#------------------------------------------------------------------------------ #$Date: 2012-09-11 12:26:43 +0300 (Tue, 11 Sep 2012) $ #$Revision: 66590 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/55/2235513.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2235513_Fobs loop_ _publ_author_name 'Brennessel, William W.' 'Ellis, John E.' _publ_section_title ; ([2.2.2]Cryptand-\k^6^O)potassium (\h^4^-cyclooctadiene)bis(\h^2^-pyrene)cobaltate(1{-}) pentane hemisolvate ; _journal_coeditor_code IM2388 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1013 _journal_page_last m1014 _journal_volume 68 _journal_year 2012 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 72.064 _cell_angle_beta 81.595 _cell_angle_gamma 68.558 _cell_length_a 12.1007 _cell_length_b 12.9869 _cell_length_c 18.7501 _exptl_crystal_F_000 1090.00 _reflns_d_resolution_high 0.7800 _[local]_cod_data_source_file im2388Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 297 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 223.34 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1609.90 1662.25 21.57 o 2 0 0 4786.90 5499.78 68.67 o 3 0 0 2285.78 2600.40 35.55 o 4 0 0 959.45 865.61 15.90 o 5 0 0 1711.07 1729.49 27.72 o 6 0 0 942.25 903.18 24.56 o 7 0 0 913.77 884.70 23.91 o 8 0 0 950.95 959.96 26.04 o 9 0 0 28.78 12.50 7.93 o 10 0 0 61.65 54.73 11.81 o 11 0 0 9.50 28.93 14.10 o 12 0 0 39.78 42.20 18.11 o 13 0 0 232.99 226.18 26.46 o 14 0 0 4.34 11.27 26.94 o -14 1 0 174.46 227.99 30.64 o -13 1 0 17.10 -7.62 19.94 o -12 1 0 753.90 780.69 37.12 o -11 1 0 226.06 235.16 20.43 o -10 1 0 3.86 0.88 13.20 o -9 1 0 1054.27 1003.38 39.52 o -8 1 0 32.68 44.02 8.25 o -7 1 0 950.56 898.66 20.04 o -6 1 0 6.76 -1.57 4.90 o -5 1 0 805.09 744.15 18.02 o -4 1 0 414.60 368.95 10.56 o -3 1 0 1460.70 1633.50 31.53 o -2 1 0 10406.42 10363.25 146.94 o -1 1 0 5765.84 5615.78 112.49 o 0 1 0 435.51 555.33 11.55 o 1 1 0 12610.35 13578.56 190.60 o 2 1 0 104.48 85.66 3.61 o 3 1 0 8362.69 8713.68 108.15 o 4 1 0 18776.55 20427.23 248.90 o 5 1 0 4921.30 5334.29 70.81 o 6 1 0 2915.38 3049.31 44.90 o 7 1 0 1706.57 1777.53 30.74 o 8 1 0 750.40 745.23 20.84 o 9 1 0 1010.05 973.71 22.84 o 10 1 0 26.08 8.78 12.30 o 11 1 0 0.05 4.15 10.61 o 12 1 0 246.69 238.82 21.55 o 13 1 0 323.81 324.56 52.65 o 14 1 0 3.44 20.25 20.30 o -13 2 0 71.50 105.61 26.20 o -12 2 0 0.54 -16.42 16.42 o -11 2 0 42.56 11.43 16.54 o -10 2 0 288.79 314.34 22.73 o -9 2 0 10.43 -3.59 9.37 o -8 2 0 203.56 227.50 17.29 o -7 2 0 108.32 115.85 9.76 o -6 2 0 918.14 822.76 21.97 o -5 2 0 2.40 -0.13 4.55 o -4 2 0 780.61 861.23 16.51 o -3 2 0 9727.04 