#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:42:33 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181279 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/57/2235792.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2235792_Fobs loop_ _publ_author_name 'Tebbaa, Mohamed' 'Benharref, Ahmed' 'Daran, Jean-Claude' 'Barkaoui, Latifa' 'Berraho, Moha' _publ_section_title ; Methyl 2-(4a,8-Dimethyl-7-oxodecahydronaphthalen-2-yl)acrylate ; _journal_coeditor_code FJ2573 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2391 _journal_volume 68 _journal_year 2012 _space_group_IT_number 92 _symmetry_space_group_name_Hall 'P 4abw 2nw' _symmetry_space_group_name_H-M 'P 41 21 2' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 7.3359 _cell_length_b 7.3359 _cell_length_c 54.7419 _exptl_crystal_F_000 1152.00 _reflns_d_resolution_high 0.8732 _cod_data_source_file fj2573Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' TM95 in P4(1)2(1)2' _shelx_refln_list_code 4 _shelx_f_calc_maximum 191.41 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z+1/2' 'x+1/2, -y+1/2, -z+3/4' '-x+1/2, y+1/2, -z+1/4' '-y, -x, -z+1/2' 'y, x, -z' 'y+1/2, -x+1/2, z+3/4' '-y+1/2, x+1/2, z+1/4' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 2 0 1228.76 1142.52 7.76 o 1 2 0 456.10 366.01 3.75 o 2 2 0 1901.58 1767.46 12.72 o 1 3 0 2572.79 2572.85 11.50 o 2 3 0 3804.91 4300.03 15.91 o 3 3 0 422.42 440.77 6.70 o 0 4 0 5.37 5.85 1.12 o 1 4 0 16.73 16.26 1.20 o 2 4 0 687.43 816.43 9.07 o 3 4 0 432.42 450.62 10.96 o 4 4 0 547.05 512.39 58.14 o 1 5 0 0.69 44.72 15.26 o 2 5 0 105.45 106.13 2.26 o 3 5 0 14.70 18.29 2.88 o 4 5 0 0.42 3.56 1.76 o 5 5 0 9.70 28.46 4.79 o 0 6 0 514.36 717.18 183.09 o 1 6 0 351.65 375.86 13.43 o 2 6 0 181.55 184.93 6.13 o 3 6 0 901.10 873.70 16.99 o 4 6 0 0.67 2.21 1.52 o 5 6 0 25.43 23.75 2.08 o 1 7 0 93.21 171.39 16.41 o 2 7 0 18.49 202.07 35.40 o 3 7 0 24.37 16.08 2.39 o 4 7 0 125.97 160.76 6.04 o 0 8 0 39.62 114.39 35.61 o 1 8 0 132.12 290.92 41.45 o 2 8 0 0.01 2.69 4.11 o 0 1 1 877.52 791.22 2.66 o 1 1 1 3955.52 3443.97 18.25 o -1 2 1 1299.31 1244.74 13.55 o 0 2 1 758.04 704.37 3.77 o 1 2 1 1306.67 1214.73 4.97 o 2 2 1 55.44 49.58 1.77 o -2 3 1 1866.43 1901.75 9.47 o -1 3 1 14.12 18.05 1.12 o 0 3 1 1986.74 2034.99 7.96 o 1 3 1 14.22 