#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:42:55 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181280 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/58/2235827.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2235827_Fobs loop_ _publ_author_name 'bin Shawkataly, Omar' 'Khan, Imthyaz Ahmed' 'Sirat, Siti Syaida' 'Quah, Ching Kheng' 'Fun, Hoong-Kun' _publ_section_title ; [\m-Bis(diphenylarsino)methane-1:2\k^2^As:As]decacarbonyl-1\k^3^C,2\k^3^C,3\k^4^C-triangulo-triosmium(0) ; _journal_coeditor_code HB6822 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1119 _journal_page_last m1120 _journal_volume 68 _journal_year 2012 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 11.2965 _cell_length_b 15.3594 _cell_length_c 20.6641 _exptl_crystal_F_000 2424.00 _reflns_d_resolution_high 0.6159 _cod_data_source_file hb6822Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' mo_iak105_0m in P2(1)2(1)2(1) (100K)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 667.46 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 58143.16 59183.76 3500.08 o 4 0 0 7047.03 7544.45 258.31 o 6 0 0 137522.66 143328.80 5098.03 o 8 0 0 191.79 508.63 80.20 o 10 0 0 24056.08 24307.72 585.45 o 12 0 0 22.16 -10.82 73.55 o 14 0 0 6599.33 6888.49 252.57 o 16 0 0 982.75 1358.21 191.70 o 18 0 0 228.16 220.44 147.15 o 2 1 0 69714.91 74753.12 2324.83 o 3 1 0 1659.36 1945.28 84.81 o 4 1 0 63588.50 67848.42 1520.20 o 5 1 0 67182.56 69037.70 1426.44 o 6 1 0 4602.93 4533.79 102.44 o 7 1 0 34794.87 35764.89 653.13 o 8 1 0 9390.87 9260.00 174.64 o 9 1 0 33452.05 33746.43 524.62 o 10 1 0 135.56 221.39 39.06 o 11 1 0 1054.36 1210.94 67.87 o 12 1 0 1551.31 1681.22 78.52 o 13 1 0 8310.40 8348.06 198.42 o 14 1 0 486.20 534.95 90.64 o 15 1 0 39846.97 39752.16 1042.66 o 16 1 0 1813.58 1744.23 149.59 o 17 1 0 11816.92 11556.12 464.05 o 18 1 0 524.89 513.05 250.21 o 1 2 0 33165.16 34741.36 748.13 o 2 2 0 237769.34 239886.25 13175.94 o 3 2 0 2311.43 2433.86 89.01 o 4 2 0 40079.64 42656.30 1238.75 o 5 2 0 38581.44 41487.77 703.03 o 6 2 0 57653.31 62610.18 1181.85 o 7 2 0 14868.05 15149.26 280.47 o 8 2 0 833.27 894.13 54.20 o 9 2 0 8748.38 8829.66 172.02 o 10 2 0 572.44 620.46 40.48 o 11 2 0 42804.12 43836.38 787.90 o 12 2 0 17.84 132.61 46.85 o 13 2 0 5215.29 5032.96 174.81 o 14 2 0 1026.11 1154.76 92.96 o 15 2 0 578.73 613.46 93.67 o 16 2 0 2575.03 2975.18 162.15 o 17 2 0 1891.07 1938.55 