#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:42:55 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181280 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/58/2235809.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2235809_Fobs loop_ _publ_author_name 'Trella, Thomas' 'Frank, Walter' _publ_section_title ; Hexaaquaaluminium(III) tris(methanesulfonate) ; _journal_coeditor_code GG2089 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1136 _journal_page_last m1137 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 117.035 _cell_angle_gamma 90.000 _cell_length_a 16.4677 _cell_length_b 6.4239 _cell_length_c 17.4295 _exptl_crystal_F_000 880.00 _reflns_d_resolution_high 0.8410 _cod_data_source_file gg2089Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Al in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 261.07 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1129.67 1326.60 55.13 o 4 0 0 14644.06 16411.04 309.28 o 6 0 0 10990.56 11301.47 111.92 o 8 0 0 38.94 26.05 25.66 o 10 0 0 62.28 91.44 24.78 o 12 0 0 10934.46 10374.72 98.78 o 14 0 0 520.81 467.31 31.92 o 16 0 0 1091.77 1200.42 41.08 o 1 1 0 56.87 21.16 25.35 o 2 1 0 4316.99 5176.83 66.80 o 3 1 0 460.42 433.17 26.03 o 4 1 0 339.57 355.06 21.32 o 5 1 0 38.21 86.33 18.48 o 6 1 0 146.14 123.23 19.82 o 7 1 0 238.98 202.00 16.66 o 8 1 0 747.79 761.32 20.53 o 9 1 0 1502.57 1437.51 22.19 o 10 1 0 1991.94 1974.50 24.55 o 11 1 0 1892.29 1816.97 23.04 o 12 1 0 24.40 10.81 19.38 o 13 1 0 1606.34 1608.68 25.38 o 14 1 0 596.62 560.51 22.75 o 15 1 0 704.85 720.74 23.39 o 16 1 0 23.12 15.13 26.39 o 17 1 0 138.68 130.96 24.22 o 0 2 0 41163.82 44009.35 1352.87 o 1 2 0 3984.37 4002.57 80.07 o 2 2 0 833.54 826.57 21.86 o 3 2 0 337.57 425.03 20.57 o 4 2 0 539.55 445.10 19.96 o 5 2 0 313.69 376.28 18.89 o 6 2 0 1978.09 2212.01 40.37 o 7 2 0 158.12 157.36 16.79 o 8 2 0 93.47 74.03 16.75 o 9 2 0 95.03 106.08 18.01 o 10 2 0 212.75 224.81 15.40 o 11 2 0 1403.91 1390.11 28.39 o 12 2 0 5822.06 5713.83 73.07 o 13 2 0 93.56 98.63 23.33 o 14 2 0 1.08 -9.41 23.30 o 15 2 0 149.93 115.62 27.49 o 16 2 0 392.33 400.20 27.68 o 1 3 0 3.46 17.41 17.07 o 2 3 0 375.29 486.40 19.73 o 3 3 0 543.59 586.07 20.00 o 4 3 0 5073.47 5405.40 100.44 o 5 3 0 4955.23 5349.50 92.75 o 6 3 0 2042.65 2270.16 43.45 o 7 3 0 1034.94 1023.86 23.51 o 8 3 0 0.02 4.44 18.18 o 9 3 0 687.09 670.21 19.02 o 10 3 0 331.74 306.34 21.17 o 11 3 0 666.81 