#------------------------------------------------------------------------------ #$Date: 2012-09-11 12:26:43 +0300 (Tue, 11 Sep 2012) $ #$Revision: 66590 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/53/2235304.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2235304_Fobs loop_ _publ_author_name 'Najafi, Ezzatollah' 'Amini, Mostafa M.' 'Ng, Seik Weng' _publ_section_title ; 2-[(Propan-2-yloxy)carbonyl]quinolin-1-ium tetrachlorido(quinoline-2-carboxylato-\k^2^N,O)stannate(IV) ; _journal_coeditor_code XU5530 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m732 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 95.156 _cell_angle_gamma 90.000 _cell_length_a 7.1932 _cell_length_b 17.8616 _cell_length_c 19.1963 _exptl_crystal_F_000 1288.00 _reflns_d_resolution_high 0.7681 _[local]_cod_data_source_file xu5530Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 276.22 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 44996.58 42644.86 196.16 o 2 0 0 42463.48 40549.01 336.19 o 3 0 0 31237.80 30496.36 264.37 o 4 0 0 25463.86 24606.34 322.17 o 5 0 0 556.24 540.57 40.84 o 6 0 0 964.74 827.48 70.46 o 7 0 0 0.08 9.90 23.61 o 8 0 0 37.49 -51.03 52.03 o 9 0 0 945.86 1112.20 155.36 o 1 1 0 531.55 508.41 15.00 o 2 1 0 1.81 14.43 4.30 o 3 1 0 1657.32 1518.73 35.26 o 4 1 0 14400.08 14187.24 125.17 o 5 1 0 8806.21 9063.10 116.32 o 6 1 0 2981.33 3030.28 76.52 o 7 1 0 2638.41 2670.05 85.03 o 8 1 0 1826.45 1927.44 135.44 o 9 1 0 74.19 59.08 39.87 o 0 2 0 7451.92 7132.36 106.96 o 1 2 0 5.64 45.72 36.63 o 2 2 0 18768.86 18908.39 127.84 o 3 2 0 5176.74 5159.44 60.76 o 4 2 0 154.49 130.55 16.51 o 5 2 0 1589.34 1637.03 46.57 o 6 2 0 2030.80 1957.52 59.73 o 7 2 0 2868.59 2761.19 82.25 o 8 2 0 5.38 3.81 26.24 o 9 2 0 203.52 233.11 53.96 o 1 3 0 4126.71 4228.06 83.06 o 2 3 0 8414.39 8333.40 155.50 o 3 3 0 30267.56 29616.67 197.53 o 4 3 0 2040.62 1941.16 51.11 o 5 3 0 12569.10 12321.87 239.24 o 6 3 0 10423.13 10345.75 144.47 o 7 3 0 3105.16 3068.55 121.26 o 8 3 0 6497.31 6094.88 239.30 o 9 3 0 1838.05 2102.64 230.82 o 0 4 0 2747.95 2781.40 49.20 o 1 4 0 6114.16 5748.98 78.41 o 2 4 0 21548.17 20464.90 123.61 o 3 4 0 8111.76 7951.08 105.08 o 4 4 0 61.05 54.46 11.54 o 5 4 0 3947.52 3561.67 107.77 o 6 4 0 655.61 677.22 45.36 o 7 4 0 249.16 196.56 36.91 o 8 4 0 60.85 28.12 31.35 o 9 4 0 107.05 131.64 68.55 o 1 5 0 1.13 6.53 8.69 o 2 5 0 69.31 76.40 10.23 o 3 5 0 119.41 146.16 13.47 o 4 5 0 1584.34 1592.68 50.83 o 5 5 0 8.30 29.75 15.00 o 6 5 0 1689.12 1862.58 72.17 o 7 5 0 1936.39 1796.86 94.98 o 8 5 0 430.81 427.83 53.43 o 9 5 0 407.16 218.63 94.14 o 0 6 0 6820.81 6727.31 118.16 o 1 6 0 16.14 15.80 5.06 o 2 6 0 