9979.86 125.01 o -2 2 0 1388.33 1364.32 20.66 o -1 2 0 4086.93 4614.95 68.57 o 0 2 0 7494.35 8430.28 105.59 o 1 2 0 54.00 65.33 5.44 o 2 2 0 45833.73 48455.82 582.91 o 3 2 0 4495.69 4831.95 61.98 o 4 2 0 11514.98 12130.00 150.18 o 5 2 0 616.27 532.73 18.47 o 6 2 0 1039.63 1039.11 19.91 o 7 2 0 2195.86 2239.25 36.25 o 8 2 0 158.96 153.12 9.58 o 9 2 0 130.17 132.27 10.97 o 10 2 0 267.09 248.42 21.57 o 11 2 0 98.19 117.50 25.66 o 12 2 0 397.89 395.98 27.56 o 13 2 0 88.53 75.50 20.51 o 14 2 0 4.89 -25.85 25.85 o -13 3 0 6.10 -21.12 21.12 o -12 3 0 167.29 194.81 28.44 o -11 3 0 15.77 10.93 17.45 o -10 3 0 775.51 754.89 69.70 o -9 3 0 145.30 161.24 15.13 o -8 3 0 673.78 694.31 30.30 o -7 3 0 863.11 856.69 25.16 o -6 3 0 1.43 4.23 7.42 o -5 3 0 7.61 -4.75 4.75 o -4 3 0 406.14 381.44 10.17 o -3 3 0 2022.14 2036.72 44.78 o -2 3 0 438.86 404.66 12.51 o -1 3 0 11973.69 12487.54 178.46 o 0 3 0 29165.32 31177.73 376.11 o 1 3 0 5604.58 6152.86 77.43 o 2 3 0 7040.77 7500.51 93.89 o 3 3 0 1169.83 1146.40 18.12 o 4 3 0 81.27 100.45 5.28 o 5 3 0 2393.36 2646.91 42.84 o 6 3 0 42.53 16.51 5.03 o 7 3 0 111.59 119.13 8.57 o 8 3 0 387.37 359.75 13.85 o 9 3 0 536.27 582.60 17.07 o 10 3 0 2054.81 2037.72 44.71 o 11 3 0 42.71 56.41 12.83 o 12 3 0 30.75 16.06 23.90 o 13 3 0 198.46 242.45 30.81 o 14 3 0 8.11 8.19 20.56 o 15 3 0 75.57 71.87 33.71 o -12 4 0 25.10 3.65 24.82 o -11 4 0 9.39 -0.91 15.86 o -10 4 0 96.89 110.95 21.97 o -9 4 0 446.92 397.76 21.19 o -8 4 0 20.55 16.46 11.21 o -7 4 0 30.31 44.59 10.48 o -6 4 0 886.15 888.50 25.64 o -5 4 0 16.41 -1.33 7.12 o -4 4 0 716.18 683.47 20.08 o -3 4 0 1909.85 1911.06 37.25 o -2 4 0 1418.27 1383.21 35.35 o -1 4 0 12.33 0.80 4.87 o 0 4 0 8210.34 8914.58 112.05 o 1 4 0 2680.04 2624.59 55.74 o 2 4 0 1581.98 1446.51 22.20 o 3 4 0 8004.74 8598.96 115.42 o 4 4 0 1985.35 2038.84 31.17 o 5 4 0 1310.27 1291.26 21.97 o 6 4 0 1645.51 1569.78 26.85 o 7 4 0 205.87 204.46 9.00 o 8 4 0 73.79 98.30 11.43 o 9 4 0 6243.25 6302.59 100.62 o 10 4 0 1044.56 1086.81 29.78 o 11 4 0 343.77 321.02 35.17 o 12 4 0 519.97 492.29 28.65 o 13 4 0 10.20 1.89 15.49 o 14 4 0 63.03 12.99 60.38 o 15 4 0 70.72 40.22 23.50 o -12 5 0 31.24 30.73 32.25 o -11 5 0 357.00 402.28 30.59 o -10 5 0 364.04 388.85 29.24 o -9 5 0 440.97 394.71 27.35 o -8 5 0 89.59 78.14 14.26 o -7 5 0 131.99 145.53 15.17 o -6 5 0 1518.68 1616.17 38.40 o -5 5 0 583.96 612.73 21.26 o -4 5 0 140.41 166.49 12.01 o -3 5 0 5753.45 5402.91 87.71 o -2 5 0 204.03 244.21 12.04 o -1 5 0 437.67 433.45 10.61 o 0 5 0 4387.48 4469.83 60.42 o 1 5 0 1067.97 1012.90 18.13 o 2 5 0 161.66 150.05 6.27 o 3 5 0 284.60 264.38 