#------------------------------------------------------------------------------ #$Date: 2012-09-11 12:26:43 +0300 (Tue, 11 Sep 2012) $ #$Revision: 66590 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/56/2235600.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2235600_Fobs loop_ _publ_author_name 'Toledano-Maga\~na, Yanis' 'Garc\'ia-Ramos, Juan-Carlos' 'Garc\'ia-Manrique, Consuelo' 'Flores-Alamo, Marcos' 'Ruiz-Azuara, Lena' _publ_section_title ; Tris(5,6-dimethyl-1,10-phenanthroline-\k^2^N,N')copper(II) bis(hexafluoridophosphate) acetonitrile monosolvate ; _journal_coeditor_code RU2037 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m987 _journal_page_last m988 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 93.603 _cell_angle_gamma 90.000 _cell_length_a 9.8566 _cell_length_b 19.9317 _cell_length_c 22.1822 _exptl_crystal_F_000 2076.00 _reflns_d_resolution_high 0.8087 _[local]_cod_data_source_file ru2037Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 5m2pf6 in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 357.13 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 72901.20 72757.20 401.87 o 4 0 0 127.75 157.56 61.68 o 6 0 0 4229.28 4107.82 132.41 o 8 0 0 1963.17 2221.97 178.19 o 10 0 0 338.57 223.93 145.48 o 12 0 0 6.14 46.44 145.81 o 2 1 0 11747.30 11891.99 120.85 o 3 1 0 10678.62 10696.94 192.13 o 4 1 0 5126.07 5305.99 118.14 o 5 1 0 929.37 1000.69 55.46 o 6 1 0 159.84 209.61 45.95 o 7 1 0 1181.35 1260.47 68.10 o 8 1 0 12.13 36.76 77.79 o 9 1 0 6.18 40.62 90.27 o 10 1 0 5623.51 5538.07 208.76 o 11 1 0 252.85 201.71 102.90 o 12 1 0 409.25 471.85 124.40 o 2 2 0 83.25 63.31 56.93 o 3 2 0 4748.54 4430.07 85.27 o 4 2 0 3589.00 3882.56 108.63 o 5 2 0 3.83 6.82 38.97 o 6 2 0 5367.82 5418.89 107.19 o 7 2 0 985.69 928.69 64.41 o 8 2 0 16.20 -9.00 86.15 o 9 2 0 31.51 4.57 96.61 o 10 2 0 373.55 257.06 101.91 o 11 2 0 211.56 220.64 96.96 o 12 2 0 878.71 970.06 128.85 o 1 3 0 6811.16 6980.06 113.57 o 2 3 0 34970.00 36026.15 318.99 o 3 3 0 1127.49 1974.57 562.25 o 4 3 0 3432.47 2927.82 61.04 o 5 3 0 681.70 647.81 58.60 o 6 3 0 371.97 299.55 49.83 o 7 3 0 2163.05 1988.88 79.49 o 8 3 0 968.69 900.43 108.09 o 9 3 0 3373.80 3462.50 168.78 o 10 3 0 3839.88 3866.91 181.53 o 11 3 0 465.32 413.66 104.02 o 12 3 0 4.52 -2.86 113.82 o 0 4 0 248.78 190.26 47.97 o 1 4 0 51475.79 52160.66 239.52 o 2 4 0 23913.87 24901.31 261.60 o 3 4 0 18166.52 19950.45 288.88 o 4 4 0 