19.33 1.10 o 2 3 1 1866.24 1900.99 9.45 o 3 3 1 2.13 1.09 0.50 o -3 4 1 121.38 113.98 2.61 o -2 4 1 513.64 503.80 5.63 o -1 4 1 246.77 276.42 4.38 o 0 4 1 36.11 39.14 1.32 o 1 4 1 242.87 270.91 4.43 o 2 4 1 510.62 502.69 7.54 o 3 4 1 122.42 114.54 2.58 o 4 4 1 123.35 156.01 5.23 o -4 5 1 103.16 117.66 6.48 o -3 5 1 702.25 746.79 15.19 o -2 5 1 86.64 81.88 4.62 o -1 5 1 485.05 433.21 15.50 o 0 5 1 41.04 37.96 1.67 o 1 5 1 485.27 465.41 4.73 o 2 5 1 86.78 76.69 3.05 o 3 5 1 703.43 744.82 16.24 o 4 5 1 102.26 111.55 6.32 o 5 5 1 37.50 47.78 7.27 o -5 6 1 66.14 73.13 3.43 o -4 6 1 169.45 160.23 5.43 o -3 6 1 153.45 159.00 15.33 o -2 6 1 25.56 173.45 74.00 o -1 6 1 231.19 230.20 7.77 o 0 6 1 487.35 467.20 10.11 o 1 6 1 230.23 208.45 14.73 o 2 6 1 25.97 32.25 2.71 o 3 6 1 153.01 152.66 7.20 o 4 6 1 170.47 167.68 7.42 o 5 6 1 65.70 70.24 3.35 o -4 7 1 87.18 92.06 4.65 o -3 7 1 4.75 7.52 1.81 o -2 7 1 171.32 183.47 4.91 o -1 7 1 104.97 198.76 24.78 o 0 7 1 1888.22 1768.72 115.21 o 1 7 1 105.47 152.95 19.25 o 2 7 1 170.06 173.42 4.63 o 3 7 1 4.45 7.93 1.97 o 4 7 1 87.67 94.83 6.93 o -2 8 1 78.28 79.24 5.63 o -1 8 1 226.27 264.35 10.13 o 0 8 1 564.40 530.57 26.08 o 1 8 1 226.39 276.16 15.43 o 2 8 1 77.51 88.66 5.86 o 0 1 2 3994.72 3717.97 7.92 o 1 1 2 9910.72 9447.65 33.70 o -1 2 2 6345.10 5981.45 14.77 o 0 2 2 155.11 123.95 2.51 o 1 2 2 6353.21 5918.22 13.53 o 2 2 2 2833.70 2928.25 16.19 o -2 3 2 5219.21 5581.48 30.72 o -1 3 2 2631.21 2629.92 17.17 o 0 3 2 514.66 514.58 4.38 o 1 3 2 2626.19 2602.52 15.82 o 2 3 2 5233.28 5575.75 31.74 o 3 3 2 7.78 1.99 0.80 o -3 4 2 910.87 884.98 25.09 o -2 4 2 78.03 71.47 2.19 o -1 4 2 1427.50 1414.52 10.79 o 0 4 2 477.24 441.07 5.43 o 1 4 2 1431.11 1403.79 12.76 o 2 4 2 78.14 74.53 2.27 o 3 4 2 910.12 864.21 30.15 o 4 4 2 116.48 115.98 6.13 o -4 5 2 27.08 46.14 4.17 o -3 5 2 179.00 197.89 7.89 o -2 5 2 389.83 359.25 9.11 o -1 5 2 292.03 276.27 4.04 o 0 5 2 116.07 103.09 3.19 o 1 5 2 289.12 272.20 5.65 o 2 5 2 387.76 360.33 8.65 o 3 5 2 177.07 187.75 7.67 o 4 5 2 26.84 42.45 3.98 o 5 5 2 824.91 775.24 16.21 o -5 6 2 24.76 26.14 2.15 o -4 6 2 134.88 123.33 4.75 o -3 6 2 61.08 67.40 4.91 o -2 6 2 395.30 426.91 20.75 o -1 6 2 127.67 189.58 31.05 o 0 6 2 400.71 365.13 11.80 o 1 6 2 129.10 185.94 21.30 o 2 6 2 392.34 411.87 7.39 