#------------------------------------------------------------------------------ #$Date: 2012-09-11 12:26:43 +0300 (Tue, 11 Sep 2012) $ #$Revision: 66590 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/54/2235462.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2235462_Fobs loop_ _publ_author_name 'Ashraf, Adnan' 'Tahir, M. Nawaz' 'Siddiqui, Waseeq Ahmad' 'Perveen, Nadia' _publ_section_title ; 2-(1H-Benzimidazol-2-yl)-N-[(E)-(dimethylamino)methylidene]benzenesulfonamide ; _journal_coeditor_code HB6832 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2069 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 110.657 _cell_angle_gamma 90.000 _cell_length_a 15.6300 _cell_length_b 10.0030 _cell_length_c 22.1220 _exptl_crystal_F_000 1376.00 _reflns_d_resolution_high 0.8107 _[local]_cod_data_source_file hb6832Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' AD24UOS_0m' _shelx_refln_list_code 4 _shelx_f_calc_maximum 388.89 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 33473.62 33346.84 525.74 o 4 0 0 7354.67 7186.84 114.83 o 6 0 0 20375.96 22545.55 377.73 o 8 0 0 14464.83 15078.14 241.40 o 10 0 0 478.75 610.32 54.28 o 12 0 0 589.26 612.43 43.90 o 14 0 0 57.16 96.85 31.09 o 16 0 0 1047.23 1022.14 102.26 o 18 0 0 7.37 21.71 46.41 o 1 1 0 2417.97 2255.98 31.64 o 2 1 0 7984.33 7912.16 83.53 o 3 1 0 4737.04 4069.83 48.12 o 4 1 0 2860.63 2705.07 36.91 o 5 1 0 3179.95 3168.12 46.15 o 6 1 0 64.00 70.92 10.13 o 7 1 0 11.13 0.19 7.91 o 8 1 0 73.93 62.28 11.24 o 9 1 0 313.54 352.49 20.41 o 10 1 0 0.44 1.64 10.09 o 11 1 0 223.69 192.94 19.16 o 12 1 0 8.19 4.23 12.85 o 13 1 0 389.44 456.83 33.73 o 14 1 0 2.53 18.34 18.92 o 15 1 0 46.03 56.52 26.52 o 16 1 0 91.28 54.31 31.01 o 17 1 0 82.61 104.42 35.48 o 0 2 0 4691.64 4588.84 86.13 o 1 2 0 2086.53 1945.69 36.45 o 2 2 0 150.63 124.01 8.42 o 3 2 0 249.31 278.14 10.17 o 4 2 0 708.85 714.54 22.95 o 5 2 0 31.81 26.38 7.56 o 6 2 0 731.45 742.46 22.64 o 7 2 0 775.04 747.86 24.34 o 8 2 0 47.48 55.40 12.33 o 9 2 0 90.40 63.92 12.28 o 10 2 0 2.35 -0.31 11.55 o 11 2 0 61.40 58.96 14.21 o 12 2 0 7.70 -8.08 12.62 o 13 2 0 25.75 27.52 17.52 o 14 2 0 7.48 8.54 20.46 o 15 2 0 16.89 -14.44 21.44 o 16 2 0 6.69 11.10 26.92 o 17 2 0 7.67 42.87 32.66 o 1 3 0 2314.76 1946.66 37.48 o 2 3 0 10465.38 10053.85 134.85 o 3 3 0 1970.51 2052.55 