205.17 o 18 2 0 2010.55 2160.78 177.52 o 1 3 0 30824.25 33528.85 799.47 o 2 3 0 28022.27 30514.66 826.81 o 3 3 0 45734.99 47305.64 2304.38 o 5 3 0 389.10 552.15 33.39 o 6 3 0 12648.74 12852.11 269.52 o 7 3 0 2696.39 2519.48 68.58 o 8 3 0 5310.87 5579.50 175.57 o 9 3 0 5420.21 5611.43 150.04 o 10 3 0 113.04 373.42 43.63 o 11 3 0 12327.81 12307.64 253.01 o 12 3 0 57.00 150.56 54.39 o 13 3 0 29903.44 29523.02 702.46 o 14 3 0 1826.39 1763.05 198.34 o 15 3 0 7524.44 7624.41 268.62 o 16 3 0 5043.38 5131.94 219.38 o 17 3 0 6231.65 5722.25 454.77 o 18 3 0 180.79 285.64 114.53 o 0 4 0 19977.26 22624.12 589.56 o 1 4 0 1363.89 1516.78 47.56 o 2 4 0 282584.59 285849.81 8799.60 o 4 4 0 239132.22 242020.13 4593.40 o 5 4 0 9299.43 9078.76 198.21 o 6 4 0 201.00 217.04 40.62 o 7 4 0 1393.63 1500.54 87.10 o 8 4 0 444.64 592.83 41.62 o 9 4 0 14802.15 14816.52 302.50 o 10 4 0 15923.69 15376.56 302.29 o 11 4 0 19457.91 19149.13 499.39 o 12 4 0 13.16 262.26 63.02 o 13 4 0 198.49 222.73 71.05 o 14 4 0 4176.51 4120.94 189.03 o 15 4 0 53.27 104.13 86.90 o 16 4 0 4366.30 4344.82 431.46 o 17 4 0 25.76 61.38 98.22 o 18 4 0 4986.89 5215.53 280.74 o 1 5 0 1202.85 1438.47 47.38 o 2 5 0 18224.71 19623.74 429.68 o 3 5 0 37890.64 37115.71 599.04 o 4 5 0 13757.59 13603.15 223.62 o 5 5 0 11509.92 12858.40 258.74 o 6 5 0 3312.93 3384.69 106.92 o 7 5 0 2730.58 2866.57 85.17 o 8 5 0 23345.80 23380.47 472.21 o 9 5 0 18128.82 17956.56 324.23 o 10 5 0 2596.29 2437.69 109.09 o 11 5 0 25596.24 24966.54 555.77 o 12 5 0 11610.60 11485.53 294.36 o 13 5 0 35201.37 34223.22 823.80 o 14 5 0 817.01 678.52 104.53 o 15 5 0 1074.36 1116.95 112.17 o 16 5 0 37.73 96.56 89.53 o 17 5 0 7083.90 7467.28 345.17 o 0 6 0 28201.33 31974.39 957.21 o 1 6 0 5201.60 5903.01 119.84 o 2 6 0 111979.73 113600.97 1723.01 o 3 6 0 53016.51 53281.67 818.95 o 4 6 0 81818.25 82575.69 1378.94 o 5 6 0 616.60 767.96 40.96 o 6 6 0 1278.20 1354.32 81.12 o 7 6 0 66165.95 64751.34 1666.07 o 8 6 0 30122.26 30060.71 569.89 o 9 6 0 6439.57 6499.36 168.96 o 10 6 0 2470.34 2589.14 99.16 o 11 6 0 344.44 402.57 73.48 o 12 6 0 283.45 455.68 80.80 o 13 6 0 17768.55 17743.96 439.05 o 14 6 0 6.09 184.20 76.57 o 15 6 0 1687.95 1603.97 148.48 o 16 6 0 1907.45 2066.80 137.16 o 17 6 0 3586.37 3647.75 192.18 o 1 7 0 18679.31 19209.62 325.60 o 2 7 0 118490.64 119912.79 1606.40 o 3 7 0 553.61 580.76 28.04 o 4 7 0 221.06 536.08 38.34 o 5 7 0 17203.23 17140.25 297.82 o 6 7 0 