105.95 106.06 17.10 o 3 6 0 2865.69 2948.09 47.00 o 4 6 0 551.94 540.56 28.30 o 5 6 0 1832.77 1909.56 71.14 o 6 6 0 2.71 -16.46 16.46 o 7 6 0 243.54 279.17 40.34 o 8 6 0 5.52 -64.38 64.38 o 9 6 0 0.80 -54.61 54.61 o 1 7 0 6.60 22.06 7.08 o 2 7 0 120.28 235.71 22.39 o 3 7 0 9963.84 10247.67 403.76 o 4 7 0 43.28 58.46 10.76 o 5 7 0 1925.04 2051.00 60.64 o 6 7 0 3572.67 3672.41 93.78 o 7 7 0 3149.99 3352.07 124.46 o 8 7 0 2163.99 1912.35 145.82 o 0 8 0 7205.45 7893.67 147.54 o 1 8 0 19294.70 19125.77 150.72 o 2 8 0 32960.51 31493.24 670.35 o 3 8 0 1870.47 1983.83 58.06 o 4 8 0 4.49 2.92 19.87 o 5 8 0 3860.66 3868.64 72.61 o 6 8 0 2878.50 2840.72 75.66 o 7 8 0 5.66 -10.64 28.35 o 8 8 0 346.82 340.60 74.12 o 1 9 0 1705.87 1778.87 42.43 o 2 9 0 3362.88 3380.51 105.39 o 3 9 0 837.68 774.29 41.92 o 4 9 0 2578.91 2394.41 149.91 o 5 9 0 6340.49 6159.49 223.81 o 6 9 0 3785.66 3655.38 130.24 o 7 9 0 457.54 383.85 70.25 o 8 9 0 148.23 61.23 115.22 o 0 10 0 3.27 18.04 10.91 o 1 10 0 7.61 6.17 7.32 o 2 10 0 5933.84 5992.24 132.38 o 3 10 0 5077.47 5311.47 116.46 o 4 10 0 268.52 286.24 53.33 o 5 10 0 87.43 76.95 35.42 o 6 10 0 1960.84 1976.57 168.13 o 7 10 0 3566.02 3412.36 197.00 o 8 10 0 196.13 86.47 82.09 o 1 11 0 7707.64 7892.80 95.31 o 2 11 0 1057.83 1060.48 27.49 o 3 11 0 49.75 45.35 25.02 o 4 11 0 4589.52 4534.42 83.71 o 5 11 0 5965.52 5831.44 425.64 o 6 11 0 1993.05 1994.36 144.82 o 7 11 0 2694.98 2623.80 176.74 o 8 11 0 3013.84 3074.24 214.53 o 0 12 0 37900.13 36686.87 620.62 o 1 12 0 20205.47 19959.46 170.88 o 2 12 0 1670.26 1617.99 37.68 o 3 12 0 13952.51 14178.89 217.13 o 4 12 0 15265.53 15143.93 186.38 o 5 12 0 1111.84 1052.79 103.11 o 6 12 0 308.27 289.58 66.71 o 7 12 0 82.52 -3.86 47.68 o 1 13 0 112.23 109.98 15.46 o 2 13 0 27.82 28.77 7.89 o 3 13 0 47.35 19.32 17.46 o 4 13 0 48.24 48.24 37.11 o 5 13 0 454.73 539.24 110.06 o 6 13 0 15.20 12.92 43.86 o 7 13 0 218.49 127.47 54.21 o 0 14 0 9952.45 9852.50 281.23 o 1 14 0 7407.60 7585.06 115.93 o 2 14 0 3462.41 3406.64 62.59 o 3 14 0 712.21 662.48 54.61 o 4 14 0 1851.04 2018.91 83.55 o 5 14 0 96.07 153.91 50.56 o 6 14 0 4.26 -42.48 42.48 o 7 14 0 616.12 607.47 213.89 o 1 15 0 1751.60 1933.98 67.58 o 2 15 0 2542.48 2519.20 56.80 o 3 15 0 8256.15 7914.12 188.65 o 4 15 0 9375.66 9830.51 194.05 o 5 15 0 8198.58 8183.66 302.07 o 6 15 0 4275.78 4927.92 251.29 o 7 15 0 3961.35 4174.60 246.01 o 0 16 0 3118.64 3011.68 138.64 o 1 16 0 2752.90 2755.09 75.16 o 2 16 0 382.43 431.07 31.29 o 3 16 0 1119.41 1087.42 75.50 o 4 16 0 2319.86 2328.36 159.09 o 5 16 0 296.73 211.54 75.19 o 6 16 0 266.49 344.05 171.22 o 1 17 0 423.99 472.55 33.65 o 2 17 0 1979.74 2001.54 68.67 o 