651.20 22.51 o 12 3 0 55.04 35.96 20.93 o 13 3 0 526.06 501.92 27.03 o 14 3 0 284.05 285.87 22.91 o 15 3 0 35.88 17.67 26.45 o 16 3 0 30.28 34.71 26.84 o 0 4 0 8614.58 8907.19 259.99 o 1 4 0 389.21 391.57 18.59 o 2 4 0 178.06 190.00 18.68 o 3 4 0 121.28 102.78 18.36 o 4 4 0 2753.71 2747.69 50.57 o 5 4 0 1058.10 1037.93 20.88 o 6 4 0 466.55 484.42 18.06 o 7 4 0 928.35 882.99 22.42 o 8 4 0 201.71 164.79 17.69 o 9 4 0 2.65 3.61 22.56 o 10 4 0 8.13 8.97 22.74 o 11 4 0 350.12 287.90 23.67 o 12 4 0 741.60 698.28 27.36 o 13 4 0 309.88 381.59 28.20 o 14 4 0 431.37 433.90 30.09 o 1 5 0 177.66 141.89 18.20 o 2 5 0 3335.48 3246.40 77.70 o 3 5 0 621.96 595.84 21.36 o 4 5 0 173.10 154.51 16.72 o 5 5 0 5011.78 5074.92 84.68 o 6 5 0 277.74 262.32 21.10 o 7 5 0 3967.57 4043.68 92.31 o 8 5 0 71.35 41.37 22.68 o 9 5 0 323.50 301.29 21.71 o 10 5 0 1058.75 1108.13 25.02 o 11 5 0 514.66 546.00 29.49 o 12 5 0 13.30 21.77 28.58 o 13 5 0 0.00 -10.49 26.65 o 0 6 0 841.58 803.66 31.85 o 1 6 0 14.67 18.43 22.05 o 2 6 0 29.74 31.75 20.43 o 3 6 0 6.69 11.30 22.51 o 4 6 0 527.25 535.87 22.96 o 5 6 0 37.76 29.47 19.80 o 6 6 0 100.57 69.07 20.17 o 7 6 0 39.81 18.95 24.24 o 8 6 0 114.25 111.26 28.26 o 9 6 0 300.98 283.63 23.15 o 10 6 0 118.43 101.07 25.67 o 1 7 0 78.14 106.67 26.87 o 2 7 0 674.08 718.59 28.22 o 3 7 0 200.09 171.70 30.02 o 4 7 0 193.52 184.06 26.44 o 5 7 0 1269.20 1294.90 31.42 o 6 7 0 29.04 14.60 26.32 o -17 0 1 99.74 69.46 38.13 o -15 0 1 3.48 -2.91 36.91 o -13 0 1 701.79 755.80 38.60 o -11 0 1 402.84 391.29 22.95 o -9 0 1 3.16 0.99 27.10 o -7 0 1 12.00 0.07 32.97 o -5 0 1 4213.13 4098.92 124.49 o -3 0 1 165.32 313.04 40.16 o 1 0 1 5354.33 7453.23 106.90 o 3 0 1 4984.37 5709.98 69.80 o 5 0 1 335.44 365.33 26.86 o 7 0 1 2638.51 2578.33 35.92 o 9 0 1 3.71 7.24 24.45 o 11 0 1 34.93 29.86 23.68 o 13 0 1 298.88 278.63 31.02 o 15 0 1 1846.72 1803.60 42.28 o -17 1 1 85.70 58.63 29.42 o -16 1 1 15.87 15.88 27.11 o -15 1 1 258.65 224.31 20.55 o -14 1 1 350.55 322.59 20.62 o -13 1 1 133.57 130.34 23.39 o -12 1 1 110.05 78.67 15.98 o -11 1 1 42.42 15.90 18.63 o -10 1 1 7774.23 7292.64 74.23 o -9 1 1 1532.40 1565.19 24.27 o -8 1 1 2872.08 3141.60 35.69 o -7 1 1 30.74 32.08 21.68 o -6 1 1 62.87 17.88 21.66 o -5 1 1 1991.21 2196.07 34.95 o -4 1 1 4057.06 4013.85 48.41 o -3 1 1 1247.84 1461.00 32.39 o -2 1 1 7551.01 9249.37 135.32 o -1 1 1 1533.61 1866.18 37.42 o 0 1 1 570.00 763.12 31.04 o 1 1 1 0.13 1.38 