5424.11 5450.45 126.50 o 7 7 0 8608.88 8227.37 237.23 o 8 7 0 48312.96 48241.42 955.42 o 9 7 0 2086.12 2175.26 101.85 o 10 7 0 790.09 871.87 74.98 o 11 7 0 2389.68 2455.87 123.48 o 12 7 0 7376.92 7482.12 228.05 o 13 7 0 6429.67 6872.17 220.55 o 14 7 0 1763.66 1918.21 121.36 o 15 7 0 10317.63 10031.84 313.10 o 16 7 0 1.00 117.77 85.11 o 17 7 0 5081.14 5070.27 227.00 o 0 8 0 133576.36 134929.91 2985.43 o 1 8 0 19747.24 19657.33 293.37 o 2 8 0 62335.10 65183.68 882.76 o 3 8 0 167.93 458.25 40.16 o 4 8 0 2168.06 2421.60 90.17 o 5 8 0 16972.52 17838.58 351.82 o 6 8 0 38757.05 38783.30 768.06 o 7 8 0 44097.09 44784.08 831.23 o 8 8 0 31934.23 32148.34 572.98 o 9 8 0 17082.42 16829.62 373.95 o 10 8 0 1730.14 1757.59 97.49 o 11 8 0 798.08 894.63 80.11 o 12 8 0 1511.81 1341.72 118.13 o 13 8 0 16383.02 16191.22 408.72 o 14 8 0 10291.65 11024.44 306.37 o 15 8 0 352.22 493.27 87.07 o 16 8 0 19.66 32.21 87.99 o 17 8 0 1150.16 1233.37 123.89 o 1 9 0 20430.20 20781.60 321.60 o 2 9 0 36871.20 38277.34 529.02 o 3 9 0 13700.46 13754.39 182.57 o 4 9 0 3460.47 3290.66 80.28 o 5 9 0 11597.66 11881.34 237.14 o 6 9 0 78996.84 77485.04 1378.64 o 7 9 0 4014.16 4040.33 129.37 o 8 9 0 12235.99 12154.80 267.90 o 9 9 0 41894.84 41125.19 831.20 o 10 9 0 988.79 933.19 82.82 o 11 9 0 65.89 47.47 63.90 o 12 9 0 577.48 611.87 92.14 o 13 9 0 308.60 462.64 87.16 o 14 9 0 2621.51 3014.95 147.22 o 15 9 0 16445.40 16653.32 425.18 o 16 9 0 3878.26 4002.30 204.68 o 17 9 0 2403.49 2328.49 155.09 o 0 10 0 162541.39 167503.31 3099.75 o 1 10 0 71360.60 73122.90 945.79 o 2 10 0 6206.46 6320.14 108.96 o 3 10 0 27330.10 28139.10 370.24 o 4 10 0 2695.22 2643.82 77.46 o 5 10 0 1710.89 1831.99 70.52 o 6 10 0 71197.70 70862.88 1207.94 o 7 10 0 118.40 208.08 55.96 o 8 10 0 6674.23 6666.26 175.64 o 9 10 0 44266.11 43309.70 813.16 o 10 10 0 1096.71 1215.21 89.55 o 11 10 0 22139.90 21786.41 477.99 o 12 10 0 6491.50 6372.46 194.29 o 13 10 0 1035.45 1015.68 101.23 o 14 10 0 4668.24 4397.88 177.19 o 15 10 0 10.75 181.11 109.48 o 16 10 0 158.80 306.02 102.17 o 1 11 0 9939.99 10369.41 152.90 o 2 11 0 157.70 310.22 32.01 o 3 11 0 9536.74 9691.13 153.78 o 4 11 0 37116.05 37244.07 565.10 o 5 11 0 27982.99 27968.00 480.08 o 6 11 0 86372.14 83278.66 1415.14 o 7 11 0 2095.42 1962.76 94.52 o 8 11 0 110.35 199.20 58.92 o 9 11 0 15908.28 15795.84 337.66 o 10 11 0 541.40 688.60 95.01 o 11 11 0 1206.13 1304.96 99.04 o 12 11 0 5729.81 5850.02 