#------------------------------------------------------------------------------ #$Date: 2012-09-11 12:26:43 +0300 (Tue, 11 Sep 2012) $ #$Revision: 66590 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/58/2235802.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2235802_Fobs loop_ _publ_author_name 'Wang, Wen-Xiang' _publ_section_title ; 2-(1H-Tetrazol-1-yl)acetic acid monohydrate ; _journal_coeditor_code FY2060 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2561 _journal_volume 68 _journal_year 2012 _space_group_IT_number 33 _symmetry_space_group_name_Hall 'P 2c -2n' _symmetry_space_group_name_H-M 'P n a 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 12.6177 _cell_length_b 5.1871 _cell_length_c 9.8736 _exptl_crystal_F_000 304.00 _reflns_d_resolution_high 0.7701 _[local]_cod_data_source_file fy2060Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' a in Pna2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 101.84 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z+1/2' 'x+1/2, -y+1/2, z' '-x+1/2, y+1/2, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 495.88 462.46 3.49 o 4 0 0 901.69 878.00 8.90 o 6 0 0 328.48 321.47 4.47 o 8 0 0 27.92 29.57 2.18 o 10 0 0 10.12 10.07 2.07 o 12 0 0 243.04 243.25 7.92 o 14 0 0 7.49 13.77 4.50 o 16 0 0 38.80 39.41 5.21 o 1 1 0 32.32 21.95 0.72 o 2 1 0 10370.98 10056.99 69.57 o 3 1 0 929.85 910.21 4.70 o 4 1 0 75.64 76.18 0.58 o 5 1 0 812.04 841.27 8.34 o 6 1 0 15.91 17.87 1.70 o 7 1 0 35.80 33.91 1.02 o 8 1 0 106.66 108.30 3.30 o 9 1 0 73.81 74.34 1.80 o 10 1 0 140.73 141.31 4.35 o 11 1 0 29.22 27.26 1.97 o 12 1 0 22.85 25.74 2.03 o 13 1 0 0.28 -1.26 1.30 o 14 1 0 32.41 31.80 2.35 o 15 1 0 1.77 0.90 1.50 o 16 1 0 4.09 4.23 1.79 o 0 2 0 47.04 46.53 0.97 o 1 2 0 230.13 210.64 2.05 o 2 2 0 1756.14 1781.77 12.58 o 3 2 0 338.21 379.71 3.69 o 4 2 0 0.44 1.90 0.37 o 5 2 0 16.53 20.11 0.72 o 6 2 0 32.40 31.79 0.75 o 7 2 0 183.92 180.08 2.98 o 8 2 0 3.66 4.64 0.89 o 9 2 0 35.23 38.23 1.83 o 10 2 0 8.97 11.32 1.40 o 11 2 0 20.28 20.07 1.31 o 12 2 0 0.98 1.03 1.42 o 13 2 0 43.87 47.94 2.68 o 14 2 0 34.24 35.38 3.55 o 15 2 0 0.90 5.95 3.53 o 1 3 0 226.40 244.63 3.02 o 2 3 0 26.05 28.59 0.78 o 3 3 0 251.61 249.96 2.87 o 4 3 0 22.52 29.54 2.39 o 5 3 0 1.51 4.27 1.12 o 6 3 0 19.62 20.27 0.83 o 7 3 0 12.01 13.51 0.89 o 8 3 0 103.60 106.47 2.52 o 9 3 0 26.21 27.57 1.59 o 10 3 0 19.96 20.23 1.44 o 11 3 0 71.46 64.73 2.31 o 12 3 0 24.71 21.97 2.05 o 13 3 0 17.50 19.61 2.04 o 14 3 0 5.84 3.71 1.73 o 0 4 0 11.89 10.31 0.99 o 1 4 0 0.58 0.38 0.49 o 2 4 0 25.04 26.64 1.03 o 3 4 0 4.54 4.03 1.13 o 4 4 0 28.03 30.89 1.11 