26.62 o 3 1 1 1184.73 1253.08 27.23 o 4 1 1 4615.33 4941.57 65.45 o 5 1 1 2726.54 2955.74 32.23 o 6 1 1 4563.70 4301.35 40.64 o 7 1 1 4435.80 4724.58 35.31 o 8 1 1 324.29 350.80 20.34 o 9 1 1 521.63 546.33 17.80 o 10 1 1 112.49 101.01 18.81 o 11 1 1 9.29 7.32 16.89 o 12 1 1 41.27 17.87 19.52 o 13 1 1 37.94 38.61 21.05 o 14 1 1 2918.25 2831.71 41.65 o 15 1 1 129.20 130.25 26.00 o 16 1 1 28.50 26.05 25.32 o -17 2 1 6.71 -8.92 29.47 o -16 2 1 357.23 360.90 35.16 o -15 2 1 20.77 19.27 21.38 o -14 2 1 5.01 17.42 22.12 o -13 2 1 352.00 318.72 25.18 o -12 2 1 863.49 831.74 26.32 o -11 2 1 6.59 6.03 20.59 o -10 2 1 1978.78 1895.41 27.79 o -9 2 1 1142.89 1061.51 21.58 o -8 2 1 1137.35 1161.74 22.04 o -7 2 1 4458.39 4829.55 73.40 o -6 2 1 3.21 -6.15 22.09 o -5 2 1 594.88 725.06 20.61 o -4 2 1 15964.19 16570.88 352.99 o -3 2 1 2490.61 2826.23 51.81 o -2 2 1 1307.26 1358.82 24.22 o -1 2 1 2015.39 2163.85 30.95 o 0 2 1 2232.78 2011.24 39.31 o 1 2 1 306.71 292.83 21.10 o 2 2 1 5755.64 5954.94 99.23 o 3 2 1 683.10 649.00 19.37 o 4 2 1 819.98 793.69 25.08 o 5 2 1 127.97 159.42 20.63 o 6 2 1 189.17 190.55 20.07 o 7 2 1 7407.88 7596.85 112.44 o 8 2 1 9.58 7.95 18.56 o 9 2 1 2029.30 1918.95 24.45 o 10 2 1 141.85 135.59 17.26 o 11 2 1 1029.11 967.46 20.00 o 12 2 1 850.14 852.65 26.48 o 13 2 1 841.57 821.85 24.73 o 14 2 1 397.65 415.95 25.82 o 15 2 1 777.59 732.04 27.03 o 16 2 1 111.14 99.18 29.49 o -16 3 1 5.84 28.57 32.59 o -15 3 1 615.59 634.44 30.19 o -14 3 1 547.90 559.60 23.80 o -13 3 1 546.96 567.06 22.59 o -12 3 1 494.47 482.09 23.05 o -11 3 1 482.41 505.60 23.96 o -10 3 1 3673.51 3489.58 80.16 o -9 3 1 5880.34 5698.02 103.98 o -8 3 1 46.81 15.77 15.52 o -7 3 1 97.69 104.34 18.56 o -6 3 1 3391.55 3534.44 60.98 o -5 3 1 1710.27 1679.39 31.31 o -4 3 1 239.50 243.45 19.96 o -3 3 1 645.99 684.19 20.88 o -2 3 1 1546.87 1525.48 26.53 o -1 3 1 45.37 54.63 19.67 o 0 3 1 137.71 104.36 17.60 o 1 3 1 1160.29 1252.61 24.14 o 2 3 1 14359.80 15181.82 254.99 o 3 3 1 1981.24 2126.16 35.09 o 4 3 1 317.27 342.29 18.57 o 5 3 1 10.22 -4.01 17.79 o 6 3 1 4806.32 4808.08 78.98 o 7 3 1 169.48 178.76 21.00 o 8 3 1 1526.09 1573.38 36.90 o 9 3 1 47.72 44.04 18.41 o 10 3 1 31.93 21.88 19.18 o 11 3 1 134.54 132.67 19.58 o 12 3 1 1.07 9.78 21.03 o 13 3 1 261.00 234.76 22.02 o 14 3 1 1611.84 1714.23 31.94 o 15 3 1 692.91 712.44 28.49 o -15 4 1 5.09 -1.22 25.62 o -14 4 1 7.99 -18.02 26.26 o -13 4 1 196.63 189.63 24.59 