3 17 0 253.00 193.22 38.78 o 4 17 0 671.07 628.44 168.22 o 5 17 0 932.07 1004.18 116.82 o 6 17 0 417.97 597.65 99.25 o 0 18 0 2784.79 2663.11 216.68 o 1 18 0 5299.17 5236.29 127.54 o 2 18 0 4165.74 4244.36 154.94 o 3 18 0 839.35 821.28 71.01 o 4 18 0 2090.19 2247.99 165.80 o 5 18 0 2060.18 1763.38 155.55 o 1 19 0 758.82 653.16 64.60 o 2 19 0 1251.89 1334.37 91.01 o 3 19 0 3455.83 3471.94 146.55 o 4 19 0 1281.69 1135.31 120.87 o 5 19 0 67.65 46.67 46.95 o 0 20 0 209.60 218.71 45.94 o 1 20 0 555.95 556.16 67.69 o 2 20 0 4507.89 4553.23 171.45 o 3 20 0 1000.12 1080.32 170.83 o 4 20 0 193.39 189.96 100.12 o 1 21 0 442.06 393.61 54.20 o 2 21 0 285.04 252.97 48.40 o 3 21 0 290.32 466.42 82.67 o 4 21 0 479.68 412.76 105.68 o 0 22 0 2290.15 2060.23 222.42 o 1 22 0 1150.18 957.17 156.54 o 2 22 0 2069.57 2087.02 129.01 o 3 22 0 1654.15 1610.06 145.89 o 1 23 0 1131.57 1141.80 122.99 o -9 1 1 275.75 311.35 64.30 o -8 1 1 2182.10 2140.25 286.76 o -7 1 1 3119.06 2984.95 88.82 o -6 1 1 2573.54 2526.60 69.50 o -5 1 1 12597.40 12305.29 144.10 o -4 1 1 19692.81 19143.67 146.22 o -3 1 1 1511.17 1453.37 33.90 o -2 1 1 67143.70 63431.73 212.17 o -1 1 1 9470.67 9615.53 103.25 o 1 1 1 5879.13 6051.12 83.02 o 2 1 1 134.58 159.54 8.32 o 3 1 1 1893.93 1965.94 38.95 o 4 1 1 1726.75 1761.11 45.51 o 5 1 1 2725.19 2695.61 62.93 o 6 1 1 3283.94 3318.81 110.15 o 7 1 1 3224.22 3218.22 99.07 o 8 1 1 2690.85 2873.83 165.57 o 9 1 1 2530.30 2447.27 165.01 o -9 2 1 594.16 568.46 83.39 o -8 2 1 2507.90 2453.31 113.49 o -7 2 1 2239.86 2177.61 71.68 o -6 2 1 1539.30 1506.20 51.68 o -5 2 1 24.89 18.25 9.33 o -4 2 1 9071.25 9349.22 95.61 o -3 2 1 6537.20 6417.41 66.07 o -2 2 1 31623.31 31885.29 215.59 o -1 2 1 9780.81 10018.15 108.63 o 0 2 1 56081.23 49140.33 338.25 o 1 2 1 67346.43 60071.61 311.96 o 2 2 1 453.11 552.82 14.78 o 3 2 1 29512.81 28687.83 132.25 o 4 2 1 29067.26 27732.91 281.82 o 5 2 1 7049.07 7176.33 99.30 o 6 2 1 1553.12 1452.27 52.96 o 7 2 1 1301.53 1242.02 57.29 o 8 2 1 1009.16 1054.54 76.97 o 9 2 1 4.82 -24.52 39.65 o -9 3 1 237.34 188.32 80.77 o -8 3 1 2866.83 2585.17 119.14 o -7 3 1 3163.54 3471.21 184.49 o -6 3 1 5282.83 5141.63 81.37 o -5 3 1 238.61 196.21 15.13 o -4 3 1 20335.28 20757.93 206.01 o -3 3 1 858.08 810.68 33.41 o -2 3 1 7654.19 8175.24 136.23 o -1 3 1 7464.94 7526.53 73.14 o 0 3 1 6111.68 6022.70 56.71 o 1 3 1 7610.56 7458.72 149.44 o 2 3 1 1242.97 1160.71 25.08 o 3 3 1 184.10 190.52 10.91 o 4 3 1 3071.41 2972.68 54.37 o 5 3 1 2564.01 2542.41 56.20 o 6 3 1 546.27 538.05 30.64 o 7 3 1 470.17 443.66 51.32 o 8 3 1 774.38 743.82 68.00 o 9 3 1 235.63 244.94 94.04 o -9 4 1 56.78 -71.25 71.25 o -8 4 1 1657.41 1571.58 