o 5 4 0 11.45 13.23 0.91 o 6 4 0 87.44 83.04 1.88 o 7 4 0 0.46 -0.11 0.57 o 8 4 0 18.91 22.71 1.44 o 9 4 0 28.68 31.44 2.31 o 10 4 0 0.54 0.25 0.99 o 11 4 0 2.47 1.04 1.35 o 12 4 0 7.71 10.11 1.73 o 13 4 0 0.06 0.55 1.70 o 1 5 0 2.78 2.34 0.69 o 2 5 0 16.80 17.46 1.31 o 3 5 0 15.71 12.11 1.56 o 4 5 0 65.79 58.10 2.95 o 5 5 0 1.52 2.32 0.98 o 6 5 0 42.31 38.06 1.80 o 7 5 0 4.59 4.39 1.39 o 8 5 0 0.16 -1.06 1.23 o 9 5 0 13.57 15.19 1.89 o 10 5 0 3.64 1.78 1.56 o 0 6 0 32.63 35.28 3.36 o 1 6 0 8.40 9.53 1.69 o 2 6 0 13.09 12.73 1.75 o 3 6 0 3.32 1.13 1.27 o 4 6 0 42.89 41.08 2.57 o 5 6 0 0.72 2.82 1.66 o 6 6 0 3.31 0.61 1.75 o 7 6 0 6.99 9.21 3.35 o 2 0 1 2621.81 2599.25 12.76 o 4 0 1 3277.53 3276.59 21.24 o 6 0 1 199.15 198.73 1.92 o 8 0 1 324.06 314.80 4.02 o 10 0 1 47.28 46.71 2.09 o 12 0 1 28.33 32.85 2.17 o 14 0 1 32.26 31.07 2.33 o 16 0 1 9.21 7.21 1.94 o 0 1 1 933.11 938.30 3.31 o 1 1 1 668.86 653.62 1.95 o 2 1 1 1995.18 1942.54 7.09 o 3 1 1 2918.61 2945.44 12.95 o 4 1 1 541.41 546.08 2.69 o 5 1 1 151.43 146.21 0.91 o 6 1 1 34.15 31.59 0.71 o 7 1 1 76.60 76.94 1.06 o 8 1 1 166.55 169.31 1.95 o 9 1 1 76.84 75.72 1.33 o 10 1 1 14.59 14.34 1.06 o 11 1 1 44.94 42.47 1.54 o 12 1 1 2.95 4.47 1.60 o 13 1 1 19.90 25.36 1.67 o 14 1 1 5.67 5.98 1.12 o 15 1 1 10.28 14.41 1.59 o 16 1 1 8.33 8.11 1.48 o 1 2 1 387.37 374.69 2.12 o 2 2 1 162.87 183.54 1.36 o 3 2 1 30.75 34.26 0.61 o 4 2 1 11.55 11.31 0.51 o 5 2 1 570.89 604.86 3.85 o 6 2 1 783.40 790.80 5.00 o 7 2 1 117.51 117.05 1.30 o 8 2 1 44.24 42.03 1.06 o 9 2 1 80.12 80.05 1.50 o 10 2 1 47.67 46.67 1.24 o 11 2 1 37.20 35.38 1.77 o 12 2 1 1.52 1.81 0.91 o 13 2 1 3.79 4.83 1.05 o 14 2 1 3.53 3.65 1.10 o 15 2 1 6.11 5.02 1.31 o 0 3 1 219.80 217.09 2.34 o 1 3 1 111.40 111.10 1.06 o 2 3 1 10.70 12.02 0.43 o 3 3 1 597.31 618.74 4.28 o 4 3 1 246.80 255.78 2.16 o 5 3 1 93.78 94.66 1.22 o 6 3 1 59.10 55.59 1.00 o 7 3 1 47.91 47.84 0.89 o 8 3 1 16.91 15.60 0.89 o 9 3 1 50.58 50.90 1.34 o 10 3 1 7.77 11.35 0.90 o 11 3 1 1.34 2.35 0.79 o 12 3 1 7.85 8.31 1.02 o 13 3 1 1.86 0.85 0.89 o 14 3 1 4.58 4.25 1.21 o 1 4 1 77.55 84.78 1.12 o 2 4 1 3.87 6.32 0.48 o 3 4 1 15.57 15.89 0.66 o 4 4 1 50.96 50.50 0.97 o 5 4 1 63.81 59.88 1.20 o 6 4 1 124.01 117.84 1.59 o 7 4 1 67.27 63.19 1.16 o 8 4 1 5.99 7.50 0.79 o 9 4 1 0.03 -0.34 0.72 o 10 4 1 38.02 37.84 1.51 o 11 4 1 3.62 4.08 1.00 o 12 4 1 1.22 2.16 1.03 o 13 4 1 0.89 -1.56 1.56 o 0 5 1 6.46 7.47 1.37 o 1 5 1 12.71 13.79 0.81 o 2 5 1 38.92 36.81 1.14 o 3 5 1 30.37 32.59 1.00 o 4 5 1 62.73 59.91 1.45 o 5 5 1 20.97 22.90 1.13 o 6 5 1 11.61 12.76 0.84 o 7 5 1 7.57 6.78 1.09 o 8 5 1 26.66 