54.24 o 4 3 0 1103.22 1231.68 24.66 o 5 3 0 5715.08 5724.82 72.61 o 6 3 0 557.97 583.03 19.19 o 7 3 0 448.09 437.61 20.62 o 8 3 0 636.04 633.29 27.95 o 9 3 0 45.71 54.50 14.37 o 10 3 0 1202.54 1366.31 63.44 o 11 3 0 173.02 167.94 22.33 o 12 3 0 5.32 5.02 17.34 o 13 3 0 367.92 361.73 33.92 o 14 3 0 348.79 287.54 32.41 o 15 3 0 0.40 1.71 19.45 o 16 3 0 2.45 16.27 21.80 o 17 3 0 51.83 35.32 41.09 o 0 4 0 9328.96 9730.04 206.55 o 1 4 0 706.88 675.09 21.28 o 2 4 0 5404.18 5311.79 99.80 o 3 4 0 1437.05 1446.20 31.13 o 4 4 0 151.04 154.93 17.82 o 5 4 0 1.96 26.65 11.89 o 6 4 0 376.54 426.30 17.18 o 7 4 0 900.67 907.65 23.77 o 8 4 0 155.24 157.31 13.97 o 9 4 0 316.11 343.40 26.41 o 10 4 0 110.77 67.53 13.73 o 11 4 0 159.77 167.09 25.16 o 12 4 0 59.16 38.90 25.32 o 13 4 0 248.75 300.94 33.83 o 14 4 0 175.53 210.57 27.31 o 15 4 0 48.97 65.28 30.04 o 16 4 0 102.63 104.43 33.97 o 17 4 0 5.26 10.50 32.73 o 1 5 0 240.83 254.47 16.76 o 2 5 0 1867.72 1695.18 44.33 o 3 5 0 1019.99 1038.80 28.04 o 4 5 0 29.96 5.47 9.37 o 5 5 0 489.25 556.66 26.56 o 6 5 0 33.55 30.84 11.38 o 7 5 0 235.65 262.25 16.75 o 8 5 0 83.43 103.05 18.91 o 9 5 0 269.58 248.76 17.25 o 10 5 0 128.09 114.08 25.33 o 11 5 0 13.43 39.32 23.05 o 12 5 0 18.12 1.42 22.46 o 13 5 0 59.55 71.38 29.25 o 14 5 0 34.24 38.83 30.48 o 15 5 0 0.22 14.41 29.43 o 16 5 0 0.03 4.00 34.53 o 0 6 0 443.03 394.31 32.01 o 1 6 0 16.77 11.45 9.46 o 2 6 0 166.79 181.90 23.98 o 3 6 0 48.87 34.26 9.97 o 4 6 0 751.31 729.34 66.58 o 5 6 0 188.54 185.18 21.52 o 6 6 0 140.49 131.76 22.69 o 7 6 0 2.79 5.79 11.83 o 8 6 0 401.77 412.94 24.45 o 9 6 0 15.00 17.07 23.69 o 10 6 0 14.18 54.33 28.90 o 11 6 0 27.66 18.60 28.43 o 12 6 0 273.01 327.69 48.44 o 13 6 0 6.54 17.13 31.32 o 14 6 0 123.97 175.38 44.55 o 15 6 0 0.90 81.96 40.27 o 1 7 0 3857.70 3940.33 76.11 o 2 7 0 812.90 917.43 47.43 o 3 7 0 2941.82 2897.02 117.39 o 4 7 0 156.28 163.90 20.26 o 5 7 0 83.17 100.52 18.45 o 6 7 0 382.98 406.64 31.73 o 7 7 0 169.54 145.26 34.31 o 8 7 0 38.39 11.61 52.19 o 9 7 0 3142.15 2959.18 111.76 o 10 7 0 212.41 285.26 46.96 o 11 7 0 244.52 296.49 47.01 o 12 7 0 16.94 -23.46 42.03 o 13 7 0 0.07 -29.72 52.35 o 14 7 0 61.02 153.31 47.60 o 0 8 0 118.32 174.00 26.83 o 1 8 0 605.04 640.65 33.57 o 2 8 0 695.63 746.26 58.63 o 3 8 0 994.03 962.25 57.34 o 4 8 0 3015.07 2825.50 77.20 