2243.81 2333.52 84.83 o 5 4 0 550.76 559.29 38.42 o 6 4 0 2397.66 2611.74 95.19 o 7 4 0 2068.67 1943.86 93.32 o 8 4 0 1931.35 1859.89 126.80 o 9 4 0 107.29 130.07 91.85 o 10 4 0 1606.02 1578.73 136.22 o 11 4 0 142.86 229.96 147.95 o 1 5 0 2354.04 2743.80 69.72 o 2 5 0 5182.73 5154.39 136.11 o 3 5 0 2143.84 2309.19 79.88 o 4 5 0 9604.74 10357.46 180.99 o 5 5 0 286.45 241.12 37.80 o 6 5 0 333.79 316.17 41.57 o 7 5 0 354.64 362.49 77.38 o 8 5 0 82.03 3.10 122.15 o 9 5 0 255.07 218.88 50.67 o 10 5 0 527.18 331.97 148.37 o 11 5 0 918.69 828.83 164.28 o 0 6 0 12721.49 12316.46 193.70 o 1 6 0 9061.40 9659.21 103.54 o 2 6 0 1960.59 2175.29 73.80 o 3 6 0 3851.52 3951.17 139.60 o 4 6 0 202.05 222.00 61.92 o 5 6 0 26.00 28.21 37.15 o 6 6 0 1132.96 1254.47 61.37 o 7 6 0 212.28 349.56 134.13 o 8 6 0 4617.09 4801.25 258.65 o 9 6 0 54.95 12.47 144.47 o 10 6 0 1243.43 1120.79 181.78 o 11 6 0 292.91 187.60 143.63 o 1 7 0 3259.61 3434.76 71.94 o 2 7 0 8429.92 8523.38 298.72 o 3 7 0 123.71 168.00 67.70 o 4 7 0 4265.57 4141.60 132.28 o 5 7 0 6.78 11.37 35.41 o 6 7 0 196.23 228.44 41.79 o 7 7 0 1904.12 1704.71 82.29 o 8 7 0 8.88 -8.31 129.72 o 9 7 0 70.86 53.19 143.04 o 10 7 0 1417.69 1332.92 183.67 o 11 7 0 887.89 847.85 182.76 o 0 8 0 351.15 348.68 52.95 o 1 8 0 19098.87 19723.76 158.02 o 2 8 0 65.34 76.41 48.92 o 3 8 0 6659.65 6620.95 187.30 o 4 8 0 2933.88 3325.39 111.29 o 5 8 0 20.94 36.83 47.78 o 6 8 0 4385.80 4015.97 125.52 o 7 8 0 114.72 118.50 47.90 o 8 8 0 4866.03 4279.37 247.53 o 9 8 0 125.79 106.26 127.23 o 10 8 0 247.91 315.77 136.45 o 11 8 0 663.07 526.30 122.47 o 1 9 0 22974.66 23331.34 165.38 o 2 9 0 2690.28 2275.01 62.98 o 3 9 0 49.04 46.24 66.52 o 4 9 0 40.28 15.40 68.55 o 5 9 0 1003.02 954.03 68.68 o 6 9 0 5084.77 5326.43 107.57 o 7 9 0 833.74 777.58 70.63 o 8 9 0 409.15 410.95 72.56 o 9 9 0 539.12 615.83 117.17 o 10 9 0 868.35 1028.45 210.33 o 11 9 0 216.64 184.28 110.23 o 0 10 0 34886.91 36045.15 484.24 o 1 10 0 1361.62 1430.10 55.61 o 2 10 0 3316.98 3512.74 77.85 o 3 10 0 22.23 76.43 46.27 o 4 10 0 1759.01 1686.18 144.13 o 5 10 0 2362.99 2451.18 143.21 o 6 10 0 2.81 25.49 44.48 o 7 10 0 329.83 321.11 61.51 o 8 10 0 767.60 765.21 73.12 o 9 10 0 2477.35 2661.22 164.19 o 10 10 0 99.73 40.85 102.38 o 11 10 0 1631.51 1894.22 164.09 o 1 11 0 11128.36 11331.09 130.15 o 2 11 0 661.25 736.83 49.67 o 3 11 0 775.22 846.78 61.60 o 4 11 0 690.25 718.95 76.03 o 5 11 0 6804.14 7280.35 183.66 