25.64 1.42 o 9 5 1 8.36 7.11 1.42 o 10 5 1 0.52 0.71 1.01 o 1 6 1 3.31 4.34 1.08 o 2 6 1 3.01 3.59 1.00 o 3 6 1 2.69 1.74 0.94 o 4 6 1 20.76 21.10 1.68 o 5 6 1 8.74 8.31 1.33 o 6 6 1 9.61 10.43 1.78 o 7 6 1 10.79 13.22 2.04 o 0 0 2 1238.46 1257.10 7.69 o 2 0 2 1395.34 1428.15 8.40 o 4 0 2 5025.47 4991.12 32.92 o 6 0 2 237.36 233.40 2.29 o 8 0 2 378.01 377.21 4.02 o 10 0 2 37.94 41.02 2.12 o 12 0 2 90.17 87.44 3.31 o 14 0 2 8.95 9.04 1.72 o 16 0 2 15.42 17.95 3.19 o 1 1 2 528.12 507.24 1.56 o 2 1 2 330.17 323.43 1.85 o 3 1 2 1883.63 1862.72 8.59 o 4 1 2 581.04 582.05 3.55 o 5 1 2 120.31 126.52 1.01 o 6 1 2 1035.72 1048.86 5.96 o 7 1 2 360.80 356.03 3.97 o 8 1 2 54.74 52.86 1.04 o 9 1 2 179.75 178.01 2.23 o 10 1 2 45.35 45.86 1.13 o 11 1 2 23.06 19.75 0.95 o 12 1 2 35.99 39.22 1.64 o 13 1 2 5.27 8.21 1.12 o 14 1 2 36.41 38.62 1.84 o 15 1 2 1.60 1.43 1.03 o 16 1 2 1.08 1.00 1.19 o 0 2 2 1269.62 1253.99 7.66 o 1 2 2 528.85 567.12 3.39 o 2 2 2 3.77 4.41 0.23 o 3 2 2 106.77 104.17 0.88 o 4 2 2 12.38 13.13 0.41 o 5 2 2 190.88 187.81 1.62 o 6 2 2 368.86 368.37 3.01 o 7 2 2 15.14 16.95 0.58 o 8 2 2 34.49 32.22 1.06 o 9 2 2 67.83 66.28 1.54 o 10 2 2 9.44 9.89 0.77 o 11 2 2 3.62 3.42 0.67 o 12 2 2 28.98 28.95 1.15 o 13 2 2 2.06 1.77 1.07 o 14 2 2 5.96 6.81 1.24 o 15 2 2 0.32 -0.38 1.09 o 1 3 2 218.73 226.05 1.92 o 2 3 2 73.97 72.95 0.88 o 3 3 2 121.26 121.66 1.34 o 4 3 2 49.91 51.14 0.75 o 5 3 2 61.74 60.18 1.04 o 6 3 2 29.23 28.47 0.83 o 7 3 2 69.77 68.26 1.22 o 8 3 2 52.30 50.22 1.18 o 9 3 2 65.19 66.62 1.50 o 10 3 2 55.73 56.41 1.52 o 11 3 2 0.56 0.71 0.68 o 12 3 2 15.14 17.50 1.33 o 13 3 2 2.05 4.86 1.75 o 14 3 2 2.21 0.98 1.27 o 0 4 2 165.02 158.11 2.91 o 1 4 2 158.20 156.89 2.24 o 2 4 2 75.20 72.15 1.30 o 3 4 2 6.42 6.84 0.60 o 4 4 2 3.14 3.44 0.59 o 5 4 2 68.25 68.89 1.38 o 6 4 2 5.45 7.82 0.67 o 7 4 2 58.26 53.19 1.69 o 8 4 2 37.89 35.61 1.28 o 9 4 2 6.08 7.50 0.96 o 10 4 2 3.34 5.30 1.17 o 11 4 2 6.87 6.62 1.09 o 12 4 2 1.18 1.85 1.06 o 1 5 2 18.06 20.52 0.95 o 2 5 2 62.83 60.78 1.44 o 3 5 2 0.44 0.92 0.65 o 4 5 2 3.41 4.75 0.73 o 5 5 2 2.61 4.50 1.20 o 6 5 2 3.15 4.87 0.74 o 7 5 2 30.04 29.41 1.44 o 8 5 2 1.64 2.69 1.44 o 9 5 2 1.04 0.96 1.06 o 10 5 2 0.85 1.14 1.26 o 0 6 2 96.52 93.68 4.45 o 1 6 2 1.69 3.25 1.13 o 2 6 2 9.52 9.67 1.27 o 3 6 2 3.76 5.68 1.14 o 4 6 2 10.70 15.10 2.06 o 5 6 2 3.84 5.39 1.61 o 6 6 2 2.45 3.28 1.39 o 2 0 3 1068.01 1037.34 6.98 o 4 0 3 1275.40 1314.56 10.06 o 6 0 3 287.40 278.41 2.97 o 8 0 3 9.44 8.77 0.76 o 10 0 3 80.08 81.60 1.91 o 12 0 3 38.66 36.35 2.26 o 14 0 3 25.50 22.89 2.29 o 0 1 3 2349.78 2333.23 11.91 o 1 1 3 269.66 289.47 