o 5 8 0 715.69 803.72 41.71 o 6 8 0 12.89 23.28 17.50 o 7 8 0 7.38 40.78 24.22 o 8 8 0 18.56 21.74 24.76 o 9 8 0 39.98 -13.48 25.21 o 10 8 0 92.96 53.48 31.95 o 11 8 0 49.77 83.84 36.86 o 12 8 0 81.56 138.03 43.93 o 13 8 0 34.78 49.74 46.85 o 1 9 0 5.23 -1.17 30.50 o 2 9 0 135.86 114.85 37.44 o 3 9 0 28.36 23.46 27.09 o 4 9 0 57.19 87.53 32.78 o 5 9 0 33.12 81.52 32.16 o 6 9 0 89.37 72.27 41.85 o 7 9 0 18.29 -25.45 37.57 o 8 9 0 1.02 5.10 40.48 o 9 9 0 3.92 20.95 63.34 o 10 9 0 0.15 31.46 43.59 o 11 9 0 3.07 184.55 86.02 o 12 9 0 25.37 165.79 90.71 o 1 10 0 60.13 46.95 30.62 o 2 10 0 214.87 262.05 45.02 o 3 10 0 30.63 50.59 32.53 o 4 10 0 842.25 1003.52 80.25 o 5 10 0 12.27 18.16 42.48 o 6 10 0 136.04 172.85 59.75 o 7 10 0 20.17 66.20 47.21 o 8 10 0 70.67 47.57 45.30 o 9 10 0 1.80 23.55 61.78 o 10 10 0 134.13 143.89 96.97 o 1 11 0 35.79 -6.56 38.67 o 2 11 0 79.29 58.52 47.71 o 3 11 0 31.69 -0.41 35.32 o 4 11 0 341.20 235.01 76.64 o 5 11 0 0.74 -15.60 57.09 o 6 11 0 214.55 409.70 79.60 o 7 11 0 0.00 86.02 84.46 o 8 11 0 89.73 59.43 82.89 o 0 12 0 62.13 126.69 75.07 o 1 12 0 6.89 32.82 43.17 o 2 12 0 74.95 104.79 76.64 o 3 12 0 8.64 38.27 47.64 o 4 12 0 121.80 118.61 54.53 o -17 0 1 0.19 48.48 42.03 o -15 0 1 20.09 11.25 26.49 o -13 0 1 20.28 42.27 23.84 o -11 0 1 17.50 8.09 16.25 o -9 0 1 198.33 189.31 23.70 o -7 0 1 42.01 34.98 14.51 o -5 0 1 0.32 11.73 11.67 o -3 0 1 54.58 -15.32 10.22 o 3 0 1 212.91 200.32 11.84 o 5 0 1 84.83 76.91 11.78 o 7 0 1 4.67 -12.12 9.32 o 9 0 1 0.09 9.69 14.12 o 11 0 1 26.98 17.58 17.76 o 13 0 1 14.88 35.57 25.96 o 15 0 1 8.84 12.63 26.31 o 17 0 1 0.70 -39.72 40.26 o -18 1 1 173.70 168.46 41.48 o -17 1 1 159.36 173.14 38.93 o -16 1 1 132.07 168.59 31.26 o -15 1 1 35.62 28.89 21.74 o -14 1 1 172.96 129.99 22.76 o -13 1 1 531.93 578.92 39.17 o -12 1 1 66.71 56.35 15.39 o -11 1 1 18.52 15.28 10.80 o -10 1 1 69.65 55.60 11.72 o -9 1 1 1123.88 1140.10 33.62 o -8 1 1 3098.30 3168.58 63.93 o -7 1 1 681.22 649.45 24.37 o -6 1 1 8622.03 8751.87 121.24 o -5 1 1 6080.89 5845.37 77.93 o -4 1 1 15549.69 15677.41 172.99 o -3 1 1 572.79 558.91 12.00 o -2 1 1 9137.08 9175.73 107.15 o -1 1 1 7129.38 6303.39 67.55 o 0 1 1 2118.82 1953.40 71.16 o 1 1 1 368.32 354.98 11.75 o 2 1 1 13016.08 12827.80 111.54 o 3 1 1 16599.66 15154.09 138.36 o 4 1 1 6750.35 6482.64 