o -12 4 1 924.66 956.76 25.50 o -11 4 1 18.84 24.57 20.85 o -10 4 1 586.06 569.79 22.17 o -9 4 1 264.87 273.55 21.40 o -8 4 1 3210.67 3034.99 80.18 o -7 4 1 548.10 516.35 19.78 o -6 4 1 0.03 -9.96 18.93 o -5 4 1 1908.29 1849.86 35.61 o -4 4 1 2440.99 2612.32 45.26 o -3 4 1 887.26 831.53 22.03 o -2 4 1 153.43 164.07 15.89 o -1 4 1 7.33 10.08 14.72 o 0 4 1 4215.20 4353.43 64.97 o 1 4 1 1789.91 1678.57 34.46 o 2 4 1 1203.27 1252.87 23.71 o 3 4 1 46.90 39.62 15.94 o 4 4 1 8464.65 8189.96 145.91 o 5 4 1 111.05 98.54 15.09 o 6 4 1 10.00 6.73 19.00 o 7 4 1 753.65 721.01 18.50 o 8 4 1 894.15 856.36 23.39 o 9 4 1 722.65 745.85 22.58 o 10 4 1 1.29 2.66 22.76 o 11 4 1 10.27 -0.23 18.28 o 12 4 1 579.79 564.60 23.37 o 13 4 1 935.60 992.35 31.45 o 14 4 1 133.22 111.28 28.27 o -13 5 1 285.93 245.71 29.65 o -12 5 1 737.71 758.27 30.43 o -11 5 1 107.84 90.74 24.51 o -10 5 1 0.02 -10.36 24.16 o -9 5 1 637.05 591.69 22.37 o -8 5 1 163.13 139.91 24.21 o -7 5 1 642.43 642.79 25.28 o -6 5 1 422.00 375.32 22.51 o -5 5 1 24.45 10.27 17.07 o -4 5 1 247.72 236.15 17.11 o -3 5 1 315.75 315.03 17.30 o -2 5 1 31.44 17.67 15.57 o -1 5 1 127.02 143.41 14.94 o 0 5 1 3195.98 3118.61 56.95 o 1 5 1 33.23 18.59 16.25 o 2 5 1 14.03 2.36 16.86 o 3 5 1 335.74 288.56 18.76 o 4 5 1 78.76 54.59 17.89 o 5 5 1 1012.58 1028.71 27.10 o 6 5 1 1064.14 1142.30 29.36 o 7 5 1 965.19 946.08 24.21 o 8 5 1 206.02 176.21 21.12 o 9 5 1 576.18 536.77 22.50 o 10 5 1 402.12 389.59 22.52 o 11 5 1 80.38 80.71 27.22 o 12 5 1 0.13 -3.55 24.24 o -11 6 1 310.41 283.87 25.30 o -10 6 1 10.84 -6.02 28.64 o -9 6 1 680.32 705.93 27.50 o -8 6 1 1292.85 1445.10 32.67 o -7 6 1 597.45 599.69 24.44 o -6 6 1 336.15 317.28 26.07 o -5 6 1 2186.67 2296.11 54.75 o -4 6 1 14.22 5.86 25.07 o -3 6 1 1482.87 1466.91 38.25 o -2 6 1 1371.77 1365.47 28.62 o -1 6 1 746.06 745.77 20.94 o 0 6 1 178.40 182.10 20.10 o 1 6 1 302.15 292.00 22.05 o 2 6 1 975.02 1012.01 24.61 o 3 6 1 16.14 6.37 18.92 o 4 6 1 1534.58 1538.92 41.29 o 5 6 1 32.59 16.05 18.51 o 6 6 1 18.14 11.69 19.30 o 7 6 1 1587.84 1665.98 33.91 o 8 6 1 94.40 85.71 25.09 o 9 6 1 1186.74 1356.10 28.36 o 10 6 1 0.10 13.09 26.27 o -7 7 1 57.41 42.83 28.99 o -6 7 1 59.81 52.52 32.06 o -5 7 1 41.50 23.89 26.00 o -4 7 1 10.36 8.56 28.14 o -3 7 1 3.12 1.85 27.20 o -2 7 1 8.53 24.90 25.39 o -1 7 1 174.54 145.84 29.89 o 0 7 1 53.54 61.44 27.90 o 1 7 1 0.76 -6.85 27.88 o 2 7 1 31.95 21.86 23.82 o 3 7 1 83.36 50.08 