94.50 o -7 4 1 5032.43 4946.81 153.51 o -6 4 1 2755.95 2579.68 91.86 o -5 4 1 2167.92 2031.33 68.73 o -4 4 1 552.05 536.52 29.35 o -3 4 1 10900.35 11277.85 162.97 o -2 4 1 10253.64 10915.78 92.43 o -1 4 1 3480.94 3433.15 44.46 o 0 4 1 5935.62 6081.16 80.10 o 1 4 1 5224.07 5256.67 110.57 o 2 4 1 118.83 128.55 9.62 o 3 4 1 4385.95 4252.51 66.66 o 4 4 1 15076.98 14620.25 199.24 o 5 4 1 479.37 411.74 32.24 o 6 4 1 119.41 118.46 22.57 o 7 4 1 72.38 49.06 25.79 o 8 4 1 375.45 279.42 55.65 o 9 4 1 1165.78 1175.67 175.71 o -9 5 1 1703.29 1950.25 230.55 o -8 5 1 696.46 829.98 71.47 o -7 5 1 6330.59 6328.89 173.85 o -6 5 1 1237.91 1235.07 59.68 o -5 5 1 11353.44 11391.41 157.21 o -4 5 1 2217.48 2036.94 58.54 o -3 5 1 18626.01 18486.25 250.28 o -2 5 1 15233.73 15117.35 149.12 o -1 5 1 433.69 545.89 17.90 o 0 5 1 1123.05 969.36 23.61 o 1 5 1 8633.43 9008.50 125.83 o 2 5 1 1218.13 1258.45 67.47 o 3 5 1 6622.66 6530.66 81.39 o 4 5 1 1429.37 1459.24 46.11 o 5 5 1 5.89 15.66 11.37 o 6 5 1 9985.64 10032.86 301.33 o 7 5 1 4784.78 5020.47 156.76 o 8 5 1 1526.31 1514.74 94.66 o 9 5 1 1956.77 2190.97 247.25 o -9 6 1 2122.90 2410.45 260.66 o -8 6 1 927.69 949.29 101.07 o -7 6 1 15.52 10.42 20.56 o -6 6 1 963.62 995.79 52.26 o -5 6 1 158.59 144.95 21.46 o -4 6 1 715.87 707.89 33.04 o -3 6 1 2181.97 2045.09 45.08 o -2 6 1 20277.38 20464.09 160.54 o -1 6 1 20452.57 20304.48 104.63 o 0 6 1 826.81 1017.94 26.38 o 1 6 1 4869.80 4656.52 50.66 o 2 6 1 63240.97 61355.36 488.88 o 3 6 1 8372.63 8668.25 118.98 o 4 6 1 277.57 324.55 30.80 o 5 6 1 3168.93 3073.76 80.02 o 6 6 1 7670.78 7543.66 139.84 o 7 6 1 525.33 433.78 64.77 o 8 6 1 36.22 -42.33 42.33 o -8 7 1 23.64 11.56 37.68 o -7 7 1 369.71 317.32 42.68 o -6 7 1 3747.21 3826.92 96.52 o -5 7 1 1726.50 1727.84 72.21 o -4 7 1 73.06 50.24 9.21 o -3 7 1 8267.75 8792.73 216.13 o -2 7 1 1997.34 1852.92 37.91 o -1 7 1 775.62 769.16 22.63 o 0 7 1 394.71 374.31 17.55 o 1 7 1 470.94 494.86 19.03 o 2 7 1 3136.54 3510.62 81.99 o 3 7 1 576.93 544.89 29.69 o 4 7 1 618.24 716.61 28.66 o 5 7 1 607.27 641.98 39.30 o 6 7 1 1906.20 1947.12 68.34 o 7 7 1 583.79 498.54 50.88 o 8 7 1 54.46 -12.38 36.76 o -8 8 1 416.37 565.76 88.87 o -7 8 1 1223.28 1415.78 121.33 o -6 8 1 2135.64 2048.54 65.92 o -5 8 1 376.83 395.55 31.21 o -4 8 1 0.90 10.80 10.61 o -3 8 1 3212.90 3278.44 74.34 o -2 8 1 4454.41 4118.84 117.36 o -1 8 1 583.48 614.85 23.65 o 0 8 1 101.95 120.61 11.31 o 1 8 1 14315.03 14913.93 104.94 o 2 8 1 1461.74 1431.56 60.66 o 3 8 1 1702.57 1763.03 56.83 o 4 8 1 142.13 84.82 52.93 o 5 8 1 57.01 63.87 11.20 o 6 8 1 524.73 520.36 40.82 o 7 8 1 724.10 664.27 84.87 o 8 8 1 14.78 26.01 34.51 o -8 9 1 657.99 