72.16 o 5 1 1 3862.77 3681.68 50.45 o 6 1 1 9480.63 9821.71 113.80 o 7 1 1 1821.61 1931.72 41.24 o 8 1 1 616.89 665.37 26.32 o 9 1 1 326.27 370.24 21.31 o 10 1 1 402.36 445.53 24.93 o 11 1 1 927.81 909.18 38.88 o 12 1 1 130.84 102.80 20.86 o 13 1 1 214.93 299.41 28.95 o 14 1 1 6.91 14.78 19.62 o 15 1 1 109.35 151.87 35.17 o 16 1 1 37.83 20.99 25.64 o 17 1 1 7.68 -2.24 27.20 o -18 2 1 2.09 2.37 27.16 o -17 2 1 8.50 29.10 24.04 o -16 2 1 2.04 30.58 23.93 o -15 2 1 724.65 863.15 61.76 o -14 2 1 52.93 21.11 19.68 o -13 2 1 34.62 11.51 16.17 o -12 2 1 103.41 118.61 17.82 o -11 2 1 306.57 305.47 27.12 o -10 2 1 78.12 62.50 13.69 o -9 2 1 129.58 177.19 22.76 o -8 2 1 339.52 401.99 19.42 o -7 2 1 9977.03 9864.94 137.54 o -6 2 1 3815.51 4296.73 67.20 o -5 2 1 7042.10 7386.37 102.79 o -4 2 1 16061.88 17176.44 201.88 o -3 2 1 482.55 392.64 11.21 o -2 2 1 18800.25 17884.43 202.30 o -1 2 1 15195.41 15079.47 173.98 o 0 2 1 91964.66 89281.90 1064.14 o 1 2 1 46526.82 44905.93 585.01 o 2 2 1 6426.27 6492.29 79.88 o 3 2 1 1144.67 1070.30 17.97 o 4 2 1 653.30 559.74 15.98 o 5 2 1 1158.26 966.61 21.76 o 6 2 1 5897.60 6271.13 83.51 o 7 2 1 1866.11 1842.58 53.81 o 8 2 1 127.23 125.65 13.86 o 9 2 1 2575.25 2464.72 49.07 o 10 2 1 80.14 117.40 20.16 o 11 2 1 822.39 795.32 36.53 o 12 2 1 0.73 -21.01 14.27 o 13 2 1 345.57 394.71 32.87 o 14 2 1 6.22 7.65 18.28 o 15 2 1 174.42 183.86 28.13 o 16 2 1 33.33 11.93 22.70 o 17 2 1 236.77 289.87 40.52 o -17 3 1 34.21 29.57 27.54 o -16 3 1 1.78 11.52 21.60 o -15 3 1 1.14 12.60 21.58 o -14 3 1 50.45 57.17 24.78 o -13 3 1 118.02 148.36 30.76 o -12 3 1 46.10 38.24 21.96 o -11 3 1 28.73 31.34 15.09 o -10 3 1 359.26 425.82 26.17 o -9 3 1 0.95 -10.79 9.32 o -8 3 1 128.62 107.92 13.21 o -7 3 1 163.81 177.10 13.30 o -6 3 1 885.58 976.08 24.21 o -5 3 1 68.07 60.59 10.53 o -4 3 1 127.78 159.74 10.43 o -3 3 1 37.26 36.58 8.40 o -2 3 1 87.48 71.85 6.50 o -1 3 1 6040.03 5766.39 76.12 o 0 3 1 4873.82 5056.86 69.01 o 1 3 1 1844.24 1844.83 35.62 o 2 3 1 4532.32 4247.58 64.25 o 3 3 1 692.77 782.98 29.58 o 4 3 1 7.86 -0.81 4.93 o 5 3 1 865.79 859.62 20.75 o 6 3 1 98.50 113.89 10.34 o 7 3 1 440.80 443.58 20.93 o 8 3 1 162.37 196.88 21.70 o 9 3 1 168.06 184.55 17.65 o 10 3 1 1.69 0.65 12.41 o 11 3 1 220.46 163.75 19.71 o 12 3 1 79.63 68.49 19.73 o 13 3 1 15.21 5.34 17.59 o 14 