10.69 o 4 5 0 1745.12 1791.33 34.97 o 5 5 0 161.21 163.95 11.25 o 6 5 0 418.61 377.68 10.81 o 7 5 0 446.37 408.31 12.10 o 8 5 0 943.29 879.73 23.87 o 9 5 0 15.84 12.73 9.03 o 10 5 0 2737.66 2598.73 67.69 o 11 5 0 87.54 90.08 18.50 o 12 5 0 45.83 35.13 16.82 o 13 5 0 233.84 263.02 24.85 o 14 5 0 101.02 110.55 23.86 o 15 5 0 0.77 -7.81 25.23 o -11 6 0 75.81 50.71 39.75 o -10 6 0 22.03 24.38 21.00 o -9 6 0 223.41 193.91 38.37 o -8 6 0 262.17 215.30 18.13 o -7 6 0 417.04 456.50 21.24 o -6 6 0 3.03 -6.93 9.85 o -5 6 0 1964.13 1760.20 75.20 o -4 6 0 2868.59 2667.32 52.73 o -3 6 0 28.06 19.86 7.86 o -2 6 0 2439.35 2338.73 45.49 o -1 6 0 8660.51 8501.44 110.53 o 0 6 0 8546.12 9205.23 118.47 o 1 6 0 718.19 735.92 16.49 o 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38.78 o 12 7 0 341.54 358.43 26.40 o 13 7 0 39.78 49.79 19.28 o 14 7 0 38.18 13.22 20.89 o 15 7 0 195.87 263.06 43.93 o -9 8 0 38.59 28.84 22.57 o -8 8 0 16.06 19.55 14.88 o -7 8 0 157.51 170.62 20.08 o -6 8 0 53.98 52.95 15.38 o -5 8 0 335.50 368.67 19.83 o -4 8 0 211.97 207.07 20.17 o -3 8 0 1625.67 1590.35 38.84 o -2 8 0 224.12 224.65 14.74 o -1 8 0 558.88 551.81 20.17 o 0 8 0 1526.07 1450.68 43.76 o 1 8 0 68.17 54.22 7.48 o 2 8 0 103.73 95.05 8.17 o 3 8 0 3018.34 2988.27 68.14 o 4 8 0 94.63 78.60 10.28 o 5 8 0 942.32 1016.30 27.19 o 6 8 0 495.45 453.72 18.13 o 7 8 0 21.24 5.96 7.90 o 8 8 0 413.80 455.54 19.27 o 9 8 0 71.32 58.73 11.50 o 10 8 0 171.67 179.30 15.74 o 11 8 0 300.16 298.62 24.46 o 12 8 0 66.31 68.33 23.36 o 13 8 0 119.40 144.91 25.10 o 14 8 0 311.36 336.80 29.74 o 15 8 0 297.48 327.89 44.66 o -8 9 0 15.02 5.30 16.49 o -7 9 0 2.55 -10.05 18.86 o -6 9 0 395.06 371.89 22.23 o -5 9 0 36.96 29.56 13.22 o -4 9 0 19.70 42.71 13.12 o -3 9 0 19.05 20.35 12.64 o -2 9 0 29.03 14.33 10.04 o -1 9 0 789.34 784.32 32.67 o 0 9 0 5.86 0.41 11.89 o 1 9 0 43.11 20.14 8.96 o 2 9 0 857.02 783.72 19.28 o 3 9 0 2545.31 2543.30 50.21 o 4 9 0 41.51 47.63 9.89 o 5 9 0 682.18 739.06 23.66 o 6 9 0 2099.56 2053.76 44.71 o 7 9 0 261.51 232.38 14.56 o 8 9 0 140.49 178.48 16.14 o 9 9 0 277.21 259.45 16.29 o 10 9 0 124.16 135.76 15.68 o 11 9 0 145.49 170.73 24.12 o 12 9 0 406.03 344.55 26.88 o 13 9 0 190.59 183.59 27.71 o 14 9 0 86.18 72.66 27.29 o -7 10 0 2.90 -6.56 16.76 o -6 10 0 137.38 197.35 21.93 o -5 10 0 36.33 15.61 15.07 o -4 10 0 2.27 -11.93 14.19 o -3 10 0 1151.73 1134.27 34.51 o -2 10 0 10.71 7.84 10.82 o -1 10 0 69.27 62.11 12.91 o 0 10 0 522.21 480.95 20.72 o 1 10 0 1890.53 1811.04 53.85 o 2 10 0 1037.45 977.21 37.39 o 3 10 0 232.45 221.33 14.26 o 4 10 0 182.53 193.08 15.03 o 5 10 0 3269.28 3148.10 61.83 