623.54 98.97 o -7 9 1 3268.40 3245.02 267.49 o -6 9 1 2679.06 2797.33 86.30 o -5 9 1 4142.25 4184.71 184.81 o -4 9 1 5228.98 5072.13 188.03 o -3 9 1 5657.57 5873.15 113.44 o -2 9 1 3102.38 3237.90 61.14 o -1 9 1 4632.92 4504.87 80.64 o 0 9 1 4190.66 4203.20 65.63 o 1 9 1 682.98 641.82 23.93 o 2 9 1 5.05 16.93 13.32 o 3 9 1 181.47 201.03 23.14 o 4 9 1 1223.05 1072.30 89.45 o 5 9 1 4050.68 4037.50 181.64 o 6 9 1 1412.76 1479.13 75.29 o 7 9 1 1370.83 1400.36 241.53 o 8 9 1 2343.83 2151.25 163.07 o -8 10 1 1063.93 1093.33 233.06 o -7 10 1 220.09 240.15 60.16 o -6 10 1 160.98 146.47 46.91 o -5 10 1 353.38 311.31 89.51 o -4 10 1 1223.61 1163.94 96.20 o -3 10 1 2649.56 2652.06 83.92 o -2 10 1 2006.07 2033.93 52.43 o -1 10 1 11308.79 11358.98 125.10 o 0 10 1 10149.81 9694.70 126.92 o 1 10 1 15022.10 15018.11 161.64 o 2 10 1 23396.32 23715.29 606.67 o 3 10 1 20508.64 20498.23 231.27 o 4 10 1 10106.81 10423.72 279.53 o 5 10 1 7919.12 8021.81 537.43 o 6 10 1 4112.96 4175.70 404.82 o 7 10 1 267.71 286.45 69.17 o 8 10 1 445.90 250.80 83.32 o -8 11 1 1.04 -49.17 49.17 o -7 11 1 345.64 361.63 72.10 o -6 11 1 1.64 -35.13 35.13 o -5 11 1 703.84 666.34 139.10 o -4 11 1 79.21 34.60 61.28 o -3 11 1 2642.83 2716.80 90.77 o -2 11 1 3757.55 3921.25 92.57 o -1 11 1 2385.15 2441.54 61.42 o 0 11 1 163.49 137.06 16.82 o 1 11 1 272.96 288.78 23.35 o 2 11 1 53.83 22.46 31.31 o 3 11 1 380.73 348.18 34.50 o 4 11 1 195.04 210.95 36.16 o 5 11 1 260.72 308.49 59.41 o 6 11 1 430.17 562.93 79.94 o 7 11 1 817.08 768.79 144.65 o 8 11 1 61.08 44.29 49.51 o -8 12 1 376.65 330.66 79.63 o -7 12 1 36.21 31.14 48.99 o -6 12 1 423.16 370.62 67.96 o -5 12 1 3472.92 3409.53 181.28 o -4 12 1 1463.77 1447.26 57.72 o -3 12 1 566.72 467.92 41.84 o -2 12 1 3058.70 3159.38 60.85 o -1 12 1 1756.17 1780.79 61.81 o 0 12 1 3018.79 3113.79 73.11 o 1 12 1 4440.28 4442.11 85.81 o 2 12 1 3355.27 3374.97 130.88 o 3 12 1 641.29 654.65 49.54 o 4 12 1 51.28 65.60 18.10 o 5 12 1 471.53 525.03 75.79 o 6 12 1 751.98 666.23 90.65 o 7 12 1 1240.27 1305.21 131.57 o -7 13 1 2908.01 3274.82 206.46 o -6 13 1 7725.87 7542.42 553.46 o -5 13 1 15268.69 15533.29 1019.84 o -4 13 1 10159.34 10532.43 173.30 o -3 13 1 4483.78 4630.86 131.90 o -2 13 1 6352.46 6559.43 90.77 o -1 13 1 15998.47 15882.85 204.41 o 0 13 1 9285.11 9326.25 227.68 o 1 13 1 685.83 729.85 37.62 o 2 13 1 2470.23 2413.18 42.95 o 3 13 1 2151.56 2070.80 88.73 o 4 13 1 3601.30 3868.06 108.89 o 5 13 1 6943.14 7406.98 274.48 o 6 13 1 4540.65 4889.71 239.61 o 7 13 1 1295.04 1374.97 138.63 o -7 14 1 379.85 269.98 71.53 o -6 14 1 393.58 367.74 73.40 o -5 14 1 763.17 735.47 92.64 o -4 14 1 173.12 153.43 25.97 o -3 14 