1.66 o 2 1 3 1794.63 1822.79 8.07 o 3 1 3 461.40 461.42 2.60 o 4 1 3 41.90 43.63 0.62 o 5 1 3 354.12 380.41 2.59 o 6 1 3 54.63 59.53 0.82 o 7 1 3 372.70 354.02 2.73 o 8 1 3 94.86 93.42 1.48 o 9 1 3 49.17 46.27 0.94 o 10 1 3 5.13 7.68 1.03 o 11 1 3 3.24 2.31 0.70 o 12 1 3 70.06 69.36 2.05 o 13 1 3 3.50 5.33 1.18 o 14 1 3 7.11 10.04 1.36 o 15 1 3 5.71 11.55 2.38 o 1 2 3 8.54 10.32 0.40 o 2 2 3 187.65 181.12 1.33 o 3 2 3 380.05 401.58 2.67 o 4 2 3 561.47 574.34 5.17 o 5 2 3 331.26 327.65 2.45 o 6 2 3 168.47 167.06 1.65 o 7 2 3 100.95 96.00 1.18 o 8 2 3 57.27 51.14 1.05 o 9 2 3 68.12 65.05 1.42 o 10 2 3 254.82 246.04 3.25 o 11 2 3 66.37 62.42 1.56 o 12 2 3 43.32 41.66 1.56 o 13 2 3 3.79 5.63 1.32 o 14 2 3 1.88 1.78 1.12 o 15 2 3 4.60 4.35 1.58 o 0 3 3 72.25 67.73 1.38 o 1 3 3 139.36 146.60 1.48 o 2 3 3 43.78 44.10 0.80 o 3 3 3 177.07 185.32 2.34 o 4 3 3 12.75 12.53 0.79 o 5 3 3 17.48 18.97 0.65 o 6 3 3 53.73 55.13 1.03 o 7 3 3 112.64 107.90 1.60 o 8 3 3 85.79 78.14 1.39 o 9 3 3 128.88 120.57 2.03 o 10 3 3 17.67 14.46 0.88 o 11 3 3 4.04 4.89 1.09 o 12 3 3 4.73 6.48 1.06 o 13 3 3 19.22 20.10 1.90 o 14 3 3 4.26 3.71 1.72 o 1 4 3 208.95 203.94 2.48 o 2 4 3 105.49 106.52 1.80 o 3 4 3 55.45 53.03 1.02 o 4 4 3 35.21 31.67 0.95 o 5 4 3 28.84 30.30 0.97 o 6 4 3 55.52 55.21 1.22 o 7 4 3 47.54 46.63 1.17 o 8 4 3 0.42 1.33 0.82 o 9 4 3 34.89 33.66 1.60 o 10 4 3 0.79 1.69 0.92 o 11 4 3 32.17 31.56 1.70 o 12 4 3 2.02 2.68 1.08 o 0 5 3 218.05 208.33 4.25 o 1 5 3 28.13 30.79 1.31 o 2 5 3 17.58 16.75 1.04 o 3 5 3 86.55 81.83 2.36 o 4 5 3 61.11 61.84 1.71 o 5 5 3 18.67 18.48 1.13 o 6 5 3 1.27 1.68 0.81 o 7 5 3 3.35 5.08 1.08 o 8 5 3 4.42 3.39 1.16 o 9 5 3 7.81 11.13 1.60 o 10 5 3 1.53 1.67 1.32 o 1 6 3 4.54 9.20 1.38 o 2 6 3 40.39 39.18 1.99 o 3 6 3 2.79 3.97 1.21 o 4 6 3 0.04 0.02 0.97 o 5 6 3 12.46 15.94 1.91 o 6 6 3 0.41 3.13 1.69 o 0 0 4 501.80 496.86 5.38 o 2 0 4 342.79 337.36 2.94 o 4 0 4 211.13 221.18 2.81 o 6 0 4 445.28 463.08 5.51 o 8 0 4 87.87 88.17 1.68 o 10 0 4 45.80 43.05 1.95 o 12 0 4 13.75 12.51 1.91 o 14 0 4 10.00 10.22 2.02 o 1 1 4 482.60 530.09 3.15 o 2 1 4 328.45 349.11 2.54 o 3 1 4 36.98 37.15 0.75 o 4 1 4 1.03 1.52 0.30 o 5 1 4 76.38 74.62 0.95 o 6 1 4 87.92 89.68 1.41 o 7 1 4 42.86 44.97 0.87 o 8 1 4 72.76 74.34 1.11 o 9 1 4 34.20 33.50 0.97 o 10 1 4 28.91 28.26 1.00 o 11 1 4 5.48 6.72 0.73 o 12 1 4 6.49 9.40 1.13 o 13 1 4 22.97 22.58 1.50 o 14 1 4 2.89 4.12 1.21 o 15 1 4 3.48 3.12 1.29 o 0 2 4 1397.37 1459.95 9.25 o 1 2 4 182.93 182.93 1.59 o 2 2 4 52.78 56.71 0.91 o 3 2 4 246.80 260.60 2.39 o 4 2 4 261.87 260.70 1.99 o 5 2 4 145.47 144.40 1.46 o 6 2 4 198.27 