29.92 o 4 7 1 9.28 8.66 28.46 o 5 7 1 52.32 40.06 30.28 o 6 7 1 458.31 386.11 27.69 o -18 0 2 63.65 17.36 38.23 o -16 0 2 2271.25 2319.02 39.08 o -14 0 2 1431.05 1425.48 41.03 o -12 0 2 248.71 222.30 22.01 o -10 0 2 557.83 500.54 29.22 o -8 0 2 74.84 175.09 32.78 o -6 0 2 7.47 17.96 29.10 o -2 0 2 4342.45 5353.40 204.06 o 0 0 2 289.36 379.03 48.77 o 2 0 2 2111.47 2674.11 57.52 o 4 0 2 2583.01 2328.90 40.35 o 6 0 2 10977.23 11783.62 66.48 o 8 0 2 7363.91 7254.71 106.03 o 10 0 2 69.99 58.80 20.80 o 12 0 2 546.49 529.28 37.94 o 14 0 2 25.29 23.02 29.80 o 16 0 2 1274.82 1317.94 37.19 o -18 1 2 199.88 166.05 27.61 o -17 1 2 364.66 345.54 25.39 o -16 1 2 107.55 100.35 21.77 o -15 1 2 288.06 275.13 21.18 o -14 1 2 1513.85 1550.05 25.31 o -13 1 2 871.49 820.97 23.41 o -12 1 2 6.96 4.57 15.65 o -11 1 2 836.36 832.49 19.47 o -10 1 2 463.21 455.18 19.04 o -9 1 2 76.01 55.87 19.38 o -8 1 2 3353.15 3543.69 60.21 o -7 1 2 820.87 876.72 22.78 o -6 1 2 1211.54 1256.38 30.45 o -5 1 2 433.72 510.68 23.82 o -4 1 2 299.14 297.16 24.95 o -3 1 2 694.71 818.52 28.26 o -2 1 2 2285.67 2551.46 57.37 o -1 1 2 1.01 -0.55 23.53 o 0 1 2 6.99 5.71 23.22 o 1 1 2 1.51 3.81 24.24 o 2 1 2 1340.29 1501.18 30.47 o 3 1 2 2880.29 3402.74 54.29 o 4 1 2 855.80 878.31 23.63 o 5 1 2 926.05 865.08 22.70 o 6 1 2 2590.64 2681.74 27.84 o 7 1 2 1700.81 1654.62 23.49 o 8 1 2 112.06 98.01 17.56 o 9 1 2 258.45 227.93 21.37 o 10 1 2 11.36 10.22 18.46 o 11 1 2 103.71 95.46 16.45 o 12 1 2 19.31 11.88 23.02 o 13 1 2 187.48 187.99 21.72 o 14 1 2 199.73 183.27 20.31 o 15 1 2 470.82 426.42 25.63 o 16 1 2 60.88 57.12 30.76 o -17 2 2 332.15 319.29 35.65 o -16 2 2 568.93 533.26 28.79 o -15 2 2 2.23 -5.11 28.00 o -14 2 2 2.90 -3.67 21.05 o -13 2 2 70.24 68.91 23.24 o -12 2 2 82.82 69.13 19.57 o -11 2 2 422.98 423.47 20.08 o -10 2 2 0.46 -7.80 16.87 o -9 2 2 1381.89 1480.57 25.14 o -8 2 2 3557.63 3318.77 58.26 o -7 2 2 423.12 371.31 20.92 o -6 2 2 267.07 272.80 22.09 o -5 2 2 1740.14 1746.03 42.21 o -4 2 2 8948.59 8735.71 178.39 o -3 2 2 992.13 853.53 22.02 o -2 2 2 77.59 124.95 19.82 o -1 2 2 528.99 486.65 19.67 o 0 2 2 343.15 355.40 19.66 o 1 2 2 804.29 753.18 23.70 o 2 2 2 1957.44 1924.33 29.90 o 3 2 2 2801.38 2950.97 54.36 o 4 2 2 926.86 804.39 23.99 o 5 2 2 435.44 450.78 19.72 o 6 2 2 1188.22 1334.02 22.33 o 7 2 2 263.06 226.68 17.93 o 8 2 2 9011.49 8691.28 131.87 o 9 2 2 18.66 14.20 18.37 o 10 2 2 92.91 62.09 17.00 o 11 2 2 70.53 