#------------------------------------------------------------------------------ #$Date: 2012-09-11 12:26:43 +0300 (Tue, 11 Sep 2012) $ #$Revision: 66590 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/54/2235442.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2235442_Fobs loop_ _publ_author_name 'Lloyd, Barry A.' 'Arif, Atta M.' _publ_section_title ; Bicyclo[2.2.1]hept-2-en-7-yl 4-bromobenzoate ; _journal_coeditor_code HB6776 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2209 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 100.072 _cell_angle_gamma 90.000 _cell_length_a 14.0633 _cell_length_b 10.0488 _cell_length_c 8.6668 _exptl_crystal_F_000 592.00 _reflns_d_resolution_high 0.7705 _[local]_cod_data_source_file hb6776Isup3.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title '2OPBB @150K Clrless Prism Monoclinic P21/c 7/22/11 ama SHELXL97' _shelx_refln_list_code 4 _shelx_f_calc_maximum 214.53 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 8692.20 8496.48 267.74 o 3 0 0 3713.25 3469.89 50.02 o 4 0 0 1806.67 1714.07 25.12 o 5 0 0 2467.98 2354.13 34.85 o 6 0 0 53.36 67.38 2.65 o 7 0 0 2696.53 2580.92 38.15 o 8 0 0 3601.67 3489.76 51.80 o 9 0 0 5359.15 5071.68 74.35 o 10 0 0 5813.20 5845.87 86.76 o 11 0 0 3721.24 3840.79 58.09 o 12 0 0 1057.43 1010.21 18.62 o 13 0 0 2436.51 2502.61 36.29 o 14 0 0 349.61 311.82 10.99 o 15 0 0 1620.08 1575.27 36.91 o 16 0 0 410.11 432.71 15.54 o 17 0 0 1038.53 1103.17 45.93 o 2 1 0 43.89 52.01 4.36 o 3 1 0 2654.48 2622.39 28.38 o 4 1 0 2088.25 2066.76 21.49 o 5 1 0 3151.27 3087.44 31.78 o 6 1 0 718.15 739.81 14.08 o 7 1 0 2728.86 2833.80 31.21 o 8 1 0 974.41 993.17 11.44 o 9 1 0 156.07 165.85 3.18 o 10 1 0 160.67 172.14 4.18 o 11 1 0 21.88 21.09 2.72 o 12 1 0 1026.78 1027.99 22.61 o 13 1 0 45.40 35.59 3.50 o 14 1 0 1055.05 1043.32 19.75 o 15 1 0 5.40 4.94 3.59 o 16 1 0 330.85 337.14 9.51 o 17 1 0 3.90 9.46 7.27 o 0 2 0 17140.22 16894.67 303.15 o 1 2 0 1808.26 1776.82 18.31 o 2 2 0 3658.92 3530.77 40.17 o 3 2 0 4662.95 4562.52 51.61 o 4 2 0 6386.90 6365.87 67.55 o 5 2 0 1015.14 991.83 13.55 o 6 2 0 3463.05 3474.01 40.25 o 7 2 0 59.81 97.03 7.38 o 8 2 0 277.20 269.88 5.36 o 9 2 0 574.82 544.22 9.19 o 10 2 0 81.57 94.88 3.82 o 11 2 0 2679.62 2739.29 32.57 o 12 2 0 6.35 4.59 2.92 o 13 2 0 884.86 911.70 20.69 o 