o 3 6 2 61.82 62.89 5.80 o 4 6 2 134.28 124.30 6.43 o 5 6 2 24.99 27.21 3.33 o -4 7 2 25.50 34.43 2.94 o -3 7 2 5.25 3.41 1.33 o -2 7 2 23.75 32.68 2.68 o -1 7 2 254.82 305.19 13.60 o 0 7 2 7.43 562.71 65.83 o 1 7 2 253.77 280.09 14.79 o 2 7 2 23.96 79.84 26.10 o 3 7 2 5.70 1.37 1.91 o 4 7 2 24.68 33.32 4.28 o -2 8 2 10.79 14.15 2.34 o -1 8 2 77.75 139.32 28.02 o 0 8 2 6.15 185.09 64.46 o 1 8 2 76.94 162.06 38.19 o 2 8 2 10.69 10.83 1.91 o 0 1 3 1284.64 1263.39 4.98 o 1 1 3 11086.92 10752.00 192.06 o -1 2 3 2463.34 2278.59 10.71 o 0 2 3 0.01 5.45 1.86 o 1 2 3 2461.97 2237.30 11.41 o 2 2 3 83.78 72.87 1.57 o -2 3 3 4208.27 4361.23 28.52 o -1 3 3 1903.17 1833.77 13.18 o 0 3 3 148.57 122.16 1.64 o 1 3 3 1905.44 1818.75 10.45 o 2 3 3 4219.36 4336.87 38.80 o 3 3 3 15.31 13.87 4.23 o -3 4 3 132.79 141.18 6.22 o -2 4 3 1863.98 1826.60 10.82 o -1 4 3 1456.24 1454.19 8.59 o 0 4 3 504.77 432.36 4.63 o 1 4 3 1444.84 1453.24 11.92 o 2 4 3 1856.28 1853.96 17.41 o 3 4 3 132.69 146.71 3.71 o 4 4 3 55.67 54.78 4.25 o -4 5 3 15.19 22.23 3.11 o -3 5 3 1075.56 1116.71 18.62 o -2 5 3 81.50 88.40 4.21 o -1 5 3 537.59 523.15 16.71 o 0 5 3 61.62 51.30 3.48 o 1 5 3 542.29 538.47 7.78 o 2 5 3 83.75 90.75 2.43 o 3 5 3 1076.72 1115.21 18.39 o 4 5 3 15.75 26.22 5.10 o 5 5 3 75.88 67.58 4.93 o -5 6 3 11.68 9.76 1.79 o -4 6 3 221.10 183.56 5.80 o -3 6 3 242.53 277.13 9.66 o -2 6 3 352.41 368.47 8.13 o -1 6 3 57.58 55.79 3.82 o 0 6 3 83.43 69.88 3.45 o 1 6 3 57.92 48.30 3.68 o 2 6 3 354.48 375.64 7.04 o 3 6 3 242.43 266.11 9.30 o 4 6 3 222.97 194.27 7.88 o 5 6 3 11.73 12.22 1.73 o -4 7 3 111.79 121.89 7.58 o -3 7 3 60.35 64.26 3.55 o -2 7 3 7.14 45.52 13.52 o -1 7 3 203.43 289.67 32.39 o 0 7 3 3.24 110.14 14.42 o 1 7 3 205.42 397.93 72.24 o 2 7 3 6.76 40.78 13.68 o 3 7 3 60.64 66.47 6.58 o 4 7 3 110.44 134.93 8.35 o -2 8 3 8.85 12.29 2.01 o -1 8 3 38.88 161.93 43.47 o 0 8 3 41.30 51.96 3.53 o 1 8 3 38.26 216.65 59.18 o 2 8 3 8.95 7.09 1.57 o 0 0 4 0.84 3.15 0.34 o 0 1 4 508.86 488.77 4.60 o 1 1 4 3297.81 3096.16 35.03 o -1 2 4 947.95 875.30 5.95 o 0 2 4 13.26 4.88 0.31 o 1 2 4 949.71 848.73 4.40 o 2 2 4 2.48 3.21 0.58 o -2 3 4 156.87 146.06 2.41 o -1 3 4 342.62 338.42 3.64 o 0 3 4 587.39 552.59 3.93 o 1 3 4 341.80 330.83 2.99 o 2 3 4 159.91 151.63 3.67 o 3 3 4 418.02 393.03 5.56 o -3 4 4 354.20 366.74 7.21 o -2 4 4 170.96 170.82 3.12 o -1 4 4 100.42 91.28 1.93 o 0 4 4 1938.51 1820.67 16.51 o 1 4 4 101.47 96.09 2.82 o 2 4 4 169.57 181.36 4.00 o 3 4 4 357.56 360.98 7.15 o 4 4 4 44.88 42.11 3.75 o -4 5 4 385.63 381.28 11.50 o -3 5 4 149.90 156.30 7.05 o -2 5 4 915.84 877.47 22.93 o -1 5 4 115.06 118.09 2.89 o 0 5 4 162.29 138.13 2.86 o 1 5 4 115.33 112.84 2.53 o 2 5 4 912.23 931.02 18.62 o 3 5 4 153.41 164.35 8.05 o 4 5 4 387.48 369.89 11.23 o 5 5 4 55.49 52.36 4.30 o -5 6 4 20.49 18.23 2.28 o -4 6 4 97.28 103.57 4.42 o -3 6 4 321.98 370.97 11.36 o -2 6 4 409.01 418.81 7.20 o -1 6 4 719.87 597.31 38.66 o 0 6 4 27.04 29.68 2.11 o 1 6 4 721.52 627.45 44.52 o 2 6 4 410.51 409.41 8.57 o 3 6 4 323.36 359.36 10.66 o 4 6 4 96.79 103.08 8.61 o 5 6 4 19.76 20.77 1.97 o -4 7 4 35.58 38.52 4.57 o -3 7 4 100.74 117.39 4.74 o -2 7 4 78.52 96.62 4.08 o -1 7 4 775.21 831.34 10.66 o 0 7 4 262.58 255.88 15.93 o 1 7 4 770.58 838.90 12.32 o 2 7 4 79.04 83.46 4.86 o 3 7 4 99.81 105.25 8.14 o 4 7 4 36.18 48.57 6.65 o -2 8 4 15.97 17.21 4.86 o -1 8 4 348.99 342.95 10.74 o 0 8 4 196.07 178.38 12.29 o 1 8 4 348.31 337.56 15.38 o 2 8 4 15.55 19.37 1.74 o 0 1 5 12433.19 13030.64 237.46 o 1 1 5 28560.64 28691.09 116.51 o -1 2 5 4439.00 4507.52 21.00 o 0 2 5 972.39 988.06 4.14 o 1 2 5 4427.60 4398.47 24.24 o 2 2 5 8858.10 9335.63 85.48 o -2 3 5 17.65 26.21 1.06 o -1 3 5 1128.40 1086.57 11.64 o 0 3 5 1366.90 1348.76 8.39 o 1 3 5 1121.77 1078.99 7.03 o 2 3 5 18.20 34.81 4.90 o 3 3 5 821.01 841.43 8.18 o -3 4 5 12.73 9.82 0.98 o -2 4 5 401.66 403.15 8.98 o -1 4 5 139.87 147.33 2.40 o 0 4 5 334.42 336.39 4.84 o 1 4 5 140.05 147.50 3.41 o 2 4 5 403.61 401.53 4.87 o 3 4 5 11.86 10.67 0.95 o 4 4 5 119.43 146.57 9.38 o -4 5 5 39.31 35.40 3.75 o -3 5 5 113.10 113.91 4.63 o -2 5 5 1671.25 1593.33 43.73 o -1 5 5 627.55 560.01 17.85 o 0 5 5 68.04 81.15 2.22 o 1 5 5 627.56 585.52 7.58 o 2 5 5 1673.21 1611.00 24.67 o 3 5 5 113.61 118.53 5.95 o 4 5 5 39.86 34.59 3.68 o 5 5 5 6.78 9.92 3.72 o -5 6 5 70.40 79.98 4.32 o -4 6 5 119.39 140.65 5.07 o -3 6 5 51.22 42.63 4.06 o -2 6 5 47.45 42.32 4.47 o -1 6 5 45.20 368.49 53.37 o 0 6 5 145.06 136.60 4.26 o 1 6 5 46.47 263.41 111.98 o 2 6 5 48.41 48.30 3.69 o 3 6 5 50.95 47.96 7.93 o 4 6 5 119.23 140.24 10.00 o 5 6 5 70.71 80.70 