30.44 22.94 o 12 2 2 66.74 37.78 25.77 o 13 2 2 304.80 304.18 22.12 o 14 2 2 21.49 15.67 25.52 o 15 2 2 363.07 335.02 27.35 o -16 3 2 483.13 508.28 30.29 o -15 3 2 646.25 669.00 27.66 o -14 3 2 394.56 367.02 21.63 o -13 3 2 43.82 29.68 23.09 o -12 3 2 172.26 162.24 22.21 o -11 3 2 299.24 288.40 17.10 o -10 3 2 3376.74 3188.50 67.07 o -9 3 2 389.02 369.61 19.34 o -8 3 2 103.64 93.54 17.07 o -7 3 2 434.46 439.21 19.11 o -6 3 2 4458.76 4424.53 73.64 o -5 3 2 75.60 56.72 16.60 o -4 3 2 7052.56 7554.71 187.18 o -3 3 2 1656.42 1966.32 28.97 o -2 3 2 3422.26 3430.26 65.52 o -1 3 2 661.50 869.32 21.21 o 0 3 2 249.22 293.81 17.71 o 1 3 2 256.80 290.34 18.86 o 2 3 2 11408.94 12009.42 200.66 o 3 3 2 1006.20 973.22 22.55 o 4 3 2 2243.66 2222.38 46.78 o 5 3 2 202.73 203.53 20.11 o 6 3 2 4601.78 4603.07 71.82 o 7 3 2 2.80 -5.99 16.74 o 8 3 2 511.34 512.48 19.94 o 9 3 2 205.31 192.74 17.15 o 10 3 2 207.67 205.02 21.11 o 11 3 2 252.58 248.89 20.07 o 12 3 2 71.09 72.06 22.13 o 13 3 2 14.30 12.20 20.53 o 14 3 2 26.44 41.01 28.89 o 15 3 2 563.93 587.50 26.23 o -15 4 2 297.56 300.28 29.87 o -14 4 2 271.04 281.29 29.43 o -13 4 2 5.70 -8.88 23.36 o -12 4 2 149.51 121.81 22.22 o -11 4 2 3036.92 3177.64 64.37 o -10 4 2 1257.15 1262.60 26.05 o -9 4 2 181.68 147.32 18.55 o -8 4 2 825.30 814.51 21.11 o -7 4 2 1483.36 1422.13 27.42 o -6 4 2 383.22 397.34 17.87 o -5 4 2 323.78 332.02 18.30 o -4 4 2 4247.93 4298.23 86.02 o -3 4 2 91.40 71.14 16.53 o -2 4 2 47.18 31.34 18.12 o -1 4 2 287.88 293.30 18.94 o 0 4 2 37.85 26.69 17.29 o 1 4 2 2749.07 2762.00 55.21 o 2 4 2 1375.58 1370.22 30.42 o 3 4 2 4.53 6.20 17.93 o 4 4 2 921.03 890.65 20.75 o 5 4 2 12.63 5.27 17.10 o 6 4 2 0.00 -1.84 17.99 o 7 4 2 2337.76 2238.38 31.17 o 8 4 2 1098.16 1099.11 29.36 o 9 4 2 32.46 16.37 21.75 o 10 4 2 304.66 320.39 20.92 o 11 4 2 444.38 422.43 22.22 o 12 4 2 652.92 689.81 29.95 o 13 4 2 291.77 296.73 23.72 o -13 5 2 30.66 38.42 27.29 o -12 5 2 3.34 25.16 27.06 o -11 5 2 123.85 111.17 22.37 o -10 5 2 667.00 628.41 24.42 o -9 5 2 2820.38 2829.10 57.84 o -8 5 2 408.65 387.63 22.78 o -7 5 2 1022.60 1047.60 25.57 o -6 5 2 4187.80 4453.37 63.04 o -5 5 2 109.57 79.55 14.37 o -4 5 2 686.35 663.94 18.77 o -3 5 2 227.47 212.99 17.70 o -2 5 2 444.60 442.92 16.60 o -1 5 2 1495.65 1418.25 33.04 o 0 5 2 2074.77 1990.42 42.89 o 1 5 2 332.75 289.02 17.05 o 2 5 2 884.59 872.50 22.23 o 3 5 2 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