#------------------------------------------------------------------------------ #$Date: 2012-09-11 12:26:43 +0300 (Tue, 11 Sep 2012) $ #$Revision: 66590 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/58/2235867.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2235867_Fobs loop_ _publ_author_name 'Katzsch, Felix' 'Weber, Edwin' _publ_section_title ; Redetermination of tetramethyl tetrathiafulvalene-2,3,6,7-tetracarboxylate ; _journal_coeditor_code IM2387 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2354 _journal_page_last o2355 _journal_volume 68 _journal_year 2012 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 100.221 _cell_angle_beta 99.255 _cell_angle_gamma 99.328 _cell_length_a 6.8666 _cell_length_b 7.8783 _cell_length_c 8.4335 _exptl_crystal_F_000 224.00 _reflns_d_resolution_high 0.8410 _[local]_cod_data_source_file im2387Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' FeKa_31_tricP in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 121.88 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 455.79 460.35 7.82 o 2 0 0 326.88 346.70 8.32 o 3 0 0 3801.13 4089.19 94.67 o 4 0 0 30.36 40.05 1.43 o 5 0 0 1101.66 1060.39 14.04 o 6 0 0 128.41 123.65 2.99 o 7 0 0 0.27 1.56 0.55 o -8 1 0 154.09 162.21 4.09 o -7 1 0 0.07 0.00 0.41 o -6 1 0 112.92 113.92 2.85 o -5 1 0 61.76 65.87 1.79 o -4 1 0 221.14 226.32 3.93 o -3 1 0 4.80 4.08 0.15 o -2 1 0 342.16 364.25 4.09 o -1 1 0 813.04 844.91 10.74 o 0 1 0 1035.20 1001.62 15.74 o 1 1 0 0.07 0.47 0.22 o 2 1 0 315.79 353.74 3.76 o 3 1 0 77.94 77.17 1.14 o 4 1 0 451.85 462.50 7.86 o 5 1 0 107.25 87.13 1.42 o 6 1 0 5.02 6.33 0.56 o 7 1 0 202.45 201.13 6.50 o -8 2 0 59.77 69.13 3.06 o -7 2 0 20.82 19.22 1.20 o -6 2 0 59.53 58.26 1.84 o -5 2 0 47.44 54.04 0.84 o -4 2 0 2157.73 2168.89 22.40 o -3 2 0 9.07 11.02 0.30 o -2 2 0 260.31 260.52 2.45 o -1 2 0 14855.18 12598.78 157.88 o 0 2 0 1404.40 1415.74 22.07 o 1 2 0 0.02 0.17 0.19 o 2 2 0 1079.52 1144.63 11.25 o 3 2 0 307.47 354.38 4.68 o 4 2 0 1855.23 1871.10 22.80 o 5 2 0 97.81 97.86 1.58 o 6 2 0 3.13 7.42 0.55 o 7 2 0 597.79 599.47 12.61 o -7 3 0 27.59 27.15 1.42 o -6 3 0 39.65 39.41 0.85 o -5 3 0 137.83 136.33 1.43 