o 6 10 0 197.20 190.26 15.86 o 7 10 0 589.93 499.63 21.08 o 8 10 0 1262.42 1335.50 36.52 o 9 10 0 257.65 248.46 16.53 o 10 10 0 185.16 208.49 16.80 o 11 10 0 118.78 131.51 23.98 o 12 10 0 463.83 419.13 30.66 o 13 10 0 6.72 -1.95 27.48 o 14 10 0 40.44 75.85 24.40 o -6 11 0 95.72 131.75 21.52 o -5 11 0 104.09 88.84 18.07 o -4 11 0 743.75 725.11 46.93 o -3 11 0 5.86 2.66 12.35 o -2 11 0 50.48 55.68 23.22 o -1 11 0 295.34 303.94 19.02 o 0 11 0 1.89 -1.18 19.94 o 1 11 0 224.68 240.29 21.80 o 2 11 0 524.84 494.38 27.39 o 3 11 0 180.88 188.15 22.04 o 4 11 0 869.49 920.48 37.22 o 5 11 0 337.21 314.71 18.85 o 6 11 0 5037.47 5058.71 141.32 o 7 11 0 270.47 280.89 17.92 o 8 11 0 505.16 494.91 23.01 o 9 11 0 9.93 10.30 12.31 o 10 11 0 107.26 127.95 16.80 o 11 11 0 58.04 62.29 39.59 o 12 11 0 17.63 6.86 18.89 o 13 11 0 260.06 259.92 31.10 o 14 11 0 17.54 26.29 33.87 o -5 12 0 0.20 -16.27 16.27 o -4 12 0 14.49 -12.30 17.07 o -3 12 0 170.86 197.49 35.70 o -2 12 0 41.52 34.63 18.65 o -1 12 0 424.08 398.24 29.37 o 0 12 0 281.88 265.41 24.59 o 1 12 0 23.85 28.26 21.49 o 2 12 0 277.62 306.46 23.94 o 3 12 0 262.04 265.16 36.23 o 4 12 0 852.72 878.12 38.08 o 5 12 0 11.87 15.12 22.25 o 6 12 0 1.56 -10.67 10.67 o 7 12 0 54.09 17.67 12.78 o 8 12 0 5.74 16.54 13.70 o 9 12 0 215.89 251.48 18.87 o 10 12 0 447.59 423.66 22.81 o 11 12 0 106.45 99.85 24.66 o 12 12 0 776.71 755.36 41.48 o 13 12 0 119.37 174.82 43.66 o -3 13 0 183.16 248.60 31.42 o -2 13 0 294.45 312.67 33.25 o -1 13 0 450.68 444.40 31.70 o 0 13 0 929.37 867.84 41.64 o 1 13 0 111.68 102.48 49.73 o 2 13 0 268.49 256.28 26.15 o 3 13 0 463.28 465.62 29.73 o 4 13 0 41.55 27.43 16.35 o 5 13 0 116.04 133.83 22.49 o 6 13 0 163.97 166.95 23.92 o 7 13 0 38.49 17.74 14.54 o 8 13 0 544.58 528.23 26.33 o 9 13 0 106.91 111.07 18.49 o 10 13 0 454.69 446.70 34.24 o 11 13 0 13.80 13.71 21.26 o 12 13 0 4.22 -12.23 32.03 o -2 14 0 121.86 207.37 37.21 o -1 14 0 112.61 152.85 26.70 o 0 14 0 284.26 378.65 34.19 o 1 14 0 145.01 240.97 55.99 o 2 14 0 89.43 64.06 20.56 o 3 14 0 291.70 348.00 28.34 o 4 14 0 14.70 -0.43 18.37 o 5 14 0 1.76 36.44 26.31 o 6 14 0 453.63 448.92 61.76 o 7 14 0 32.97 44.36 19.58 o 8 14 0 0.96 -15.66 17.63 o 9 14 0 326.23 329.18 27.17 o 10 14 0 0.42 0.69 16.77 o 11 14 0 23.30 -18.17 27.26 o 1 15 0 164.29 183.50 67.01 o 2 15 0 588.20 636.35 39.02 o 3 15 0 89.29 85.62 24.55 o 4 15 0 13.00 -17.98 17.98 o 5 15 0 507.83 538.95 35.16 o 6 15 0 7.30 39.81 20.82 o 7 15 0 7.94 6.75 20.15 o 8 15 0 179.65 222.52 30.04 o 9 15 0 157.13 162.00 37.61 o -8 -15 1 449.68 494.28 48.13 o -7 -15 1 16.46 2.14 20.65 o -6 -15 1 127.26 159.87 27.53 