233.69 o 13 11 0 924.72 1013.13 102.58 o 14 11 0 3170.96 3341.15 160.51 o 15 11 0 1296.57 1269.71 122.21 o 16 11 0 5777.35 5965.31 259.15 o 0 12 0 13955.95 14533.93 288.81 o 1 12 0 17861.92 18140.22 235.65 o 2 12 0 1313.36 1410.53 52.66 o 3 12 0 177.49 203.66 36.75 o 4 12 0 39208.77 39737.63 602.89 o 5 12 0 2485.33 2444.19 91.36 o 6 12 0 14381.42 14445.85 289.24 o 7 12 0 506.19 574.98 55.50 o 8 12 0 1894.98 1845.90 97.21 o 9 12 0 24566.15 24095.05 485.62 o 10 12 0 46068.74 45781.74 930.25 o 11 12 0 22834.33 22242.16 492.25 o 12 12 0 8904.52 9005.90 247.92 o 13 12 0 144.05 109.30 73.02 o 14 12 0 319.74 287.89 91.72 o 15 12 0 72.04 4.87 102.18 o 16 12 0 1534.26 1284.88 194.18 o 1 13 0 27504.25 27783.13 341.14 o 2 13 0 207.40 243.08 38.73 o 3 13 0 7115.88 6992.47 137.10 o 4 13 0 43934.59 43207.20 654.67 o 5 13 0 83302.76 81523.80 1390.36 o 6 13 0 5115.13 5027.97 140.32 o 7 13 0 3771.95 3616.93 116.81 o 8 13 0 6658.43 6200.53 178.78 o 9 13 0 49.21 106.35 68.52 o 10 13 0 3957.88 4000.74 139.13 o 11 13 0 7264.68 7386.88 248.76 o 12 13 0 523.89 502.49 87.91 o 13 13 0 2034.23 2099.77 121.57 o 14 13 0 543.19 495.07 102.34 o 15 13 0 1060.65 1238.25 140.40 o 0 14 0 6991.09 7051.66 166.14 o 1 14 0 2578.66 2631.03 74.99 o 2 14 0 3924.20 3986.57 99.36 o 3 14 0 38530.85 38285.60 562.99 o 4 14 0 43286.95 43006.84 686.62 o 5 14 0 10432.34 10191.98 224.53 o 6 14 0 5272.38 5242.62 147.23 o 7 14 0 28247.86 27339.41 505.94 o 8 14 0 11398.14 11380.74 268.66 o 9 14 0 2733.33 2652.43 123.19 o 10 14 0 39137.73 39088.76 754.10 o 11 14 0 4117.25 4132.31 161.94 o 12 14 0 6268.67 6697.85 213.38 o 13 14 0 3999.91 4146.98 172.07 o 14 14 0 9.10 -26.34 140.77 o 15 14 0 1312.61 1246.06 142.23 o 1 15 0 2238.59 2348.94 79.96 o 2 15 0 14684.51 14424.38 252.19 o 3 15 0 6888.52 6623.76 150.92 o 4 15 0 4983.82 5018.84 128.26 o 5 15 0 15111.66 15045.62 328.88 o 6 15 0 850.20 926.90 82.06 o 7 15 0 15302.13 15654.22 317.84 o 8 15 0 17519.71 17419.25 377.62 o 9 15 0 1936.75 2021.05 114.59 o 10 15 0 5974.13 5991.15 181.56 o 11 15 0 1588.85 1784.63 119.15 o 12 15 0 5136.49 5067.40 186.17 o 13 15 0 9.82 144.22 99.54 o 14 15 0 233.08 265.12 93.07 o 0 16 0 430.03 447.86 81.51 o 1 16 0 8402.12 8116.99 166.08 o 2 16 0 4318.00 4180.23 113.91 o 3 16 0 17361.74 17052.18 306.59 o 4 16 0 50.87 121.88 50.87 o 5 16 0 4816.85 4749.88 156.72 o 6 16 0 12212.12 12256.48 283.63 o 7 16 0 16341.90 16194.52 351.82 o 8 16 0 38819.96 38364.84 