o -4 3 0 365.73 344.64 3.33 o -3 3 0 53.31 53.51 0.64 o -2 3 0 379.86 385.08 3.57 o -1 3 0 1503.51 1436.92 24.82 o 0 3 0 148.61 156.43 2.88 o 1 3 0 382.89 418.83 6.06 o 2 3 0 17.58 21.32 0.45 o 3 3 0 313.62 309.40 3.51 o 4 3 0 248.68 216.90 3.03 o 5 3 0 11.76 14.14 0.37 o 6 3 0 200.39 195.56 2.82 o -7 4 0 3.72 2.68 0.30 o -6 4 0 30.31 29.19 0.55 o -5 4 0 1048.62 1033.83 8.60 o -4 4 0 125.09 121.46 1.14 o -3 4 0 114.67 113.95 1.05 o -2 4 0 811.69 835.32 7.45 o -1 4 0 23.59 26.38 0.76 o 0 4 0 2.79 1.35 0.22 o 1 4 0 52.35 51.66 0.83 o 2 4 0 414.70 429.84 4.11 o 3 4 0 718.12 697.67 6.03 o 4 4 0 131.79 131.89 1.37 o 5 4 0 32.69 39.71 0.87 o 6 4 0 142.90 144.17 2.36 o -7 5 0 87.14 84.67 1.52 o -6 5 0 220.52 218.78 2.37 o -5 5 0 699.44 677.38 5.85 o -4 5 0 221.40 221.75 1.77 o -3 5 0 335.02 335.75 2.91 o -2 5 0 1231.28 1195.78 11.17 o -1 5 0 394.08 384.27 5.05 o 0 5 0 7.81 6.60 0.54 o 1 5 0 0.63 0.24 0.16 o 2 5 0 73.40 74.08 1.05 o 3 5 0 1082.11 1046.10 9.59 o 4 5 0 0.48 0.38 0.19 o 5 5 0 35.83 35.55 0.88 o -7 6 0 6.07 7.42 0.47 o -6 6 0 384.24 383.43 3.91 o -5 6 0 68.31 66.90 0.99 o -4 6 0 4.31 4.53 0.28 o -3 6 0 121.40 124.12 1.39 o -2 6 0 1.39 1.96 0.26 o -1 6 0 181.00 168.99 1.97 o 0 6 0 64.06 60.43 1.36 o 1 6 0 238.76 237.82 2.89 o 2 6 0 208.78 205.51 2.45 o 3 6 0 109.96 109.06 1.43 o 4 6 0 0.19 0.76 0.23 o -6 7 0 233.51 232.56 3.12 o -5 7 0 181.56 175.82 2.17 o -4 7 0 284.75 281.85 4.35 o -3 7 0 225.00 227.17 3.27 o -2 7 0 257.02 259.18 3.38 o -1 7 0 104.75 108.28 1.68 o 0 7 0 6.30 6.23 0.47 o 1 7 0 69.55 67.12 1.35 o 2 7 0 1096.65 1084.96 10.42 o 3 7 0 36.85 35.20 0.84 o -5 8 0 11.13 13.12 0.82 o -4 8 0 43.92 41.85 0.94 o -3 8 0 42.16 41.35 1.05 o -2 8 0 142.71 149.41 2.53 o -1 8 0 6.46 6.51 0.58 o 0 8 0 120.56 122.53 2.09 o 1 8 0 71.88 75.83 1.55 o 2 8 0 27.15 25.89 0.93 o -3 9 0 31.47 32.40 1.13 o -2 9 0 75.18 84.89 1.86 o -1 9 0 11.72 12.57 0.84 o 0 9 0 30.69 30.89 1.30 o 0 -9 1 148.79 149.28 2.71 o 1 -9 1 12.89 10.96 0.76 o 2 -9 1 121.64 135.16 2.48 o 3 -9 1 0.75 0.00 0.44 o -2 -8 1 19.32 18.38 0.95 o -1 -8 1 21.84 23.54 0.86 o 0 -8 1 37.61 37.58 1.05 o 1 -8 1 47.30 47.79 1.25 o 2 -8 1 27.04 30.41 1.01 o 3 -8 1 0.41 0.26 0.29 o 4 -8 1 47.81 51.33 1.15 o 5 -8 1 160.58 167.46 3.23 o -4 -7 1 288.75 303.37 3.49 o -3 -7 1 116.32 116.92 1.73 o -2 -7 1 256.28 256.57 2.97 o -1 -7 1 21.55 21.67 0.74 o 0 -7 1 0.40 0.28 0.25 o 1 -7 1 321.35 324.89 3.77 o 2 -7 1 50.88 47.47 1.07 o 3 -7 1 0.91 0.87 0.26 o 4 -7 1 177.75 184.72 2.02 o 5 -7 1 5.13 5.36 0.36 o 6 -7 1 5.36 8.04 0.46 o -5 -6 1 29.94 31.82 0.80 o -4 -6 1 76.47 74.71 1.18 o -3 -6 1 33.14 32.28 0.67 o -2 -6 1 0.02 0.00 0.20 o -1 -6 1 0.10 0.22 0.18 o 0 -6 1 213.33 215.74 2.76 o 1 -6 1 14.26 10.62 0.42 o 2 -6 1 145.94 147.99 2.12 o 3 -6 1 82.15 82.67 0.99 o 4 -6 1 212.88 208.81 1.92 o 5 -6 1 28.37 27.11 0.57 o 6 -6 1 6.60 6.99 0.36 o -5 -5 1 235.08 243.20 3.18 o -4 -5 1 167.77 157.60 1.90 o -3 -5 1 702.72 709.34 6.16 o -2 -5 1 89.72 86.60 1.09 o -1 -5 1 127.85 126.70 1.45 o 0 -5 1 783.23 769.14 8.12 o 1 -5 1 405.87 392.94 4.09 o 2 -5 1 26.61 24.94 0.48 o 3 -5 1 0.46 1.31 0.16 o 4 -5 1 24.13 22.14 0.40 o 5 -5 1 2.51 2.98 0.24 o 6 -5 1 239.68 231.98 2.30 o 7 -5 1 0.37 0.65 0.28 o -6 -4 1 0.52 0.82 0.45 o -5 -4 1 382.84 372.99 4.03 o -4 -4 1 52.79 53.07 0.67 o -3 -4 1 119.78 122.74 1.30 o -2 -4 1 2.92 4.36 0.21 o -1 -4 1 502.11 507.22 4.78 o 0 -4 1 609.16 553.64 5.36 o 1 -4 1 297.40 312.46 3.01 o 2 -4 1 22.06 27.59 0.49 o 3 -4 1 635.18 603.58 5.26 o 4 -4 1 239.42 246.58 1.91 o 5 -4 1 129.90 127.29 1.37 o 6 -4 1 3.74 3.43 0.29 o 7 -4 1 224.52 226.15 2.97 o -7 -3 1 6.56 8.15 0.54 o -6 -3 1 33.17 36.77 0.88 o -5 -3 1 29.61 23.46 0.57 o -4 -3 1 947.47 964.70 10.44 o -3 -3 1 46.36 44.84 0.65 o -2 -3 1 52.33 47.92 0.74 o -1 -3 1 1638.54 1621.77 14.41 o 0 -3 1 58.85 64.58 1.08 o 1 -3 1 67.80 68.22 1.05 o 2 -3 1 294.29 329.70 2.95 o 3 -3 1 333.84 328.73 2.97 o 4 -3 1 129.62 122.68 1.24 o 5 -3 1 884.65 881.84 7.37 o 6 -3 1 81.54 80.81 1.25 o 7 -3 1 4.80 4.98 0.59 o -7 -2 1 19.03 16.65 1.43 o -6 -2 1 369.00 359.14 5.41 o -5 -2 1 300.59 301.28 4.00 o -4 -2 1 453.78 468.50 5.89 o -3 -2 1 136.33 154.48 1.62 o -2 -2 1 765.72 805.25 7.91 o -1 -2 1 2745.20 2682.22 27.01 o 0 -2 1 11.56 9.52 0.25 o 1 -2 1 308.66 341.56 3.49 o 2 -2 1 915.79 912.57 7.55 o 3 -2 1 1002.36 1036.32 7.73 o 4 -2 1 688.12 669.43 5.57 o 5 -2 1 21.25 22.00 0.51 o 6 -2 1 82.75 83.71 3.58 o 7 -2 1 326.12 320.38 6.48 o -7 -1 1 71.46 60.31 2.07 o -6 -1 1 0.03 0.18 0.35 o -5 -1 1 516.72 528.66 6.43 o -4 -1 1 0.30 0.30 0.11 o -3 -1 1 561.53 610.11 7.72 o -2 -1 1 445.89 426.87 4.23 o -1 -1 1 421.79 432.89 3.84 o 0 -1 1 60.32 63.53 0.67 o 1 -1 1 615.03 612.01 4.81 o 2 -1 1 98.46 97.36 0.94 o 3 -1 1 1254.64 1308.65 13.30 o 4 -1 1 203.53 195.74 2.30 o 5 -1 1 72.28 76.01 1.62 o 6 -1 1 148.44 158.65 3.63 o 7 -1 1 208.65 197.89 6.76 o -8 0 1 125.14 122.68 3.36 o -7 0 1 98.02 87.77 2.53 o -6 0 1 131.96 130.73 3.08 o -5 0 1 1233.58 1227.83 16.93 o -4 0 1 545.07 584.68 11.00 o -3 0 1 0.09 0.46 0.18 o -2 0 1 1540.22 1531.46 12.44 o -1 0 1 342.14 347.91 2.99 o 0 0 1 1899.74 1782.60 51.64 o 1 0 1 792.89 793.69 7.76 o 2 0 1 273.39 288.17 2.59 o 3 0 1 1716.93 1796.94 17.24 o 4 0 1 395.90 422.50 7.66 o 5 0 1 2.89 2.20 0.26 o 6 0 1 234.41 248.27 5.10 o 7 0 1 15.30 15.27 1.37 o -8 1 1 137.93 129.27 3.51 o -7 1 1 20.79 16.62 1.05 o -6 1 1 493.86 478.65 8.73 o -5 1 1 79.19 68.90 2.60 o -4 1 1 465.95 498.84 6.48 o -3 1 1 10.94 20.34 0.64 o -2 1 1 6.25 6.20 0.36 o -1 1 1 4.80 3.21 0.20 o 0 1 1 673.75 688.97 9.05 o 1 1 1 2.29 1.40 0.16 o 2 1 1 1463.39 1491.30 13.47 o 3 1 1 0.11 1.15 0.13 o 4 1 1 6.10 4.70 0.72 o 5 1 1 109.62 121.83 1.91 o 6 1 1 71.33 63.14 2.02 o 7 1 1 231.60 221.39 6.50 o -8 2 1 2.50 3.16 0.42 o -7 2 1 97.09 97.90 2.71 o -6 2 1 1259.23 1221.72 20.55 o -5 2 1 151.37 160.35 2.97 o -4 2 1 173.34 178.72 2.31 o -3 2 1 348.84 349.30 4.00 o -2 2 1 596.52 647.54 7.20 o -1 2 1 6082.18 5705.91 88.40 o 0 2 1 2884.14 2882.19 44.60 o 1 2 1 722.24 771.50 7.69 o 2 2 1 3598.81 3767.00 36.66 o 3 2 1 635.02 644.59 6.33 o 4 2 1 317.21 314.36 3.71 o 5 2 1 12.43 20.05 0.78 o 6 2 1 0.50 1.35 0.91 o 7 2 1 318.13 326.72 6.71 o -8 3 1 23.77 22.01 0.95 o -7 3 1 500.69 485.82 7.21 o -6 3 1 130.88 132.19 1.83 o -5 3 1 0.43 0.17 0.13 o -4 3 1 0.17 0.22 0.10 o -3 3 1 340.19 341.80 4.37 o -2 3 1 1001.13 998.75 9.84 o -1 3 1 284.53 308.53 3.54 o 0 3 1 9.43 9.50 0.37 o 1 3 1 1089.07 1100.32 10.96 o 2 3 1 199.37 187.95 2.15 o 3 3 1 11.78 11.75 0.37 o 4 3 1 0.00 0.66 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3.43 o 2 6 1 220.04 