3 1 142.64 125.20 25.42 o 15 3 1 0.65 16.22 20.55 o 16 3 1 15.02 43.45 26.52 o 17 3 1 1.53 12.18 41.21 o -17 4 1 0.26 58.89 34.99 o -16 4 1 22.58 49.81 30.24 o -15 4 1 17.77 26.52 24.06 o -14 4 1 44.97 72.79 25.39 o -13 4 1 4.20 9.59 18.92 o -12 4 1 111.10 92.85 32.16 o -11 4 1 0.43 -20.38 13.58 o -10 4 1 25.71 0.20 13.33 o -9 4 1 0.64 -8.20 11.53 o -8 4 1 163.24 160.72 16.76 o -7 4 1 185.87 209.03 21.40 o -6 4 1 87.89 105.32 7.53 o -5 4 1 151.70 163.23 15.24 o -4 4 1 11.61 2.93 8.30 o -3 4 1 1361.46 1354.58 27.00 o -2 4 1 7.46 19.54 10.10 o -1 4 1 18.60 17.38 7.56 o 0 4 1 46.40 46.74 9.17 o 1 4 1 490.43 493.49 21.32 o 2 4 1 999.88 1007.63 36.23 o 3 4 1 15.45 9.86 6.66 o 4 4 1 74.97 76.59 11.88 o 5 4 1 44.39 47.37 25.12 o 6 4 1 200.56 225.96 15.03 o 7 4 1 127.02 146.47 12.72 o 8 4 1 96.16 92.96 12.84 o 9 4 1 39.32 33.19 11.90 o 10 4 1 44.17 19.46 12.77 o 11 4 1 51.37 74.06 21.54 o 12 4 1 95.45 96.09 20.29 o 13 4 1 0.06 -20.70 16.89 o 14 4 1 0.16 19.33 25.39 o 15 4 1 44.81 54.03 29.30 o 16 4 1 22.63 -4.39 30.11 o -16 5 1 145.88 128.71 37.43 o -15 5 1 16.74 4.74 34.31 o -14 5 1 302.07 361.05 45.15 o -13 5 1 311.76 323.65 42.15 o -12 5 1 73.71 88.38 47.63 o -11 5 1 11.69 3.48 16.04 o -10 5 1 1111.23 1101.17 74.74 o -9 5 1 232.67 292.69 18.28 o -8 5 1 858.20 781.87 42.41 o -7 5 1 144.64 210.91 13.49 o -6 5 1 1756.85 1576.83 50.60 o -5 5 1 773.52 876.07 44.76 o -4 5 1 283.48 417.83 28.55 o -3 5 1 23.72 16.73 7.97 o -2 5 1 1482.23 1283.82 43.33 o -1 5 1 13912.80 14127.53 223.34 o 0 5 1 0.38 15.11 10.21 o 1 5 1 7715.87 8391.95 123.10 o 2 5 1 4075.18 4063.33 77.52 o 3 5 1 2892.36 3291.30 61.76 o 4 5 1 92.27 105.16 14.56 o 5 5 1 3484.60 3398.61 81.39 o 6 5 1 610.82 568.72 33.32 o 7 5 1 1761.21 1725.14 91.65 o 8 5 1 55.40 40.26 13.53 o 9 5 1 730.01 754.44 27.78 o 10 5 1 896.12 896.28 43.33 o 11 5 1 63.71 81.49 36.09 o 12 5 1 30.83 6.06 40.51 o 13 5 1 119.05 153.16 43.89 o 14 5 1 496.91 550.28 64.00 o 15 5 1 52.54 8.94 53.35 o 16 5 1 4.79 25.00 47.18 o -16 6 1 51.63 72.49 72.73 o -15 6 1 23.66 -11.72 34.76 o -14 6 1 143.02 140.80 42.03 o -13 6 1 66.77 98.10 37.33 o -12 6 1 254.37 220.47 42.28 o -11 6 1 180.29 158.29 36.82 o -10 6 1 56.70 37.31 27.96 o -9 6 1 0.58 -3.79 21.81 o -8 6 1 89.32 114.41 43.64 o -7 6 1 6.42 6.16 10.40 o -6 6 1 430.78 416.69 30.38 o -5 6 1 24.80 33.39 14.64 