#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:41:35 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181276 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/54/2235448.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2235448_Fobs loop_ _publ_author_name 'Parvez, Masood' 'Jalilehvand, Farideh' 'Amini, Zahra' _publ_section_title ; Tetraaquabis(thiourea-\kS)cadmium(II) triaquatris(thiourea-\kS)cadmium(II) disulfate ; _journal_coeditor_code HB6807 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m949 _journal_page_last m950 _journal_volume 68 _journal_year 2012 _space_group_IT_number 7 _symmetry_space_group_name_Hall 'P -2yc' _symmetry_space_group_name_H-M 'P 1 c 1' _cell_angle_alpha 90.000 _cell_angle_beta 98.917 _cell_angle_gamma 90.000 _cell_length_a 10.9941 _cell_length_b 11.7602 _cell_length_c 24.0100 _exptl_crystal_F_000 1848.00 _reflns_d_resolution_high 0.8409 _cod_data_source_file hb6807Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Compound X' _shelx_refln_list_code 4 _shelx_f_calc_maximum 488.12 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x, -y, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 -28 24215.95 22703.11 1152.81 o 2 0 -28 3943.57 3973.21 306.91 o 3 0 -28 13742.77 11717.05 640.28 o 1 1 -28 396.92 256.26 127.75 o 2 1 -28 640.79 579.80 133.80 o 3 1 -28 3133.10 3703.17 220.19 o 1 2 -28 1094.19 1018.71 319.38 o 2 2 -28 3452.66 3704.10 306.91 o 3 2 -28 103.29 268.99 73.82 o -2 1 -27 234.37 323.54 90.71 o -1 1 -27 724.15 769.55 120.95 o 1 1 -27 224.80 226.03 60.48 o 2 1 -27 2128.29 2730.27 381.37 o 3 1 -27 2254.36 1663.07 198.81 o 4 1 -27 2259.73 2483.13 221.49 o 5 1 -27 1782.26 1932.00 247.57 o 6 1 -27 1117.94 1257.30 485.31 o -1 2 -27 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6184.41 6310.29 829.64 o 3 2 -24 7061.46 7488.62 201.84 o 4 2 -24 325.14 655.91 379.10 o 5 2 -24 717.56 585.96 100.16 o 6 2 -24 1399.24 1184.26 88.56 o 7 2 -24 438.19 1040.17 190.50 o 8 2 -24 6004.40 5926.70 207.80 o -4 3 -24 1126.82 726.46 145.14 o -3 3 -24 1369.63 1359.18 211.66 o -2 3 -24 598.97 836.34 94.94 o -1 3 -24 590.19 605.51 106.59 o 0 3 -24 611.31 703.02 92.22 o 1 3 -24 300.70 285.75 59.37 o 2 3 -24 1678.27 1390.93 84.67 o 3 3 -24 1701.63 1886.55 213.55 o 4 3 -24 131.29 232.39 82.40 o 5 3 -24 2777.87 2552.05 210.91 o 6 3 -24 1128.08 1807.89 319.01 o 7 3 -24 2275.90 2028.51 228.67 o 8 3 -24 5461.71 6540.04 317.63 o -2 4 -24 563.74 1080.24 148.92 o -1 4 -24 3607.91 4061.66 199.57 o 0 4 -24 143.71 62.43 46.67 o 1 4 -24 1895.29 2596.81 659.18 o 2 4 -24 831.02 829.75 117.17 o 3 4 -24 3467.98 4305.10 202.97 o 4 4 -24 4044.79 3735.85 138.34 o 5 4 -24 6362.87 7084.81 1407.56 o 6 4 -24 2071.30 2155.94 226.03 o 7 4 -24 275.86 75.59 83.15 o -3 5 -24 437.58 468.68 127.75 o -2 5 -24 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