213.97 2.52 o 3 6 1 1.47 1.29 0.34 o 4 6 1 67.48 70.32 1.27 o -6 7 1 57.29 56.08 1.14 o -5 7 1 17.85 18.24 0.61 o -4 7 1 118.40 113.51 1.55 o -3 7 1 563.14 554.23 5.39 o -2 7 1 0.04 0.36 0.33 o -1 7 1 5.70 4.20 0.50 o 0 7 1 276.11 277.29 4.18 o 1 7 1 60.84 61.25 1.45 o 2 7 1 195.29 203.06 2.70 o 3 7 1 1.01 0.81 0.31 o -5 8 1 4.81 3.68 0.44 o -4 8 1 560.30 556.08 5.96 o -3 8 1 3.29 3.48 0.45 o -2 8 1 0.03 0.00 0.34 o -1 8 1 99.09 97.85 1.95 o 0 8 1 177.35 177.46 3.45 o 1 8 1 131.64 136.02 2.55 o 2 8 1 2.72 3.14 0.43 o -2 9 1 0.64 1.67 0.47 o 0 -9 2 298.83 302.33 4.52 o 1 -9 2 3.04 2.88 0.86 o 2 -9 2 2.47 2.54 0.51 o 3 -9 2 172.35 180.45 2.70 o -3 -8 2 43.86 41.86 1.19 o -2 -8 2 157.79 151.11 2.40 o -1 -8 2 112.46 105.14 1.88 o 0 -8 2 240.06 233.81 3.74 o 1 -8 2 1.56 1.36 0.39 o 2 -8 2 43.81 38.74 0.93 o 3 -8 2 78.58 82.71 1.32 o 4 -8 2 61.64 62.65 1.23 o 5 -8 2 136.14 146.69 2.02 o -4 -7 2 255.84 255.98 2.71 o -3 -7 2 5.25 5.60 0.41 o -2 -7 2 11.69 12.76 0.57 o -1 -7 2 425.15 412.19 5.05 o 0 -7 2 71.14 73.33 1.19 o 1 -7 2 92.43 98.02 1.44 o 2 -7 2 129.24 123.42 1.63 o 3 -7 2 9.02 9.91 0.49 o 4 -7 2 123.32 131.02 1.72 o 5 -7 2 20.29 20.81 0.65 o 6 -7 2 14.70 13.98 0.56 o -5 -6 2 208.63 211.90 2.67 o -4 -6 2 26.66 27.36 0.57 o -3 -6 2 209.11 205.08 2.24 o -2 -6 2 922.21 903.75 8.23 o -1 -6 2 241.59 228.98 2.37 o 0 -6 2 61.49 60.94 1.13 o 1 -6 2 60.69 57.43 0.91 o 2 -6 2 332.87 331.83 3.27 o 3 -6 2 38.05 36.96 0.61 o 4 -6 2 576.27 588.26 4.88 o 5 -6 2 118.37 118.21 1.47 o 6 -6 2 125.88 129.31 1.55 o -6 -5 2 0.76 1.39 0.26 o -5 -5 2 221.80 231.08 3.37 o -4 -5 2 224.38 223.40 2.51 o -3 -5 2 115.28 116.81 1.34 o -2 -5 2 397.87 380.28 3.77 o -1 -5 2 133.19 126.30 1.43 o 0 -5 2 250.29 251.01 2.75 o 1 -5 2 28.66 29.24 0.59 o 2 -5 2 5.35 6.31 0.26 o 3 -5 2 208.06 200.48 1.69 o 4 -5 2 145.88 140.26 1.28 o 5 -5 2 99.13 102.16 1.41 o 6 -5 2 301.54 305.20 2.91 o 7 -5 2 17.06 19.18 0.71 o -6 -4 2 419.73 426.65 5.54 o -5 -4 2 23.11 26.38 0.92 o -4 -4 2 10.43 10.94 0.33 o -3 -4 2 1326.26 1320.65 11.77 o -2 -4 2 31.66 26.95 0.47 o -1 -4 2 190.99 212.64 2.19 o 0 -4 2 115.08 124.91 1.42 o 1 -4 2 340.37 347.91 3.34 o 2 -4 2 1194.66 1184.31 9.02 o 3 -4 2 