o -5 -15 1 93.00 103.53 72.06 o -4 -15 1 70.10 75.05 23.38 o -3 -15 1 0.95 -5.85 33.87 o -2 -15 1 127.59 170.95 29.41 o -10 -14 1 35.62 15.50 18.74 o -9 -14 1 48.05 39.32 23.65 o -8 -14 1 13.45 13.83 19.39 o -7 -14 1 147.73 181.06 26.46 o -6 -14 1 11.74 -26.23 26.23 o -5 -14 1 212.82 228.52 65.58 o -4 -14 1 95.19 134.55 24.00 o -3 -14 1 0.02 -6.54 17.07 o -2 -14 1 400.94 416.58 35.17 o -1 -14 1 65.11 45.87 20.55 o 0 -14 1 12.11 -6.24 19.21 o 1 -14 1 283.00 313.01 48.26 o -12 -13 1 8.96 -11.70 20.97 o -11 -13 1 17.54 37.15 18.58 o -10 -13 1 178.26 171.28 21.79 o -9 -13 1 230.66 256.85 25.02 o -8 -13 1 17.52 6.58 23.58 o -7 -13 1 24.58 0.47 19.11 o -6 -13 1 4.83 -8.72 15.22 o -5 -13 1 1.46 -2.53 16.79 o -4 -13 1 268.26 274.68 24.85 o -3 -13 1 1.59 3.85 21.73 o -2 -13 1 115.43 118.15 21.54 o -1 -13 1 707.78 720.34 38.65 o 0 -13 1 0.85 -17.19 17.19 o 1 -13 1 130.62 128.77 24.25 o 2 -13 1 182.36 203.88 78.64 o 3 -13 1 82.95 153.53 74.63 o -13 -12 1 20.47 49.75 33.28 o -12 -12 1 27.19 -18.24 21.46 o -11 -12 1 64.60 57.75 17.99 o -10 -12 1 65.57 47.87 14.77 o -9 -12 1 32.71 22.42 14.16 o -8 -12 1 752.99 850.13 31.12 o -7 -12 1 327.87 271.33 19.64 o -6 -12 1 74.97 65.41 15.54 o -5 -12 1 316.28 337.08 24.56 o -4 -12 1 184.28 217.57 22.69 o -3 -12 1 3.21 -7.39 12.66 o -2 -12 1 308.79 366.78 29.62 o -1 -12 1 252.70 247.91 26.15 o 0 -12 1 20.89 12.91 15.79 o 1 -12 1 4.07 -9.80 14.37 o 2 -12 1 161.77 147.22 25.16 o 3 -12 1 188.34 230.60 29.45 o 4 -12 1 9.99 -11.42 15.36 o 5 -12 1 191.11 250.90 25.91 o -13 -11 1 95.90 117.16 24.26 o -12 -11 1 155.13 163.39 26.95 o -11 -11 1 35.79 4.67 14.66 o -10 -11 1 532.06 548.31 33.38 o -9 -11 1 151.10 150.30 18.73 o -8 -11 1 57.19 55.63 13.76 o -7 -11 1 344.94 362.52 36.11 o -6 -11 1 6.01 -1.22 10.54 o -5 -11 1 5.41 3.84 11.02 o -4 -11 1 53.41 47.34 23.60 o -3 -11 1 291.17 293.88 22.64 o -2 -11 1 1091.40 992.48 39.57 o -1 -11 1 835.51 704.66 49.73 o 0 -11 1 146.75 186.43 27.72 o 1 -11 1 615.57 581.26 32.26 o 2 -11 1 97.68 36.80 13.97 o 3 -11 1 428.22 383.80 26.12 o 4 -11 1 382.40 359.21 34.66 o 5 -11 1 240.54 289.44 25.36 o 6 -11 1 401.47 392.58 25.66 o -14 -10 1 555.24 663.43 58.48 o -13 -10 1 1.67 -9.84 20.69 o -12 -10 1 2.41 4.83 18.92 o -11 -10 1 956.51 1014.16 43.61 o -10 -10 1 24.01 3.78 12.28 o -9 -10 1 39.73 36.97 13.10 o -8 -10 1 586.95 575.02 23.81 o -7 -10 1 39.51 41.58 12.52 o -6 -10 1 550.27 481.11 28.97 o -5 -10 1 1707.06 1749.29 41.75 o -4 -10 1 2167.89 2171.76 48.52 o -3 -10 1 132.03 129.73 14.32 o -2 -10 1 763.57 723.41 32.00 o -1 -10 1 122.57 160.57 21.21 o 0 -10 1 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