200.04 1.87 o 7 2 4 79.22 77.66 1.11 o 8 2 4 44.19 43.43 0.88 o 9 2 4 32.09 27.65 0.92 o 10 2 4 5.15 5.32 0.75 o 11 2 4 11.40 11.18 1.02 o 12 2 4 4.68 7.03 0.98 o 13 2 4 5.92 4.74 1.08 o 14 2 4 5.25 7.82 1.63 o 1 3 4 71.38 72.50 1.24 o 2 3 4 142.01 143.88 1.62 o 3 3 4 11.28 13.83 0.81 o 4 3 4 68.21 67.87 1.23 o 5 3 4 243.37 238.78 2.86 o 6 3 4 21.57 21.35 0.90 o 7 3 4 184.43 176.84 2.30 o 8 3 4 19.56 20.57 1.00 o 9 3 4 28.91 26.05 1.19 o 10 3 4 3.24 4.84 0.95 o 11 3 4 5.74 6.68 1.10 o 12 3 4 13.78 13.35 1.32 o 13 3 4 10.69 13.20 1.80 o 0 4 4 65.88 66.82 1.70 o 1 4 4 25.69 26.25 0.98 o 2 4 4 16.61 16.72 0.88 o 3 4 4 266.02 265.02 3.70 o 4 4 4 4.77 5.87 0.61 o 5 4 4 74.82 69.40 1.45 o 6 4 4 13.64 13.28 0.95 o 7 4 4 9.45 10.85 0.83 o 8 4 4 2.58 2.78 0.90 o 9 4 4 25.31 23.02 1.46 o 10 4 4 5.08 5.48 1.11 o 11 4 4 5.35 3.55 1.17 o 12 4 4 0.53 0.25 1.12 o 1 5 4 63.49 60.17 1.89 o 2 5 4 4.63 8.02 1.02 o 3 5 4 17.08 15.53 1.08 o 4 5 4 24.76 27.74 1.86 o 5 5 4 9.12 9.41 0.96 o 6 5 4 8.98 10.47 1.10 o 7 5 4 19.98 21.05 1.63 o 8 5 4 3.18 2.47 1.18 o 9 5 4 15.00 15.72 1.74 o 0 6 4 4.18 6.63 1.85 o 1 6 4 9.21 9.87 1.29 o 2 6 4 7.23 7.90 1.26 o 3 6 4 0.54 0.35 1.06 o 4 6 4 0.55 1.76 1.11 o 5 6 4 2.01 2.22 1.49 o 2 0 5 417.47 422.12 3.98 o 4 0 5 38.35 37.07 1.42 o 6 0 5 35.38 37.62 1.86 o 8 0 5 71.16 67.95 1.94 o 10 0 5 63.76 60.00 1.64 o 12 0 5 5.84 7.38 1.65 o 14 0 5 9.42 15.28 2.20 o 0 1 5 1067.12 1094.13 8.08 o 1 1 5 554.84 573.56 3.17 o 2 1 5 1.78 1.66 0.27 o 3 1 5 222.72 238.97 1.88 o 4 1 5 254.95 261.69 2.10 o 5 1 5 41.53 42.78 0.76 o 6 1 5 106.13 107.05 1.34 o 7 1 5 23.54 24.69 0.73 o 8 1 5 17.85 17.66 0.70 o 9 1 5 38.56 38.36 0.91 o 10 1 5 19.85 19.59 1.45 o 11 1 5 13.86 14.62 0.94 o 12 1 5 2.15 2.42 0.91 o 13 1 5 7.78 10.46 1.36 o 14 1 5 2.61 1.07 1.16 o 1 2 5 195.22 181.67 2.16 o 2 2 5 347.45 366.40 3.18 o 3 2 5 110.33 110.48 1.58 o 4 2 5 14.98 19.29 0.95 o 5 2 5 42.79 39.94 1.48 o 6 2 5 123.77 118.32 1.59 o 7 2 5 100.02 99.66 1.38 o 8 2 5 44.71 43.60 0.93 o 9 2 5 4.83 4.61 0.59 o 10 2 5 22.16 21.83 1.04 o 11 2 5 11.56 16.65 1.48 o 12 2 5 21.90 23.12 1.60 o 13 2 5 14.61 17.45 1.76 o 14 2 5 10.64 12.72 1.87 o 0 3 5 132.90 137.48 3.52 o 1 3 5 80.52 77.82 1.75 o 2 3 5 166.03 156.85 2.18 o 3 3 5 295.78 290.25 3.08 o 4 3 5 16.78 16.32 0.76 o 5 3 5 85.43 81.80 1.69 o 6 3 5 44.29 43.84 1.18 o 7 3 5 32.99 32.73 1.07 o 8 3 5 19.21 21.35 1.16 o 9 3 5 18.13 19.34 1.51 o 10 3 5 2.55 1.15 0.95 o 11 3 5 13.66 16.39 1.69 o 12 3 5 4.52 4.37 1.33 o 13 3 5 9.10 12.36 1.79 o 1 4 5 15.60 17.72 1.12 o 2 4 5 16.92 18.66 1.12 o 3 4 5 104.02 98.90 1.94 o 4 4 5 60.41 56.20 2.69 o 5 4 5 98.49 