702.20 702.34 5.51 o 4 -4 2 250.82 257.73 2.00 o 5 -4 2 293.03 282.33 2.63 o 6 -4 2 540.24 524.35 5.51 o 7 -4 2 128.36 130.18 1.94 o -7 -3 2 8.84 11.30 0.86 o -6 -3 2 203.81 215.02 3.00 o -5 -3 2 485.39 482.25 4.96 o -4 -3 2 346.27 358.18 3.66 o -3 -3 2 157.75 157.19 1.49 o -2 -3 2 85.05 78.78 0.98 o -1 -3 2 151.33 143.46 1.53 o 0 -3 2 240.02 249.70 2.30 o 1 -3 2 14.69 11.47 0.30 o 2 -3 2 82.23 63.28 0.97 o 3 -3 2 182.39 169.30 1.58 o 4 -3 2 25.51 27.34 0.46 o 5 -3 2 339.09 336.88 2.86 o 6 -3 2 39.48 42.86 0.79 o 7 -3 2 1.08 1.60 0.73 o -7 -2 2 305.69 301.84 6.16 o -6 -2 2 207.14 206.93 2.98 o -5 -2 2 54.81 56.80 1.72 o -4 -2 2 71.80 68.88 1.04 o -3 -2 2 120.43 111.10 1.28 o -2 -2 2 27.17 34.51 0.45 o -1 -2 2 338.36 308.03 2.87 o 0 -2 2 106.06 99.15 1.09 o 1 -2 2 934.15 943.41 7.92 o 2 -2 2 876.45 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5 7 2.34 2.53 0.54 o -1 5 7 80.17 77.85 1.81 o 0 5 7 210.89 213.71 3.57 o -2 -6 8 245.44 244.17 3.04 o -1 -6 8 168.27 174.31 2.40 o 0 -6 8 60.30 59.13 1.35 o 1 -6 8 14.62 15.76 0.78 o 2 -6 8 18.59 21.04 0.77 o -3 -5 8 136.39 130.23 1.80 o -2 -5 8 184.52 190.44 2.35 o -1 -5 8 50.46 47.49 1.05 o 0 -5 8 44.38 47.41 1.08 o 1 -5 8 21.37 19.97 0.67 o 2 -5 8 59.43 59.39 1.15 o 3 -5 8 342.57 344.39 3.79 o -4 -4 8 37.18 35.47 0.81 o -3 -4 8 261.84 259.22 2.90 o -2 -4 8 158.32 171.41 2.17 o -1 -4 8 342.28 336.83 3.93 o 0 -4 8 30.81 30.15 0.84 o 1 -4 8 0.86 1.25 0.34 o 2 -4 8 336.91 341.92 4.97 o 3 -4 8 336.62 332.59 3.98 o -5 -3 8 36.52 36.57 1.00 o -4 -3 8 169.92 169.53 2.06 o -3 -3 8 53.94 54.81 0.90 o -2 -3 8 273.45 270.64 2.68 o -1 -3 8 5.78 6.30 0.36 o 0 -3 8 67.80 63.60 1.13 o 1 -3 8 481.81 479.00 4.65 o 2 -3 8 180.12 185.39 2.21 o 3 -3 8 24.76 26.63 0.84 o -5 -2 8 75.09 75.72 1.25 o -4 -2 8 43.48 42.51 0.80 o -3 -2 8 24.50 30.72 0.68 o -2 -2 8 257.74 261.50 2.59 o -1 -2 8 274.54 285.69 2.97 o 0 -2 8 0.09 0.00 0.21 o 1 -2 8 283.25 277.45 3.50 o 2 -2 8 299.93 288.06 3.31 o 3 -2 8 99.71 97.76 1.64 o -5 -1 8 0.25 0.39 0.26 o -4 -1 8 30.39 31.81 0.66 o -3 -1 8 208.50 198.51 2.21 o -2 -1 8 0.95 0.87 0.27 o -1 -1 8 3.67 4.39 0.43 o 0 -1 8 390.02 401.33 4.25 o 1 -1 8 10.25 12.73 0.59 o 2 -1 8 1.87 1.08 