o 6 11 0 198.24 122.59 48.60 o 7 11 0 6372.93 6425.22 149.25 o 8 11 0 252.80 224.69 60.23 o 9 11 0 1205.62 1216.28 137.96 o 10 11 0 444.83 486.53 118.54 o 0 12 0 2021.72 2582.23 104.34 o 1 12 0 2090.24 2208.50 69.32 o 2 12 0 76.24 82.67 39.75 o 3 12 0 6260.13 5825.47 123.17 o 4 12 0 415.50 424.58 72.80 o 5 12 0 682.11 638.25 88.66 o 6 12 0 425.86 397.11 56.92 o 7 12 0 2360.60 2313.14 108.62 o 8 12 0 1350.79 1582.41 144.48 o 9 12 0 976.50 1137.56 133.69 o 10 12 0 1.65 -39.91 105.04 o 1 13 0 1599.57 1759.29 66.75 o 2 13 0 0.48 13.74 40.84 o 3 13 0 131.18 224.41 66.88 o 4 13 0 138.44 45.50 61.61 o 5 13 0 291.81 367.89 71.96 o 6 13 0 2.71 -77.30 137.52 o 7 13 0 1186.14 1222.48 87.88 o 8 13 0 331.36 320.22 110.34 o 9 13 0 601.99 479.68 108.58 o 10 13 0 0.03 21.39 108.57 o 0 14 0 9573.55 9859.41 194.57 o 1 14 0 102.19 92.42 43.44 o 2 14 0 4455.44 4719.36 138.77 o 3 14 0 3568.77 3796.43 130.49 o 4 14 0 570.69 551.24 76.50 o 5 14 0 910.22 931.33 88.35 o 6 14 0 15.65 0.82 126.39 o 7 14 0 21.73 15.05 63.05 o 8 14 0 36.97 -5.84 101.50 o 9 14 0 26.82 -15.39 113.10 o 10 14 0 123.35 243.09 105.46 o 1 15 0 2641.25 2620.83 82.85 o 2 15 0 294.12 242.41 48.02 o 3 15 0 321.16 267.08 57.08 o 4 15 0 510.27 462.47 77.06 o 5 15 0 237.26 88.63 133.56 o 6 15 0 693.21 656.15 167.46 o 7 15 0 1380.28 1396.62 131.55 o 8 15 0 227.70 306.74 115.31 o 9 15 0 616.99 656.59 125.37 o 0 16 0 5512.30 5971.02 167.42 o 1 16 0 355.17 329.32 49.98 o 2 16 0 664.27 763.54 68.13 o 3 16 0 18.27 15.40 49.94 o 4 16 0 991.89 1101.60 93.12 o 5 16 0 55.32 37.73 113.88 o 6 16 0 308.84 209.71 137.36 o 7 16 0 108.65 145.04 106.44 o 8 16 0 98.06 113.64 105.60 o 9 16 0 798.35 718.21 127.15 o 1 17 0 2165.99 2088.83 93.78 o 2 17 0 354.25 323.45 58.14 o 3 17 0 811.45 867.74 98.60 o 4 17 0 470.51 381.15 134.48 o 5 17 0 457.69 359.31 151.39 o 6 17 0 407.37 346.02 147.34 o 7 17 0 1207.81 1181.99 133.80 o 8 17 0 1.32 -26.46 107.22 o 0 18 0 841.70 764.24 144.53 o 1 18 0 910.15 895.28 97.99 o 2 18 0 312.86 166.56 79.83 o 3 18 0 999.29 1066.13 141.60 o 4 18 0 288.58 290.68 87.42 o 5 18 0 1179.64 1084.04 177.22 o 6 18 0 34.06 57.46 143.52 o 7 18 0 132.92 48.57 101.87 o 8 18 0 119.10 149.03 112.72 o 1 19 0 3463.76 3327.98 153.75 o 2 19 0 2.93 -4.14 78.63 o 3 19 0 144.99 115.87 89.63 o 4 19 0 1659.24 1719.96 125.64 o 5 19 0 389.27 434.69 138.58 o 6 19 0 65.41 16.11 126.22 o 7 19 0 1555.32 1246.18 204.89 o 0 20 0 1024.44 1144.76 153.09 o 1 20 0 