14 2 0 87.67 81.86 4.18 o 15 2 0 997.62 1009.27 20.50 o 16 2 0 7.24 7.82 6.23 o 17 2 0 208.95 188.71 9.33 o 1 3 0 9601.17 9389.10 99.75 o 2 3 0 373.06 341.67 4.54 o 3 3 0 7078.01 6991.23 70.56 o 4 3 0 716.69 658.92 8.69 o 5 3 0 348.76 269.34 6.26 o 6 3 0 5020.26 5016.13 90.48 o 7 3 0 6926.22 7434.79 95.29 o 8 3 0 4715.04 4732.68 51.44 o 9 3 0 2452.44 2445.07 28.12 o 10 3 0 5694.40 5745.77 73.36 o 11 3 0 3025.86 3001.77 39.04 o 12 3 0 2139.76 2114.41 29.98 o 13 3 0 26.75 18.86 3.55 o 14 3 0 1426.39 1448.60 34.04 o 15 3 0 197.40 186.55 6.30 o 16 3 0 1122.02 1099.12 26.48 o 17 3 0 125.30 110.81 8.71 o 0 4 0 804.73 823.18 14.68 o 1 4 0 627.56 646.15 10.46 o 2 4 0 1914.93 1874.15 23.25 o 3 4 0 407.72 429.08 5.22 o 4 4 0 174.45 151.93 2.63 o 5 4 0 650.46 691.29 8.34 o 6 4 0 272.43 275.71 4.82 o 7 4 0 594.49 639.84 9.87 o 8 4 0 251.87 254.23 4.76 o 9 4 0 72.50 67.35 2.92 o 10 4 0 7.90 10.51 5.68 o 11 4 0 8.03 13.66 3.55 o 12 4 0 217.81 218.56 5.73 o 13 4 0 329.08 310.42 9.66 o 14 4 0 19.03 17.50 3.91 o 15 4 0 136.40 130.91 7.57 o 16 4 0 3.31 2.44 6.52 o 17 4 0 42.56 54.64 19.87 o 1 5 0 4016.35 3965.88 43.00 o 2 5 0 2235.23 2316.63 26.51 o 3 5 0 756.53 665.51 9.67 o 4 5 0 2332.46 2309.91 26.18 o 5 5 0 1799.30 1743.28 19.05 o 6 5 0 686.37 648.83 13.86 o 7 5 0 2235.58 2297.50 25.31 o 8 5 0 681.63 702.01 9.19 o 9 5 0 2285.14 2316.77 25.92 o 10 5 0 2420.88 2484.44 35.92 o 11 5 0 576.08 603.93 9.02 o 12 5 0 1351.49 1385.75 20.67 o 13 5 0 82.85 81.57 10.22 o 14 5 0 983.72 973.90 24.49 o 15 5 0 0.69 5.05 9.08 o 16 5 0 225.25 213.75 24.99 o 0 6 0 6220.86 5879.73 85.24 o 1 6 0 77.07 74.10 4.54 o 2 6 0 12420.33 12695.92 135.36 o 3 6 0 454.67 404.99 7.35 o 4 6 0 2727.70 2879.88 35.11 o 5 6 0 559.25 534.14 7.79 o 6 6 0 771.26 747.74 18.99 o 7 6 0 1948.65 1951.54 22.01 o 8 6 0 506.60 490.87 7.35 o 9 6 0 2181.84 2268.55 25.37 o 10 6 0 73.72 78.49 3.03 o 11 6 0 1316.98 1371.09 22.24 o 12 6 0 256.80 239.58 5.01 o 13 6 0 1327.97 1362.08 24.03 o 14 6 0 122.95 105.26 7.35 o 15 6 0 406.21 338.96 23.30 o 1 7 0 155.93 168.76 3.79 o 2 7 0 1.97 1.73 8.51 o 3 7 0 199.47 232.47 5.45 o 4 7 0 186.10 208.84 10.04 o 5 7 0 229.21 227.03 5.16 o 6 7 0 106.55 106.11 3.90 o 7 7 0 9.77 11.98 4.16 o 8 7 0 5.98 10.12 2.84 o 9 7 0 8.25 6.43 2.37 o 10 7 0 0.39 0.79 2.65 o 11 7 0 107.51 100.50 3.60 o 12 7 0 9.78 9.25 3.26 