94.52 2.04 o 6 4 5 33.49 33.85 1.49 o 7 4 5 33.28 30.75 1.15 o 8 4 5 3.02 4.28 0.99 o 9 4 5 17.64 21.05 1.45 o 10 4 5 8.95 11.18 1.35 o 11 4 5 2.66 3.63 1.39 o 0 5 5 124.40 120.05 3.95 o 1 5 5 6.07 9.45 1.14 o 2 5 5 11.05 11.74 1.16 o 3 5 5 18.44 20.00 1.64 o 4 5 5 11.40 13.17 1.19 o 5 5 5 22.44 20.88 1.38 o 6 5 5 1.61 3.61 1.09 o 7 5 5 4.67 3.08 1.36 o 8 5 5 3.01 3.07 1.32 o 1 6 5 3.25 3.36 1.22 o 2 6 5 17.99 15.34 1.57 o 3 6 5 5.37 7.47 1.29 o 0 0 6 547.15 555.07 7.49 o 2 0 6 1608.29 1674.95 15.14 o 4 0 6 13.50 14.27 0.74 o 6 0 6 172.13 176.16 3.23 o 8 0 6 28.81 29.49 1.28 o 10 0 6 17.40 15.85 1.11 o 12 0 6 11.41 14.89 1.88 o 14 0 6 4.20 3.98 2.15 o 1 1 6 48.67 47.33 0.74 o 2 1 6 52.49 52.31 1.11 o 3 1 6 95.76 97.20 1.31 o 4 1 6 500.31 503.03 5.10 o 5 1 6 27.05 28.65 0.72 o 6 1 6 35.13 35.13 0.97 o 7 1 6 127.53 124.88 1.66 o 8 1 6 56.62 57.03 1.16 o 9 1 6 118.15 116.50 1.78 o 10 1 6 49.87 46.73 1.31 o 11 1 6 18.31 21.84 1.19 o 12 1 6 1.57 4.70 1.22 o 13 1 6 1.08 1.09 1.02 o 14 1 6 3.19 3.47 1.58 o 0 2 6 329.86 321.60 4.19 o 1 2 6 89.69 91.40 1.33 o 2 2 6 50.01 47.66 1.04 o 3 2 6 65.64 67.78 1.21 o 4 2 6 162.81 162.21 2.17 o 5 2 6 74.67 73.32 1.49 o 6 2 6 2.44 4.90 0.63 o 7 2 6 124.31 117.93 1.92 o 8 2 6 40.22 43.48 1.69 o 9 2 6 135.58 132.10 2.28 o 10 2 6 0.24 1.77 1.27 o 11 2 6 20.97 20.53 1.65 o 12 2 6 25.71 24.13 1.78 o 13 2 6 5.21 5.87 1.53 o 1 3 6 31.14 31.82 1.37 o 2 3 6 3.23 3.14 0.80 o 3 3 6 126.03 122.57 1.78 o 4 3 6 21.85 21.22 0.86 o 5 3 6 118.61 115.37 1.97 o 6 3 6 108.73 110.73 1.95 o 7 3 6 113.28 109.95 2.07 o 8 3 6 1.80 3.09 0.83 o 9 3 6 69.00 61.75 2.10 o 10 3 6 25.23 26.79 1.81 o 11 3 6 42.73 40.86 2.01 o 12 3 6 8.73 8.40 1.49 o 0 4 6 139.06 140.51 4.16 o 1 4 6 29.70 28.82 1.57 o 2 4 6 20.33 20.03 1.28 o 3 4 6 10.57 12.65 1.15 o 4 4 6 42.92 44.98 1.66 o 5 4 6 39.70 36.99 1.86 o 6 4 6 14.81 15.30 1.60 o 7 4 6 40.23 38.35 1.79 o 8 4 6 2.75 3.11 1.28 o 9 4 6 21.02 21.58 1.89 o 10 4 6 4.10 4.78 1.45 o 1 5 6 7.55 8.86 1.10 o 2 5 6 50.84 52.71 2.06 o 3 5 6 1.99 3.05 1.03 o 4 5 6 2.07 1.37 1.00 o 5 5 6 3.19 3.20 1.10 o 6 5 6 12.37 14.70 1.51 o 7 5 6 1.19 2.33 1.40 o 2 0 7 142.75 142.27 2.11 o 4 0 7 408.51 413.10 5.12 o 6 0 7 557.10 549.82 7.16 o 8 0 7 5.01 7.71 1.01 o 10 0 7 82.73 77.84 2.48 o 12 0 7 60.56 57.34 3.54 o 0 1 7 239.75 230.76 5.01 o 1 1 7 30.51 31.08 0.75 o 2 1 7 70.79 69.42 1.08 o 3 1 7 155.94 152.14 1.85 o 4 1 7 130.74 133.02 1.86 o 5 1 7 11.88 12.71 0.83 o 6 1 7 74.50 73.91 1.43 o 7 1 7 18.88 20.28 1.31 o 8 1 7 35.50 36.92 1.13 o 9 1 7 17.83 17.58 1.01 o 10 1 7 19.18 19.88 1.06 o 11 1 7 16.09 17.90 1.31 o 12 1 7 26.32 27.49 1.80 o 13 1 