 0.17 -0.65 0.89 o -11 1 2 507.72 536.20 8.05 o -9 1 2 231.67 229.56 3.72 o -7 1 2 123.23 91.30 1.48 o -5 1 2 160.19 192.38 2.93 o -3 1 2 5859.31 5607.25 107.23 o -1 1 2 9081.17 8307.52 113.62 o 1 1 2 5454.73 5354.05 50.80 o 3 1 2 3848.07 3712.45 29.05 o 5 1 2 202.81 204.91 2.26 o 7 1 2 715.24 726.51 7.41 o 9 1 2 68.15 61.77 1.57 o 11 1 2 110.94 111.27 3.06 o 13 1 2 448.76 427.60 8.14 o 15 1 2 12.39 11.58 2.61 o 17 1 2 120.56 129.78 6.31 o -18 2 2 31.63 31.08 3.23 o -16 2 2 32.31 40.36 3.64 o -14 2 2 23.56 25.68 1.38 o -12 2 2 252.84 224.81 6.76 o -10 2 2 191.53 181.78 2.93 o -8 2 2 12.45 20.28 0.79 o -6 2 2 7.90 2.58 0.61 o -4 2 2 275.29 263.14 4.21 o -2 2 2 5027.11 5295.57 44.93 o 0 2 2 727.40 642.26 5.40 o 2 2 2 42469.93 41757.10 362.87 o 4 2 2 1252.05 1214.28 11.97 o 6 2 2 2552.04 2557.99 24.73 o 8 2 2 339.36 337.85 3.80 o 10 2 2 4.16 4.56 0.84 o 12 2 2 213.63 211.33 4.74 o 14 2 2 592.03 602.10 13.28 o 16 2 2 0.40 2.03 3.96 o -17 3 2 104.56 103.80 5.02 o -15 3 2 117.59 111.32 5.11 o -13 3 2 6.40 6.73 1.05 o -11 3 2 627.73 617.43 9.17 o -9 3 2 1031.47 1086.43 15.37 o -7 3 2 88.12 77.17 1.49 o -5 3 2 1401.40 1306.27 15.31 o -3 3 2 3661.40 3824.05 35.03 o -1 3 2 163.86 145.21 1.44 o 1 3 2 116.68 110.96 1.31 o 3 3 2 29232.16 30479.16 307.36 o 5 3 2 1323.87 1381.25 14.33 o 7 3 2 1808.39 1792.18 18.53 o 9 3 2 0.58 2.14 0.70 o 11 3 2 12.40 7.53 1.15 o 13 3 2 127.64 126.79 3.62 o 15 3 2 61.32 60.94 4.12 o -16 4 2 18.84 16.72 2.48 o -14 4 2 628.66 596.30 11.87 o -12 4 2 84.23 75.34 3.20 o -10 4 2 2117.44 2073.73 29.04 o -8 4 2 0.86 0.39 0.61 o -6 4 2 928.44 1020.88 13.25 o -4 4 2 3847.81 4200.89 42.58 o -2 4 2 2078.02 2068.53 18.66 o 0 4 2 4.73 9.51 0.60 o 2 4 2 5614.96 6249.80 54.75 o 4 4 2 2822.02 3225.61 34.93 o 6 4 2 104.07 103.43 2.46 o 8 4 2 238.74 213.99 4.50 o 10 4 2 2698.56 2583.22 30.41 o 12 4 2 354.72 346.66 6.89 o 14 4 2 151.82 158.43 4.92 o 16 4 2 85.89 103.46 5.60 o -17 5 2 114.73 105.91 5.30 o -15 5 2 45.71 45.04 3.75 o -13 5 2 293.85 267.55 5.49 o -11 5 2 385.39 415.73 6.64 o -9 5 2 18.37 16.37 0.75 o -7 5 2 160.69 163.86 2.95 o -5 5 2 912.18 983.74 10.57 o -3 5 2 539.92 494.76 5.68 o -1 5 2 4602.64 4856.10 41.06 o 1 5 2 2897.52 3060.32 28.42 o 3 5 2 93.90 120.97 1.61 o 5 5 2 313.08 368.22 7.19 o 7 5 2 47.89 54.59 1.53 o 9 5 2 2748.43 2518.96 41.02 o 11 5 2 1899.32 1901.74 33.81 o 13 5 2 41.20 47.60 2.73 o 15 5 2 4.87 7.33 2.68 o -16 6 2 0.44 4.60 2.48 o -14 6 2 113.81 104.55 3.64 o -12 6 2 6.60 3.69 1.13 o -10 6 2 1166.80 1173.49 13.55 o -8 6 2 191.16 218.07 3.28 o -6 6 2 127.85 175.03 2.67 o -4 6 2 896.89 1025.94 11.55 o -2 6 2 86.02 74.80 1.24 o 0 6 2 11.21 16.88 0.76 o 2 6 2 657.02 721.32 7.28 o 4 6 2 4.00 0.97 0.61 o 6 6 2 57.16 65.64 1.55 o 8 6 2 313.84 304.18 4.43 o 10 6 2 0.21 2.11 1.06 o 12 