3.49 o -4 7 5 185.56 187.74 9.61 o -3 7 5 161.32 188.09 5.87 o -2 7 5 85.12 84.83 4.10 o -1 7 5 179.13 374.44 63.58 o 0 7 5 29.61 122.07 44.45 o 1 7 5 177.72 252.52 14.18 o 2 7 5 85.34 88.73 3.98 o 3 7 5 161.54 178.36 10.53 o 4 7 5 184.75 182.57 6.45 o -2 8 5 6.04 13.33 7.37 o -1 8 5 56.12 64.64 3.79 o 0 8 5 11.01 51.48 2.97 o 1 8 5 56.35 155.22 32.16 o 2 8 5 5.84 6.98 2.03 o 0 1 6 1350.41 1294.12 7.15 o 1 1 6 3427.47 3336.40 46.75 o -1 2 6 1956.82 1955.51 15.36 o 0 2 6 700.89 695.19 3.07 o 1 2 6 1950.63 1892.01 5.01 o 2 2 6 1494.76 1584.36 8.21 o -2 3 6 79.23 103.41 2.18 o -1 3 6 2755.77 2629.53 13.24 o 0 3 6 304.25 294.45 2.73 o 1 3 6 2739.29 2581.19 21.45 o 2 3 6 78.69 101.72 2.68 o 3 3 6 1.10 2.92 0.85 o -3 4 6 217.11 229.48 4.66 o -2 4 6 684.89 715.55 7.56 o -1 4 6 514.09 508.74 4.46 o 0 4 6 0.02 3.12 0.94 o 1 4 6 514.06 508.69 7.36 o 2 4 6 682.72 706.03 8.15 o 3 4 6 215.26 217.59 5.05 o 4 4 6 298.92 301.82 9.76 o -4 5 6 468.33 482.26 20.73 o -3 5 6 106.61 120.98 5.79 o -2 5 6 231.00 248.02 5.12 o -1 5 6 131.32 137.42 2.89 o 0 5 6 1557.42 1455.84 19.11 o 1 5 6 129.88 134.44 2.70 o 2 5 6 231.95 273.67 20.89 o 3 5 6 106.31 118.00 5.93 o 4 5 6 466.21 473.38 9.22 o 5 5 6 263.09 240.82 8.58 o -5 6 6 0.36 7.27 5.79 o -4 6 6 169.33 158.86 6.50 o -3 6 6 56.36 60.26 3.69 o -2 6 6 204.76 199.97 9.93 o -1 6 6 565.88 574.55 18.25 o 0 6 6 276.19 299.20 15.70 o 1 6 6 566.63 581.56 12.53 o 2 6 6 205.23 206.91 6.38 o 3 6 6 58.50 66.45 6.92 o 4 6 6 170.25 159.62 10.72 o 5 6 6 0.42 6.68 3.98 o -4 7 6 156.63 150.93 8.71 o -3 7 6 235.05 244.29 8.23 o -2 7 6 159.13 170.73 7.82 o -1 7 6 38.80 104.23 26.59 o 0 7 6 122.68 123.04 5.43 o 1 7 6 38.91 52.52 13.10 o 2 7 6 158.45 154.21 5.22 o 3 7 6 235.86 238.10 12.11 o 4 7 6 158.02 164.79 8.84 o -2 8 6 55.32 61.90 5.42 o -1 8 6 48.54 62.11 2.39 o 0 8 6 6.77 8.00 1.06 o 1 8 6 46.99 65.66 2.66 o 2 8 6 56.62 61.84 6.43 o 0 1 7 4859.40 4798.69 23.98 o 1 1 7 1007.32 1030.82 9.51 o -1 2 7 4748.97 4785.73 22.74 o 0 2 7 2366.24 2289.08 19.21 o 1 2 7 4733.03 4676.34 23.71 o 2 2 7 1462.17 1524.37 10.43 o -2 3 7 74.79 76.65 1.85 o -1 3 7 574.67 584.09 4.72 o 0 3 7 440.22 431.06 4.34 o 1 3 7 580.16 571.60 4.76 o 2 3 7 75.92 79.65 2.49 o 3 3 7 449.70 455.81 6.09 o -3 4 7 218.75 233.39 4.04 o -2 4 7 452.78 482.41 6.24 o -1 4 7 671.15 