7 2.03 2.81 1.37 o 1 2 7 57.50 55.74 1.20 o 2 2 7 15.47 16.60 0.86 o 3 2 7 9.51 11.00 0.73 o 4 2 7 40.01 40.72 1.09 o 5 2 7 24.46 25.54 1.00 o 6 2 7 47.45 48.65 1.35 o 7 2 7 85.17 80.10 1.82 o 8 2 7 59.98 58.51 2.18 o 9 2 7 14.86 13.85 1.12 o 10 2 7 7.90 11.83 1.18 o 11 2 7 2.64 2.77 1.09 o 12 2 7 0.27 -0.43 1.23 o 0 3 7 49.35 47.62 2.19 o 1 3 7 144.97 138.99 2.59 o 2 3 7 45.01 43.96 1.59 o 3 3 7 30.17 26.17 1.23 o 4 3 7 29.08 28.46 1.30 o 5 3 7 43.67 44.45 1.74 o 6 3 7 31.03 28.27 1.11 o 7 3 7 1.68 0.88 0.67 o 8 3 7 8.86 10.65 1.07 o 9 3 7 8.24 10.83 1.35 o 10 3 7 2.79 1.81 1.06 o 11 3 7 1.95 2.38 1.17 o 1 4 7 23.20 21.51 1.29 o 2 4 7 33.32 29.49 1.42 o 3 4 7 21.13 20.25 1.33 o 4 4 7 3.22 4.41 1.03 o 5 4 7 11.14 12.29 1.29 o 6 4 7 4.87 5.64 1.16 o 7 4 7 2.65 4.64 1.21 o 8 4 7 0.52 -0.44 1.18 o 9 4 7 18.29 24.17 2.01 o 0 5 7 26.41 33.93 3.57 o 1 5 7 4.72 5.74 1.19 o 2 5 7 7.82 10.45 1.38 o 3 5 7 20.63 21.33 1.48 o 4 5 7 5.91 7.85 1.66 o 5 5 7 1.18 1.13 1.13 o 6 5 7 0.28 0.98 1.24 o 0 0 8 417.86 411.54 10.16 o 2 0 8 285.40 278.80 3.84 o 4 0 8 41.48 39.95 1.29 o 6 0 8 4.08 3.39 0.90 o 8 0 8 66.84 64.47 1.86 o 10 0 8 34.05 31.34 2.22 o 12 0 8 3.78 3.21 1.87 o 1 1 8 76.17 80.08 1.76 o 2 1 8 47.66 48.69 1.23 o 3 1 8 44.91 41.40 1.13 o 4 1 8 77.15 72.67 1.53 o 5 1 8 145.25 142.47 2.25 o 6 1 8 13.32 15.75 1.01 o 7 1 8 28.19 25.97 1.09 o 8 1 8 11.07 16.22 1.00 o 9 1 8 25.75 25.01 1.15 o 10 1 8 18.49 15.46 1.07 o 11 1 8 7.07 7.89 1.30 o 12 1 8 13.89 14.05 2.01 o 0 2 8 198.40 183.76 4.33 o 1 2 8 56.08 53.80 1.38 o 2 2 8 62.95 58.32 1.50 o 3 2 8 205.29 198.90 3.03 o 4 2 8 36.57 37.71 1.39 o 5 2 8 14.10 14.68 0.97 o 6 2 8 9.71 13.44 0.98 o 7 2 8 41.50 41.68 1.40 o 8 2 8 13.78 14.28 0.99 o 9 2 8 14.94 18.01 1.27 o 10 2 8 3.26 4.49 1.10 o 11 2 8 0.21 0.78 1.11 o 1 3 8 79.74 69.03 1.97 o 2 3 8 7.94 6.54 1.03 o 3 3 8 65.11 62.12 1.89 o 4 3 8 5.58 6.91 1.05 o 5 3 8 62.95 61.00 2.07 o 6 3 8 5.00 7.01 1.29 o 7 3 8 16.08 14.75 1.44 o 8 3 8 1.65 3.51 1.18 o 9 3 8 11.76 12.17 1.41 o 10 3 8 15.86 20.18 1.79 o 0 4 8 28.14 29.55 2.36 o 1 4 8 20.27 20.90 2.10 o 2 4 8 19.15 21.42 1.45 o 3 4 8 25.00 25.65 1.62 o 4 4 8 6.53 8.27 1.25 o 5 4 8 19.90 24.08 1.43 o 6 4 8 5.95 7.69 1.21 o 7 4 8 6.85 6.96 1.48 o 8 4 8 4.55 7.16 1.66 o 1 5 8 0.33 -1.13 1.13 o 2 5 8 6.02 8.89 1.64 o 3 5 8 4.30 5.30 1.35 o 4 5 8 11.34 13.84 1.59 o 2 0 9 611.42 575.80 7.39 o 4 0 9 8.05 8.98 1.31 o 6 0 9 170.65 173.78 4.00 o 8 0 9 22.38 21.91 1.77 o 10 0 9 31.65 35.30 2.55 o 0 1 9 640.91 622.37 9.35 o 1 1 9 53.59 54.39 1.44 o 2 1 9 31.17 30.23 1.18 o 3 1 9 190.36 182.77 2.93 o 4 1 9 99.03 99.57 1.92 o 5 1 9 32.42 32.35 