o 13 7 0 14.99 11.92 4.92 o 14 7 0 1.76 3.73 9.21 o 15 7 0 33.50 22.06 8.89 o 0 8 0 3017.83 3004.38 39.06 o 1 8 0 89.10 86.98 3.79 o 2 8 0 4072.57 4188.38 48.02 o 3 8 0 684.26 671.37 10.02 o 4 8 0 1025.04 1085.20 16.06 o 5 8 0 203.24 200.70 5.32 o 6 8 0 803.94 836.74 13.09 o 7 8 0 229.08 251.76 5.90 o 8 8 0 1410.33 1483.17 20.40 o 9 8 0 295.40 295.15 10.61 o 10 8 0 27.43 22.65 2.84 o 11 8 0 876.48 914.96 19.73 o 12 8 0 14.89 14.98 8.51 o 13 8 0 1569.93 1615.00 46.76 o 14 8 0 90.74 98.80 23.28 o 1 9 0 1711.92 1813.90 22.40 o 2 9 0 328.35 311.14 10.04 o 3 9 0 378.98 376.45 7.37 o 4 9 0 33.29 42.05 3.55 o 5 9 0 1445.71 1392.99 19.97 o 6 9 0 1513.53 1508.50 23.10 o 7 9 0 57.95 60.14 6.62 o 8 9 0 2139.04 2126.30 31.63 o 9 9 0 1613.00 1660.18 31.62 o 10 9 0 154.66 156.29 6.44 o 11 9 0 6.76 12.32 4.85 o 12 9 0 315.02 299.81 14.59 o 13 9 0 68.17 61.49 10.57 o 0 10 0 95.03 82.93 7.95 o 1 10 0 24.26 23.22 2.29 o 2 10 0 97.88 87.16 7.00 o 3 10 0 53.31 43.69 4.54 o 4 10 0 0.69 -3.48 3.48 o 5 10 0 76.53 74.10 4.36 o 6 10 0 14.41 14.90 3.87 o 7 10 0 9.86 7.77 4.36 o 8 10 0 85.81 75.60 5.62 o 9 10 0 0.06 -2.09 4.90 o 10 10 0 51.08 41.98 6.73 o 11 10 0 86.41 83.27 17.22 o 1 11 0 268.54 253.54 7.40 o 2 11 0 307.28 313.79 16.10 o 3 11 0 876.00 906.23 16.50 o 4 11 0 270.90 277.49 7.90 o 5 11 0 960.04 914.21 31.51 o 6 11 0 335.30 282.66 10.04 o 7 11 0 362.98 348.60 19.51 o 8 11 0 275.77 253.27 10.65 o 9 11 0 226.57 205.86 11.63 o 0 12 0 555.06 656.35 34.12 o 1 12 0 28.29 32.93 7.82 o 2 12 0 968.52 1013.41 44.67 o 3 12 0 40.78 21.78 9.23 o 4 12 0 23.75 49.99 10.22 o 5 12 0 331.13 323.62 21.42 o 6 12 0 95.11 97.76 29.33 o 7 12 0 417.40 427.12 27.03 o 1 13 0 77.97 58.29 15.14 o -18 1 1 464.07 424.91 42.44 o -17 1 1 18.09 26.56 5.71 o -16 1 1 1660.58 1800.33 72.29 o -15 1 1 5.36 6.05 4.92 o -14 1 1 2247.46 2279.28 41.77 o -13 1 1 76.44 73.20 3.34 o -12 1 1 2415.30 2393.32 28.88 o -11 1 1 884.49 831.71 13.87 o -10 1 1 3732.89 3772.50 40.05 o -9 1 1 155.75 139.04 3.21 o -8 1 1 8284.49 8460.11 85.76 o -7 1 1 12368.11 13047.22 125.65 o -6 1 1 9311.69 9791.22 93.46 o -5 1 1 7034.97 6948.21 67.01 o -4 1 1 1016.64 983.30 10.30 o -3 1 1 5550.00 5548.97 53.44 o -2 1 1 2682.18 2640.76 24.63 o -1 1 1 174.98 183.28 2.81 o 0 1 1 1369.20 1355.36 16.96 o 1 1 1 4945.03 4825.43 46.28 o 2 1 1 2825.15 2902.54 29.76 