616.50 668.31 102.08 o 2 20 0 659.06 703.07 101.48 o 3 20 0 2686.03 2665.01 183.58 o 4 20 0 156.59 179.35 83.40 o 5 20 0 558.09 581.51 162.18 o 6 20 0 295.98 303.55 136.41 o 7 20 0 87.74 57.99 147.62 o 1 21 0 2084.76 2340.37 141.68 o 2 21 0 1178.47 1167.35 115.77 o 3 21 0 1.20 -28.16 87.56 o 4 21 0 271.55 341.73 137.12 o 5 21 0 618.51 680.71 173.64 o 6 21 0 510.80 530.82 167.37 o 0 22 0 205.25 127.57 120.15 o 1 22 0 4.12 -49.54 86.07 o 2 22 0 232.40 263.39 93.43 o 3 22 0 88.95 44.16 88.05 o 4 22 0 7.24 -6.27 128.46 o 5 22 0 3.38 29.32 145.67 o 1 23 0 103.67 111.27 85.17 o 2 23 0 344.23 265.49 94.68 o 3 23 0 91.08 95.78 86.62 o 4 23 0 1010.26 864.00 188.43 o 0 24 0 740.51 749.86 158.18 o 1 24 0 642.63 560.45 105.08 o 2 24 0 1010.99 957.69 121.14 o -11 0 1 456.76 460.28 170.47 o -9 0 1 2750.95 2779.93 226.69 o -7 0 1 443.32 325.19 73.48 o -5 0 1 5785.27 6766.71 212.28 o -3 0 1 1748.11 1581.33 93.77 o 3 0 1 17701.80 17966.23 242.25 o 5 0 1 14606.51 14283.60 563.57 o 7 0 1 8584.03 8429.62 194.26 o 9 0 1 4021.36 3996.25 243.05 o 11 0 1 195.01 79.96 133.77 o -12 1 1 2.65 18.81 107.11 o -11 1 1 623.66 542.44 116.42 o -10 1 1 29.34 25.92 92.47 o -9 1 1 4223.97 4174.91 180.25 o -8 1 1 140.51 144.52 84.66 o -7 1 1 66.89 113.68 48.27 o -6 1 1 371.33 359.17 50.62 o -5 1 1 3813.29 3798.57 98.26 o -4 1 1 1259.75 1460.38 95.08 o -3 1 1 7228.71 6512.46 260.70 o -2 1 1 6089.71 6382.02 94.25 o 2 1 1 5547.88 5277.01 57.50 o 3 1 1 1775.53 1804.93 84.89 o 4 1 1 36.77 155.89 37.90 o 5 1 1 3700.77 3848.23 82.63 o 6 1 1 3187.31 3463.31 87.31 o 7 1 1 84.58 131.05 46.24 o 8 1 1 259.98 274.68 83.54 o 9 1 1 610.62 546.16 105.05 o 10 1 1 52.33 61.36 95.78 o 11 1 1 165.84 103.95 94.39 o 12 1 1 312.56 260.05 101.53 o -12 2 1 2.97 -2.99 106.66 o -11 2 1 37.72 -15.35 103.35 o -10 2 1 485.65 502.56 131.81 o -9 2 1 3756.13 3707.23 173.87 o -8 2 1 102.91 62.66 86.65 o -7 2 1 5609.41 5659.69 136.07 o -6 2 1 38.87 46.50 44.80 o -5 2 1 8984.03 8544.29 139.74 o -4 2 1 102.70 62.43 45.68 o -3 2 1 15096.21 15142.59 405.00 o -2 2 1 98766.95 93531.88 496.63 o 2 2 1 2450.37 2291.27 116.80 o 3 2 1 42.71 45.40 27.11 o 4 2 1 583.99 598.99 44.11 o 5 2 1 3178.25 3708.23 81.80 o 6 2 1 4410.54 4959.99 101.06 o 7 2 1 2324.66 2245.43 82.19 o 8 2 1 2667.83 3008.19 475.58 o 9 2 1 464.04 478.11 104.71 o 10 2 1 2130.31 2023.38 143.07 o 11 2 1 28.98 -1.16 94.06 o 12 2 1 144.37 97.24 95.69 o -12 3 1 210.07 146.43 96.47 o -11 3 1 1260.78 