6 2 118.39 128.21 4.85 o 14 6 2 208.56 234.48 8.74 o -15 7 2 89.86 97.86 5.31 o -13 7 2 3.77 0.99 2.12 o -11 7 2 43.54 44.46 2.97 o -9 7 2 213.94 216.05 3.72 o -7 7 2 1087.08 1021.90 12.07 o -5 7 2 58.26 69.32 1.65 o -3 7 2 265.46 270.27 3.75 o -1 7 2 407.54 441.81 4.67 o 1 7 2 79.46 75.05 1.56 o 3 7 2 353.16 329.50 3.81 o 5 7 2 205.58 209.12 3.45 o 7 7 2 1368.17 1257.90 14.75 o 9 7 2 109.58 144.39 3.39 o 11 7 2 13.67 14.30 1.78 o 13 7 2 12.45 14.49 3.08 o -14 8 2 39.21 42.83 4.06 o -12 8 2 12.63 17.04 2.12 o -10 8 2 48.12 64.12 2.67 o -8 8 2 0.93 3.97 1.30 o -6 8 2 105.17 100.40 2.55 o -4 8 2 5.28 2.45 1.04 o -2 8 2 249.33 217.03 2.96 o 0 8 2 536.74 533.83 6.12 o 2 8 2 0.00 -1.07 0.71 o 4 8 2 0.57 -0.53 0.94 o 6 8 2 90.70 54.20 2.13 o 8 8 2 66.81 74.01 4.03 o 10 8 2 62.01 54.77 3.24 o 12 8 2 65.68 68.99 4.75 o -13 9 2 11.11 5.94 3.11 o -11 9 2 0.90 -2.43 2.30 o -9 9 2 39.29 58.25 2.96 o -7 9 2 656.62 578.50 9.75 o -5 9 2 724.56 746.23 12.69 o -3 9 2 844.71 830.83 11.94 o -1 9 2 506.08 494.68 5.64 o 1 9 2 3.30 4.47 0.91 o 3 9 2 251.99 261.52 5.40 o 5 9 2 78.00 58.16 2.55 o 7 9 2 88.11 89.05 3.68 o 9 9 2 6.15 4.54 1.89 o 11 9 2 36.26 36.51 3.94 o -10 10 2 127.61 147.80 8.03 o -8 10 2 0.04 -2.26 1.71 o -6 10 2 39.07 41.48 2.69 o -4 10 2 26.79 18.34 2.24 o -2 10 2 1.00 2.47 1.72 o 0 10 2 23.95 30.33 2.11 o 2 10 2 125.95 98.47 5.99 o 4 10 2 5.98 6.46 2.24 o 6 10 2 44.75 59.86 5.58 o 8 10 2 157.70 159.25 5.14 o 10 10 2 0.91 1.81 5.25 o -9 11 2 2.67 -0.09 3.42 o -7 11 2 0.73 -1.40 2.37 o -5 11 2 315.85 321.87 9.01 o -3 11 2 303.14 314.25 8.83 o -1 11 2 29.21 28.24 3.84 o 1 11 2 13.82 17.95 3.62 o 3 11 2 73.73 70.13 5.15 o 5 11 2 159.91 184.71 6.65 o 7 11 2 0.10 -1.18 2.43 o -6 12 2 130.01 131.82 7.42 o -4 12 2 0.64 0.83 3.47 o -2 12 2 91.26 85.31 5.92 o 0 12 2 0.39 0.66 3.16 o 2 12 2 5.91 11.98 4.33 o 4 12 2 1.38 -4.67 3.11 o -17 1 3 118.74 131.88 4.33 o -15 1 3 3.28 4.63 1.23 o -13 1 3 108.04 106.58 2.23 o -11 1 3 15.05 24.32 2.09 o -9 1 3 5.80 4.90 0.54 o -7 1 3 1838.30 1966.16 39.12 o -5 1 3 2809.89 2833.18 34.99 o -3 1 3 37960.97 36471.28 629.11 o -1 1 3 8323.07 7880.51 66.65 o 1 1 3 29601.81 28697.97 240.24 o 3 1 3 2079.63 2067.01 18.28 o 5 1 3 37.70 36.44 0.69 o 7 1 3 52.74 71.48 1.26 o 9 1 3 1257.41 1289.17 16.02 o 11 1 3 396.94 389.01 7.34 o 13 1 3 126.59 134.73 4.48 o 15 1 3 946.46 943.58 23.09 o -18 2 3 191.99 184.42 6.82 o -16 2 3 1.75 1.05 1.39 o -14 2 3 543.30 543.65 8.25 o -12 2 3 1310.60 1321.89 20.73 o -10 2 3 900.79 890.59 12.62 o -8 2 3 2382.22 2602.70 39.64 o -6 2 3 990.77 987.83 20.67 o -4 2 3 1488.28 1532.42 35.00 o -2 2 3 522.53 513.93 4.73 o 0 2 3 12436.17 11767.29 98.94 o 2 2 3 15126.44 15072.64 127.11 o 4 2 3 4493.47 4664.14 42.70 o 6 2 3 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