o 3 1 1 19961.33 20463.17 192.18 o 4 1 1 4272.80 4156.99 45.22 o 5 1 1 5087.91 5030.22 51.32 o 6 1 1 4973.67 4962.99 50.46 o 7 1 1 5043.20 5206.52 53.37 o 8 1 1 4983.96 4936.51 50.55 o 9 1 1 246.51 254.29 4.46 o 10 1 1 2384.95 2407.32 27.02 o 11 1 1 3269.17 3284.63 33.65 o 12 1 1 236.59 246.46 4.34 o 13 1 1 280.68 273.75 4.69 o 14 1 1 2825.42 2901.66 35.40 o 15 1 1 19.23 25.30 5.87 o 16 1 1 1383.54 1474.26 28.83 o 17 1 1 251.19 227.19 11.90 o -17 2 1 801.41 822.46 23.24 o -16 2 1 206.37 217.72 7.82 o -15 2 1 1626.55 1676.44 25.34 o -14 2 1 5.60 6.22 3.55 o -13 2 1 1264.92 1315.12 18.56 o -12 2 1 91.12 78.42 5.30 o -11 2 1 1155.07 1140.18 14.13 o -10 2 1 1040.66 1065.60 12.77 o -9 2 1 1466.81 1345.69 14.56 o -8 2 1 1012.95 972.34 10.60 o -7 2 1 2252.80 2141.06 22.78 o -6 2 1 1003.54 942.58 10.52 o -5 2 1 3555.24 3581.74 37.16 o -4 2 1 7316.34 7281.05 77.06 o -3 2 1 594.98 585.51 6.33 o -2 2 1 7945.36 7697.71 73.23 o -1 2 1 25.45 39.69 0.95 o 0 2 1 46023.83 48194.88 860.88 o 1 2 1 664.23 675.77 6.79 o 2 2 1 4659.35 4327.53 43.76 o 3 2 1 89.67 102.06 3.98 o 4 2 1 5383.60 5222.12 59.03 o 5 2 1 833.37 771.04 9.99 o 6 2 1 1849.36 1708.25 20.62 o 7 2 1 4636.28 4833.48 56.08 o 8 2 1 1523.39 1558.04 25.18 o 9 2 1 3261.41 3154.57 37.79 o 10 2 1 900.18 898.90 12.09 o 11 2 1 1446.40 1414.04 19.21 o 12 2 1 657.06 655.50 11.38 o 13 2 1 1250.86 1220.12 15.75 o 14 2 1 9.92 7.58 4.92 o 15 2 1 1283.81 1264.54 23.56 o 16 2 1 59.91 61.61 6.82 o 17 2 1 892.37 871.65 30.54 o -17 3 1 11.42 19.34 8.40 o -16 3 1 22.88 20.41 8.33 o -15 3 1 7.79 4.79 6.05 o -14 3 1 102.19 85.46 4.53 o -13 3 1 82.52 68.10 6.25 o -12 3 1 74.37 61.24 3.78 o -11 3 1 1171.50 1163.33 27.38 o -10 3 1 1317.27 1337.32 16.76 o -9 3 1 2.36 3.59 1.87 o -8 3 1 267.24 288.80 4.64 o -7 3 1 4.33 9.65 2.08 o -6 3 1 23.34 23.15 2.46 o -5 3 1 111.80 129.18 2.80 o -4 3 1 41.29 45.34 1.89 o -3 3 1 77.39 72.90 1.73 o -2 3 1 89.15 93.63 2.27 o -1 3 1 4771.76 4844.75 47.09 o 0 3 1 1609.45 1632.67 16.54 o 1 3 1 803.80 861.35 8.79 o 2 3 1 184.85 203.76 3.00 o 3 3 1 14.25 18.02 4.54 o 4 3 1 1094.64 1155.47 14.02 o 5 3 1 795.11 898.27 12.33 o 6 3 1 299.55 302.19 5.12 o 7 3 1 781.05 816.26 11.15 o 8 3 1 9.67 8.40 2.53 o 9 3 1 53.38 49.00 3.07 o 10 3 1 94.71 94.32 3.61 o 11 3 1 2.68 5.51 2.72 o 12 3 1 23.63 27.59 3.43 o 13 3 1 7.69 1.67 3.08 