1251.42 136.39 o -10 3 1 203.12 218.69 104.89 o -9 3 1 9790.61 9894.96 256.49 o -8 3 1 161.15 231.27 95.40 o -7 3 1 224.25 170.65 30.23 o -6 3 1 6.89 4.34 39.92 o -5 3 1 1011.37 994.41 85.30 o -4 3 1 4371.17 4479.12 164.54 o -3 3 1 48366.05 49204.38 439.67 o -2 3 1 47627.62 48422.59 261.58 o -1 3 1 14384.44 15228.07 177.93 o 1 3 1 7208.70 7706.93 207.58 o 2 3 1 9698.09 9894.47 199.22 o 3 3 1 5236.17 4631.84 72.25 o 4 3 1 2385.76 2859.12 58.08 o 5 3 1 4433.25 3837.27 97.75 o 6 3 1 2.27 14.81 52.00 o 7 3 1 158.92 261.07 59.57 o 8 3 1 1206.03 1074.28 107.19 o 9 3 1 711.41 614.95 105.49 o 10 3 1 158.74 101.12 97.70 o 11 3 1 871.29 907.11 117.80 o 12 3 1 9.03 -38.78 140.62 o -12 4 1 32.66 15.36 145.57 o -11 4 1 263.43 278.55 101.04 o -10 4 1 964.17 1090.59 129.96 o -9 4 1 3016.14 2886.56 160.72 o -8 4 1 1390.79 1167.91 247.40 o -7 4 1 4460.49 4541.73 130.02 o -6 4 1 305.26 324.82 59.94 o -5 4 1 3808.22 3795.12 73.33 o -4 4 1 965.87 906.06 98.70 o -3 4 1 8151.84 8220.90 191.55 o -2 4 1 27874.89 26912.04 288.92 o -1 4 1 2980.79 2682.33 92.90 o 0 4 1 7948.38 7825.96 90.37 o 1 4 1 127544.27 125110.97 741.72 o 2 4 1 210.12 243.60 54.28 o 3 4 1 42.16 86.34 34.44 o 4 4 1 7387.53 8047.17 146.97 o 5 4 1 69.14 49.80 33.39 o 6 4 1 165.84 211.09 52.58 o 7 4 1 4230.48 4200.51 120.37 o 8 4 1 864.92 850.68 104.73 o 9 4 1 1409.52 1298.76 150.34 o 10 4 1 2661.98 2940.60 233.53 o 11 4 1 360.88 247.38 136.99 o -11 5 1 1156.20 1153.10 192.72 o -10 5 1 718.74 649.97 157.97 o -9 5 1 5891.63 6015.83 296.43 o -8 5 1 598.52 533.23 43.12 o -7 5 1 546.44 471.37 133.54 o -6 5 1 6802.54 7093.13 121.89 o -5 5 1 3784.39 3940.71 82.81 o -4 5 1 0.53 -5.31 76.73 o -3 5 1 3721.82 3432.39 96.87 o -2 5 1 4558.30 5122.94 141.76 o -1 5 1 23064.81 23433.34 218.06 o 0 5 1 5140.36 5105.60 84.14 o 1 5 1 10181.11 9818.44 130.57 o 2 5 1 9256.93 9364.62 166.52 o 3 5 1 184.31 389.90 47.79 o 4 5 1 131.89 190.33 40.93 o 5 5 1 2668.38 2989.07 235.27 o 6 5 1 2278.02 2120.43 106.49 o 7 5 1 1274.32 1356.97 101.48 o 8 5 1 1313.80 1104.40 158.17 o 9 5 1 4410.35 4709.61 262.02 o 10 5 1 1.13 -11.37 127.81 o 11 5 1 2448.64 2253.40 212.62 o -11 6 1 471.06 390.56 161.47 o -10 6 1 909.73 909.27 177.98 o -9 6 1 621.95 597.02 145.37 o -8 6 1 173.90 219.32 145.65 o -7 6 1 807.33 662.22 62.23 o -6 6 1 176.60 221.75 40.75 o -5 6 1 2127.64 1949.86 79.51 o -4 6 1 16887.73 17638.48 224.88 o -3 6 1 24.75 24.48 44.80 o -2 6 1 1142.94 1324.94 65.93 o -1 