1.17 o 6 1 9 17.00 18.54 1.08 o 7 1 9 19.49 21.32 1.05 o 8 1 9 11.19 13.61 1.07 o 9 1 9 16.41 16.44 1.34 o 10 1 9 2.89 2.15 1.26 o 11 1 9 0.71 -1.46 1.46 o 1 2 9 65.72 63.37 1.83 o 2 2 9 42.08 42.44 1.36 o 3 2 9 8.27 10.78 0.97 o 4 2 9 11.59 13.49 1.03 o 5 2 9 31.75 25.99 1.32 o 6 2 9 27.30 35.65 3.40 o 7 2 9 3.75 7.45 1.09 o 8 2 9 21.37 20.90 1.37 o 9 2 9 2.88 3.78 1.13 o 10 2 9 1.67 0.77 1.10 o 0 3 9 21.81 25.46 2.85 o 1 3 9 10.16 11.69 1.10 o 2 3 9 4.56 4.69 0.97 o 3 3 9 9.62 11.02 1.22 o 4 3 9 16.92 16.09 1.40 o 5 3 9 8.13 12.12 1.24 o 6 3 9 18.82 20.46 1.49 o 7 3 9 6.72 9.56 1.42 o 8 3 9 2.13 2.05 1.41 o 9 3 9 9.63 15.37 2.82 o 1 4 9 20.33 21.45 1.58 o 2 4 9 19.50 19.52 1.96 o 3 4 9 2.56 3.52 1.16 o 4 4 9 7.92 11.08 1.37 o 5 4 9 4.02 2.56 1.17 o 6 4 9 0.99 1.80 1.28 o 0 0 10 64.13 60.38 4.55 o 2 0 10 17.91 17.09 1.37 o 4 0 10 45.35 48.39 2.79 o 6 0 10 3.73 4.59 1.26 o 8 0 10 11.05 13.53 1.56 o 10 0 10 0.34 0.37 2.02 o 1 1 10 44.90 43.23 1.35 o 2 1 10 49.32 50.14 1.42 o 3 1 10 52.24 49.84 1.56 o 4 1 10 23.86 25.28 1.56 o 5 1 10 6.57 6.73 1.01 o 6 1 10 13.34 12.26 1.17 o 7 1 10 3.82 4.27 1.08 o 8 1 10 0.71 1.94 1.04 o 9 1 10 23.27 25.37 3.07 o 0 2 10 98.65 94.21 3.55 o 1 2 10 20.98 21.96 1.41 o 2 2 10 56.31 55.28 1.93 o 3 2 10 17.16 16.53 1.62 o 4 2 10 46.78 44.76 1.86 o 5 2 10 11.85 13.09 1.36 o 6 2 10 13.01 16.23 1.40 o 7 2 10 6.94 9.46 1.23 o 8 2 10 4.07 6.35 1.56 o 9 2 10 10.54 12.43 2.29 o 1 3 10 5.84 6.58 1.17 o 2 3 10 14.14 14.40 1.35 o 3 3 10 1.44 2.02 1.07 o 4 3 10 12.12 14.42 1.43 o 5 3 10 14.15 13.87 1.43 o 6 3 10 0.93 1.47 1.02 o 7 3 10 2.81 3.18 1.30 o 0 4 10 23.68 31.51 3.01 o 1 4 10 4.39 4.40 1.27 o 2 4 10 0.09 2.00 1.18 o 3 4 10 17.98 18.38 1.73 o 2 0 11 61.73 58.18 2.80 o 4 0 11 0.33 0.11 1.29 o 6 0 11 131.48 128.17 5.98 o 8 0 11 24.59 24.30 3.02 o 0 1 11 29.77 29.43 2.06 o 1 1 11 18.49 18.30 1.27 o 2 1 11 4.77 6.63 1.30 o 3 1 11 3.56 5.79 1.08 o 4 1 11 52.54 50.86 2.04 o 5 1 11 11.32 12.43 1.34 o 6 1 11 29.43 29.91 1.78 o 7 1 11 13.53 16.08 1.52 o 8 1 11 26.35 26.81 1.97 o 1 2 11 1.64 1.08 0.93 o 2 2 11 9.84 12.65 1.34 o 3 2 11 23.03 25.48 1.69 o 4 2 11 26.39 30.67 1.86 o 5 2 11 11.73 14.80 1.63 o 6 2 11 21.80 25.15 1.93 o 0 3 11 27.36 23.44 2.23 o 1 3 11 7.28 6.08 1.28 o 2 3 11 2.49 3.06 1.20 o 3 3 11 21.46 24.88 1.66 o 4 3 11 7.86 10.52 1.47 o 0 0 12 89.61 83.73 5.28 o 2 0 12 24.56 21.80 2.43 o 4 0 12 25.08 20.45 2.93 o 1 1 12 2.88 4.07 1.50 o 2 1 12 44.97 50.44 2.65 o 3 1 12 3.72 4.57 1.51 o 4 1 12 20.60 24.22 2.13 o 5 1 12 3.34 1.45 1.40 o 0 2 12 47.97 48.11 3.50 o 1 2 12 1.32 2.31 1.53 o 2 2 12 27.93 28.45 2.20 o 3 2 12 2.91 3.02 1.44 o