o 14 3 1 92.49 79.11 3.82 o 15 3 1 24.85 31.70 8.33 o 16 3 1 20.71 11.53 5.60 o 17 3 1 5.79 17.65 8.89 o -17 4 1 1426.01 1453.44 44.87 o -16 4 1 98.57 94.91 9.27 o -15 4 1 2456.74 2524.20 38.48 o -14 4 1 6.63 7.65 3.55 o -13 4 1 1436.73 1454.54 19.99 o -12 4 1 67.43 61.83 3.01 o -11 4 1 670.22 675.43 9.68 o -10 4 1 202.16 214.53 4.82 o -9 4 1 2206.07 2169.25 24.59 o -8 4 1 330.34 329.15 5.39 o -7 4 1 2834.12 2764.73 31.55 o -6 4 1 4827.28 4705.36 50.90 o -5 4 1 2649.07 2700.46 30.11 o -4 4 1 10822.78 11157.94 111.66 o -3 4 1 237.58 195.74 6.25 o -2 4 1 12189.25 12198.55 128.30 o -1 4 1 1.30 5.05 1.18 o 0 4 1 8725.02 8572.44 85.50 o 1 4 1 1265.91 1351.08 17.20 o 2 4 1 9694.36 9383.56 93.91 o 3 4 1 87.65 74.67 5.11 o 4 4 1 13331.35 13956.19 146.62 o 5 4 1 480.11 413.47 6.54 o 6 4 1 3071.30 2951.79 32.69 o 7 4 1 4455.34 4461.65 51.89 o 8 4 1 277.59 260.24 5.08 o 9 4 1 2639.65 2652.12 35.17 o 10 4 1 14.96 15.09 3.35 o 11 4 1 2506.51 2519.15 36.56 o 12 4 1 210.74 204.27 7.76 o 13 4 1 1477.29 1461.10 21.24 o 14 4 1 32.39 42.02 4.36 o 15 4 1 1426.22 1429.84 31.27 o 16 4 1 131.59 123.71 10.03 o -16 5 1 527.80 471.49 14.86 o -15 5 1 66.58 70.55 13.81 o -14 5 1 424.79 447.81 9.17 o -13 5 1 10.52 13.51 3.59 o -12 5 1 1035.16 1038.77 14.72 o -11 5 1 74.81 77.29 3.31 o -10 5 1 2392.76 2349.14 27.19 o -9 5 1 1560.30 1518.78 19.38 o -8 5 1 2443.20 2513.11 29.23 o -7 5 1 1359.56 1381.50 16.63 o -6 5 1 1298.90 1276.23 14.86 o -5 5 1 1113.75 972.14 11.30 o -4 5 1 69.43 95.39 2.45 o -3 5 1 2192.61 2143.22 24.41 o -2 5 1 100.65 112.30 2.91 o -1 5 1 1786.40 1702.02 17.70 o 0 5 1 348.56 366.89 4.96 o 1 5 1 2057.67 1947.02 21.01 o 2 5 1 848.91 862.98 11.34 o 3 5 1 2180.97 2128.96 23.98 o 4 5 1 234.85 212.88 11.18 o 5 5 1 604.32 536.62 11.01 o 6 5 1 2018.20 2023.58 23.15 o 7 5 1 1455.40 1568.68 33.72 o 8 5 1 541.29 565.54 16.88 o 9 5 1 1061.12 1037.40 16.72 o 10 5 1 653.97 666.98 10.48 o 11 5 1 183.83 183.86 5.98 o 12 5 1 1304.14 1332.23 46.38 o 13 5 1 111.46 104.17 5.34 o 14 5 1 255.70 250.80 8.41 o 15 5 1 85.81 73.59 5.82 o 16 5 1 717.37 693.51 20.67 o -16 6 1 2.72 -1.40 13.43 o -15 6 1 131.23 126.73 12.87 o -14 6 1 51.02 44.04 5.33 o -13 6 1 238.38 229.98 5.79 o -12 6 1 29.93 23.65 3.60 o -11 6 1 297.26 303.01 6.37 o -10 6 1 212.76 213.39 4.76 o -9 6 1 23.19 25.71 5.68 o -8 6 1 458.23 489.71 