0.31 o 3 -1 8 2.38 2.53 0.38 o -5 0 8 8.59 9.10 0.42 o -4 0 8 5.54 6.39 0.36 o -3 0 8 196.57 204.23 2.68 o -2 0 8 444.82 452.38 4.70 o -1 0 8 29.87 29.09 1.24 o 0 0 8 135.09 131.25 1.83 o 1 0 8 104.42 99.85 1.72 o 2 0 8 109.34 107.81 1.64 o 3 0 8 9.70 10.29 0.64 o -5 1 8 84.96 91.89 1.37 o -4 1 8 84.90 78.57 1.29 o -3 1 8 54.19 54.85 1.06 o -2 1 8 97.47 96.16 1.58 o -1 1 8 0.19 0.00 0.32 o 0 1 8 22.26 23.35 0.81 o 1 1 8 92.59 89.46 1.62 o 2 1 8 139.10 139.80 2.09 o -5 2 8 0.01 0.00 0.25 o -4 2 8 259.26 269.27 3.31 o -3 2 8 86.60 94.39 1.77 o -2 2 8 73.92 70.22 1.48 o -1 2 8 91.46 87.12 1.68 o 0 2 8 3.75 4.92 0.51 o 1 2 8 167.66 168.19 2.24 o 2 2 8 44.76 45.70 1.11 o -4 3 8 54.31 57.63 1.99 o -3 3 8 95.40 97.78 2.68 o -2 3 8 127.93 131.66 2.43 o -1 3 8 65.76 65.28 1.46 o 0 3 8 53.90 53.79 1.34 o 1 3 8 330.77 336.41 4.11 o -3 4 8 22.30 23.78 1.00 o -2 4 8 5.94 4.76 0.60 o -1 4 8 5.18 4.85 0.60 o -2 -5 9 113.81 118.93 1.87 o -1 -5 9 0.22 0.35 0.36 o 0 -5 9 247.46 251.55 3.45 o 1 -5 9 64.12 63.35 1.63 o -3 -4 9 518.66 530.28 5.33 o -2 -4 9 108.73 104.52 1.68 o -1 -4 9 69.23 73.56 1.51 o 0 -4 9 151.88 155.40 2.41 o 1 -4 9 51.55 50.50 1.17 o -4 -3 9 237.00 249.72 3.18 o -3 -3 9 271.61 276.22 2.91 o -2 -3 9 22.39 23.51 0.79 o -1 -3 9 174.19 180.70 2.44 o 0 -3 9 40.45 39.48 1.01 o 1 -3 9 18.48 17.65 0.73 o 2 -3 9 76.55 83.50 1.58 o -4 -2 9 424.62 447.72 4.55 o -3 -2 9 308.94 305.18 3.12 o -2 -2 9 4.45 3.54 0.41 o -1 -2 9 13.35 11.97 0.60 o 0 -2 9 82.72 81.40 1.51 o 1 -2 9 348.60 371.65 4.92 o 2 -2 9 84.87 78.47 1.56 o -4 -1 9 315.19 323.75 3.49 o -3 -1 9 125.89 126.13 1.76 o -2 -1 9 81.50 84.74 1.59 o -1 -1 9 89.15 84.10 1.91 o 0 -1 9 60.94 60.83 1.29 o 1 -1 9 393.78 420.01 5.65 o 2 -1 9 29.43 30.24 1.10 o -4 0 9 119.51 118.99 1.70 o -3 0 9 69.45 65.73 1.39 o -2 0 9 9.38 8.90 0.65 o -1 0 9 0.20 0.06 0.34 o 0 0 9 398.30 413.15 5.35 o 1 0 9 122.21 123.88 2.21 o -4 1 9 46.48 45.68 1.08 o -3 1 9 9.96 9.35 0.62 o -2 1 9 36.76 37.49 1.20 o -1 1 9 120.68 119.62 2.30 o 0 1 9 362.74 379.07 5.02 o 1 1 9 55.96 62.10 1.49 o -3 2 9 0.12 0.32 0.36 o -2 2 9 29.55 29.98 1.09 o -1 2 9 204.21 216.24 3.51 o 0 2 9 97.01 100.81 2.16 o -1 -2 10 491.10 508.99 6.14 o