735.25 5.36 o 0 4 7 1245.16 1210.00 9.27 o 1 4 7 674.12 737.99 8.95 o 2 4 7 452.52 479.78 5.96 o 3 4 7 219.78 232.10 4.76 o 4 4 7 81.31 95.70 5.50 o -4 5 7 365.86 339.65 17.58 o -3 5 7 367.41 377.90 6.87 o -2 5 7 422.55 418.97 13.80 o -1 5 7 111.92 113.97 2.44 o 0 5 7 1186.13 1126.11 12.45 o 1 5 7 111.73 114.84 2.23 o 2 5 7 423.37 436.19 5.78 o 3 5 7 368.45 378.80 10.00 o 4 5 7 368.17 478.01 120.92 o 5 5 7 2.52 14.57 11.40 o -5 6 7 183.39 173.75 6.29 o -4 6 7 111.88 97.80 5.18 o -3 6 7 75.24 84.76 4.27 o -2 6 7 8.78 11.09 1.84 o -1 6 7 501.76 586.17 40.60 o 0 6 7 191.16 185.17 9.99 o 1 6 7 502.63 520.90 55.34 o 2 6 7 9.25 318.28 9.07 o 3 6 7 74.83 114.05 26.52 o 4 6 7 112.66 102.72 8.67 o 5 6 7 182.52 182.84 6.80 o -4 7 7 171.20 165.29 9.07 o -3 7 7 16.66 17.25 2.76 o -2 7 7 223.12 220.73 13.05 o -1 7 7 108.26 125.90 4.49 o 0 7 7 8.42 23.72 10.73 o 1 7 7 108.62 117.27 6.27 o 2 7 7 222.84 221.81 6.08 o 3 7 7 16.84 14.97 3.72 o 4 7 7 171.64 175.17 6.29 o -2 8 7 157.18 187.63 8.88 o -1 8 7 33.89 42.43 2.89 o 0 8 7 0.02 0.86 0.82 o 1 8 7 34.50 65.24 14.90 o 2 8 7 155.45 168.90 6.09 o 0 0 8 10141.14 9658.04 30.40 o 0 1 8 36637.25 37430.39 291.00 o 1 1 8 17292.17 17874.21 100.76 o -1 2 8 1991.03 1979.49 6.81 o 0 2 8 4951.64 4961.89 12.03 o 1 2 8 2005.79 1944.37 10.20 o 2 2 8 2881.73 2783.95 10.09 o -2 3 8 3360.81 3659.92 15.37 o -1 3 8 987.39 1002.68 6.08 o 0 3 8 985.52 978.71 6.32 o 1 3 8 975.85 973.15 6.67 o 2 3 8 3351.65 3626.06 22.97 o 3 3 8 515.42 509.10 5.69 o -3 4 8 66.12 71.41 2.53 o -2 4 8 688.06 676.78 8.84 o -1 4 8 384.60 389.73 4.19 o 0 4 8 857.45 889.25 7.94 o 1 4 8 385.97 383.31 5.66 o 2 4 8 691.77 685.32 6.52 o 3 4 8 67.07 74.95 2.20 o 4 4 8 916.02 773.78 86.24 o -4 5 8 246.24 216.75 8.13 o -3 5 8 204.82 201.63 6.24 o -2 5 8 260.24 266.47 7.10 o -1 5 8 363.45 349.13 8.46 o 0 5 8 30.90 29.36 1.21 o 1 5 8 362.93 365.99 5.09 o 2 5 8 259.60 272.78 5.57 o 3 5 8 202.66 204.03 11.55 o 4 5 8 247.93 330.51 78.64 o 5 5 8 4.41 2.77 1.71 o -5 6 8 20.01 23.12 2.54 o -4 6 8 135.54 136.18 7.17 o -3 6 8 145.61 155.56 5.28 o -2 6 8 452.93 407.36 23.02 o -1 6 8 2.93 140.64 58.32 o 0 6 8 13.24 285.91 133.24 o 1 6 8 2.88 205.39 55.24 o 2 6 8 454.13 405.90 27.48 o 3 6 8 147.12 200.66 27.14 o 4 6 8 134.33 137.02 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