806.01 o 9 16 0 532.77 617.67 87.54 o 10 16 0 4492.01 4840.79 169.99 o 11 16 0 683.08 624.03 95.22 o 12 16 0 8278.38 8564.29 263.39 o 13 16 0 4557.44 4723.65 212.97 o 14 16 0 6163.28 6538.56 576.32 o 1 17 0 44953.89 44232.97 750.42 o 2 17 0 390.15 561.88 60.76 o 3 17 0 14410.02 14058.86 279.21 o 4 17 0 784.21 767.25 65.94 o 5 17 0 471.71 518.80 76.91 o 6 17 0 942.93 970.38 87.25 o 7 17 0 19463.61 19234.32 409.95 o 8 17 0 3002.38 3166.13 151.70 o 9 17 0 10527.81 10317.80 283.94 o 10 17 0 595.47 567.83 95.15 o 11 17 0 50.43 175.76 87.00 o 12 17 0 103.81 70.38 99.70 o 13 17 0 723.83 1014.53 129.21 o 0 18 0 766.03 686.14 115.18 o 1 18 0 57.92 173.36 73.60 o 2 18 0 1114.10 1108.25 80.72 o 3 18 0 9797.61 9985.67 219.64 o 4 18 0 142.48 101.96 54.64 o 5 18 0 1002.63 1109.35 92.75 o 6 18 0 10849.29 11142.57 271.17 o 7 18 0 354.55 476.27 78.42 o 8 18 0 34802.36 35342.20 756.27 o 9 18 0 2936.65 2744.12 145.55 o 10 18 0 1758.92 1985.37 130.52 o 11 18 0 2347.08 2383.31 191.63 o 12 18 0 7180.32 7876.18 336.53 o 1 19 0 8860.79 9206.48 253.52 o 2 19 0 673.03 645.05 76.08 o 3 19 0 6678.31 6849.05 183.24 o 4 19 0 24.01 23.68 59.84 o 5 19 0 3678.59 3694.03 148.25 o 6 19 0 10977.72 10827.14 268.27 o 7 19 0 18892.16 18857.38 407.74 o 8 19 0 1035.81 1158.30 115.27 o 9 19 0 2701.15 3014.45 173.67 o 10 19 0 148.69 195.41 130.45 o 11 19 0 57.63 110.12 127.65 o 0 20 0 1730.07 1784.68 153.14 o 1 20 0 92.02 104.94 75.06 o 2 20 0 200.44 272.54 75.59 o 3 20 0 34829.64 34693.13 645.39 o 4 20 0 4265.65 4181.07 142.13 o 5 20 0 38.75 4.82 79.72 o 6 20 0 3309.25 3176.32 141.69 o 7 20 0 1170.98 1292.91 108.75 o 8 20 0 5627.34 5907.03 253.62 o 9 20 0 3431.58 3378.13 232.89 o 10 20 0 11395.81 11427.53 592.84 o 1 21 0 3396.00 3331.62 151.69 o 2 21 0 22.73 77.94 79.77 o 3 21 0 3396.65 3357.67 151.07 o 4 21 0 2190.01 2229.62 108.61 o 5 21 0 23825.64 23976.41 592.03 o 6 21 0 736.12 673.24 96.49 o 7 21 0 3010.30 3041.93 158.61 o 8 21 0 186.77 29.59 126.89 o 9 21 0 132.92 257.38 162.30 o 0 22 0 647.82 882.71 133.80 o 1 22 0 6459.29 6469.62 215.17 o 2 22 0 19.66 30.84 78.88 o 3 22 0 6750.37 7043.06 222.85 o 4 22 0 7857.02 7841.05 297.54 o 5 22 0 107.02 151.18 117.93 o 6 22 0 1991.23 2089.19 154.69 o 7 22 0 593.25 770.08 121.68 o 8 22 0 617.32 538.71 147.65 o 1 23 0 1725.01 1958.09 182.46 o 2 23 0 1169.64 1219.15 195.30 o 3 23 0 2209.99 2514.08 202.38 o 4 23 0 2285.18 2114.46 283.29 o 5 23 0 13624.65 14377.09 835.38 