6 1 8601.18 8744.32 205.12 o 0 6 1 834.87 1070.65 60.42 o 1 6 1 12902.63 12472.74 111.28 o 2 6 1 13660.52 13018.82 173.89 o 3 6 1 1271.15 1252.41 90.17 o 4 6 1 4484.29 3941.30 75.03 o 5 6 1 124.49 91.69 39.51 o 6 6 1 3640.57 3474.09 128.91 o 7 6 1 1901.70 2007.22 172.61 o 8 6 1 124.10 165.82 121.43 o 9 6 1 1140.94 1018.39 161.02 o 10 6 1 1604.57 1718.28 195.20 o 11 6 1 7.31 -2.05 144.69 o -11 7 1 358.79 541.33 156.44 o -10 7 1 104.21 102.79 131.41 o -9 7 1 111.42 78.20 143.47 o -8 7 1 3983.81 3710.42 244.87 o -7 7 1 4250.23 4281.79 189.51 o -6 7 1 13490.38 12989.02 145.55 o -5 7 1 448.59 612.13 61.22 o -4 7 1 3763.91 3698.08 115.28 o -3 7 1 3042.78 2875.67 131.53 o -2 7 1 3589.12 4157.96 119.88 o -1 7 1 2572.09 2791.75 58.80 o 0 7 1 9939.21 8950.89 102.77 o 1 7 1 3878.66 4392.17 76.52 o 2 7 1 10049.26 11081.13 121.21 o 3 7 1 15071.49 16442.60 263.14 o 4 7 1 191.06 115.97 37.97 o 5 7 1 4207.17 4079.36 83.33 o 6 7 1 3463.78 3516.07 95.20 o 7 7 1 38.78 35.06 52.41 o 8 7 1 3898.85 3776.77 230.30 o 9 7 1 409.04 301.12 131.50 o 10 7 1 10.28 -41.64 137.93 o 11 7 1 914.19 941.31 172.90 o -11 8 1 39.38 65.38 134.77 o -10 8 1 392.95 223.67 151.24 o -9 8 1 188.38 201.84 128.95 o -8 8 1 2.84 -5.91 43.73 o -7 8 1 91.94 111.25 56.81 o -6 8 1 71.17 83.43 39.10 o -5 8 1 719.69 678.52 62.02 o -4 8 1 1457.63 1339.73 80.31 o -3 8 1 2913.73 3248.48 145.54 o -2 8 1 9959.95 10133.25 130.10 o -1 8 1 3755.04 4065.95 118.20 o 0 8 1 7851.87 7723.42 91.21 o 1 8 1 26603.66 27088.52 199.01 o 2 8 1 11063.57 11895.78 190.71 o 3 8 1 286.48 179.69 63.00 o 4 8 1 758.11 770.37 65.50 o 5 8 1 115.54 144.31 37.56 o 6 8 1 820.58 791.74 48.73 o 7 8 1 395.75 357.42 48.65 o 8 8 1 53.97 51.37 89.34 o 9 8 1 391.18 237.65 98.62 o 10 8 1 749.19 953.31 207.66 o 11 8 1 362.16 187.46 97.59 o -11 9 1 48.66 106.64 101.66 o -10 9 1 7.85 51.63 103.18 o -9 9 1 521.83 367.38 153.23 o -8 9 1 140.83 141.23 55.06 o -7 9 1 5083.96 5312.61 243.38 o -6 9 1 22.71 10.19 43.09 o -5 9 1 392.59 312.13 49.15 o -4 9 1 1271.20 1297.96 70.61 o -3 9 1 618.45 459.95 52.84 o -2 9 1 3733.66 3963.35 92.07 o -1 9 1 11640.56 12021.70 122.02 o 0 9 1 2139.40 2238.77 59.12 o 1 9 1 371.90 345.37 38.89 o 2 9 1 451.74 441.03 44.64 o 3 9 1 12649.82 12229.81 247.76 o 4 9 1 673.10 685.01 87.52 o 5 9 1 36.49 22.80 37.05 o 6 9 1 5528.80 5791.02 111.78 o 7 9 1 847.77 951.61 62.72 o 8 9 1 489.27 549.22 63.01 o 9 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