o -4 6 1 467.61 516.61 30.69 o -3 6 1 289.32 241.47 14.57 o -2 6 1 402.71 383.16 34.08 o -1 6 1 43.16 18.45 11.11 o 0 6 1 83.40 121.26 23.86 o 1 6 1 161.57 159.29 16.01 o 2 6 1 5068.50 5315.70 212.09 o 3 6 1 0.01 11.36 15.91 o 4 6 1 1040.85 1037.31 68.00 o 5 6 1 797.50 745.84 45.38 o 6 6 1 704.40 762.86 42.40 o 7 6 1 180.51 206.74 21.22 o 8 6 1 986.28 932.02 40.52 o 9 6 1 233.05 238.89 27.01 o 10 6 1 387.93 398.22 50.05 o 11 6 1 99.88 96.73 34.73 o 12 6 1 324.92 362.22 52.16 o 13 6 1 253.45 218.20 48.03 o 14 6 1 0.06 -3.23 33.10 o 15 6 1 111.15 95.64 42.49 o -15 7 1 1.69 27.21 42.96 o -14 7 1 0.57 50.89 36.84 o -13 7 1 92.84 78.02 38.51 o -12 7 1 2.30 -5.24 27.80 o -11 7 1 42.96 19.77 28.25 o -10 7 1 13.48 26.86 28.82 o -9 7 1 146.97 133.07 34.66 o -8 7 1 11.16 4.15 23.79 o -7 7 1 17.50 17.12 15.19 o -6 7 1 14.92 32.29 19.19 o -5 7 1 249.82 221.11 29.80 o -4 7 1 36.84 49.65 21.10 o -3 7 1 57.20 34.07 11.82 o -2 7 1 87.70 90.51 24.69 o -1 7 1 25.59 35.56 13.24 o 0 7 1 123.74 124.54 16.03 o 1 7 1 361.61 363.58 25.18 o 2 7 1 21.20 54.10 22.80 o 3 7 1 63.14 61.58 20.97 o 4 7 1 233.47 172.23 22.80 o 5 7 1 171.73 146.97 22.80 o 6 7 1 25.38 12.67 27.77 o 7 7 1 48.56 45.15 17.89 o 8 7 1 8.95 20.62 18.20 o 9 7 1 273.71 285.34 42.44 o 10 7 1 21.96 7.92 27.94 o 11 7 1 16.61 -14.15 37.95 o 12 7 1 16.70 34.97 33.48 o 13 7 1 52.19 53.64 35.28 o 14 7 1 17.08 -18.77 40.48 o -13 8 1 7.71 11.47 42.53 o -12 8 1 14.24 36.58 35.75 o -11 8 1 303.06 301.03 53.65 o -10 8 1 208.82 199.19 42.48 o -9 8 1 51.66 44.79 27.80 o -8 8 1 13.96 -16.06 24.60 o -7 8 1 167.56 171.27 31.12 o -6 8 1 9.98 -4.27 15.82 o -5 8 1 35.96 28.62 18.44 o -4 8 1 858.26 847.82 42.34 o -3 8 1 1495.47 1530.40 47.10 o -2 8 1 312.94 333.23 24.13 o -1 8 1 148.37 119.62 20.73 o 0 8 1 2.55 1.58 12.24 o 1 8 1 276.29 303.94 23.13 o 2 8 1 221.11 207.78 29.32 o 3 8 1 156.31 206.73 98.12 o 4 8 1 850.45 909.78 69.19 o 5 8 1 1061.71 1182.31 90.50 o 6 8 1 42.41 40.36 19.67 o 7 8 1 123.11 165.42 36.95 o 8 8 1 22.08 34.09 50.21 o 9 8 1 97.12 224.85 76.59 o 10 8 1 18.96 16.03 28.63 o 11 8 1 7.72 -40.61 28.41 o 12 8 1 38.26 78.08 53.48 o 13 8 1 80.77 105.51 51.83 o -12 9 1 49.75 -3.13 71.94 o -11 9 1 7.64 0.34 46.14 o -10 9 1 47.83 114.37 51.42 o -9 9 1 244.33 141.05 54.16 o -8 9 1 464.75 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