1 505.21 435.98 44.76 o -2 14 1 102.70 100.48 23.42 o -1 14 1 3774.37 3866.27 91.32 o 0 14 1 18250.23 18356.32 174.13 o 1 14 1 8898.20 9088.48 151.24 o 2 14 1 61.96 67.38 11.73 o 3 14 1 2776.37 2988.40 111.22 o 4 14 1 9882.51 10615.36 192.72 o 5 14 1 2906.55 3192.20 202.48 o 6 14 1 165.06 81.18 45.87 o 7 14 1 1293.97 1235.44 136.91 o -7 15 1 1015.71 1156.98 135.46 o -6 15 1 314.26 293.80 67.96 o -5 15 1 72.56 23.02 62.55 o -4 15 1 503.14 504.71 46.70 o -3 15 1 128.18 79.13 29.59 o -2 15 1 1875.93 1908.79 54.08 o -1 15 1 24.52 24.96 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196.46 o -6 11 8 5933.74 6271.37 387.08 o -5 11 8 3314.18 1152.29 1622.94 o -4 11 8 21549.16 21184.35 336.05 o -3 11 8 7669.60 7479.80 138.06 o -2 11 8 1842.50 1817.32 69.40 o -1 11 8 3059.39 3083.67 82.84 o 0 11 8 1608.65 1559.23 65.29 o 1 11 8 228.91 237.05 25.74 o 2 11 8 4903.07 4953.05 106.53 o 3 11 8 833.57 852.98 40.54 o 4 11 8 2391.34 2552.36 94.76 o 5 11 8 8024.60 7984.86 298.19 o 6 11 8 4626.50 4479.09 236.85 o 7 11 8 2628.30 2567.99 190.33 o -7 12 8 140.01 85.82 50.17 o -6 12 8 1506.80 1497.83 134.20 o -5 12 8 131.27 22.73 12.00 o -4 12 8 2682.76 2559.21 85.18 o -3 12 8 6070.44 5980.47 178.71 o -2 12 8 12028.86 11936.90 180.07 o -1 12 8 3684.62 3608.27 91.73 o 0 12 8 4084.54 4060.87 106.78 o 1 12 8 17777.81 17193.74 352.08 o 2 12 8 11006.25 11021.55 158.89 o 3 12 8 601.50 652.19 50.69 o 4 12 8 1094.78 917.70 101.01 o 5 12 8 2659.16 2465.70 181.93 o 6 12 8 1212.60 1270.08 130.16 o 7 12 8 404.36 472.94 92.62 o -7 13 8 1054.88 1250.06 136.67 o -6 13 8 1591.29 1434.43 240.68 o -5 13 8 161.90 128.67 33.63 o -4 13 8 787.09 142.13 372.16 o -3 13 8 878.76 913.73 49.58 o -2 13 8 11.34 56.49 23.02 o -1 13 8 4.07 -7.53 13.70 o 0 13 8 337.05 354.89 30.60 o 1 13 8 0.97 9.20 13.76 o 2 13 8 501.12 505.09 61.59 o 3 13 8 29.97 71.81 24.13 o 4 13 8 1068.02 966.42 106.06 o 5 13 8 1614.18 1803.68 151.34 o 6 13 8 203.87 140.37 56.51 o -7 14 8 95.00 102.01 51.45 o -6 14 8 169.72 183.95 81.24 o -5 14 8 528.69 619.73 86.89 o -4 14 8 1474.27 1514.52 88.97 o -3 14 8 4901.53 4904.47 148.39 o -2 14 8 4998.45 4789.66 161.73 o -1 14 8 11430.90 11006.19 258.73 o 0 14 8 906.38 936.75 66.85 o 1 14 8 1539.10 1367.58 78.62 o 2 14 8 6295.58 6442.35 163.84 o 3 14 8 1896.30 2009.28 147.18 o 4 14 8 188.33 137.36 55.07 o 5 14 8 8.90 -49.28 49.28 o 6 14 8 328.23 277.30 70.74 o -6 15 8 5411.44 5571.56 272.02 o -5 15 8 2760.61 3101.35 192.69 o -4 15 8 4032.89 4368.69 153.34 o -3 15 8 8337.04 8323.82 252.65 o -2 15 8 3420.38 3330.63 117.34 o -1 15 8 942.14 849.73 54.50 o 0 15 8 9.89 1.70 16.50 o 1 15 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