15.36 o -7 6 1 490.26 494.52 7.06 o -6 6 1 621.71 612.49 8.20 o -5 6 1 23.33 33.93 1.72 o -4 6 1 2890.81 3124.42 35.80 o -3 6 1 145.67 168.21 4.09 o -2 6 1 135.37 115.47 3.18 o -1 6 1 145.33 168.40 3.18 o 0 6 1 650.21 604.65 7.51 o 1 6 1 330.39 376.16 5.45 o 2 6 1 1391.47 1374.53 16.39 o 3 6 1 105.06 127.36 4.16 o 4 6 1 936.20 1011.55 13.52 o 5 6 1 185.72 217.92 12.50 o 6 6 1 632.77 628.63 8.35 o 7 6 1 167.25 177.72 3.98 o 8 6 1 41.34 40.83 7.57 o 9 6 1 341.24 317.20 12.31 o 10 6 1 31.31 29.55 3.03 o 11 6 1 18.89 19.57 1.85 o 12 6 1 77.21 77.14 8.89 o 13 6 1 201.71 194.81 14.58 o 14 6 1 15.98 11.18 4.12 o 15 6 1 505.00 482.68 15.19 o -15 7 1 2.00 8.75 7.49 o -14 7 1 855.12 832.29 23.97 o -13 7 1 46.06 47.36 4.62 o -12 7 1 1225.35 1214.45 16.50 o -11 7 1 50.05 46.82 3.31 o -10 7 1 2339.71 2305.39 26.26 o -9 7 1 2599.39 2665.90 29.15 o -8 7 1 3245.57 3246.21 36.40 o -7 7 1 1045.74 1041.16 12.65 o -6 7 1 2901.12 2926.80 35.58 o -5 7 1 2791.12 2714.04 32.18 o -4 7 1 132.50 128.09 3.82 o -3 7 1 1469.16 1403.13 17.46 o -2 7 1 15.36 21.72 2.80 o -1 7 1 2339.75 2393.36 25.44 o 0 7 1 4.66 6.36 1.89 o 1 7 1 4234.31 4365.91 49.18 o 2 7 1 188.90 203.58 4.41 o 3 7 1 1866.01 1789.81 23.67 o 4 7 1 555.70 573.91 8.93 o 5 7 1 3357.56 3357.58 54.34 o 6 7 1 2802.83 2863.41 49.97 o 7 7 1 823.96 840.44 25.06 o 8 7 1 1517.54 1532.70 17.82 o 9 7 1 2065.47 2002.42 21.71 o 10 7 1 634.60 674.08 8.88 o 11 7 1 243.04 232.35 7.20 o 12 7 1 862.77 864.23 13.54 o 13 7 1 77.09 85.96 6.06 o 14 7 1 884.76 919.92 21.38 o -14 8 1 48.04 51.17 10.82 o -13 8 1 503.19 463.87 30.89 o -12 8 1 17.72 8.99 5.87 o -11 8 1 151.05 147.38 5.48 o -10 8 1 1.97 -0.76 2.37 o -9 8 1 92.39 100.90 4.36 o -8 8 1 184.23 172.42 5.25 o -7 8 1 378.84 381.04 15.35 o -6 8 1 116.39 114.55 4.54 o -5 8 1 336.05 330.35 6.72 o -4 8 1 162.89 173.59 11.55 o -3 8 1 607.42 588.43 11.95 o -2 8 1 1843.20 1871.08 22.73 o -1 8 1 19.33 24.10 2.65 o 0 8 1 595.06 580.98 7.64 o 1 8 1 140.36 143.38 7.57 o 2 8 1 2330.77 2411.83 29.21 o 3 8 1 34.82 25.20 7.19 o 4 8 1 154.24 146.66 4.46 o 5 8 1 211.39 203.76 4.82 o 6 8 1 292.64 295.48 6.02 o 7 8 1 197.05 187.00 10.41 o 8 8 1 219.51 211.97 18.75 o 9 8 1 1060.40 1131.48 23.93 o 10 8 1 12.26 16.64 2.29 o 11 8 1 280.89 289.86 11.36 o 12 8 1 0.15 1.48 7.09 o 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