o 6 23 0 3445.15 3932.96 265.73 o 7 23 0 277.91 327.09 228.76 o 0 24 0 1838.02 1783.49 227.87 o 1 24 0 17014.13 17836.25 611.76 o 2 24 0 2.97 150.33 159.41 o 3 24 0 195.29 51.90 152.09 o 4 24 0 385.79 573.56 214.07 o 1 0 1 8320.86 7345.88 1133.81 o 2 0 1 37.90 100.47 24.51 o 3 0 1 8018.51 8850.30 266.09 o 4 0 1 10301.56 10701.85 300.75 o 5 0 1 2282.91 2316.41 92.98 o 6 0 1 168244.63 173351.31 3367.20 o 7 0 1 41059.72 41336.52 706.86 o 8 0 1 14454.84 14550.54 272.86 o 9 0 1 2328.20 2326.21 66.67 o 10 0 1 28400.55 28852.83 483.63 o 11 0 1 6579.66 6633.92 161.44 o 12 0 1 649.89 722.59 60.23 o 13 0 1 5619.85 5656.58 154.44 o 14 0 1 26950.89 27397.94 567.10 o 15 0 1 7.88 -76.70 76.70 o 16 0 1 31423.29 28807.65 1306.08 o 17 0 1 239.92 193.14 99.71 o 18 0 1 1241.21 930.93 129.75 o -18 1 1 564.26 497.42 113.62 o -17 1 1 73.79 171.77 98.99 o -16 1 1 1099.23 1021.45 121.08 o -15 1 1 2098.91 2404.18 125.78 o -14 1 1 2409.76 2353.68 115.31 o -13 1 1 2600.71 2763.16 104.48 o -12 1 1 1079.84 1369.15 74.15 o -11 1 1 6730.32 6834.65 164.12 o -10 1 1 21896.97 22361.59 394.83 o -9 1 1 10072.05 10347.29 203.85 o -8 1 1 9817.94 10274.63 216.81 o -7 1 1 21118.61 21938.91 443.63 o -6 1 1 21625.16 23134.40 419.20 o -5 1 1 62859.98 65154.76 1274.93 o -4 1 1 12705.29 13025.64 361.00 o -3 1 1 380.82 661.55 58.97 o -2 1 1 13054.85 13733.03 711.36 o 0 1 1 15836.81 17076.06 398.30 o 2 1 1 13279.06 14529.33 423.43 o 3 1 1 744.86 971.51 49.21 o 5 1 1 64668.82 69475.12 1355.65 o 6 1 1 20437.96 21585.87 391.41 o 7 1 1 24152.87 25126.15 393.32 o 8 1 1 11441.23 11724.60 182.05 o 9 1 1 9479.27 9552.77 175.99 o 10 1 1 20418.27 21179.21 371.46 o 11 1 1 8043.63 8299.24 169.71 o 12 1 1 1105.08 1229.51 71.68 o 13 1 1 2580.81 2619.18 106.25 o 14 1 1 2544.52 2389.45 121.45 o 15 1 1 1945.34 2070.23 133.10 o 16 1 1 1088.94 877.54 117.17 o 17 1 1 80.27 172.65 102.72 o 18 1 1 522.14 505.58 114.15 o -18 2 1 4952.58 4766.80 259.44 o -17 2 1 443.55 341.66 108.32 o -16 2 1 13798.82 13583.92 686.14 o -15 2 1 6116.13 6411.16 229.29 o -14 2 1 21110.06 21320.45 516.90 o -13 2 1 5098.32 5095.32 157.59 o -12 2 1 8943.32 9082.96 205.88 o -11 2 1 10767.74 11349.64 244.82 o -10 2 1 10146.15 10593.09 230.27 o -9 2 1 15029.68 15302.26 298.56 o -8 2 1 608.11 715.66 51.48 o -7 2 1 23356.57 24246.10 424.14 o -6 2 1 31230.72 32601.98 649.84 o -5 2 1 127724.33 131859.14 2169.79 o -4 2 1 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